CN104544542B - Preparation method for vacuum freeze drying mint grain electronic cigarette liquid - Google Patents
Preparation method for vacuum freeze drying mint grain electronic cigarette liquid Download PDFInfo
- Publication number
- CN104544542B CN104544542B CN201410818382.9A CN201410818382A CN104544542B CN 104544542 B CN104544542 B CN 104544542B CN 201410818382 A CN201410818382 A CN 201410818382A CN 104544542 B CN104544542 B CN 104544542B
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- China
- Prior art keywords
- mint
- electronic cigarette
- grain
- herba menthae
- vacuum
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Abstract
The invention discloses a preparation method for vacuum freeze drying mint grain electronic cigarette liquid. The preparation method is characterized in that 1%-90% of vacuum freeze drying mint grains in percentage by weight are added into base oil of the electronic cigarette liquid, and the mint grains are formed by pressing mint leaves into mint blocks, carrying out vacuum freeze drying, and then breaking the mint blocks into grains; the base oil comprises the components in percentage by weight: 0-10% of essence and flavor, 0-15% of deionized water, 2%-80% of glycerol and the balance of propylene glycol or polyethylene glycol which is supplemented to be 100%, and the vacuum freeze drying mint grain electronic cigarette liquid can be obtained by uniformly stirring and mixing. The vacuum freeze drying mint grains are used in the electronic cigarette liquid for increasing the coordination and the cooling sense of smoke flavor of the electronic cigarette liquid, reducing the irritation on the oral cavity and the throat and keeping more durable and stable cooling sense; meanwhile, a traditional flavor blending mode of mint electronic cigarette is broken through, the preparation process of the vacuum freeze drying mint grains is simple, the industrial production technology is mature, and the practicability is higher.
Description
Technical field
The present invention relates to a kind of preparation method of vacuum lyophilization Herba Menthae grain electronics ree-oil, belongs to Nicotiana tabacum L. manufacturing technology neck
Domain.
Background technology
Electronic cigarette is a kind of novel electronic product, and it has outward appearance, the ree-oil (electronic as medicated cigarette
Cigarette liquid) can produce smog, suction out taste with feeling also like medicated cigarette is the same in the presence of electronic smoke atomizer
Come.It is different from medicated cigarette, without tobacco shred, does not burn, without harmful substances such as tar, carbon monoxides, therefore in fragrance, mouthfeel etc.
Aspect with medicated cigarette feel be essentially different.Herba Menthae is a kind of spice that people are relatively happy to benefit from, and gives people's one kind thin
The fragrant and refrigerant jealous sensation of lotus, Herba Menthae flavor and taste brings out the best in each other with the smog fragrance of electronics ree-oil, is welcome by smoker very much.Mesh
Before, commercially available mint flavored electronics ree-oil is the product being deployed into essence and flavoring agents such as menthols, and perfumery mode is more single.Mentha leave
Briquet after mixing vacuum lyophilization is smashed, it is then damaged to add the method that perfumery is carried out in ree-oil but not appear in the newspapers into granule
Road.Briquet after mentha leave vacuum lyophilization, it is then damaged to add ree-oil into granule, effectively keep the cool of original Herba Menthae
Taste vacuum lyophilization Herba Menthae grain has loose loose structure, and fragrance matter dissolubility is good, and its addition can give ree-oil band
Come natural mint flavored, and see in ree-oil see green Herba Menthae grain, to a kind of brand-new impression of consumer and experience.
The content of the invention
It is an object of the invention to provide a kind of vacuum lyophilization Herba Menthae grain, in being applied to electronics ree-oil compatibility, lifts cigarette
The fragrance and quality of oil suction.
The purpose of the present invention is achieved through the following technical solutions.
A kind of preparation method of vacuum lyophilization Herba Menthae grain electronics ree-oil, preparation method is as follows：
It is added in electronic cigarette oil base oil by the weight ratio of vacuum lyophilization Herba Menthae grain 1～90%, stirring and evenly mixing
Obtain final product vacuum lyophilization Herba Menthae grain electronic cigarette oil product.
The vacuum lyophilization Herba Menthae grain refers to that Herba Menthae leaf raw material is fitted in lyophilized plate, cold at being put into -20 DEG C～-30 DEG C
Pre-cooling 15～30 minutes and briquet in storehouse；Then the Herba Menthae leaf raw material of the in bulk of pre-cooling is put into into vacuum freeze drier
In, control temperature of heating plate is dried 30～40 hours, vacuum in control heating process at rising to 50 DEG C～60 DEG C from room temperature
For 30～80Pa；Granular size is broken into after vacuum lyophilization for 5～80 mesh.
The base oil be essence and flavoring agent 0～10%, deionized water 0～15%, glycerol 2～80%, surplus is again with third
Glycol or Polyethylene Glycol are supplied to 100% weight.
Vacuum lyophilization Herba Menthae grain of the present invention is without any additive and preservative.Described essence is fragrant
Material, glycerol, Propylene Glycol or Polyethylene Glycol, are edible rank.
The invention has the beneficial effects as follows：
The perfuming mode that the present invention breaches existing mint flavored electronic cigarette tobacco tar presence is single, gives ree-oil and stably continues
Natural refrigerant sense receive, improve the glamour of mint flavored electronics ree-oil.For the perfume (or spice) that electronic cigarette tobacco tar industry provides more high-quality
Taste material adding technique and product, improve plus cigarette oil added value.
Specific embodiment
The present invention is more fully understood for convenience, is illustrated by following instance.These examples belong to the protection of the present invention
Scope, but do not limit the scope of the invention.
Embodiment 1
Mentha leave be fitted into be put into -28 DEG C in lyophilized plate at pre-cooling 25 minutes and briquet in freezer；Then by pre-cooling
The Herba Menthae leaf raw material of in bulk is put in vacuum freeze drier, control temperature of heating plate from room temperature rise to 50 DEG C at be dried 40 it is little
When, it is 80pa to control vacuum in heating process, the damaged spheroidal particle into 5 mesh after vacuum lyophilization.Weigh vacuum freezing
Dried Herba Menthae grain 10g, is added to 990g base oils (by essence and flavoring agent：Deionized water:Glycerol:Propylene Glycol is 100g：
150g：20g：730g is mixed) in, it is uniformly mixed and obtains final product vacuum lyophilization Herba Menthae grain electronic cigarette oil product.
Embodiment 2
Mentha leave be fitted into be put into -20 DEG C in lyophilized plate at pre-cooling 30 minutes and briquet in freezer；Then by pre-cooling
The Herba Menthae leaf raw material of in bulk is put in vacuum freeze drier, control temperature of heating plate from room temperature rise to 55 DEG C at be dried 40 it is little
When, it is 30pa to control vacuum in heating process, the damaged irregular particle into 80 mesh after vacuum lyophilization.Weigh vacuum cold
Freeze dried Herba Menthae grain 900g, be added to 100g base oils (by essence and flavoring agent：Deionized water:Glycerol:Polyethylene Glycol is
50g：50g：800g：100g is mixed) in, it is uniformly mixed and obtains final product vacuum lyophilization Herba Menthae grain electronic cigarette oil product.
Embodiment 3
Mentha leave be fitted into be put into -30 DEG C in lyophilized plate at pre-cooling 15 minutes and briquet in freezer；Then by pre-cooling
The Herba Menthae leaf raw material of in bulk is put in vacuum freeze drier, control temperature of heating plate from room temperature rise to 60 DEG C at be dried 30 it is little
When, it is 50pa to control vacuum in heating process, the damaged spheroidal particle into 20 mesh after vacuum lyophilization.Weigh vacuum freezing
Dried Herba Menthae grain 500g, is added to 500g base oils (by essence and flavoring agent：Glycerol:Propylene Glycol is 50g：500g：450g is mixed
Conjunction is made) in, it is uniformly mixed and obtains final product vacuum lyophilization Herba Menthae grain electronic cigarette oil product.
Embodiment 4
Mentha leave be fitted into be put into -25 DEG C in lyophilized plate at pre-cooling 20 minutes and briquet in freezer；Then by pre-cooling
The Herba Menthae leaf raw material of in bulk is put in vacuum freeze drier, control temperature of heating plate from room temperature rise to 50 DEG C at be dried 40 it is little
When, it is 80pa to control vacuum in heating process, the damaged irregular particle into 50 mesh after vacuum lyophilization.Weigh vacuum cold
Freeze dried Herba Menthae grain 300g, be added to 700g base oils (by deionized water：Glycerol:Propylene Glycol is 150g：300g：
550g is mixed) in, it is uniformly mixed and obtains final product vacuum lyophilization Herba Menthae grain electronic cigarette oil product.
Claims (1)
1. a kind of preparation method of vacuum lyophilization Herba Menthae grain electronics ree-oil, it is characterised in that preparation method is as follows:By vacuum
The weight ratio of lyophilization Herba Menthae grain 1～90% is added in electronic cigarette oil base oil, and stirring and evenly mixing obtains final product vacuum freezing and does
Dry Herba Menthae grain electronic cigarette oil product；
The vacuum lyophilization Herba Menthae grain refers to that Herba Menthae leaf raw material is fitted in lyophilized plate, is put in -20 DEG C～-30 DEG C freezers pre-
Cold 15～30 minutes and briquet；Then the Herba Menthae leaf raw material of the in bulk of pre-cooling is put in vacuum freeze drier, is controlled
Temperature of heating plate is dried 30～40 hours at rising to 50 DEG C～60 DEG C from room temperature, control in heating process vacuum for 30～
80Pa；Granular size is broken into after vacuum lyophilization for 5～80 mesh；
The base oil be essence and flavoring agent 0～10%, deionized water 0～15%, glycerol 2～80%, surplus is again with Propylene Glycol
Or Polyethylene Glycol is supplied to 100% weight；
Described vacuum lyophilization Herba Menthae grain is without any additive and preservative；
Described essence and flavoring agent, glycerol, Propylene Glycol or Polyethylene Glycol, are edible rank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410818382.9A CN104544542B (en) | 2014-12-24 | 2014-12-24 | Preparation method for vacuum freeze drying mint grain electronic cigarette liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410818382.9A CN104544542B (en) | 2014-12-24 | 2014-12-24 | Preparation method for vacuum freeze drying mint grain electronic cigarette liquid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104544542A CN104544542A (en) | 2015-04-29 |
| CN104544542B true CN104544542B (en) | 2017-04-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410818382.9A Active CN104544542B (en) | 2014-12-24 | 2014-12-24 | Preparation method for vacuum freeze drying mint grain electronic cigarette liquid |
Country Status (1)
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107048464B (en) * | 2017-01-16 | 2018-07-27 | 云南中烟新材料科技有限公司 | One reuse method for growing tobacco useless object |
| CN114680362B (en) * | 2021-12-28 | 2023-03-21 | 四川三联新材料有限公司 | Electronic cigarette liquid with refreshing function |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20090005477U (en) * | 2007-12-03 | 2009-06-08 | 김완중 | Electronic cigaret |
| US20140088044A1 (en) * | 2012-09-21 | 2014-03-27 | Basil Rigas | Product comprising a nicotine-containing material and an anti-cancer agent |
| CN102960852B (en) * | 2012-11-14 | 2015-04-22 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| CN103919281A (en) * | 2013-01-16 | 2014-07-16 | 深圳瀚星翔科技有限公司 | Electronic cigarette atomized liquid |
| CN103919274B (en) * | 2013-01-16 | 2016-08-10 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette atomizing liquid |
| CN103054171A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from flat-flavor tobacco |
| CN104068468B (en) * | 2014-07-11 | 2016-02-03 | 张伟滨 | Shredded tobacco for water pipes fruit combustion being applied to electronic smoking set and traditional shredded tobacco for water pipes smoking set and preparation method thereof |
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| CN104544542A (en) | 2015-04-29 |
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