CN107474960A - A kind of cigarette smoke sensitive color change releases the production method of fragrant particle - Google Patents
A kind of cigarette smoke sensitive color change releases the production method of fragrant particle Download PDFInfo
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- CN107474960A CN107474960A CN201710754307.4A CN201710754307A CN107474960A CN 107474960 A CN107474960 A CN 107474960A CN 201710754307 A CN201710754307 A CN 201710754307A CN 107474960 A CN107474960 A CN 107474960A
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- Prior art keywords
- cigarette
- compound
- capsule core
- production method
- binding agent
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Abstract
The present invention relates to the production method that a kind of cigarette smoke sensitive color change releases fragrant particle, this method includes preparing the steps such as compound, parcel, drying.The present invention uses color-change powder, binding agent and the uniform compound of major ingredient, has high mechanical strength so as to ensure that fragrant particle is released in discoloration, realizes that discoloration releases fragrant particle and effectively carries perfume (or spice) by being atomized perfuming mode.Consumer experiences electrochromic particles as flue gas is by and the color change that occurs during cigarette smoking, while experiences the fragrance of release, allows consumer all to obtain pleasant sensation in vision and the aspect of the sense of taste two, at the same time can also realize the effective false proof of cigarette.
Description
【Technical field】
The invention belongs to cigarette material technical field, more particularly it relates to which a kind of cigarette smoke sensitive color change is released
The production method of fragrant particle.
【Background technology】
Chinese-style cigarette, particularly low tar Virginian-type cigarette, in the prevalence of inhale taste physiology satisfaction is low, and perfume quantity is few,
Concentration is low, evacuates the defects of sense is obvious, dry sensation is strong, in order to make up this defect, constantly develops new cigarette functional material
Material, there is the particle of difference in functionality to turn into one kind and effectively carry fragrant material.Such as CN 201010239046 is related to a kind of new increasing
Fragrant mouth rod, fragrant particle is caused to be formed using aluminosilicate as carrier in comminutor, the particle can only be added in fibroin, and is being granulated
During realize and carry fragrant, single varieties.But this kind of material can not allow consumer to obtain good visual experience.If rolling up
Electrochromic particles are added in cigarette, during cigarette smoking, as certain temperature flue gas is by the way that electrochromic particles are in the same of color change
When can also effectively discharge fragrance, allow consumer to obtain the multiple impression of vision and the sense of taste, moreover it is possible to realize the effective false proof of cigarette.
CN 201210024284 discloses a kind of preparation method of active release type cigarette flavor complementing particles, to discharge bed material, have
Machine acid, organic polymer skeleton are primary raw material.Perfume is mended by carrying the technique formation active release type cigarette such as perfume, granulation, solidification
Particle.Machine mechanical strength cannot be guaranteed on this particle.
For these technological deficiencies existing for prior art, the present inventor develops a kind of cigarette smoke sensitive color change and releases perfume (or spice)
The production method of particle.
【The content of the invention】
[technical problems to be solved]
It is an object of the invention to provide the production method that a kind of cigarette smoke sensitive color change releases fragrant particle.
[technical scheme]
The present invention is achieved through the following technical solutions.
The present invention relates to the production method that a kind of cigarette smoke sensitive color change releases fragrant particle.
The step of production method, is as follows：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:50~200, the weight of binding agent and major ingredient is than 1~4:5~8, make
Color-change powder, major ingredient are well mixed with binding agent with mixing plant, obtain a kind of compound；
B, wrap up
Cigarette is added in granulating disc with capsule core, the mixing that step A is obtained in the case where granulating disc rotates
Material is sprinkling upon in cigarette capsule core, while sprays moisture, is uniformly adhered described compound and is wrapped in cigarette capsule core, obtains
The cigarette capsule core of compound parcel；
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the mixed of circle
Material parcel cigarette capsule core, then forced air drying are closed, drying, using atomization perfuming method load tobacco essence, obtains described cigarette
Flue gas sensitive color change releases fragrant particle.
A preferred embodiment of the invention, described color-change powder are one or more orange, green selected from red change
Turn yellow, palm fibre reddens, purple turns the blue or green color-change powder to bleach.
According to another preferred embodiment of the present invention, described major ingredient is that one or more are selected from plant amylum, gathered
Ethylene glycol 1000, polyethylene glycol 2000, the major ingredient of calcium carbonate or sodium acid carbonate.
According to another preferred embodiment of the present invention, described plant amylum is that one or more are selected from porous shallow lake
Powder, rice starch, wheaten starch, the starch of farina or crosslinked starch.
A preferred embodiment of the invention, described binding agent be it is one or more selected from microcrystalline cellulose,
Hydroxymethyl starch, polyacrylic resin, propane diols, the binding agent of sodium alginate or shellac.
According to the present invention another preferred embodiment, the amount for spraying moisture be the compound weight 20~
50%.
According to another preferred embodiment of the present invention, the weight of described compound and cigarette capsule core is than 5：1~25.
According to the present invention another preferred embodiment, described circular compound wrap up cigarette capsule core temperature 30~
100~200min of forced air drying under conditions of 60 DEG C.
According to the present invention another preferred embodiment, forced air drying compound parcel cigarette capsule core temperature 50~
60~150min is dried under conditions of 60 DEG C.
According to another preferred embodiment of the present invention, atomization perfuming amount is that every kilogram of cigarette smoke sensitive color change releases perfume (or spice)
Particle is 10~60g tobacco essences.
The present invention is described in more detail below.
The present invention relates to the production method that a kind of cigarette smoke sensitive color change releases fragrant particle.
The step of production method, is as follows：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:50~200, the weight of binding agent and major ingredient is than 1~4:5~8, make
Color-change powder, major ingredient are well mixed with binding agent with mixing plant, obtain a kind of compound；
Color-change powder (heat discoloration pigment) is prepared by electron transfer type organic compound system.Electron transfer type is organic
Compound is a kind of organic chromophoric system with special chemical structure.At a certain temperature because electronics transfer makes the organic matter
Molecular structure changes, so as to realize color transition.
According to the present invention, described color-change powder be it is one or more selected from red change it is orange, it is green turn yellow, palm fibre reddens, purple becomes
The blue or green color-change powder to bleach.The color-change powder that the present invention uses all is current market sales of product.
According to the present invention, described major ingredient (or base-material) is that one or more are selected from plant amylum, cetomacrogol 1000, gathered
The major ingredient of ethylene glycol 2000, calcium carbonate or sodium acid carbonate.
Wherein, described plant amylum is one or more selected from porous-starch, rice starch, wheaten starch, potato shallow lake
The starch of powder or crosslinked starch.Porous-starch, i.e. micropore starch, it is a kind of New Modified Starch, there is uncooked amylum enzyme activity
Enzyme forms aperture less than the porous cellular products for acting on uncooked amylum under gelatinization point and being formed on its pellet surface,
And extend to inside particle, it is a kind of hollow particle of similar hornet's nest shape, various materials can be contained in wherein, had
Good adsorptivity.The plant amylum that the present invention uses all is current market sales of product.
The binding agent that the present invention uses be it is one or more selected from microcrystalline cellulose, hydroxymethyl starch, polyacrylic resin,
The binding agent of propane diols, sodium alginate or shellac.The binding agent that the present invention uses all is current market sales of product.
B, wrap up
Cigarette is added in granulating disc with capsule core, the mixing that step A is obtained in the case where granulating disc rotates
Material is sprinkling upon in cigarette capsule core, while sprays moisture, is uniformly adhered described compound and is wrapped in cigarette capsule core, obtains
The cigarette capsule core of compound parcel；
Preferably, described compound is 5 with the weight ratio of capsule core with cigarette：1~25.
According to the present invention, the amount for spraying moisture is the 20~50% of the compound weight.
The cigarette capsule core and granulating disc that the present invention uses all are known to those skilled in the art of the present technique.
The granulating disc that the present invention uses is current market sales of product.Granulating disc is carried according to factory
Operated for the condition described in specification.
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the mixed of circle
Material parcel cigarette capsule core, then forced air drying are closed, drying, using atomization perfuming method load tobacco essence, obtains described cigarette
Flue gas sensitive color change releases fragrant particle.
According to the present invention, described circular compound wraps up the forced air drying under conditions of 30~60 DEG C of temperature of cigarette capsule core
100~200min, then, the compound of forced air drying parcel cigarette capsule core under conditions of 50~60 DEG C of temperature drying 60~
150min.In the present invention, the blast drier used in forced air drying is current market sales of product.
Preferably, atomization perfuming amount is that to release fragrant particle be 10~60g tobacco essences to every kilogram of cigarette smoke sensitive color change.Institute
The tobacco essence stated is any flavouring essence for tobacco generally added in cigarette processing process at present.
The bursling pressure value (kg) that cigarette smoke sensitive color change of the present invention releases fragrant particle is detected according to GB/T 16447；Using
Texture instrument (property tester, TA.newplus) is measured by grain.As a result represented with pressure value qualification rate and pressure value average.
Wherein pressure value qualification rate calculation formula：The total grain number * 100% of the qualified grain number/measurement of qualification rate=pressure value.Pressure value average is
Take the average of 50 test pressure data.Pressure value qualification rate is represented with %, is retained to 2 significant digits；Pressure value average with
Kg is represented, is retained to 2 significant digits.
The specific surface area of fragrant particle is released according to medicinal fine pellet core company standard detection cigarette smoke sensitive color change of the present invention
(m2/g)；
The adsorption capacity of fragrant particle is released according to medicinal fine pellet core company standard detection cigarette smoke sensitive color change of the present invention
(ml/g)；
The fragrance remaining time of fragrant particle is released according to medicinal fine pellet core company standard detection cigarette smoke sensitive color change of the present invention
(my god)；Its testing result is listed in Table 1 below.
Table 1：Discoloration carries the physical index determination data of fragrant particle
| Project | Bursling pressure value (kg) | Specific surface area (m2/g) | Adsorption capacity (ml/g) | Fragrance remaining time (my god) |
| Discoloration carries fragrant particle | 2.9-3.3 | 35 | 0.06 | 150 days |
[beneficial effect]
The beneficial effects of the invention are as follows：In cigarette smoke sensitive color change of the present invention releases fragrant particulate manufacturing method, change is used
The uniform compound of toner, binding agent and major ingredient, there is high mechanical strength so as to ensure that fragrant particle is released in discoloration, added by atomization
Fragrant mode realizes that discoloration releases fragrant particle and effectively carries perfume (or spice).Consumer experiences electrochromic particles with flue gas during cigarette smoking
By and the color change that occurs, while the fragrance of release is experienced, allow consumer all to be obtained in vision and the aspect of the sense of taste two fast
Sense, at the same time can also realize the effective false proof of cigarette.
【Embodiment】
The present invention is will be better understood that by following embodiments.
Embodiment 1：Production cigarette smoke sensitive color change releases fragrant particle
The implementation steps of the embodiment are as follows：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:50th, the weight of binding agent and major ingredient is than 3:7, will using mixing plant
The orange color-change powder of red change, porous-starch plant amylum major ingredient are well mixed with microcrystalline cellulose binding agent, obtain a kind of compound；
B, wrap up
It is 5 according to compound and the weight ratio of cigarette capsule core：20, cigarette is added in granulating disc with capsule core, in disk
Comminutor is sprinkling upon step A obtained compounds in cigarette capsule core in the case of rotating, while it is the compound weight to spray
46% moisture, it is uniformly adhered described compound and is wrapped in cigarette capsule core, obtains the cigarette ball of compound parcel
Core；
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the mixed of circle
Material parcel cigarette capsule core, then the forced air drying 120min under conditions of 55 DEG C of temperature are closed, is dried under conditions of 52 DEG C of temperature
120min, it is 30g tobacco essences to release fragrant particle according to every kilogram of cigarette smoke sensitive color change, using atomization perfuming method load cigarette
Hay-scented essence, obtain described cigarette smoke sensitive color change and release fragrant particle.
Embodiment 2：Production cigarette smoke sensitive color change releases fragrant particle
The implementation steps of the embodiment are as follows：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:80th, the weight of binding agent and major ingredient is than 2:6, will using mixing plant
Green flavescence color-change powder, cetomacrogol 1000 major ingredient are well mixed with hydroxymethyl starch binding agent, obtain a kind of compound；
B, wrap up
It is 5 according to compound and the weight ratio of cigarette capsule core：6, cigarette is added in granulating disc with capsule core, made in disk
Grain machine is sprinkling upon step A obtained compounds in cigarette capsule core in the case of rotating, while it is the compound weight to spray
20% moisture, it is uniformly adhered described compound and is wrapped in cigarette capsule core, obtains the cigarette ball of compound parcel
Core；
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the mixed of circle
Close material parcel cigarette capsule core, then the forced air drying 100min under conditions of temperature 60 C, dried under conditions of 54 DEG C of temperature
100min, it is 10g tobacco essences to release fragrant particle according to every kilogram of cigarette smoke sensitive color change, using atomization perfuming method load cigarette
Hay-scented essence, obtain described cigarette smoke sensitive color change and release fragrant particle.
Embodiment 3：Production cigarette smoke sensitive color change releases fragrant particle
The implementation steps of the embodiment are as follows：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:120th, the weight of binding agent and major ingredient is than 1:5, use mixing plant
Redden color-change powder, farina plant amylum major ingredient of palm fibre is well mixed with polyacrylic resin binding agent, obtained a kind of mixed
Close material；
B, wrap up
It is 5 according to compound and the weight ratio of cigarette capsule core：16, cigarette is added in granulating disc with capsule core, in disk
Comminutor is sprinkling upon step A obtained compounds in cigarette capsule core in the case of rotating, while it is the compound weight to spray
32% moisture, it is uniformly adhered described compound and is wrapped in cigarette capsule core, obtains the cigarette ball of compound parcel
Core；
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the mixed of circle
Material parcel cigarette capsule core, then the forced air drying 200min under conditions of 30 DEG C of temperature are closed, is dried under conditions of 58 DEG C of temperature
600min, it is 60g tobacco essences to release fragrant particle according to every kilogram of cigarette smoke sensitive color change, using atomization perfuming method load cigarette
Hay-scented essence, obtain described cigarette smoke sensitive color change and release fragrant particle.
Embodiment 4：Production cigarette smoke sensitive color change releases fragrant particle
The implementation steps of the embodiment are as follows：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:150th, the weight of binding agent and major ingredient is than 4:7, use mixing plant
Purple change blue variable colour powder, polyethylene glycol 2000 major ingredient are well mixed with propane diols binding agent, obtain a kind of compound；
B, wrap up
It is 5 according to compound and the weight ratio of cigarette capsule core：1, cigarette is added in granulating disc with capsule core, made in disk
Grain machine is sprinkling upon step A obtained compounds in cigarette capsule core in the case of rotating, while it is the compound weight to spray
40% moisture, it is uniformly adhered described compound and is wrapped in cigarette capsule core, obtains the cigarette ball of compound parcel
Core；
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the mixed of circle
Material parcel cigarette capsule core, then the forced air drying 180min under conditions of 36 DEG C of temperature are closed, is dried under conditions of temperature 50 C
150min, it is 40g tobacco essences to release fragrant particle according to every kilogram of cigarette smoke sensitive color change, using atomization perfuming method load cigarette
Hay-scented essence, obtain described cigarette smoke sensitive color change and release fragrant particle.
Embodiment 5：Production cigarette smoke sensitive color change releases fragrant particle
The implementation steps of the embodiment are as follows：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:180th, the weight of binding agent and major ingredient is than 3:6, use mixing plant
The green color-change powder that bleaches, crosslinked starch plant amylum major ingredient are well mixed with sodium alginate binding agent, obtain a kind of compound；
B, wrap up
It is 5 according to compound and the weight ratio of cigarette capsule core：25, cigarette is added in granulating disc with capsule core, in disk
Comminutor is sprinkling upon step A obtained compounds in cigarette capsule core in the case of rotating, while it is the compound weight to spray
50% moisture, it is uniformly adhered described compound and is wrapped in cigarette capsule core, obtains the cigarette ball of compound parcel
Core；
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the mixed of circle
Material parcel cigarette capsule core, then the forced air drying 140min under conditions of 42 DEG C of temperature are closed, is dried under conditions of 5 DEG C of temperature
80min, it is 20g tobacco essences to release fragrant particle according to every kilogram of cigarette smoke sensitive color change, using atomization perfuming method load cigarette
Hay-scented essence, obtain described cigarette smoke sensitive color change and release fragrant particle.
Embodiment 6：Production cigarette smoke sensitive color change releases fragrant particle
The implementation steps of the embodiment are as follows：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:200th, the weight of binding agent and major ingredient is than 2:8, use mixing plant
The orange color-change powder of red change, calcium carbonate major ingredient are well mixed with shellac bond, obtain a kind of compound；
B, wrap up
It is 5 according to compound and the weight ratio of cigarette capsule core：12, cigarette is added in granulating disc with capsule core, in disk
Comminutor is sprinkling upon step A obtained compounds in cigarette capsule core in the case of rotating, while it is the compound weight to spray
26% moisture, it is uniformly adhered described compound and is wrapped in cigarette capsule core, obtains the cigarette ball of compound parcel
Core；
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the mixed of circle
Material parcel cigarette capsule core, then the forced air drying 160min under conditions of 48 DEG C of temperature are closed, is dried under conditions of temperature 60 C
100min, it is 50g tobacco essences to release fragrant particle according to every kilogram of cigarette smoke sensitive color change, using atomization perfuming method load cigarette
Hay-scented essence, obtain described cigarette smoke sensitive color change and release fragrant particle.
Test example 1：Add cigarette smoke sensitive color change of the present invention and release fragrant particle cigarette and smoke panel test
Fragrant particle cigarette progress sense organ is released to adding cigarette smoke sensitive color change of the present invention according to standard GB5006.4-2005
Performance rating.Evaluation result is listed in Table 2 below.
Table 2：Add present invention discoloration and carry fragrant particle cigarette smoking result
The result of table 2 shows, adds flue gas sensitive color change of the present invention and releases the cigarette of fragrant particle its particle in aspiration procedure
Color changes, and organoleptic quality evaluation determines, suction perfume quantity is enriched, and flue gas harmony is preferable, and miscellaneous gas weakens with excitant,
Pleasant impression is sweet.
Claims (10)
1. a kind of cigarette smoke sensitive color change releases the production method of fragrant particle, it is characterised in that as follows the step of this method：
A, compound is prepared
According to color-change powder and the weight of binding agent than 1:50~200, the weight of binding agent and major ingredient is than 1~4:5~8, using stirring
Color-change powder, major ingredient are well mixed by mixing equipment with binding agent, obtain a kind of compound；
B, wrap up
Cigarette is added in granulating disc with capsule core, the obtained compounds of step A spread in the case where granulating disc rotates
In cigarette capsule core, while moisture is sprayed, be uniformly adhered described compound and be wrapped in cigarette capsule core, mixed
Expect the cigarette capsule core of parcel；
C, dry
The compound parcel cigarette for allowing step B to obtain is rotated further with capsule core in granulating disc, until obtaining the compound of circle
Cigarette capsule core, then forced air drying are wrapped up, drying, using atomization perfuming method load tobacco essence, obtains described cigarette smoke
Sensitive color change releases fragrant particle.
2. production method according to claim 1, it is characterised in that described color-change powder is that one or more are selected from red change
Orange, green flavescence, palm fibre reddens, purple turns the blue or green color-change powder to bleach.
3. production method according to claim 1, it is characterised in that described major ingredient is one or more selected from plant shallow lake
Powder, cetomacrogol 1000, polyethylene glycol 2000, the major ingredient of calcium carbonate or sodium acid carbonate.
4. production method according to claim 1, it is characterised in that described plant amylum is one or more selected from more
Hole starch, rice starch, wheaten starch, the starch of farina or crosslinked starch.
5. production method according to claim 1, it is characterised in that described binding agent is that one or more are selected from crystallite
Cellulose, hydroxymethyl starch, polyacrylic resin, propane diols, the binding agent of sodium alginate or shellac.
6. production method according to claim 1, it is characterised in that the amount for spraying moisture is the 20 of the compound weight
~50%.
7. production method according to claim 1, it is characterised in that described compound and the weight of cigarette capsule core are than 5：1
~25.
8. production method according to claim 1, it is characterised in that described circular compound wraps up cigarette capsule core in temperature
100~200min of forced air drying under conditions of 30~60 DEG C of degree.
9. production method according to claim 1, it is characterised in that the compound of forced air drying wraps up cigarette capsule core in temperature
60~150min is dried under conditions of 50~60 DEG C of degree.
10. production method according to claim 9, it is characterised in that atomization perfuming amount, which is that every kilogram of cigarette smoke is sensitive, to be become
It is 10~60g tobacco essences that color, which releases fragrant particle,.
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|---|---|---|---|
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110280223A (en) * | 2019-07-05 | 2019-09-27 | 上海华宝生物科技有限公司 | A kind of preparation method of the cigarette absorption colorful particle of essence |
| CN110833204A (en) * | 2018-08-17 | 2020-02-25 | 上海新型烟草制品研究院有限公司 | Manufacturing method of smoking article and smoking article |
| CN114027548A (en) * | 2021-05-17 | 2022-02-11 | 云南芯韵科技开发有限公司 | Aroma releasing bead for cigarette and preparation method and application thereof |
| CN115109320A (en) * | 2022-07-12 | 2022-09-27 | 云南巴菰生物科技股份有限公司 | Color-changing particle for cigarette, preparation method and application thereof |
| CN115449432B (en) * | 2022-09-22 | 2023-06-02 | 云南中烟工业有限责任公司 | Color-changeable spice, preparation method and application thereof |
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| KR20150144089A (en) * | 2014-06-16 | 2015-12-24 | 주식회사 케이티앤지 | Filter changing by smoking speed and cigarette having the same |
| JP6473016B2 (en) * | 2015-03-04 | 2019-02-20 | 株式会社ダイセル | Tobacco filter, tobacco, and filter discoloration method |
| CN205030513U (en) * | 2015-05-28 | 2016-02-17 | 江苏大亚滤嘴材料有限公司 | Compound cigarette filter rod of ternary |
| CN106617285A (en) * | 2016-09-27 | 2017-05-10 | 湖北中烟工业有限责任公司 | Variable color fragrance bead for tobacco and preparation method of the fragrance bead |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110833204A (en) * | 2018-08-17 | 2020-02-25 | 上海新型烟草制品研究院有限公司 | Manufacturing method of smoking article and smoking article |
| CN110280223A (en) * | 2019-07-05 | 2019-09-27 | 上海华宝生物科技有限公司 | A kind of preparation method of the cigarette absorption colorful particle of essence |
| CN114027548A (en) * | 2021-05-17 | 2022-02-11 | 云南芯韵科技开发有限公司 | Aroma releasing bead for cigarette and preparation method and application thereof |
| CN115109320A (en) * | 2022-07-12 | 2022-09-27 | 云南巴菰生物科技股份有限公司 | Color-changing particle for cigarette, preparation method and application thereof |
| CN115449432B (en) * | 2022-09-22 | 2023-06-02 | 云南中烟工业有限责任公司 | Color-changeable spice, preparation method and application thereof |
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Application publication date: 20171215 |