CN109619649B - Preparation method of novel high-filling-value sheet special for tobacco products - Google Patents
Preparation method of novel high-filling-value sheet special for tobacco products Download PDFInfo
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- CN109619649B CN109619649B CN201811398053.8A CN201811398053A CN109619649B CN 109619649 B CN109619649 B CN 109619649B CN 201811398053 A CN201811398053 A CN 201811398053A CN 109619649 B CN109619649 B CN 109619649B
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- powder
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- 235000019505 tobacco product Nutrition 0.000 title claims abstract description 49
- 238000011049 filling Methods 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 241000208125 Nicotiana Species 0.000 claims abstract description 52
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 52
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 34
- 238000002156 mixing Methods 0.000 claims abstract description 30
- 239000000843 powder Substances 0.000 claims abstract description 30
- 238000001035 drying Methods 0.000 claims abstract description 18
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 17
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 17
- 239000000835 fiber Substances 0.000 claims abstract description 17
- 238000005096 rolling process Methods 0.000 claims abstract description 14
- 238000005303 weighing Methods 0.000 claims abstract description 14
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000004088 foaming agent Substances 0.000 claims abstract description 11
- 239000000463 material Substances 0.000 claims abstract description 10
- 235000009508 confectionery Nutrition 0.000 claims abstract description 9
- 238000006243 chemical reaction Methods 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 7
- 238000009740 moulding (composite fabrication) Methods 0.000 claims abstract description 7
- 238000004537 pulping Methods 0.000 claims abstract description 7
- 239000011344 liquid material Substances 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 230000008961 swelling Effects 0.000 claims abstract description 6
- 230000002378 acidificating effect Effects 0.000 claims abstract description 5
- 239000000853 adhesive Substances 0.000 claims abstract description 5
- 230000001070 adhesive effect Effects 0.000 claims abstract description 5
- 238000000034 method Methods 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 16
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 6
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 6
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 6
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 235000016337 monopotassium tartrate Nutrition 0.000 claims description 6
- GBCAVSYHPPARHX-UHFFFAOYSA-M n'-cyclohexyl-n-[2-(4-methylmorpholin-4-ium-4-yl)ethyl]methanediimine;4-methylbenzenesulfonate Chemical compound CC1=CC=C(S([O-])(=O)=O)C=C1.C1CCCCC1N=C=NCC[N+]1(C)CCOCC1 GBCAVSYHPPARHX-UHFFFAOYSA-M 0.000 claims description 6
- KYKNRZGSIGMXFH-ZVGUSBNCSA-M potassium bitartrate Chemical compound [K+].OC(=O)[C@H](O)[C@@H](O)C([O-])=O KYKNRZGSIGMXFH-ZVGUSBNCSA-M 0.000 claims description 6
- 229940086065 potassium hydrogentartrate Drugs 0.000 claims description 6
- 239000000661 sodium alginate Substances 0.000 claims description 6
- 235000010413 sodium alginate Nutrition 0.000 claims description 6
- 229940005550 sodium alginate Drugs 0.000 claims description 6
- 229960002920 sorbitol Drugs 0.000 claims description 6
- 235000013599 spices Nutrition 0.000 claims description 6
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 4
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
- 108010010803 Gelatin Proteins 0.000 claims description 2
- 239000001358 L(+)-tartaric acid Substances 0.000 claims description 2
- 235000011002 L(+)-tartaric acid Nutrition 0.000 claims description 2
- FEWJPZIEWOKRBE-LWMBPPNESA-N L-(+)-Tartaric acid Natural products OC(=O)[C@@H](O)[C@H](O)C(O)=O FEWJPZIEWOKRBE-LWMBPPNESA-N 0.000 claims description 2
- 229910019142 PO4 Inorganic materials 0.000 claims description 2
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 2
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 2
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 claims description 2
- 229910000020 calcium bicarbonate Inorganic materials 0.000 claims description 2
- 229920006184 cellulose methylcellulose Polymers 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- 239000000845 maltitol Substances 0.000 claims description 2
- 235000010449 maltitol Nutrition 0.000 claims description 2
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 claims description 2
- 229940035436 maltitol Drugs 0.000 claims description 2
- 235000010355 mannitol Nutrition 0.000 claims description 2
- 239000010452 phosphate Substances 0.000 claims description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 2
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 claims description 2
- 235000015497 potassium bicarbonate Nutrition 0.000 claims description 2
- 229910000028 potassium bicarbonate Inorganic materials 0.000 claims description 2
- 239000011736 potassium bicarbonate Substances 0.000 claims description 2
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 2
- 235000011181 potassium carbonates Nutrition 0.000 claims description 2
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- 239000001540 sodium lactate Substances 0.000 claims description 2
- 235000011088 sodium lactate Nutrition 0.000 claims description 2
- 229940005581 sodium lactate Drugs 0.000 claims description 2
- 159000000000 sodium salts Chemical class 0.000 claims description 2
- 239000002304 perfume Substances 0.000 abstract 1
- 239000002002 slurry Substances 0.000 abstract 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 27
- 239000000779 smoke Substances 0.000 description 10
- 230000001953 sensory effect Effects 0.000 description 9
- 239000011122 softwood Substances 0.000 description 9
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 8
- 230000000694 effects Effects 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 5
- 238000013441 quality evaluation Methods 0.000 description 5
- 238000000889 atomisation Methods 0.000 description 4
- 239000002526 disodium citrate Substances 0.000 description 4
- 235000019262 disodium citrate Nutrition 0.000 description 4
- 229940079896 disodium hydrogen citrate Drugs 0.000 description 4
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 description 4
- 239000000686 essence Substances 0.000 description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 description 4
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 4
- 239000001509 sodium citrate Substances 0.000 description 4
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 description 4
- 229940038773 trisodium citrate Drugs 0.000 description 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 235000019640 taste Nutrition 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 235000019614 sour taste Nutrition 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241001076388 Fimbria Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000003571 electronic cigarette Substances 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention provides a preparation method of a novel high-filling-value special sheet for tobacco products, which comprises the following steps: 1) drying the tobacco raw material, and crushing into tobacco powder; 2) the tobacco powder is mixed with adhesive, alkaline foaming agent and acidic foaming agent to form powder material; 3) mixing a certain amount of water with sweet swelling agent, acidity regulator, essence, and perfume to obtain liquid material, introducing carbon dioxide, and pressurizing; 4) weighing the additional fiber, pulping into slurry by adopting a disc mill, introducing carbon dioxide, and pressurizing; 5) weighing an atomizing agent; 6) fully mixing the powder, the liquid material, the additional fiber and the atomizing agent in a pressurized homogeneous reaction kettle; 7) and 6) after the mixed material is discharged, preparing the novel sheet special for the tobacco product with the high filling value by rolling, forming, drying, shredding, cooling and drying under normal pressure.
Description
Technical Field
The invention relates to the technical field of tobacco sheets, in particular to a preparation method of a novel high-filling-value special sheet for tobacco products.
Background
In recent years, with the increasing preference of consumers for electronic cigarettes, new types of heat-not-combustible tobacco products such as iQos of fimbria, Glo of Yinmei tobacco, Ploom Tech of Japanese tobacco, and the like have rapidly emerged, and are attracting high attention in the tobacco industry. The non-combustible product is generally used together with traditional tobacco or novel tobacco products, and is produced by baking and heating tobacco through a special heating rod, the working mode is to heat solid tobacco to a low temperature below 350 ℃ to achieve an atomization degree, and the non-combustible product is heated by carbon, electric, ceramic and the like. As the user still sucks the tobacco or tobacco products, the taste is close to the real tobacco, and the acceptability is high. The novel special sheet for the tobacco products is one of the main raw materials for heating and non-burning the novel tobacco products, and the problems of poor filling capability, poor atomization effect, low product rolling yield and the like exist at present.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a preparation method of a novel sheet special for tobacco products with high filling value, which is used for preparing the novel sheet special for the tobacco products by using a novel rolling method, wherein the sheet is mainly prepared from tobacco components, can bear fragrance and atomize smoke, can improve filling capacity, enhance atomization effect and product rolling yield, and has positive promotion effect on the development of the novel tobacco products.
The technical scheme adopted by the invention for solving the technical problems is as follows: the preparation method of the novel special sheet for the tobacco products comprises the following steps:
1) drying the tobacco raw material, and crushing into tobacco powder;
2) mixing a certain amount of tobacco powder, an adhesive, an alkaline foaming agent and an acidic foaming agent according to the weight ratio of 100: 0.1-5: homogenizing and mixing at a ratio of 0.1-5:0.1-1 to obtain powder;
3) mixing a certain amount of water, a sweet swelling agent, an acidity regulator and essence and spice in a weight ratio of 100: 0.1-5: homogenizing and mixing at a ratio of 0.1-1:0.1-1 to obtain liquid material, introducing sufficient carbon dioxide, and pressurizing;
4) weighing a certain amount of added fibers, pulping to 15-25 DEG SR by using a disc mill, introducing sufficient carbon dioxide into the pulped pulp with the concentration of 10-20%, and pressurizing;
5) weighing a certain amount of atomizing agent;
6) mixing the powder obtained in the step 2), the liquid obtained in the step 3), the external fiber weighed in the step 4) and the atomizing agent weighed in the step 5) in a weight ratio of 1: 1-2: 0.1-0.5: 0.2-0.4, fully mixing in a homogeneous reaction kettle with the pressure of 2-3 atmospheres;
7) and 6) after the mixed material is discharged, preparing the novel sheet special for the tobacco product with the high filling value by rolling, forming, drying, shredding, cooling and drying under normal atmospheric pressure.
Further, the tobacco raw material in the step 1) is one or a mixture of several of tobacco leaves, tobacco shreds, tobacco stems and tobacco stem shreds.
Further, the water content of the tobacco powder in the step 1) is 1-10%.
Further, the adhesive in the step 2) is one or a mixture of more of sodium alginate, CMC and gelatin.
Further, the alkaline foaming agent in the step 2) is one or a mixture of more of potassium bicarbonate, sodium bicarbonate, calcium bicarbonate, potassium carbonate and sodium carbonate.
Further, the acidic foaming agent in the step 2) is potassium hydrogen tartrate.
Further, the sweet swelling agent in the step 3) is one or a mixture of more of D-mannitol, maltitol and D-sorbitol.
Further, the acidity regulator in the step 3) is one or a mixture of L (+) -tartaric acid, phosphate, citric acid and sodium salt, potassium salt and sodium lactate thereof.
Further, the essence in the step 3) is one or a mixture of more of a tobacco extract and a tobacco essence.
Further, the pressure of the pressurization in the step 4) is 2-3 atmospheric pressures.
Further, the additional fiber is one or a mixture of two of hardwood fiber and softwood fiber.
Further, the atomizing agent is one or a mixture of two of glycerol and propylene glycol.
The invention has the beneficial effects that:
the method organically combines a thick pulp method and a rolling method, applies a novel rolling method to prepare the novel special tobacco product sheet which takes tobacco components as main bodies, can bear fragrance and atomize smoke, utilizes the carbon dioxide to release after atmospheric pressure is reduced and to generate carbon dioxide through chemical reaction after drying and heating, so that bubbles are generated inside the sheet and the sheet is porous, increases the internal surface area, solves the problems of poor filling capability, poor atomizing effect and low product rolling yield, and has positive promotion effect on the development of novel tobacco products.
Detailed description of the invention
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. The specific embodiments described herein are merely illustrative of the invention and do not delimit the invention.
Example 1
A preparation method of a novel special sheet for tobacco products comprises the following steps:
1) the method comprises the following steps of (1) mixing tobacco shreds and tobacco stem shreds in a weight ratio of 9: 1, crushing into tobacco powder with the water content of 8 percent;
2) mixing a certain amount of tobacco powder with sodium alginate, CMC, sodium bicarbonate and potassium hydrogen tartrate in a weight ratio of 100: 2: 1: 2: 0.5 into powder;
3) mixing a certain amount of water with D-sorbitol, disodium hydrogen citrate, trisodium citrate and essence and spice according to the weight ratio of 100: 1.5: 0.1: 0.4: 0.5 into liquid material, introducing sufficient carbon dioxide, and pressurizing under 2.5 atmospheres;
4) weighing a certain amount of softwood fiber, pulping to 20-degree SR by using a disc mill, introducing sufficient carbon dioxide into the pulped pulp with the concentration of 10%, and pressurizing at the pressure of 2.5 atmospheric pressures.
5) Weighing a certain amount of glycerol;
6) mixing powder, liquid, softwood fiber pulp and glycerol in a weight ratio of 1: 1: 0.3: 0.3 in a homogenizing reaction kettle with the pressure of 2.5 atmospheres.
7) After the mixed material in the step 6) is discharged, the sheet special for the novel tobacco product with the high filling value is prepared by rolling and forming for 5 times, drying at 105 ℃, shredding and cooling and drying under normal atmospheric pressure, and the sheet special for the novel tobacco product with the high filling value is prepared into the novel tobacco product for sensory quality evaluation.
Example 2
A preparation method of a novel special sheet for tobacco products comprises the following steps:
1) the method comprises the following steps of (1) mixing tobacco shreds and tobacco stem shreds in a weight ratio of 9: 1, crushing into tobacco powder with the water content of 8 percent;
2) mixing a certain amount of tobacco powder with sodium alginate, CMC, sodium bicarbonate and potassium hydrogen tartrate in a weight ratio of 100: 1.5: 1.5: 2: 1 into powder material;
3) mixing a certain amount of water with D-sorbitol, disodium hydrogen citrate, trisodium citrate and essence and spice according to the weight ratio of 100: 1.5: 0.1: 0.4: 0.5 into liquid material, introducing sufficient carbon dioxide, and pressurizing under 2.5 atmospheres;
4) weighing a certain amount of softwood fiber, pulping to 20-degree SR by using a disc mill, introducing sufficient carbon dioxide into the pulped pulp with the concentration of 10%, and pressurizing at the pressure of 2.5 atmospheric pressures.
5) Weighing a certain amount of glycerol;
6) mixing powder, liquid, softwood fiber pulp and glycerol in a weight ratio of 1: 1: 0.3: 0.3 in a homogenizing reaction kettle with the pressure of 2.5 atmospheres.
7) After the mixed material in the step 6) is discharged, the sheet special for the novel tobacco product with the high filling value is prepared by rolling and forming for 5 times, drying at 105 ℃, shredding and cooling and drying under normal atmospheric pressure, and the sheet special for the novel tobacco product with the high filling value is prepared into the novel tobacco product for sensory quality evaluation.
Example 3
A preparation method of a novel special sheet for tobacco products comprises the following steps:
1) the method comprises the following steps of (1) mixing tobacco shreds and tobacco stem shreds in a weight ratio of 8: 2, crushing the mixture into tobacco powder with the water content of 8 percent;
2) mixing a certain amount of tobacco powder with sodium alginate, CMC, sodium bicarbonate and potassium hydrogen tartrate in a weight ratio of 100: 2: 1: 2: 1 into powder material;
3) mixing a certain amount of water with D-sorbitol, disodium hydrogen citrate, trisodium citrate and essence and spice according to the weight ratio of 100: 1.0: 0.1: 0.4: 1.0, introducing sufficient carbon dioxide, and pressurizing under 2.5 atmospheres;
4) weighing a certain amount of softwood fiber, pulping to 22 DEG SR by adopting a disc mill, introducing sufficient carbon dioxide into the pulped pulp with the concentration of 10%, and pressurizing with the pressure of 2.5 atmospheric pressures.
5) Weighing a certain amount of glycerol;
6) mixing powder, liquid, softwood fiber pulp and glycerol in a weight ratio of 1: 1: 0.3: 0.3 in a homogenizing reaction kettle with the pressure of 2.5 atmospheres.
7) After the mixed material in the step 6) is discharged, the sheet special for the novel tobacco product with the high filling value is prepared by rolling and forming for 5 times, drying at 105 ℃, shredding and cooling and drying under normal atmospheric pressure, and the sheet special for the novel tobacco product with the high filling value is prepared into the novel tobacco product for sensory quality evaluation.
Example 4
A preparation method of a novel special sheet for tobacco products comprises the following steps:
1) the method comprises the following steps of (1) mixing tobacco shreds and tobacco stem shreds in a weight ratio of 8: 2, crushing the mixture into tobacco powder with the water content of 8 percent;
2) mixing a certain amount of tobacco powder with sodium alginate, CMC, sodium bicarbonate and potassium hydrogen tartrate in a weight ratio of 100: 2: 1: 3: 0.5 into powder;
3) mixing a certain amount of water with D-sorbitol, disodium hydrogen citrate, trisodium citrate and essence and spice according to the weight ratio of 100: 1.5: 0.1: 0.4: 1.0, introducing sufficient carbon dioxide, and pressurizing under 2 atmospheric pressures;
4) weighing a certain amount of softwood fibers, pulping to 22-degree SR by adopting a disc mill, introducing sufficient carbon dioxide into the pulped pulp with the concentration of 10%, and pressurizing at the pressure of 2 atmospheric pressures.
5) Weighing a certain amount of glycerol;
6) mixing powder, liquid, softwood fiber pulp and glycerol in a weight ratio of 1: 1: 0.3: 0.3 in a homogenizing reaction kettle with the pressure of 2 atmospheres.
7) After the mixed material in the step 6) is discharged, the sheet special for the novel tobacco product with the high filling value is prepared by rolling and forming for 5 times, drying at 105 ℃, shredding and cooling and drying under normal atmospheric pressure, and the sheet special for the novel tobacco product with the high filling value is prepared into the novel tobacco product for sensory quality evaluation.
The special thin sheet prepared in the embodiment 1-4 has good filling capacity, good atomization effect and higher product rolling yield, and compared with the treatment without adding a foaming agent, a swelling agent and an acidity regulator and introducing carbon dioxide, the thin sheet filling value is improved by 5-15%. The special sheets prepared in examples 1 to 4 were prepared into tobacco products which were not burned by heating, and the results of sensory quality evaluation were as follows:
example 1 the non-combustible heated tobacco product has stable sensory quality, sufficient aroma, large smoke amount, dense smoke, good conglobation, strong sweet feeling and no obvious defect of smoking taste;
example 2 the non-burning tobacco product heated has stable sensory quality, sufficient aroma, large smoke amount, dense smoke, good conglobation, strong sweet feeling and weak cool sour taste;
example 3 the non-burning tobacco product heated has stable sensory quality, sufficient aroma, large smoke amount, fine and smooth smoke, better conglobation, stronger sweet feeling and weak cool sour taste;
example 4 the non-combustible tobacco product heated has stable sensory quality, sufficient aroma, large smoke amount, smooth smoke, good conglobation, strong sweet feeling and no obvious defect of smoking taste.
The above description is only an embodiment of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions that can be easily conceived by those skilled in the art within the technical scope of the present invention are included in the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.
Claims (10)
1. A preparation method of a novel high-filling-value sheet special for tobacco products is characterized by comprising the following steps: the method comprises the following steps:
1) drying the tobacco raw material, and crushing into tobacco powder;
2) mixing a certain amount of tobacco powder, an adhesive, an alkaline foaming agent and an acidic foaming agent according to the weight ratio of 100: 0.1-5: homogenizing and mixing at a ratio of 0.1-5:0.1-1 to obtain powder;
3) mixing a certain amount of water, a sweet swelling agent, an acidity regulator and essence and spice in a weight ratio of 100: 0.1-5: homogenizing and mixing at a ratio of 0.1-1:0.1-1 to obtain liquid material, introducing sufficient carbon dioxide, and pressurizing;
4) weighing a certain amount of added fibers, pulping to 15-25 DEG SR by using a disc mill, introducing sufficient carbon dioxide into the pulped pulp with the concentration of 10-20%, and pressurizing;
5) weighing a certain amount of atomizing agent;
6) mixing the powder obtained in the step 2), the liquid obtained in the step 3), the external fiber weighed in the step 4) and the atomizing agent weighed in the step 5) in a weight ratio of 1: 1-2: 0.1-0.5: 0.2-0.4, fully mixing in a homogeneous reaction kettle with the pressure of 2-3 atmospheres;
7) and 6) after the mixed material is discharged, preparing the novel sheet special for the tobacco product with the high filling value by rolling, forming, drying, shredding, cooling and drying under normal atmospheric pressure.
2. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the tobacco raw material in the step 1) is one or a mixture of more of tobacco leaves, tobacco shreds, tobacco stems and tobacco stem shreds.
3. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the water content of the tobacco powder in the step 1) is 1-10%.
4. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the adhesive in the step 2) is one or a mixture of more of sodium alginate, CMC and gelatin.
5. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the alkaline foaming agent in the step 2) is one or a mixture of more of potassium bicarbonate, sodium bicarbonate, calcium bicarbonate, potassium carbonate and sodium carbonate.
6. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the acidic foaming agent in the step 2) is potassium hydrogen tartrate.
7. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the sweet swelling agent in the step 3) is one or a mixture of more of D-mannitol, maltitol and D-sorbitol.
8. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the acidity regulator in the step 3) is one or a mixture of L (+) -tartaric acid, phosphate, citric acid and sodium salt, potassium salt and sodium lactate thereof.
9. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the essence in the step 3) is one or a mixture of more of tobacco extract and tobacco essence.
10. The method for preparing the novel high-filling-value special sheet for tobacco products according to claim 1, is characterized in that: the pressure of the pressurization in the step 4) is 2-3 atmospheric pressures.
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| CN111227298A (en) * | 2020-01-07 | 2020-06-05 | 湖北中烟工业有限责任公司 | Preparation method of high-smoke-quantity heating non-combustion tobacco cartridge |
| CN112137153B (en) * | 2020-10-23 | 2022-06-21 | 湖北中烟工业有限责任公司 | HNB cut tobacco atomizing agent processing technology |
| CN113349431A (en) * | 2021-07-14 | 2021-09-07 | 中国烟草总公司郑州烟草研究院 | Heating atomization body for single-port suction and application mode |
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