CN107164092B - Preparation method of high-boiling-point radix puerariae fragrant particles and high-boiling-point radix puerariae fragrant particles - Google Patents
Preparation method of high-boiling-point radix puerariae fragrant particles and high-boiling-point radix puerariae fragrant particles Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Oil, Petroleum & Natural Gas (AREA)
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- Fats And Perfumes (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to a preparation method of high-boiling-point radix puerariae fragrant particles and the high-boiling-point radix puerariae fragrant particles, and belongs to the field of cigarette filter materials. Adding essence perfume into low-concentration gelatinized kudzu root powder colloidal solution, keeping the flow state, spraying into a fluidized bed in a top spraying manner, and performing primary granulation; and then a small amount of dried radix puerariae powder is mixed, and secondary granulation is carried out by adopting an unflavored radix puerariae colloidal solution, so that the prepared radix puerariae particles wrap the essence and the spice inside the particles, the slow release performance of the particles is improved, the inherent sweet feeling of radix puerariae is kept, and the product quality is improved.
Description
Technical Field
The invention relates to a preparation method of kudzuvine root fragrant particles, in particular to a preparation method of high-boiling-point kudzuvine root fragrant particles, and also relates to high-boiling-point kudzuvine root fragrant particles, belonging to the field of cigarette filter materials.
Background
The filter tip is used as a bridge between a smoker and the mainstream smoke, can filter partial harmful components in the smoke, is connected with the filter tip on the cigarette, can effectively intercept total particulate matters in the mainstream smoke of the cigarette, reduces the tar content and reduces the harm of the smoke to the human health and the environment.
Kudzu root is a perennial plant of Pueraria of Leguminosae, is a common vegetable in some provinces of south China, is sweet, cool and delicious in taste, and is often used as soup. Can also be used as medicine. The flavone extracted from radix Puerariae can increase blood flow of brain and coronary blood vessel, and reduce vascular resistance. The soybean flavone has multiple functions of spasmolysis, blood sugar reduction and the like. Radix Puerariae itself also has effects of promoting fluid production to quench thirst, etc. China has 14 species of Pueraria plants, is the most abundant in germplasm resources and is the top of the world.
With the increasing requirements of consumers on the cigarette quality, how to enhance the smoke comfort and improve the cigarette quality becomes a hot point for research and development of various cigarette production enterprises. The application of the kudzu root granular material to cigarette filters has already been realized in the prior art and is widely favored. However, there are two main methods of use at present, that is, pulverizing the root of kudzu vine into particles of 20-80 mesh, or adding other plant powder into the root of kudzu vine, then adding a certain amount of adhesive, and preparing into particles by various molding methods. Both methods directly utilize the properties of the kudzu root powder without any improvement. Therefore, the variety of kudzu granular materials currently used is single in variability and has not undergone perfuming treatment. The reason is that the kudzu root powder has strong rigidity and is not easy to directly load essence and flavor. Therefore, how to improve the kudzu root particle material and load the kudzu root particle material with the essence and spice becomes a bottleneck for further expanding the application of the kudzu root in cigarettes.
Disclosure of Invention
The invention aims to provide a method for manufacturing a kudzu root flavoring granular material for cigarettes, which is characterized in that essence perfume is added into low-concentration gelatinized kudzu root powder colloidal solution, the flowing state of the kudzu root powder colloidal solution is kept, and the kudzu root powder colloidal solution is sprayed into a fluidized bed in a top spraying mode for primary granulation; and then a small amount of dried radix puerariae powder is mixed, and secondary granulation is carried out by adopting an unflavored radix puerariae colloidal solution, so that the prepared radix puerariae particles wrap the essence and the spice inside the particles, the slow release performance of the particles is improved, the inherent sweet feeling of radix puerariae is kept, and the product quality is improved.
The technical scheme for solving the technical problem of the invention is as follows:
a preparation method of high-boiling-point kudzuvine root fragrant granules comprises the following steps:
(1) adding a certain amount of water into the dried radix puerariae powder, heating and pasting to obtain a radix puerariae powder colloidal solution with the mass concentration of 3-8%;
(2) keeping the gelatinized pueraria powder colloidal solution at the temperature of more than 80 ℃, then adding a certain amount of essence and flavor, and stirring to uniformly mix to obtain a first mixture;
(3) taking the first mixture obtained in the step (2) as an adhesive, and performing primary granulation on the dried radix puerariae powder by using a conventional fluidized bed, wherein the adhesive is sprayed at the bottom, the granularity of the particles is controlled to be 60-80 meshes, and the prepared particles are screened to obtain particles with required meshes and are dried at low temperature;
(4) and (2) mixing the dried particles obtained in the step (3) with a small amount of dried radix puerariae powder, and performing secondary granulation by using a conventional fluidized bed, wherein the adhesive is sprayed on the top, the particle size of the particles is controlled to be 40-60 meshes, and the prepared particles are screened to obtain the required particles and dried to obtain the high-boiling-point radix puerariae fragrant particles.
Further, the essence used in the step (2) is an essence which has a boiling point higher than 80 ℃ and is soluble in water;
further, the essence and flavor is soluble plum essence, soluble agarwood extract, soluble tobacco extract, soluble dried orange peel extract or menthol, and the essence and flavor accounts for 1-2% of the first mixture by mass.
Further, the temperature for drying the particles in the step (3) and the step (4) is not more than 60 ℃, and the drying time is 3-6 h.
Further, the concentration of the kudzu root powder colloidal solution in the step (4) is the same as that of the kudzu root powder colloidal solution prepared in the step (1), and the amount of the adhesive used in the step (4) is 1/2 of the mass of the adhesive in the step (3).
Further, the amount of the dried radix puerariae powder in the step (3) is 30-40 times of the absolute dry amount of the gelatinized radix puerariae powder in the step (1), and the added dried radix puerariae powder in the step (4) accounts for 10% of the mass of the dried radix puerariae powder used in the primary granulation. The amount of the kudzu root powder is different according to the specific granulator and the amount of the adhesive, and the ratio of the dry powder to the adhesive is fixed under the same granulator as long as the particle size is controlled.
Further, in the step (1), adding water with a volume 15 times of that of the radix puerariae powder, gelatinizing at 85-90 ℃, and controlling the heating time for 30-120min, wherein the mass concentration of the obtained colloidal solution is 3-8%. The radix puerariae powder is used in a large amount, the particle size of the obtained particles is small, and otherwise, the particle size is large.
The invention relates to a high-boiling-point kudzuvine root fragrant granule prepared by the preparation method.
Compared with the prior art, the invention has the advantages that:
(1) the method can effectively add essence perfume into radix Puerariae granule, and solve the problem of difficulty in perfuming radix Puerariae granule;
(2) the added essence and spice is wrapped on the inner layer of the particles, so that the slow release effect can be enhanced, the inherent sweet feeling of the kudzuvine root is kept, and the quality of the product is improved.
Detailed Description
The following will clearly and completely describe the technical solutions in the embodiments, and it is obvious that the described embodiments are only a part of examples of the present invention, and not all examples. All other embodiments, which can be obtained by a person skilled in the art without inventive effort based on the embodiments of the present invention, are within the scope of the present invention. In the examples, a commercially available boiling fluidized bed granulator was used for primary granulation and secondary granulation, and the granulation process was a conventional boiling fluidized bed granulation process. The filter stick forming process is a conventional process.
Example 1
(1) Preparing dried radix Puerariae powder according to the requirement of granulation equipment, adding water 15 times of radix Puerariae powder volume into radix Puerariae powder, gelatinizing at 90 deg.C, and heating for 30min to obtain colloidal solution with mass concentration of 3%; the colloidal solution was free of visible particulates.
(2) Keeping the gelatinized pueraria powder colloidal solution at 90 +/-5 ℃, adding soluble plum essence, and stirring to uniformly mix to obtain a first mixture; the soluble plum essence accounts for 1% of the first mixture by mass;
(3) and (3) taking the first mixture obtained in the step (2) as an adhesive, and performing primary granulation on the dried radix puerariae powder by using a conventional fluidized bed, wherein the adhesive is sprayed at the bottom, the using amount of the dried radix puerariae powder is 35 times of the absolute dry amount of the gelatinized radix puerariae powder obtained in the step (1), the granularity of the particles is controlled to be about 60-80 meshes, the prepared particles are screened to obtain particles with required meshes, and the particles are dried at low temperature, the drying temperature is controlled to be 60 ℃, and the drying time is 3 hours.
(4) And (2) preparing a kudzu root powder colloidal solution according to the step (1), using the kudzu root powder colloidal solution as an adhesive, mixing the dried particles obtained in the step (3) with the kudzu root powder, and performing secondary granulation by using a conventional fluidized bed, wherein the adhesive is sprayed on the top, the amount of the kudzu root powder is 10% of the mass of the kudzu root powder used in the primary granulation, the amount of the adhesive is 1/2% of the amount of the adhesive used in the step (3), the particle size of the particles is controlled to be about 40-60 meshes, the prepared particles are screened to obtain the required particles, and are dried, the drying temperature is controlled to be 60 ℃, and the drying time is 3 hours, so that the high-boiling-point kudzu root fragrant particles are obtained.
And putting the finally obtained kudzuvine root flavor particles into a filter tip forming device for production to obtain a cigarette filter containing filter tip particles, and manufacturing cigarettes. Compared with cigarettes manufactured by using kudzu vine root particles without adding essence and spice, the cigarette has the advantages that the smoke moisture-producing feeling is remarkably improved, the plum fragrance is obvious, the smoke comfort is improved, and the sensory evaluation score is increased by 1.5.
Example 2
(1) Preparing dried radix Puerariae powder according to the requirement of granulation equipment, adding water 15 times the volume of radix Puerariae powder into radix Puerariae powder, gelatinizing at 85 deg.C, and heating for 120min to obtain colloidal solution with mass concentration of 8%;
(2) keeping the gelatinized pueraria powder colloidal solution at 90 +/-5 ℃, adding the soluble agarwood extract, and stirring to uniformly mix to obtain a first mixture; the soluble agarwood extract accounts for 2% of the mass fraction of the first mixture;
(3) and (3) taking the first mixture obtained in the step (2) as an adhesive, and performing primary granulation on the dried radix puerariae powder by using a conventional fluidized bed, wherein the adhesive is sprayed at the bottom, the using amount of the dried radix puerariae powder is 40 times of the absolute dry amount of the gelatinized radix puerariae powder obtained in the step (1), the granularity of the particles is controlled to be about 60-80 meshes, the prepared particles are screened to obtain particles with required meshes, and the particles are dried at low temperature, the drying temperature is controlled to be 60 ℃, and the drying time is 4 hours.
(4) And (2) preparing a kudzu root powder colloidal solution according to the step (1), using the kudzu root powder colloidal solution as an adhesive, mixing the dried particles obtained in the step (3) with the kudzu root powder, and performing secondary granulation by using a conventional fluidized bed, wherein the adhesive is sprayed on the top, the amount of the kudzu root powder is 10% of the mass of the kudzu root powder used in the primary granulation, the amount of the adhesive is 1/2% of the amount of the adhesive used in the step (3), the particle size of the particles is controlled to be about 40-60 meshes, the prepared particles are screened to obtain the required particles, and are dried, the drying temperature is controlled to be 60 ℃, and the drying time is 4 hours, so that the high-boiling-point kudzu root fragrant particles are obtained.
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production to obtain a cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes manufactured by using the kudzu root particles without adding essence and spice, the cigarette has the advantages that the smell of the smoke and the costustoot is obvious, the smoke comfort is improved, and the sensory evaluation score is increased by 1 point.
Example 3
(1) Preparing dried radix Puerariae powder according to the requirement of granulation equipment, adding water 15 times of radix Puerariae powder volume into radix Puerariae powder, gelatinizing at 88 deg.C, and controlling heating time for 60min to obtain colloidal solution with mass concentration of 5%;
(2) keeping the gelatinized pueraria powder colloidal solution at 90 +/-5 ℃, adding the soluble tobacco extract, and stirring to uniformly mix to obtain a first mixture; the soluble tobacco extract accounts for 1.5 percent of the mass fraction of the first mixture;
(3) and (3) taking the first mixture obtained in the step (2) as an adhesive, and performing primary granulation on the dried radix puerariae powder by using a conventional fluidized bed, wherein the adhesive is sprayed at the bottom, the using amount of the dried radix puerariae powder is 30 times of the absolute dry amount of the gelatinized radix puerariae powder obtained in the step (1), the granularity of the particles is controlled to be about 60-80 meshes, the prepared particles are screened to obtain particles with required meshes, and the particles are dried at low temperature, the drying temperature is controlled to be 50 ℃, and the drying time is 6 hours.
(4) And (2) preparing a kudzu root powder colloidal solution according to the step (1), using the kudzu root powder colloidal solution as an adhesive, mixing the dried particles obtained in the step (3) with the kudzu root powder, and performing secondary granulation by using a conventional fluidized bed, wherein the adhesive is sprayed on the top, the amount of the kudzu root powder is 10% of the mass of the kudzu root powder used in the primary granulation, the amount of the adhesive is 1/2% of the amount of the adhesive used in the step (3), the particle size of the particles is controlled to be about 40-60 meshes, the prepared particles are screened to obtain the required particles, and are dried, the drying temperature is controlled to be 50 ℃, and the drying time is 6 hours, so that the high-boiling-point kudzu root fragrant particles are obtained.
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production to obtain a cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes made of the kudzu root particles without the essence and spice, the cigarette has the advantages that the sweet taste of smoke is remarkably improved, the tobacco fragrance is outstanding, the smoke harmony is good, and the sensory evaluation score is increased by 1.5.
Example 4
(1) Preparing dried radix Puerariae powder according to the requirement of granulation equipment, adding water 15 times of radix Puerariae powder volume into radix Puerariae powder, gelatinizing at 85 deg.C, and heating for 100min to obtain colloidal solution with mass concentration of 7%;
(2) keeping the gelatinized pueraria powder colloidal solution at 90 +/-5 ℃, adding the soluble dried orange peel extract, and stirring to uniformly mix to obtain a first mixture; the soluble dried orange peel extract accounts for 1% of the mass fraction of the first mixture;
(3) and (3) taking the first mixture obtained in the step (2) as an adhesive, and performing primary granulation on the dried radix puerariae powder by using a conventional fluidized bed, wherein the adhesive is sprayed at the bottom, the using amount of the dried radix puerariae powder is 32 times of the absolute dry amount of the gelatinized radix puerariae powder obtained in the step (1), the granularity of the particles is controlled to be about 60-80 meshes, the prepared particles are screened to obtain particles with required meshes, and the particles are dried at low temperature, the drying temperature is controlled to be 40 ℃, and the drying time is 6 hours.
(4) And (2) preparing a kudzu root powder colloidal solution according to the step (1), using the kudzu root powder colloidal solution as an adhesive, mixing the dried particles obtained in the step (3) with the kudzu root powder, and performing secondary granulation by using a conventional fluidized bed, wherein the adhesive is sprayed on the top, the amount of the kudzu root powder is 10% of the mass of the kudzu root powder used in the primary granulation, the amount of the adhesive is 1/2% of the amount of the adhesive used in the step (3), the particle size of the particles is controlled to be about 40-60 meshes, the prepared particles are screened to obtain the required particles, and are dried, the drying temperature is controlled to be 40 ℃, and the drying time is 6 hours, so that the high-boiling-point kudzu root fragrant particles are obtained.
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production to obtain a cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes manufactured by using kudzu vine root particles without adding essence and spice, the cigarette has the advantages that the smoke moisture-producing feeling is remarkably improved, the orange fragrance is obvious, the smoke comfort is improved, and the sensory evaluation score is increased by 1.5.
Example 5
(1) Preparing dried radix Puerariae powder according to the requirement of granulation equipment, adding water 15 times of radix Puerariae powder volume into radix Puerariae powder, gelatinizing at 85 deg.C, and heating for 50min until the mass concentration of the obtained colloidal solution is 4%;
(2) keeping the gelatinized pueraria powder colloidal solution at 90 +/-5 ℃, adding menthol, and stirring to uniformly mix to obtain a first mixture; menthol accounts for 1.5% of the first mixture by mass;
(3) and (3) taking the first mixture obtained in the step (2) as an adhesive, and performing primary granulation on the dried radix puerariae powder by using a conventional fluidized bed, wherein the adhesive is sprayed at the bottom, the using amount of the dried radix puerariae powder is 40 times of the absolute dry amount of the gelatinized radix puerariae powder obtained in the step (1), the granularity of the particles is controlled to be about 60-80 meshes, the prepared particles are screened to obtain particles with required meshes, and the particles are dried at low temperature, the drying temperature is controlled to be 40 ℃, and the drying time is 6 hours.
(4) And (2) preparing a kudzu root powder colloidal solution according to the step (1), using the kudzu root powder colloidal solution as an adhesive, mixing the dried particles obtained in the step (3) with the kudzu root powder, and performing secondary granulation by using a conventional fluidized bed, wherein the adhesive is sprayed on the top, the amount of the kudzu root powder is 10% of the mass of the kudzu root powder used in the primary granulation, the amount of the adhesive is 1/2% of the amount of the adhesive used in the step (3), the particle size of the particles is controlled to be about 40-60 meshes, the prepared particles are screened to obtain the required particles, and are dried, the drying temperature is controlled to be 40 ℃, and the drying time is 6 hours, so that the high-boiling-point kudzu root fragrant particles are obtained.
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production to obtain a cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes made of the kudzu root particles without the essence and spice, the cigarette has the advantages that the smoke cooling feeling is remarkably improved, the oral cavity generates body fluid, the cigarette is comfortable, the smoke is elegant, and the sensory evaluation score is increased by 1 point.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (6)
1. A preparation method of high-boiling-point kudzuvine root fragrant granules is characterized by comprising the following steps: the method comprises the following steps:
(1) adding a certain amount of water into the dried radix puerariae powder, heating and pasting to obtain a radix puerariae powder colloidal solution with the mass concentration of 3-8%;
(2) keeping the gelatinized pueraria powder colloidal solution at the temperature of more than 80 ℃, then adding a certain amount of essence and flavor, and stirring to uniformly mix to obtain a first mixture; the used essence is soluble in water with boiling point higher than 80 deg.C; the essence and flavor is water-soluble plum essence, water-soluble agarwood extract, water-soluble tobacco extract, water-soluble tangerine peel extract or menthol, and the essence and flavor accounts for 1-2% of the first mixture by mass;
(3) taking the first mixture obtained in the step (2) as an adhesive, and performing primary granulation on the dried radix puerariae powder by using a conventional fluidized bed, wherein the adhesive is sprayed at the bottom, the granularity of the particles is controlled to be 60-80 meshes, and the prepared particles are screened to obtain particles with required meshes and are dried at low temperature;
(4) and (2) mixing the dried particles obtained in the step (3) with a small amount of dried radix puerariae powder, and performing secondary granulation by using a conventional fluidized bed, wherein the adhesive is sprayed on the top, the particle size of the particles is controlled to be 40-60 meshes, and the prepared particles are screened to obtain the required particles and dried to obtain the high-boiling-point radix puerariae fragrant particles.
2. The method for preparing high-boiling-point pueraria lobata particles according to claim 1, wherein the method comprises the steps of: in the step (3) and the step (4), the drying temperature of the particles is not more than 60 ℃, and the drying time is 3-6 h.
3. The method for preparing high-boiling-point pueraria lobata particles according to claim 1, wherein the method comprises the steps of: the concentration of the kudzu root powder colloidal solution in the step (4) is the same as that of the kudzu root powder colloidal solution prepared in the step (1), and the using amount of the adhesive in the step (4) is 1/2 of the mass of the adhesive in the step (3).
4. The method for preparing high-boiling-point pueraria lobata particles according to claim 1, wherein the method comprises the steps of: the amount of the dried kudzu root powder in the step (3) is 30-40 times of the absolute dry amount of the gelatinized kudzu root powder in the step (1), and the amount of the dried kudzu root powder added in the step (4) is 10% of the mass of the dried kudzu root powder used in the primary granulation.
5. The method for preparing high-boiling-point pueraria lobata particles according to claim 1, wherein the method comprises the steps of: in the step (1), water with a volume 15 times of that of the kudzu powder is added, gelatinization is carried out at 85-90 ℃, heating time is controlled for 30-120min, and the mass concentration of the obtained colloidal solution is 3-8%.
6. A high boiling point kudzu flavor granule obtained by the production method according to any one of claims 1 to 5.
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