CN102940309B - Preparation method of burley tobacco for simple and elegant fragrant cigarettes - Google Patents
Preparation method of burley tobacco for simple and elegant fragrant cigarettes Download PDFInfo
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- CN102940309B CN102940309B CN201210442675.2A CN201210442675A CN102940309B CN 102940309 B CN102940309 B CN 102940309B CN 201210442675 A CN201210442675 A CN 201210442675A CN 102940309 B CN102940309 B CN 102940309B
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 106
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 106
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 150000001413 amino acids Chemical class 0.000 claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims abstract description 12
- 238000002137 ultrasound extraction Methods 0.000 claims abstract description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 230000018044 dehydration Effects 0.000 claims abstract description 4
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 4
- 235000001014 amino acid Nutrition 0.000 claims description 13
- 229940024606 amino acid Drugs 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 12
- 239000002904 solvent Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- SRBFZHDQGSBBOR-LECHCGJUSA-N alpha-D-xylose Chemical compound O[C@@H]1CO[C@H](O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-LECHCGJUSA-N 0.000 claims description 7
- 229960003487 xylose Drugs 0.000 claims description 7
- DCXYFEDJOCDNAF-UHFFFAOYSA-N Asparagine Natural products OC(=O)C(N)CC(N)=O DCXYFEDJOCDNAF-UHFFFAOYSA-N 0.000 claims description 6
- DCXYFEDJOCDNAF-REOHCLBHSA-N L-asparagine Chemical compound OC(=O)[C@@H](N)CC(N)=O DCXYFEDJOCDNAF-REOHCLBHSA-N 0.000 claims description 6
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 claims description 6
- 229960001230 asparagine Drugs 0.000 claims description 6
- 235000009582 asparagine Nutrition 0.000 claims description 6
- 235000003704 aspartic acid Nutrition 0.000 claims description 6
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 claims description 6
- 238000007654 immersion Methods 0.000 claims description 6
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 5
- 239000008101 lactose Substances 0.000 claims description 5
- 150000007524 organic acids Chemical class 0.000 claims description 5
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- 238000010009 beating Methods 0.000 claims description 2
- 238000002791 soaking Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 14
- 239000003205 fragrance Substances 0.000 abstract description 9
- 230000008569 process Effects 0.000 abstract description 8
- 238000011049 filling Methods 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 2
- 238000001035 drying Methods 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- 230000001007 puffing effect Effects 0.000 abstract 2
- MIDXCONKKJTLDX-UHFFFAOYSA-N 3,5-dimethylcyclopentane-1,2-dione Chemical compound CC1CC(C)C(=O)C1=O MIDXCONKKJTLDX-UHFFFAOYSA-N 0.000 abstract 1
- 235000013736 caramel Nutrition 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000002023 wood Substances 0.000 abstract 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 229960002715 nicotine Drugs 0.000 description 6
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 6
- 241000227425 Pieris rapae crucivora Species 0.000 description 5
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 239000002932 luster Substances 0.000 description 4
- 210000000214 mouth Anatomy 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000007598 dipping method Methods 0.000 description 3
- 235000019640 taste Nutrition 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 150000003216 pyrazines Chemical class 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000287828 Gallus gallus Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- -1 nitrogen-containing compound Chemical class 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
- 229940089401 xylon Drugs 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
Abstract
The invention provides a preparation method of burley tobacco for simple and elegant fragrant cigarettes, which comprises the following steps of: immersing the burley tobacco, ultrasonic extraction, dehydration, steam heating, storage, slicing, tobacco primary process, feeding, drying and puffing. The burley tobacco immersing process is as follows: the burley tobacco which is subjected to threshing and redrying is added into edible alcohol as an immersing agent according to a weight ratio of 1:12-30 for immersing, the immersing time is 20-40 minutes, and the temperature is 50-70 DEG C; ultrasonic extraction is carried out, and the processing time is 30-60 minutes; the steam heating, storage, slicing and tobacco primary process are carried out on the processed burley tobacco after dehydration; in the feeding step, the fed material liquid is a sugar material containing amino acid, which is 8-20% of the weight of the burley tobacco; and then, the drying and puffing are carried out to prepare the burley tobacco. Compared with the prior art, the preparation method disclosed by the invention has the following advantages that the burley tobacco is high in filling value, good in elasticity, less in wood gas and obvious in fragrance, and can endow a certain caramel fragrance to the cigarettes.
Description
Technical field
The present invention relates to tobacco industry burley tobaccos silk processing technique field, specifically the preparation method of burley tobaccos silk for a kind of simple and elegant fragrant category cigarette.
Background technology
Burley tobaccos are by the sudden change of Maryland dark sun-cured tobacco kind, and stem and vein are creamy white, and are different from other tobacco.Its cultural method is similar to flue-cured tobacco, after ripe harvesting, hangs in dry in the air canopy or the room that dries in the air and dries.Burley tobaccos moisture is higher, and blade is thin and light, institutional framework is loosened and not coarse, and elasticity is strong, and filling value is high, absorbs fragrance performance good, and nicotine and total nitrogen content are higher than flue-cured tobacco, and flue gas strength is large, and sugar content is low, has very strong absorbability.Burley tobaccos have the fragrance of mediation and jealous effect, are the important source material of blended type cigarette, are also pipe tobacco raw materials.
Because the nitrogen content of burley tobaccos is high, sugar content is low, therefore burley tobaccos bitter taste in combustion process is heavier, assorted gas is heavy, it is large to stimulate, strength is large, inconsistent with the style of simple and elegant fragrant category cigarette, affect quality and the characteristic of cigarette, limited the use of burley tobaccos silk in simple and elegant fragrant category cigarette product.For this reason, the present invention is intended to make by burley tobaccos being carried out to specially treated the personalized burley tobaccos that meet developer's needs, improves its inherent quality, thereby improves the utilization rate of burley tobaccos in simple and elegant fragrant category cigarette.
Summary of the invention
For the above-mentioned deficiency of prior art, the invention provides the preparation method of burley tobaccos silk for a kind of simple and elegant fragrant category cigarette, can improve the quality of burley tobaccos silk, increase the utilization rate of burley tobaccos silk, and be applied in simple and elegant fragrant category cigarette.
The preparation method of burley tobaccos silk for a kind of simple and elegant fragrant category cigarette, comprise successively that burley tobaccos immersion, ultrasonic extraction, dehydration, steam are heated, stored, section, throwing, feed in raw material, dry expanded operation, it is characterized in that: in the burley tobaccos immersion treatment stage, be by the burley tobaccos after beating and double roasting, by weight 1: 12-30 adds edible alcohol to soak as soaking solvent, soak time is 20-40 minute, and temperature is 50-70 ℃; Then carry out ultrasonic extraction, processing time is 30-60 minute, burley tobaccos after processing carry out after processed that steam is heated, stored, section, throwing, in the reinforced stage, the feed liquid adding is that the amino acid whose sugar that contains that accounts for the 8-12% of burley tobaccos silk weight is expected, then dry the expanded burley tobaccos silk for preparing, wherein
Described immersion solvent is comprised of following component and percentage by weight:
Organic acid 1%~10%;
Edible alcohol 50%~95%;
Surplus is water;
Describedly contain amino acid whose sugar material and formed by following component and percentage by weight:
Sugar material 30%~50%;
Amino acid/11 0%;
Surplus is water.
The preparation method of burley tobaccos silk for simple and elegant fragrant category cigarette as above, described organic acid is citric acid, acetic acid or its mixture.
The preparation method of burley tobaccos silk for simple and elegant fragrant category cigarette as above, described amino acid is aspartic acid, asparagine or its mixture.
The preparation method of burley tobaccos silk for simple and elegant fragrant category cigarette as above, described sugar material is lactose, wood sugar or its mixture.
The preparation method of burley tobaccos silk for simple and elegant fragrant category cigarette as above, processed mode is a kind of in following mode: extruding, centrifuge dewatering, dry.
The preparation method of burley tobaccos silk for simple and elegant fragrant category cigarette as above, the processed after ultrasonic extraction is that burley tobaccos silk moisture is reduced to 30-40% by 60-120% left and right.
The present invention compared with prior art has following advantage: tobacco burley tobaccos silk filling value is high, and good springiness, xylon gas is few, fragrance is obvious, and it is fragrant and sweet to give certain Jiao of cigarette.Adopt acid flux material to soak and ultrasonic processing burley tobaccos, organic acid can with tobacco leaf in nicotine and nitrogenous alkali compounds in conjunction with salify, improve the polarity of nicotine and nitrogen-containing compound, be conducive to their water-soluble and two kinds of polarity of alcohol compared with strong solvent, be convenient to extract, improve recovery rate and yield, reduce nicotine, total nitrogen and some characteristic perfume compositions in burley tobaccos, reduce the odor characteristic of burley tobaccos, improve the flavour absorbing quality of burley tobaccos; In reinforced, add sugar and amino acid, under higher temperature conditions, carry out Maillard reaction, generate a large amount of pyrazine class fragrance matters simultaneously, and reactant color is dark-brown, can increase feature perfume (or spice), improve burley tobaccos silk quality, improve the color and luster of burley tobaccos simultaneously.
The specific embodiment
Below in conjunction with specific embodiment, the technical scheme in the present invention is clearly and completely described.
It is ultrasonic processing technique after polar solvent soaks that technique of the present invention changes traditional leaves moisting mode, is conducive to reduce characteristic perfume composition and nicotine composition in burley tobaccos, improves the smoking quality of burley tobaccos.Burley tobaccos moisture after ultrasonic processing technique is larger, by dewater unit, burley tobaccos silk moisture is reduced to 30-40% left and right by 60-120% left and right, is beneficial to cut-tobacco drier dialogue rib pipe tobacco and dries.
The present invention, after cutting burley tobaccos, feeds in raw material, and adds sugar material different from tradition, and the present invention is reinforced take sugar material and amino acid as main, then dries expanded.Owing at high temperature Maillard reaction occurring between amino-compound and reduced sugar, generating a large amount of pyrazine class fragrance matters is tobacco characteristic chicken flavor material, with tobacco flavor harmony, and reactant color is dark-brown, be conducive to improve the quality of burley tobaccos silk, avoided problem in tobacco shred blending process, the problem includes: aberration problem simultaneously.Amino acid comprises aspartic acid, asparagine or their mixture; Sugar material comprises lactose, wood sugar or their mixture.Sugared and amino acid whose weight ratio is 3-5: 1.Described sugar and amino acid whose total amount account for the 8-12% of burley tobaccos silk weight.
Burley tobaccos silk prepared by employing the present invention and common white rib pipe tobacco chemical composition comparing result are in Table 1.Total reducing sugar and the content of reducing sugar of the burley tobaccos silk that the present invention processes are high, and total nitrogen content is lower than common white rib pipe tobacco, and nicotine content is low, is conducive to the improvement of interior quality.Reduced sugar participates in the synthetic flavor matter of Maillard reaction, is conducive to increase feature perfume (or spice).
Burley tobaccos silk and the contrast of common white rib pipe tobacco chemical composition that table 1 adopts the present invention to prepare
The burley tobaccos silk and the common white rib pipe tobacco that adopt the present invention to prepare, the ratio according to 5% disastrously fits in certain flue-cured tobacco group and aspirates, and the fragrance while comparing smoking by method of comparison and jealous, carries out sensory evaluation by the special personnel that smoke panel test.Comparing result is in Table 2.Found that, burley tobaccos silk comparison common white rib pipe tobacco prepared by the present invention, fragrance increases, and flue gas is smooth and easy soft, and assorted gas reduces, and oral cavity is cleaner, and overall assessment is better than the latter.
The Contrast on effect of table 2 burley tobaccos silk
Below embodiments of the invention are described.
Embodiment 1: burley tobaccos are placed in to dipping tank, by weight adding 95% edible alcohol solvent at 1: 12, contain 1.5% citric acid in solvent, surplus is water.Flood 30 minutes, temperature is 50 ℃, then carry out ultrasonic extraction, the processing time is 30 minutes, then uses dewater unit that burley tobaccos moisture is become to 30% left and right, carry out steam and heat, store burley tobaccos, section throwing, add the feed liquid that contains lactose and aspartic acid, component and the percentage by weight of feed liquid consist of: lactose 30%, aspartic acid 10%, water 60%, the total amount of feed liquid accounts for 8% of burley tobaccos silk weight.Then dry expandedly, prepare burley tobaccos silk.It is gentle that the burley tobaccos silk that goes out by this processes is inhaled taste, and assorted gas reduces, and oral cavity is cleaner, increased burnt fragrant and sweetly, also more has oil content sense in appearance luster.
Embodiment 2: burley tobaccos are placed in to dipping tank, by weight adding 75% edible alcohol solvent at 1: 15, contain 1.0% acetic acid in solvent, surplus is water.Flood 40 minutes, temperature is 60 ℃, then carry out ultrasonic extraction, the processing time is 40 minutes, then uses dewater unit that burley tobaccos moisture is become to 30% left and right, carry out steam and heat, store burley tobaccos, section throwing, add the feed liquid that contains wood sugar and asparagine, component and the percentage by weight of feed liquid consist of: wood sugar 50%, asparagine 10%, water 40%, the total amount of feed liquid accounts for 10% of burley tobaccos silk weight.Then dry expandedly, prepare burley tobaccos silk.It is gentle that the burley tobaccos silk that goes out by this processes is inhaled taste, and assorted gas reduces, and oral cavity is cleaner, increased burnt fragrant and sweetly, also more has oil content sense in appearance luster.
Embodiment 3: burley tobaccos are placed in to dipping tank, by weight adding 60% edible alcohol solvent at 1: 20, contain 1.0% citric acid and 1.0% acetic acid in solvent, surplus is water.Flood 35 minutes, temperature is 65 ℃, then carry out ultrasonic extraction, the processing time is 50 minutes, then uses dewater unit that burley tobaccos moisture is become to 30% left and right, carry out steam and heat, store burley tobaccos, section throwing, add the feed liquid that contains wood sugar and aspartic acid, component and the percentage by weight of feed liquid consist of: wood sugar 40%, asparagine 10%, water 50%, the total amount of feed liquid accounts for 12% of burley tobaccos silk weight.Then dry expandedly, prepare burley tobaccos silk.It is gentle that the burley tobaccos silk that goes out by this processes is inhaled taste, and assorted gas reduces, and oral cavity is cleaner, increased burnt fragrant and sweetly, also more has oil content sense in appearance luster.
The above; be only the specific embodiment of the present invention, but protection scope of the present invention is not limited to this, anyly belongs to those skilled in the art in the technical scope that the present invention discloses; the variation that can expect easily or replacement, within all should being encompassed in protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claim.
Claims (4)
1. the preparation method of burley tobaccos silk for a simple and elegant fragrant category cigarette, comprise successively that burley tobaccos immersion, ultrasonic extraction, dehydration, steam are heated, stored, section, throwing, feed in raw material, dry expanded operation, it is characterized in that: in the burley tobaccos immersion treatment stage, be by the burley tobaccos after beating and double roasting, by weight 1:12-30, add edible alcohol to soak as soaking solvent, soak time is 20-40 minute, and temperature is 50-70 ℃; Then carry out ultrasonic extraction, processing time is 30-60 minute, burley tobaccos after processing carry out after processed that steam is heated, stored, section, throwing, in the reinforced stage, the feed liquid adding is that the amino acid whose sugar that contains that accounts for the 8-12% of burley tobaccos silk weight is expected, then dries the expanded burley tobaccos silk for preparing;
Described immersion solvent is comprised of following component and percentage by weight:
Organic acid 1%~10%;
Edible alcohol 50%~95%;
Surplus is water;
Describedly contain amino acid whose sugar material and formed by following component and percentage by weight:
Sugar material 30%~50%;
Amino acid/11 0%;
Surplus is water;
Described amino acid is aspartic acid, asparagine or its mixture; Described sugar material is lactose, wood sugar or its mixture.
2. the preparation method of burley tobaccos silk for simple and elegant fragrant category cigarette as claimed in claim 1, is characterized in that: described organic acid is citric acid, acetic acid or its mixture.
3. the preparation method of burley tobaccos silk for simple and elegant fragrant category cigarette as claimed in claim 1, is characterized in that: processed mode is a kind of in following mode: extruding, centrifuge dewatering, dry.
4. the preparation method of burley tobaccos silk for simple and elegant fragrant category cigarette as claimed in claim 1, is characterized in that: the processed after ultrasonic extraction is that burley tobaccos silk moisture is reduced to 30-40% by 60-120% left and right.
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CN103445288A (en) * | 2013-09-06 | 2013-12-18 | 湖北中烟工业有限责任公司 | Processing method for increasing usability of burley tobacco |
CN104382225A (en) * | 2014-10-29 | 2015-03-04 | 湖北中烟工业有限责任公司 | Mixed processing method for aromatic tobacco and burley tobacco |
CN104886752B (en) * | 2015-04-29 | 2016-09-07 | 湖北中烟工业有限责任公司 | Improve burley tobaccos preprocess method of availability in simple and elegant fragrant cigarette |
CN105394805B (en) * | 2015-11-25 | 2017-01-25 | 安徽中烟工业有限责任公司 | Method for enabling carbon dioxide expanded tobacco to highlight sweet aroma style |
CN105707971A (en) * | 2016-04-28 | 2016-06-29 | 吉林烟草工业有限责任公司 | Treatment method of regenerated cut stem backfilling material liquid, regenerated cut stems and application thereof |
CN107660811B (en) * | 2016-07-27 | 2021-02-23 | 湖南中烟工业有限责任公司 | Burley tobacco nicotine extract and extraction process |
CN111920078B (en) * | 2016-07-27 | 2022-04-29 | 湖南中烟工业有限责任公司 | Modified activated carbon |
CN106490667B (en) * | 2016-11-04 | 2018-06-08 | 湖北中烟工业有限责任公司 | A kind of lining for improving burley tobaccos fragrance harmony and its preparation method and application |
CN113040420B (en) * | 2019-12-27 | 2022-09-16 | 湖南中烟工业有限责任公司 | Preparation method of tobacco raw material for heating cigarette and heating cigarette product |
CN113854620A (en) * | 2021-09-02 | 2021-12-31 | 深圳市艾普生物科技有限公司 | Electronic cigarette liquid additive and preparation method and application thereof |
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