CN104544540B - A kind of preparation method of vacuum freeze drying fruit grain electronics tobacco tar - Google Patents
A kind of preparation method of vacuum freeze drying fruit grain electronics tobacco tar Download PDFInfo
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- CN104544540B CN104544540B CN201410817941.4A CN201410817941A CN104544540B CN 104544540 B CN104544540 B CN 104544540B CN 201410817941 A CN201410817941 A CN 201410817941A CN 104544540 B CN104544540 B CN 104544540B
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- Prior art keywords
- vacuum freeze
- freeze drying
- fruit
- fruit grain
- electronic cigarette
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Abstract
The invention discloses a kind of preparation method of vacuum freeze drying fruit grain electronics tobacco tar. Joined in electronic cigarette oil base oil by the weight ratio of vacuum freeze drying fruit grain 1～90%, fruit pulp is vacuum freeze drying in any proportion, then damaged one-tenth particle; Base oil comprises essence and flavoring agent 0～10%, deionized water 0～15%, and glycerine 2～80%, surplus is supplied 100% weight with propane diols or polyethylene glycol again, stirs and evenly mixs and obtain vacuum freeze drying fruit grain electronic cigarette oil product. Adding of vacuum freeze drying fruit grain can bring natural fruit aroma to tobacco tar, aspect flavouring, has clear superiority. The present invention makes these fragrance components immerse electronics tobacco tar, gives electronic cigarette profit fruit characteristic perfume, can promote fragrance matter and the perfume quantity of electronic cigarette, has better covered the thorn larynx that Alevaire brings, and improves consumer's satisfaction.
Description
Technical field
The preparation method who the present invention relates to a kind of vacuum freeze drying fruit grain electronics tobacco tar, belongs to tobacco preparing technical field.
Background technology
Electronic cigarette has the outward appearance similar to cigarette, and tobacco tar (electroniccigaretteliquid) produces under the effect of electronic smoke atomizerFog is similar to true cigarette flue gas, but not containing harmful substances such as tar, carbon monoxide. At present, commercially available electronics tobacco tar is deployed into various essence and flavoring agentsProduct, larger in the perceptual difference distance of the aspect such as fragrance, mouthfeel and cigarette, allow people be difficult to accept or be accustomed to its fragrance and taste, even exhaust headSwoon and nauseating sensation. Vacuum freeze drying fruit grain effectively keeps perfume (or spice), taste, the look of original fruit, it add can bring to tobacco tar naturalFruit aroma, and in tobacco tar, see see fruit grain, give a kind of brand-new impression of consumer and experience.
Summary of the invention
The object of this invention is to provide a kind of vacuum freeze drying fruit grain, be applied in electronics tobacco tar compatibility, promote fragrance and the quality of tobacco tar suction.
Object of the present invention is achieved through the following technical solutions.
A preparation method for vacuum freeze drying fruit grain electronics tobacco tar, preparation method is as follows:
Joined in electronic cigarette oil base oil by the weight ratio of vacuum freeze drying fruit grain 1～90%, stir and evenly mix and obtain vacuumFreeze drying fruit grain electronic cigarette oil product.
Described fruit grain comprises: apple, strawberry, banana, pears, lemon, blueberry, Kiwi berry, peach, durian, dragon fruit,The fruit of at least one fruit in pineapple, jackfruit, "Hami" melon, rambutan, grape, lichee, mango, shaddock, orange, jujubeMeat smash after through vacuum freeze drying, then damaged become size be 5～80 object particles.
Described vacuum freeze-drying technique condition is that fruit packs in freeze-drying dish and puts into-20 DEG C～-30 DEG C freezer precoolings 15～30Minute, then precooling is crossed to fruit and put into vacuum freeze drier, control temperature of heating plate and rise to 50 DEG C～60 DEG C from room temperatureDry 30～40 hours, controlling vacuum in heating process was 30～80pa.
Described base oil comprises essence and flavoring agent 0～10%, deionized water 0～15%, and glycerine 2～80%, surplus is again with the third twoAlcohol or polyethylene glycol are supplied 100% weight.
Described vacuum freeze drying fruit grain does not add any additive and anticorrisive agent.
Described essence and flavoring agent, glycerine, propane diols or polyethylene glycol, be edible rank.
The invention has the beneficial effects as follows:
The present invention has broken through the fragrance nature sense organ of existing electronic cigarette tobacco tar existence and has experienced not enough bottleneck, gives tobacco tar lasting, good, naturally fragrantSense of taste is subject to, and for electronic cigarette tobacco tar industry provides more fragrance matter adding technique and the product of high-quality, improves and adds cigarette oil added value.
Detailed description of the invention
For convenience of understanding the present invention better, be illustrated by following instance. These examples belong to protection scope of the present invention, but do not limit thisBright protection domain.
Embodiment 1
Get apple pulp, pack in freeze-drying dish and put into-30 DEG C of freezer precoolings 15 minutes, smash and briquet; Then by the one-tenth piece apple of precoolingPut into vacuum freeze drier, control temperature of heating plate and rise to 60 DEG C and be dried 30 hours from room temperature, in control heating process, vacuum is30pa, the breakage after vacuum freeze drying becomes 5 object spheric granules. Take the apple grain 10g after vacuum freeze drying, join base oil (byEssence and flavoring agent: deionized water: glycerine: propane diols is that 150g: 150g: 650g: 50g is mixed and made into 1000g base oil) in 990g, stirMix and obtain performing vacuum freeze drying on apple grain electronic cigarette oil product.
Embodiment 2
Get strawberry pulp and pack in freeze-drying dish and put into-28 DEG C of freezer precoolings 25 minutes, smash and briquet; Then by the one-tenth piece strawberry of precoolingPut into vacuum freeze drier, control temperature of heating plate and rise to 55 DEG C and be dried 35 hours from room temperature, controlling vacuum in heating process is 60Pa. After vacuum freeze drying, damaged one-tenth 20 object spheric granules, measure the strawberry grain 500g after vacuum freeze drying by weight percentage, joinIn base oil (by deionized water: glycerine: propane diols is that 100g: 800g: 100g is mixed and made into 1000g base oil) 500g, be uniformly mixed allThe even vacuum freeze drying strawberry grain electronic cigarette oil product that obtains.
Embodiment 3
Get peach pulp and pack in freeze-drying dish and put into-28 DEG C of freezer precoolings 25 minutes, smash and briquet; Then the one-tenth piece peach of precooling is putEnter in vacuum freeze drier, control temperature of heating plate and rise to 60 DEG C and be dried 22 hours from room temperature, controlling vacuum in heating process is 30pa.Damaged one-tenth 80 object irregular particles after vacuum freeze drying, measure the peach grain after vacuum freeze drying by weight percentage: essence and flavoring agent 900g,Join in base oil (by essence and flavoring agent: glycerine: polyethylene glycol is that 150g: 700g: 150g is mixed and made into 1000g base oil) 100g, stirMix and mix and obtain vacuum freeze drying peach grain electronic cigarette oil product.
Embodiment 4
Get mango, dragon fruit, pineapple pulp and put into-20 DEG C of freezer precoolings 30 minutes by weight packing at 50: 30: 20 in freeze-drying dish, smashMix and briquet; Then the one-tenth piece fruit of precooling is put into vacuum freeze drier, control temperature of heating plate and rise to 60 DEG C dry from room temperatureDry 30 hours, controlling vacuum in heating process was 50pa. Damaged one-tenth 40 object spheric granules after vacuum freeze drying, by weight percentageMeasure the mixed fruit grain 200g after vacuum freeze drying, join base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 100g:100g: 500g: 300g is mixed and made into 1000g base oil) in 800g, be uniformly mixed and obtain vacuum freeze drying mixed fruit grain electronics tobacco tarProduct.
Embodiment 5
Get rambutan, lichee, shaddock pulp and pack in any proportion in freeze-drying dish and put into-28 DEG C of freezer precoolings 25 minutes, smash and mix and suppressBecome piece; Then the one-tenth piece fruit of precooling is put into vacuum freeze drier, controls temperature of heating plate and rise to 50 DEG C and be dried 40 hours from room temperature,Controlling vacuum in heating process is 60pa. After vacuum freeze drying, damaged one-tenth 50 object spheric granules, measure vacuum refrigeration by weight percentageDried mixed fruit grain 400g, join base oil (by essence and flavoring agent: deionized water: glycerine: polyethylene glycol is 50g: 150g: 750g:50g is mixed and made into 1000g base oil) in 600g, be uniformly mixed and obtain vacuum freeze drying mixed fruit grain electronic cigarette oil product.
Embodiment 6
Get durian, jackfruit, Hami melon pulp and put into-30 DEG C of freezer precoolings 20 minutes by weight packing at 20: 50: 30 in freeze-drying dish, beatBroken mixing briquet; Then the one-tenth piece fruit of precooling is put into vacuum freeze drier, control temperature of heating plate and rise to 60 DEG C from room temperatureDry 30 hours, controlling vacuum in heating process was 50pa. Damaged one-tenth 60 object spheric granules, by weight percentages after vacuum freeze dryingThan the mixed fruit grain 100g measuring after vacuum freeze drying, join base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 150g:150g: 20g: 680g is mixed and made into 1000g base oil) in 900g, be uniformly mixed and obtain vacuum freeze drying mixed fruit grain electronics tobacco tarProduct.
Embodiment 7
Get apple, strawberry, banana, pears, lemon, blueberry, Kiwi berry, peach, durian, dragon fruit, pineapple, jackfruit, "Hami" melon, red hairThe pulp of pellet, grape, lichee, mango, shaddock, orange, jujube packs in freeze-drying dish and puts into-30 DEG C of freezer precoolings 30 minutes by any ratio,Smash and mix and briquet; Then the one-tenth piece fruit of precooling is put into vacuum freeze drier, control temperature of heating plate and rise to 50 DEG C from room temperatureDry 40 hours down, controlling vacuum in heating process was 30pa. After vacuum freeze drying damaged become 80 object spheric granules, by weight hundredProportion by subtraction measures the mixed fruit grain 600g after vacuum freeze drying, joins base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is150g: 150g: 200g: 500g is mixed and made into 1000g base oil) in 400g, be uniformly mixed and obtain vacuum freeze drying mixed fruit grain electricitySub-tobacco tar product.
Claims (1)
1. a preparation method for vacuum freeze drying fruit grain electronics tobacco tar, is characterized in that, preparation method is as follows: by vacuumThe weight ratio of freeze drying fruit grain 1～90% joins in electronic cigarette oil base oil, stirs and evenly mixs and obtain vacuum freeze drying waterFruit grain electronic cigarette oil product;
Described fruit grain comprises: apple, strawberry, banana, pears, lemon, blueberry, Kiwi berry, peach, durian, dragon fruit, spinachThe pulp of at least one fruit in trailing plants, jackfruit, "Hami" melon, rambutan, grape, lichee, mango, shaddock, orange, jujubeVacuum freeze drying in any proportion, then damaged one-tenth size is 5～80 object particles;
Described vacuum freeze-drying technique condition is that fruit packs in freeze-drying dish and puts into-20 DEG C～-30 DEG C freezer precoolings 15～30Minute, smash and mix and briquet, then precooling is crossed to fruit chunk and put into vacuum freeze drier, control temperature of heating plateRise to 50 DEG C～60 DEG C from room temperature and be dried 30～40 hours, controlling vacuum in heating process is 30～80pa;
Described base oil comprises essence and flavoring agent 0～10%, deionized water 0～15%, and glycerine 2～80%, surplus is again with the third twoAlcohol or polyethylene glycol are supplied 100% weight;
Described vacuum freeze drying fruit grain does not add any additive and anticorrisive agent;
Described essence and flavoring agent, glycerine, propane diols or polyethylene glycol, be edible rank.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410817941.4A CN104544540B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum freeze drying fruit grain electronics tobacco tar |
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| CN201410817941.4A CN104544540B (en) | 2014-12-24 | 2014-12-24 | A kind of preparation method of vacuum freeze drying fruit grain electronics tobacco tar |
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| CN104544540A CN104544540A (en) | 2015-04-29 |
| CN104544540B true CN104544540B (en) | 2016-05-04 |
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| CN106136301A (en) * | 2016-07-15 | 2016-11-23 | 广西中烟工业有限责任公司 | The preparation method of a kind of Hylocereus undatus extract and the application in Medicated cigarette thereof |
| CN106136298A (en) * | 2016-08-23 | 2016-11-23 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of litchi spirit odor type electronic cigarette tobacco tar |
| CN106108102A (en) * | 2016-08-23 | 2016-11-16 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of red pitaya wine odor type electronic cigarette tobacco tar |
| CN106307601A (en) * | 2016-08-23 | 2017-01-11 | 广西壮族自治区农业科学院农产品加工研究所 | Longan wine scent type electronic cigarette liquid |
| CN106723306B (en) * | 2017-01-16 | 2018-05-18 | 云南中烟新材料科技有限公司 | A kind of method that cigarette filter rod additive is prepared with American mint |
| CN107853750A (en) * | 2017-10-11 | 2018-03-30 | 吴雷 | A kind of solid tobacco tar and its processing method |
| GB201718033D0 (en) * | 2017-11-01 | 2017-12-13 | Nicoventures Holdings Ltd | Flavoured vaporisable formulation |
| CN109757783A (en) * | 2019-03-05 | 2019-05-17 | 铂德（深圳）科技有限公司 | Fragaia ananassa Duchesne extract solution, strawberry electronics tobacco tar and preparation method thereof |
| CN109984372A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Mango extract solution, mango electronics tobacco tar and preparation method thereof |
| CN110655986A (en) * | 2019-09-25 | 2020-01-07 | 武汉黄鹤楼香精香料有限公司 | Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103054170A (en) * | 2012-12-28 | 2013-04-24 | 昌宁德康生物科技有限公司 | Preparation method of water tobacco pulp atomized liquid |
| CN103054171A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from flat-flavor tobacco |
| CN104041935B (en) * | 2014-06-06 | 2016-08-24 | 山东中烟工业有限责任公司 | A kind of extracting method of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice |
| CN104068468B (en) * | 2014-07-11 | 2016-02-03 | 张伟滨 | Shredded tobacco for water pipes fruit combustion being applied to electronic smoking set and traditional shredded tobacco for water pipes smoking set and preparation method thereof |
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