CN104801277A - Bombax ceiba flower porous particle and applications thereof - Google Patents
Bombax ceiba flower porous particle and applications thereof Download PDFInfo
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- CN104801277A CN104801277A CN201510078723.8A CN201510078723A CN104801277A CN 104801277 A CN104801277 A CN 104801277A CN 201510078723 A CN201510078723 A CN 201510078723A CN 104801277 A CN104801277 A CN 104801277A
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- porous particle
- common bombax
- bombax flower
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Abstract
The invention discloses a bombax ceiba flower porous particle, and applications thereof. According to a preparation method, bombax ceiba flower powder with a water content ranging from 8 to 10% and a particle size ranging from 80 to 140 meshes is taken as a raw material; hydroxypropyl methyl cellulose is taken as an adhesive; and fluidized bed top spraying is adopted so as to prepare the bombax ceiba flower porous particle with a particle size ranging from 20 to 60 meshes. The surface of the bombax ceiba flower porous particle is rough; specific surface area is relatively large; effective contact area of the bombax ceiba flower porous particle with cigarette smoke is enlarged substantially; preferential adsorption of phenol in cigarette smoke can be realized; the bombax ceiba flower porous particle is capable of reducing risks, enriching flue-cured tobacco natural smoke fragrance, and reducing cigarette smoke irritation. The preparation method is simple; operability and standardability are high; the raw material is easily available; cost is low; industrialized production is convenient to realize; and application prospect is promising.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of common bombax flower porous particle that can improve flavor quality of cigarette.Meanwhile, the invention still further relates to the application of this porous particle in Cigarette processing.
Background technology
Along with smoking and healthy problem more and more receive publicity, that how to improve cigarette sucks security, reduces the harmful components in cigarette smoke, improves the focus that the comfort of suction just becomes the research and development of each tobacco productive corporation.Cigarette material researcher utilizes natural plant material to develop some filter stick granular materials, the mode of main employing is the particle be directly ground into by vegetable material between 20 ~ 80 orders, or vegetable material is prepared into particle by extrusion, although at cigarette flavouring, harm reduction aspect achieves certain effect, but also there is the shortcoming of the following aspects: vegetable material is directly ground into particle by (1), grain shape is uneven, physical instability, when cigarette filter tip shaping, particle is easily made broken thus is produced a large amount of dust, stock utilization is not high, (2) particle is prepared by extrusion, the hole embedding that vegetable material itself easily has by the adhesive added, the contact area of granular materials and cigarette smoke is limited, its reducing tar and reducing harm limited use, particle is simultaneously comparatively tight, hardness is comparatively large, is unfavorable for the preparation of composite cigarette filter stick.For above-mentioned shortcoming, how to adopt suitable technology, preparation is applicable to the plant porous material of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Common bombax flower is the flower of Bombacaceae plant kapok.To gather spring open flower, dry or dry.Its slightly sweet flavor of common bombax flower, cool in nature, there is effect of clearing heat and promoting diuresis, deciphering, hemostasis, cure mainly have loose bowels, the illness such as dysentery, sore.Also containing the abundant nutriment such as carbohydrate, protein in common bombax flower, wherein polysaccharide is the important component of common bombax flower, in addition containing various trace element, is eat the suitable plant of medicine two.Among the peoplely many pick up flower dry kapok when the flowers are in blossom in the early spring, decoct water take or cook congee, Baoshang eats.But in the prior art about common bombax flower being made honeycombed grain material and the research being applied to cigarette filter rod there is not yet relevant report.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide that a kind of resist processing is strong, uniform particles, security are high, flavouring successful, there is the common bombax flower porous particle of certain harm reduction effect.
The present invention also aims to provide the described application of common bombax flower porous particle in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
Except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of common bombax flower porous particle, is obtained by the method for following steps:
(1) naturally being dried by common bombax flower to moisture content is 8 ~ 10%, then to be ground into particle diameter be further 80 ~ 140 object powder, for subsequent use;
(2) take hydroxypropyl methylcellulose 3 ~ 6 parts according to weight portion, then be mixed with distilled water the binder solution that concentration is 3 ~ 6%, for subsequent use;
(3) take common bombax flower powder 300 ~ 1000g for subsequent use and be placed in fluid bed granulation, prilling specifically comprises the steps:
(a) under fluidisation air pressure 0.15 ~ 0.18Bar, gas flow temperature 50 ~ 60 DEG C of conditions dry 4 ~ 8 minutes; B () is fluidisation air pressure 0.18 ~ 0.22Bar, gas flow temperature 50 ~ 70 DEG C, under atomisation pressure 0.10 ~ 0.14Bar, the hydrojet speed condition of 8 ~ 10g/ minute, employing top spray mode applies the binder solution that step (2) is prepared, and binder solution consumption is 30% ~ 50% of dry material weight; C () adhesive has applied after, repeat step (a), preparing moisture is 8 ~ 10%, shaggy similar round particle, is required common bombax flower porous particle.
Wherein, obtained its particle diameter of common bombax flower porous particle is 20 ~ 60 orders.
Described fluid bed is preferably Midi Glatt fluid bed.
Described common bombax flower porous particle is applied in cigarette, it is characterized in that: the common bombax flower porous particle adding 1 ~ 2mg in every millimeter of composite cigarette filter stick.
Compared with prior art, the present invention has the following advantages:
1. gained common bombax flower porous particle effectively can reduce cigarette smoke excitant, enrich cigarette perfume (or spice), has the effect increasing the sweet sense of flue gas simultaneously.
2. the common bombax flower porous particle size prepared by the present invention is even, stable in physicochemical property, there is good resist processing, what avoid that granular materials in filter stick formation process produces because of machining makes broken and dust, and granular materials can be uniformly distributed in filter stick tow.
3. gained common bombax flower porous particle rough surface, has higher specific area, significantly improves effective contact area of granular materials and cigarette smoke, can phenol in selective absorption cigarette smoke.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, operability and normative strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has application prospect well.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
Take from the common bombax flower 800g so dried to moisture 10%, dry common bombax flower being ground into particle diameter is 140 object powder again, made common bombax flower powder is placed in the granulation of Midi Glatt fluid bed, fluid bed fluidisation air pressure is 0.15Bar, gas flow temperature is under 50 DEG C of conditions dry 5 minutes; Then hydroxypropyl methylcellulose distilled water is mixed with the binder solution that concentration is 6%, fluidisation air pressure be 0.2Bar, gas flow temperature is 60 DEG C, atomisation pressure is 0.12Bar, hydrojet speed is under 8g/ minute condition, adopts top spray mode to spray 320g binder solution; After adhesive has applied, setting fluidisation air pressure 0.16Bar, gas flow temperature are under 50 DEG C of conditions dry 5 minutes, moisture is adjusted to 10%, crosses 60 mesh sieves and namely obtain cigarette filter rod common bombax flower porous particle.
Embodiment 2
Take from the common bombax flower 600g so dried to moisture 9%, dry common bombax flower being ground into particle diameter is 100 object powder again, made common bombax flower powder is placed in the granulation of Midi Glatt fluid bed, fluid bed fluidisation air pressure is 0.18Bar, gas flow temperature is under 60 DEG C of conditions dry 4 minutes; Then hydroxypropyl methylcellulose distilled water is mixed with the binder solution that concentration is 4%, fluidisation air pressure be 0.18Bar, gas flow temperature is 60 DEG C, atomisation pressure is 0.14Bar, hydrojet speed is under 10g/ minute condition, adopts top spray mode to spray 280g binder solution; After adhesive has applied, setting fluidisation air pressure 0.18Bar, gas flow temperature are under 60 DEG C of conditions dry 6 minutes, moisture is adjusted to 9%, crosses 20 mesh sieves and namely obtain cigarette filter rod common bombax flower porous particle.
Embodiment 3
Take from the common bombax flower 400g so dried to moisture 8%, dry common bombax flower being ground into particle diameter is 80 object powder again, made common bombax flower powder is placed in the granulation of Midi Glatt fluid bed, fluid bed fluidisation air pressure is 0.15Bar, gas flow temperature is under 60 DEG C of conditions dry 8 minutes; Then hydroxypropyl methylcellulose distilled water is mixed with the binder solution that concentration is 4%, fluidisation air pressure be 0.22Bar, gas flow temperature is 65 DEG C, atomisation pressure is 0.10Bar, hydrojet speed is under 9g/ minute condition, adopts top spray mode to spray 180g binder solution; After adhesive has applied, setting fluidisation air pressure 0.18Bar, gas flow temperature are under 60 DEG C of conditions dry 4 minutes, moisture is adjusted to 8%, crosses 40 mesh sieves and namely obtain cigarette filter rod common bombax flower porous particle.
Application Example 1
Gained common bombax flower porous particle being prepared by embodiment 1 is applied in composite cigarette filter stick, and every millimeter of cigarette filter rod adds 1mg granular materials, is prepared into experiment cigarette, carries out sensory evaluating smoking and harmful ingredients in flue gas detection with the cigarette of not adding above-mentioned particle for contrasting.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas excitant of adding above-mentioned porous particle obviously reduces, and fragrance is abundanter; Harmful ingredients in flue gas detects and shows: phenol reduced rate is 20.3%, and this porous particle can phenol in selective absorption cigarette smoke.
Application Example 2
Gained common bombax flower porous particle being prepared by embodiment 2 is applied in composite cigarette filter stick, and every millimeter of cigarette filter rod adds 2mg granular materials, is prepared into experiment cigarette, carries out sensory evaluating smoking and harmful ingredients in flue gas detection with the cigarette of not adding above-mentioned particle for contrasting.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas excitant of adding above-mentioned porous particle obviously reduces, and fragrance is abundanter; Harmful ingredients in flue gas detects and shows: phenol reduced rate is 21.6%, and this porous particle can phenol in selective absorption cigarette smoke.
Application Example 3
Gained common bombax flower porous particle being prepared by embodiment 3 is applied in composite cigarette filter stick, every millimeter of cigarette filter rod adds 1.5mg granular materials, being prepared into experiment cigarette, carrying out sensory evaluating smoking and harmful ingredients in flue gas detection with the cigarette of not adding above-mentioned particle for contrasting.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas excitant of adding above-mentioned porous particle obviously reduces, and fragrance is abundanter; Harmful ingredients in flue gas detects and shows: phenol reduced rate is 19.5%, and this porous particle can phenol in selective absorption cigarette smoke.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (4)
1. a common bombax flower porous particle, is obtained by the method for following steps:
(1) naturally being dried by common bombax flower to moisture content is 8 ~ 10%, then to be ground into particle diameter be further 80 ~ 140 object powder, for subsequent use;
(2) take hydroxypropyl methylcellulose 3 ~ 6 parts according to weight portion, then be mixed with distilled water the binder solution that concentration is 3 ~ 6%, for subsequent use;
(3) take common bombax flower powder 300 ~ 1000g for subsequent use and be placed in fluid bed granulation, prilling specifically comprises the steps:
(a) under fluidisation air pressure 0.15 ~ 0.18Bar, gas flow temperature 50 ~ 60 DEG C of conditions dry 4 ~ 8 minutes; B () is fluidisation air pressure 0.18 ~ 0.22Bar, gas flow temperature 50 ~ 70 DEG C, under atomisation pressure 0.10 ~ 0.14Bar, the hydrojet speed condition of 8 ~ 10g/ minute, employing top spray mode applies the binder solution that step (2) is prepared, and binder solution consumption is 30% ~ 50% of dry material weight; C () adhesive has applied after, repeat step (a), preparing moisture is 8 ~ 10%, shaggy similar round particle, is required common bombax flower porous particle.
2. common bombax flower porous particle according to claim 1, is characterized in that: obtained its particle diameter of common bombax flower porous particle is 20 ~ 60 orders.
3. common bombax flower porous particle according to claim 1, is characterized in that: described fluid bed is preferably Midi Glatt fluid bed.
4. common bombax flower porous particle according to claim 1 is applied in cigarette, it is characterized in that: the common bombax flower porous particle adding 1 ~ 2mg in every millimeter of composite cigarette filter stick.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510078723.8A CN104801277A (en) | 2015-02-13 | 2015-02-13 | Bombax ceiba flower porous particle and applications thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510078723.8A CN104801277A (en) | 2015-02-13 | 2015-02-13 | Bombax ceiba flower porous particle and applications thereof |
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| CN104801277A true CN104801277A (en) | 2015-07-29 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105725270A (en) * | 2016-03-07 | 2016-07-06 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of astaxanthin particles and application thereof in cigarette filter sticks |
| CN106666825A (en) * | 2017-02-04 | 2017-05-17 | 云南热丽康生物科技有限公司 | Method for producing cigarette filter sticks by adding Taxus cuspidata particles |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2586322A1 (en) * | 2011-10-27 | 2013-05-01 | Creepservice S.à.r.l. | Filter and method of making same |
| CN103540407A (en) * | 2013-11-04 | 2014-01-29 | 成都宏亿实业集团有限公司 | Kapok essential oil |
| CN103689794A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Pelargonium graveolens porous particles and application thereof in cigarettes |
-
2015
- 2015-02-13 CN CN201510078723.8A patent/CN104801277A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2586322A1 (en) * | 2011-10-27 | 2013-05-01 | Creepservice S.à.r.l. | Filter and method of making same |
| CN103540407A (en) * | 2013-11-04 | 2014-01-29 | 成都宏亿实业集团有限公司 | Kapok essential oil |
| CN103689794A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Pelargonium graveolens porous particles and application thereof in cigarettes |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105725270A (en) * | 2016-03-07 | 2016-07-06 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of astaxanthin particles and application thereof in cigarette filter sticks |
| CN106666825A (en) * | 2017-02-04 | 2017-05-17 | 云南热丽康生物科技有限公司 | Method for producing cigarette filter sticks by adding Taxus cuspidata particles |
| CN106666825B (en) * | 2017-02-04 | 2019-10-29 | 云南热丽康生物科技有限公司 | A kind of cigarette filter rod preparation method for adding yew plants particle |
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