CN104544542A - Preparation method for vacuum freeze drying mint grain electronic cigarette liquid - Google Patents
Preparation method for vacuum freeze drying mint grain electronic cigarette liquid Download PDFInfo
- Publication number
- CN104544542A CN104544542A CN201410818382.9A CN201410818382A CN104544542A CN 104544542 A CN104544542 A CN 104544542A CN 201410818382 A CN201410818382 A CN 201410818382A CN 104544542 A CN104544542 A CN 104544542A
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- China
- Prior art keywords
- vacuum freeze
- freeze drying
- grain
- mint
- peppermint
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Abstract
The invention discloses a preparation method for vacuum freeze drying mint grain electronic cigarette liquid. The preparation method is characterized in that 1%-90% of vacuum freeze drying mint grains in percentage by weight are added into base oil of the electronic cigarette liquid, and the mint grains are formed by pressing mint leaves into mint blocks, carrying out vacuum freeze drying, and then breaking the mint blocks into grains; the base oil comprises the components in percentage by weight: 0-10% of essence and flavor, 0-15% of deionized water, 2%-80% of glycerol and the balance of propylene glycol or polyethylene glycol which is supplemented to be 100%, and the vacuum freeze drying mint grain electronic cigarette liquid can be obtained by uniformly stirring and mixing. The vacuum freeze drying mint grains are used in the electronic cigarette liquid for increasing the coordination and the cooling sense of smoke flavor of the electronic cigarette liquid, reducing the irritation on the oral cavity and the throat and keeping more durable and stable cooling sense; meanwhile, a traditional flavor blending mode of mint electronic cigarette is broken through, the preparation process of the vacuum freeze drying mint grains is simple, the industrial production technology is mature, and the practicability is higher.
Description
Technical field
The present invention relates to a kind of preparation method of vacuum freeze drying peppermint grain electronics tobacco tar, belong to technical field of tobacco production.
Background technology
Electronic cigarette is a kind of Novel electronic product, and it has the outward appearance the same with cigarette, tobacco tar (electronic cigarette liquid) also can produce smog under the effect of electronic smoke atomizer as cigarette, sucking-off taste comes with sensation.It is different from cigarette, not containing pipe tobacco, does not burn, not containing the harmful substance such as tar, carbon monoxide, therefore in fragrance, mouthfeel etc. with cigarette feel be essentially different.Peppermint is that people compare a kind of spices being happy to benefit from, and give a kind of peppermint of people fragrance and refrigerant jealous sensation, minty note is jealous to bring out the best in each other with the smog fragrance of electronics tobacco tar, welcomes by smoker very much.At present, commercially available mint flavored electronics tobacco tar is the product be deployed into essence and flavoring agents such as menthols, and blending mode is comparatively single.Dried peppermint leaf smashes briquet after mixing vacuum freeze drying, then damaged become particle add the method for carrying out blending in tobacco tar and but have no report.Briquet after dried peppermint leaf vacuum freeze drying, then damaged one-tenth particle adds tobacco tar, the cool taste vacuum freeze drying peppermint grain of the original peppermint of effective maintenance has loose loose structure, fragrance matter dissolubility is good, it add can bring to tobacco tar natural mint flavored, and see in tobacco tar see green peppermint grain, to a kind of brand-new impression of consumer and experience.
Summary of the invention
The object of this invention is to provide a kind of vacuum freeze drying peppermint grain, be applied in electronics tobacco tar compatibility, promote fragrance and the quality of tobacco tar suction.
Object of the present invention is achieved through the following technical solutions.
A preparation method for vacuum freeze drying peppermint grain electronics tobacco tar, preparation method is as follows:
Joined in electronic cigarette oil base oil by the weight ratio of vacuum freeze drying peppermint grain 1 ~ 90%, stir and evenly mix and obtain vacuum freeze drying peppermint grain electronic cigarette oil product.
Described vacuum freeze drying peppermint grain refers to that dried peppermint leaf raw material loads in lyophilized plate, freezer precooling 15 ~ 30 minutes at putting into-20 DEG C ~-30 DEG C briquet; Then the dried peppermint leaf raw material of the one-tenth block of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C ~ 60 DEG C dry 30 ~ 40 hours, controlling vacuum in heating process is 30 ~ 80Pa; Being broken into granular size after vacuum freeze drying is 5 ~ 80 orders.
Described base oil is essence and flavoring agent 0 ~ 10%, deionized water 0 ~ 15%, glycerine 2 ~ 80%, and surplus supplies 100% weight with propane diols or polyethylene glycol again.
Vacuum freeze drying peppermint grain of the present invention does not add any additive and anticorrisive agent.Described essence and flavoring agent, glycerine, propane diols or polyethylene glycol, be edible rank.
The invention has the beneficial effects as follows:
The perfuming mode that the present invention breaches the existence of existing mint flavored electronic cigarette tobacco tar is single, gives tobacco tar and stablizes lasting naturally refrigerant impression, improve the glamour of mint flavored electronics tobacco tar.For electronic cigarette tobacco tar industry provides fragrance matter adding technique and the product of more high-quality, improve and add cigarette oil added value.
Detailed description of the invention
For convenience of understanding the present invention better, be illustrated by following instance.These examples belong to protection scope of the present invention, but do not limit the scope of the invention.
Embodiment 1
Dried peppermint leaf load in lyophilized plate put into-28 DEG C at freezer precooling 25 minutes briquet; Then the dried peppermint leaf raw material of the one-tenth block of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C DEG C dry 40 hours, controlling vacuum in heating process is 80pa, after vacuum freeze drying damaged become 5 object spheric granules.Take the peppermint grain 10g after vacuum freeze drying, join in 990g base oil (by essence and flavoring agent: deionized water: glycerine: propane diols is 100g: 150g: 20g: 730g to be mixed), be uniformly mixed and obtain vacuum freeze drying peppermint grain electronic cigarette oil product.
Embodiment 2
Dried peppermint leaf load in lyophilized plate put into-20 DEG C at freezer precooling 30 minutes briquet; Then the dried peppermint leaf raw material of the one-tenth block of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 55 DEG C dry 40 hours, controlling vacuum in heating process is 30pa, after vacuum freeze drying damaged become 80 object irregular particles.Take the peppermint grain 900g after vacuum freeze drying, join in 100g base oil (by essence and flavoring agent: deionized water: glycerine: polyethylene glycol is 50g: 50g: 800g: 100g to be mixed), be uniformly mixed and obtain vacuum freeze drying peppermint grain electronic cigarette oil product.
Embodiment 3
Dried peppermint leaf load in lyophilized plate put into-30 DEG C at freezer precooling 15 minutes briquet; Then the dried peppermint leaf raw material of the one-tenth block of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 60 DEG C dry 30 hours, controlling vacuum in heating process is 50pa, after vacuum freeze drying damaged become 20 object spheric granules.Take the peppermint grain 500g after vacuum freeze drying, join in 500g base oil (by essence and flavoring agent: glycerine: propane diols is 50g: 500g: 450g to be mixed), be uniformly mixed and obtain vacuum freeze drying peppermint grain electronic cigarette oil product.
Embodiment 4
Dried peppermint leaf load in lyophilized plate put into-25 DEG C at freezer precooling 20 minutes briquet; Then the dried peppermint leaf raw material of the one-tenth block of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C dry 40 hours, controlling vacuum in heating process is 80pa, after vacuum freeze drying damaged become 50 object irregular particles.Take the peppermint grain 300g after vacuum freeze drying, join in 700g base oil (by deionized water: glycerine: propane diols is 150g: 300g: 550g to be mixed), be uniformly mixed and obtain vacuum freeze drying peppermint grain electronic cigarette oil product.
Claims (5)
1. the preparation method of a vacuum freeze drying peppermint grain electronics tobacco tar, it is characterized in that, preparation method is as follows: joined in electronic cigarette oil base oil by the weight ratio of vacuum freeze drying peppermint grain 1 ~ 90%, stirs and evenly mixs and obtain vacuum freeze drying peppermint grain electronic cigarette oil product.
2. the preparation method of a kind of vacuum freeze drying peppermint grain electronics tobacco tar according to claim 1, it is characterized in that, described vacuum freeze drying peppermint grain refers to that dried peppermint leaf raw material loads in lyophilized plate, puts into-20 DEG C ~-30 DEG C freezer precoolings 15 ~ 30 minutes and briquet; Then the dried peppermint leaf raw material of the one-tenth block of precooling is put into vacuum freeze drier, control temperature of heating plate from room temperature rises to 50 DEG C ~ 60 DEG C dry 30 ~ 40 hours, controlling vacuum in heating process is 30 ~ 80Pa; Being broken into granular size after vacuum freeze drying is 5 ~ 80 orders.
3. the preparation method of a kind of vacuum freeze drying peppermint grain electronics tobacco tar according to claim 1, it is characterized in that, described base oil is essence and flavoring agent 0 ~ 10%, deionized water 0 ~ 15%, glycerine 2 ~ 80%, surplus supplies 100% weight with propane diols or polyethylene glycol again.
4., according to the preparation method of the arbitrary described a kind of vacuum freeze drying peppermint grain electronics tobacco tar of claim 1-3, it is characterized in that, described vacuum freeze drying peppermint grain does not add any additive and anticorrisive agent.
5., according to the preparation method of the arbitrary described a kind of vacuum freeze drying peppermint grain electronics tobacco tar of claim 1-3, it is characterized in that described essence and flavoring agent, glycerine, propane diols or polyethylene glycol are edible rank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410818382.9A CN104544542B (en) | 2014-12-24 | 2014-12-24 | Preparation method for vacuum freeze drying mint grain electronic cigarette liquid |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410818382.9A CN104544542B (en) | 2014-12-24 | 2014-12-24 | Preparation method for vacuum freeze drying mint grain electronic cigarette liquid |
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| Publication Number | Publication Date |
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| CN104544542A true CN104544542A (en) | 2015-04-29 |
| CN104544542B CN104544542B (en) | 2017-04-26 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410818382.9A Active CN104544542B (en) | 2014-12-24 | 2014-12-24 | Preparation method for vacuum freeze drying mint grain electronic cigarette liquid |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107048464A (en) * | 2017-01-16 | 2017-08-18 | 云南中烟新材料科技有限公司 | One reuse method for growing tobacco useless thing |
| CN114680362A (en) * | 2021-12-28 | 2022-07-01 | 四川三联新材料有限公司 | Electronic cigarette liquid with refreshing function |
Citations (7)
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| KR20090005477U (en) * | 2007-12-03 | 2009-06-08 | 김완중 | Electronic cigaret |
| CN102960852A (en) * | 2012-11-14 | 2013-03-13 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| CN103054171A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from flat-flavor tobacco |
| WO2014047569A9 (en) * | 2012-09-21 | 2014-05-30 | Basil Rigas | Product comprising a nicotine-containing material and an anti-cancer agent |
| CN103919281A (en) * | 2013-01-16 | 2014-07-16 | 深圳瀚星翔科技有限公司 | Electronic cigarette atomized liquid |
| CN103919274A (en) * | 2013-01-16 | 2014-07-16 | 深圳瀚星翔科技有限公司 | Electronic cigarette atomized liquid |
| CN104068468A (en) * | 2014-07-11 | 2014-10-01 | 张伟滨 | Hookah fruit tobacco for electronic smoking set and traditional hookah smoking set and preparing method of hookah fruit tobacco |
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2014
- 2014-12-24 CN CN201410818382.9A patent/CN104544542B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20090005477U (en) * | 2007-12-03 | 2009-06-08 | 김완중 | Electronic cigaret |
| WO2014047569A9 (en) * | 2012-09-21 | 2014-05-30 | Basil Rigas | Product comprising a nicotine-containing material and an anti-cancer agent |
| CN102960852A (en) * | 2012-11-14 | 2013-03-13 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| CN103919281A (en) * | 2013-01-16 | 2014-07-16 | 深圳瀚星翔科技有限公司 | Electronic cigarette atomized liquid |
| CN103919274A (en) * | 2013-01-16 | 2014-07-16 | 深圳瀚星翔科技有限公司 | Electronic cigarette atomized liquid |
| CN103054171A (en) * | 2013-01-25 | 2013-04-24 | 红云红河烟草(集团)有限责任公司 | Electronic cigarette liquid prepared from flat-flavor tobacco |
| CN104068468A (en) * | 2014-07-11 | 2014-10-01 | 张伟滨 | Hookah fruit tobacco for electronic smoking set and traditional hookah smoking set and preparing method of hookah fruit tobacco |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107048464A (en) * | 2017-01-16 | 2017-08-18 | 云南中烟新材料科技有限公司 | One reuse method for growing tobacco useless thing |
| CN114680362A (en) * | 2021-12-28 | 2022-07-01 | 四川三联新材料有限公司 | Electronic cigarette liquid with refreshing function |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104544542B (en) | 2017-04-26 |
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