CN108004023A - Iris extract and its application in cigarette - Google Patents
Iris extract and its application in cigarette Download PDFInfo
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- CN108004023A CN108004023A CN201711338919.1A CN201711338919A CN108004023A CN 108004023 A CN108004023 A CN 108004023A CN 201711338919 A CN201711338919 A CN 201711338919A CN 108004023 A CN108004023 A CN 108004023A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/305—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation
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- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of iris extract, preparation process includes：(1) fresh iris leaf is mashed is soaked with deionized water, and soak and immersion slag are obtained after immersion；(2) soak is extracted with triacetyl glycerine, extract is concentrated under reduced pressure to obtain solution A；(3) slag will be soaked and be immersed in the complex enzyme for hydrolyzing liquid of cellulase, pectase, citric acid, vitamin C, acetic acid and water, liquid and Production With Residue of Enzymatic Hydrolysis after being digested after immersion, liquid carries out the solution B that is concentrated under reduced pressure to obtain after enzymolysis；(4) Production With Residue of Enzymatic Hydrolysis is subjected to microwave radiation exaraction, extractant is the ethanol solution of malic acid/potassium sorbate, separation of solid and liquid after the completion of extraction, and collection liquid mutually depressurizes and is concentrated to give solution C；(5) solution A, solution B and solution C are mixed into obtain iris extract.The cigarette that pipe tobacco containing iris extract of the present invention is made, the cigarette that heavy metal in flue gas Pb, Cd content and the tar content ratio discharged in regular combustion process does not include the present invention are remarkably decreased, and harmfulness weakens, and beneficial effect is obvious.
Description
Technical field
The invention belongs to cigarette additive technical field, more particularly to a kind of iris extract and its answering in cigarette
With.
Background technology
Iris, is a kind of herbaceos perennial, is distributed widely in China.Orrisroot for irides iris (Iris
Tectorum rhizome), bitter, sweet, property is cold.It is born in woods periphery, moist waterside and the knob towards sunny side.Iris
There is anti-inflammatory, have significant curative effect to asthma, pharyngolaryngitis etc.；Orrisroot as Chinese medicine, main component include Flavonoid substances and
Volatile oil, and saponin, tannin etc..
Microwave Extraction process is to penetrate medium by frequency electromagnetic waves and go directly to realize inside plant material.Microwave radiation can
Heated rapidly with being converted into thermal energy, make cell interior temperature rapid increase, cell interior moisture largely evaporates, so that thin to plant
Cell wall produces pressure.When the pressure exceedes cell membrane ability to bear, cell wall rupture, intracellular chemical constituent is diffused into week
In the solvent enclosed, so as to complete the process of extraction.The technology that the extracting solution of Microwave Extraction plant is used for tobacco curing is relatively ripe,
Belong to the hot spot studied both at home and abroad.
There is relevant technology to disclose using iris extract as the technology that additive is added in cigarette, such as middle promulgated by the State Council
Bright patent CN104886761A discloses a kind of flavoring essence for increasing the sour-sweet note of cigarette.It is by 1% laurine 0.5-
0.8th, ethyl acetate 1-2, isoamyl acetate 5-8, dorinone 0.01-0.5, dihydroactinidiolide 0.01-0.8, α-purple sieve
Blue ketone 0.01-0.8, vanillic aldehyde 1-2.5, butyl butyrate 0.5-4, acetic acid 0.5-5, lactic acid 0.5-5, dried apricot extract 4-10, plum
Sub- medicinal extract 4-10, tomato extract 1-5, iris extract 0.5-2, Zimbabwe leaf tobacco extract 3-8, propane diols 20-30,
70% alcohol 4.1-61.67 is mixed.It is dull to solve fragrance existing for existing cigarette, miscellaneous gas is more apparent, stimulates obvious
Problem, improve cigarette sucks satisfaction and pleasure degree.Present invention increase cigarette flavor amount, assigns the significantly sour-sweet perfume (or spice) of cigarette
Rhythm, fragrance enrich, and reducing stimulates.Patent CN103361176A discloses a kind of cause aroma compounds, is extracted from cause perfume material
Obtain, the cause perfume material can also select pale flag.Patent CN103263078A discloses a kind of be used for without burning volume
The preparation method of the low temperature tobacco-containing material of cigarette, tobacco-containing material is obtained by supercritical extract natural perfume plant (including iris),
So that the miscellaneous gas of low temperature tobacco-containing material is less, fragrance enriches, sense organ comfort level is obviously improved.Patent CN103305342A one kind is used for
The flavoring essence of expanded cut tobacco, essence is interior to contain orrisroot extract so that the fragrant and sweet note of expanded cut tobacco fruit, enriches fragrance, subtract
Small throat stimulates, and significantly improves the aesthetic quality of expanded cut tobacco.Above-mentioned patent is all that iris extract is changed perfume for flue gas
Spices, improves the aesthetic quality of smoking smoke.
Patent CN101461560A discloses a kind of fire-cured tobacco type low-coke tar cigarette formula and preparation process, wherein employing kite
Root of the tail extract makes tobacco leaf delicate fragrance style more prominent, releasing content of coke tar reduces as flavouring cleaner.Patent CN101461561A
A kind of cured tobacco leaf odor type transition agent and preparation method thereof and application method are disclosed, it is disclosed that orrisroot is former as extraction
One of material prepared plant extracts, the plant extracts are added in cigarette transition agent, reduce the miscellaneous gas of flue gas, reduction is harmful into
Point, prominent cigarette flavor style effect is obvious.Although refer to reduce harmful components, the species of harmful components is not filled
Defend oneself bright, also do not enlighten accordingly, therefore iris extract in the invention is still used primarily as spices.
The content of the invention
The present invention provides a kind of iris extraction that can reduce heavy metal Pb in cigarette smoke, Cd contents and tar content
Thing, the preparation process of the iris extract include：
(1) fresh iris leaf is mashed, adds 80~90 DEG C of immersion more than 24h of deionized water, separation of solid and liquid obtains after the completion of immersion
Obtain soak and immersion slag；
(2) soak is extracted with triacetyl glycerine, extraction temperature is less than 10 DEG C, is stood after the completion of extraction, removes top
Water layer, is concentrated under reduced pressure triacetyl glycerine layer, obtains solution A；
(3) by it is described immersion slag be immersed in complex enzyme for hydrolyzing liquid, the complex enzyme for hydrolyzing liquid include cellulase, pectase,
Citric acid, vitamin C, acetic acid and water, the temperature that complex enzyme for hydrolyzing liquid is kept in immersion process is 50~55 DEG C, after the completion of immersion
Liquid and Production With Residue of Enzymatic Hydrolysis after separation of solid and liquid is digested, liquid is concentrated under reduced pressure after the enzymolysis, obtains solution B；
(4) Production With Residue of Enzymatic Hydrolysis is subjected to microwave radiation exaraction, extractant is the ethanol solution of malic acid/potassium sorbate, has been extracted
Into rear separation of solid and liquid, collection liquid is mutually concentrated under reduced pressure, and obtains solution C；
(5) solution A, solution B and solution C are mixed, that is, obtains the iris extract.
Further, in the step (1), the mass ratio of deionized water and fresh iris leaf is 4~6:1.
Further, in the step (2), the volume of triacetyl glycerine used is the 0.8 of soak volume to be extracted
~1 times, extraction time >=5h, triacetyl glycerine layer is concentrated under reduced pressure into the 1/3~1/2 of original volume.
Further, in the complex enzyme for hydrolyzing liquid, by mass percentage, the content of each component is：Cellulase
0.5%~0.8%, pectase 0.5%~0.8%, citric acid 12%~17%, vitamin C 6%~8%, acetic acid 1%~5%, remaining is water,
The sum of each component percentage is 100%.
Further, in the step (3), the liquid of the complex enzyme for hydrolyzing liquid and immersion slag consolidates mass ratio as 4~6:1,
The enzymolysis time of complex enzyme for hydrolyzing liquid is more than 48h, and be concentrated under reduced pressure into original volume 1/3~1/2 obtains solution B.
Further, in the ethanol solution of the malic acid/potassium sorbate, the mass fraction of malic acid and potassium sorbate is
13%~16%, 5%~10%.
Further, the parameter of the microwave radiation exaraction is：Microwave Extraction solid-to-liquid ratio is 1:10~15, Extracting temperature is
60~80 DEG C, microwave power is 800~1000W, 5~10min of extraction time；Original volume is concentrated under reduced pressure into the step (4)
1/5~1/4 obtain solution C.
Further, in the step (5), solution A, solution B and solution C are according to mass ratio 1:1:1 mixes.
The invention also discloses the application by above-mentioned iris extract in cigarette, and the iris extract is uniformly added
Into cigarette shreds.
Further, the additive amount of the iris extract is the 0.2 ~ 0.3% of pipe tobacco weight.
As can be seen from the above technical solutions, it is an advantage of the invention that：By improving extracting method, by iris leaf extract
The cigarette made for cigarette shreds additive, the pipe tobacco containing iris extract of the present invention, in regular combustion process
What the pipe tobacco that heavy metal in flue gas Pb, Cd content and the tar content ratio of release do not include iris extract of the present invention was made
Cigarette is remarkably decreased, and harmfulness weakens, and beneficial effect is obvious.
Embodiment
It is described in detail with reference to embodiment：
Embodiment 1
A kind of iris extract that can reduce heavy metal Pb in cigarette smoke, Cd contents and tar content, the iris extraction
The preparation process of thing includes：
(1) fresh iris leaf is mashed, adds the matter of 80~90 DEG C of immersion 24h of deionized water, deionized water and fresh iris leaf
Amount is than being 4:1, separation of solid and liquid obtains soak and immersion slag after the completion of immersion；
(2) soak is extracted with the triacetyl glycerine of 0.8 times of the soak volume, extraction temperature is less than 10 DEG C, extraction
It is 5h to take the time, is stood after the completion of extraction, removes top aqueous layer, is concentrated under reduced pressure, is concentrated under reduced pressure to triacetyl glycerine layer
1/3 to original volume obtains solution A；
(3) the immersion slag is immersed in the complex enzyme for hydrolyzing liquid of 4 times of its quality, in the complex enzyme for hydrolyzing liquid, by quality
Percentages, the content of each component are：Cellulase 0.5%, pectase 0.5%, citric acid 12%, vitamin C 6%, acetic acid 1%, its
The sum of Yu Weishui, each component percentage is 100%.The temperature that complex enzyme for hydrolyzing liquid is kept in immersion process is 50~55 DEG C, compound
The enzymolysis time of enzyme hydrolyzate is 48h, liquid and Production With Residue of Enzymatic Hydrolysis after separation of solid and liquid is digested after the completion of immersion, after the enzymolysis liquid into
Row is concentrated under reduced pressure, and be concentrated under reduced pressure into original volume 1/3 obtains solution B；
(4) by the Production With Residue of Enzymatic Hydrolysis carry out microwave radiation exaraction, extractant be malic acid/potassium sorbate ethanol solution, the apple
In the ethanol solution of tartaric acid/potassium sorbate, the mass fraction of malic acid and potassium sorbate is respectively 13%, 5%.Microwave Extraction solid-liquid
Than for 1:10, Extracting temperature is 60 DEG C, microwave power 800W, extraction time 5min；Separation of solid and liquid after the completion of extraction, collection liquid
Mutually it is concentrated under reduced pressure, be concentrated under reduced pressure into original volume 1/5 obtains solution C；
(5) by the solution A, solution B and solution C according to mass ratio 1:1:1 mixes, that is, obtains the iris extract.
Embodiment 2
A kind of iris extract that can reduce heavy metal Pb in cigarette smoke, Cd contents and tar content, the iris extraction
The preparation process of thing includes：
(1) fresh iris leaf is mashed, adds the matter of 80~90 DEG C of immersion 26h of deionized water, deionized water and fresh iris leaf
Amount is than being 5:1, separation of solid and liquid obtains soak and immersion slag after the completion of immersion；
(2) soak is extracted with the triacetyl glycerine of 0.8 times of the soak volume, extraction temperature is less than 10 DEG C, extraction
It is 6h to take the time, is stood after the completion of extraction, removes top aqueous layer, is concentrated under reduced pressure, is concentrated under reduced pressure to triacetyl glycerine layer
1/3 to original volume obtains solution A；
(3) the immersion slag is immersed in the complex enzyme for hydrolyzing liquid of 4 times of its quality, in the complex enzyme for hydrolyzing liquid, by quality
Percentages, the content of each component are：Cellulase 0.6%, pectase 0.6%, citric acid 16%, vitamin C 8%, acetic acid 4%, its
The sum of Yu Weishui, each component percentage is 100%.The temperature that complex enzyme for hydrolyzing liquid is kept in immersion process is 50~55 DEG C, compound
The enzymolysis time of enzyme hydrolyzate is 48h, liquid and Production With Residue of Enzymatic Hydrolysis after separation of solid and liquid is digested after the completion of immersion, after the enzymolysis liquid into
Row is concentrated under reduced pressure, and be concentrated under reduced pressure into original volume 1/3 obtains solution B；
(4) by the Production With Residue of Enzymatic Hydrolysis carry out microwave radiation exaraction, extractant be malic acid/potassium sorbate ethanol solution, the apple
In the ethanol solution of tartaric acid/potassium sorbate, the mass fraction of malic acid and potassium sorbate is respectively 14%, 8%.Microwave Extraction solid-liquid
Than for 1:12, Extracting temperature is 60 DEG C, microwave power 800W, extraction time 8min；Separation of solid and liquid after the completion of extraction, collection liquid
Mutually it is concentrated under reduced pressure, be concentrated under reduced pressure into original volume 1/4 obtains solution C；
(5) by the solution A, solution B and solution C according to mass ratio 1:1:1 mixes, that is, obtains the iris extract.
Embodiment 3
A kind of iris extract that can reduce heavy metal Pb in cigarette smoke, Cd contents and tar content, the iris extraction
The preparation process of thing includes：
(1) fresh iris leaf is mashed, adds the matter of 80~90 DEG C of immersion 26h of deionized water, deionized water and fresh iris leaf
Amount is than being 6:1, separation of solid and liquid obtains soak and immersion slag after the completion of immersion；
(2) soak is extracted with the triacetyl glycerine of 1 times of the soak volume, extraction temperature is less than 10 DEG C, extraction
Time is 5h, is stood after the completion of extraction, removes top aqueous layer, is concentrated under reduced pressure, is concentrated under reduced pressure into triacetyl glycerine layer
The 1/2 of original volume obtains solution A；
(3) the immersion slag is immersed in the complex enzyme for hydrolyzing liquid of 5 times of its quality, in the complex enzyme for hydrolyzing liquid, by quality
Percentages, the content of each component are：Cellulase 0.7%, pectase 0.7%, citric acid 17%, vitamin C 7%, acetic acid 5%, its
The sum of Yu Weishui, each component percentage is 100%.The temperature that complex enzyme for hydrolyzing liquid is kept in immersion process is 50~55 DEG C, compound
The enzymolysis time of enzyme hydrolyzate is more than 48h, liquid and Production With Residue of Enzymatic Hydrolysis after separation of solid and liquid is digested after the completion of immersion, after the enzymolysis
Liquid is concentrated under reduced pressure, and be concentrated under reduced pressure into original volume 1/2 obtains solution B；
(4) by the Production With Residue of Enzymatic Hydrolysis carry out microwave radiation exaraction, extractant be malic acid/potassium sorbate ethanol solution, the apple
In the ethanol solution of tartaric acid/potassium sorbate, the mass fraction of malic acid and potassium sorbate is respectively 16%, 7%.Microwave Extraction solid-liquid
Than for 1:15, Extracting temperature is 80 DEG C, microwave power 1000W, extraction time 10min；Separation of solid and liquid after the completion of extraction, is collected
Liquid phase is concentrated under reduced pressure, and be concentrated under reduced pressure into original volume 1/4 obtains solution C；
(5) by the solution A, solution B and solution C according to mass ratio 1:1:1 mixes, that is, obtains the iris extract.
Embodiment 4
A kind of iris extract that can reduce heavy metal Pb in cigarette smoke, Cd contents and tar content, the iris extraction
The preparation process of thing includes：
(1) fresh iris leaf is mashed, adds the matter of 80~90 DEG C of immersion 26h of deionized water, deionized water and fresh iris leaf
Amount is than being 6:1, separation of solid and liquid obtains soak and immersion slag after the completion of immersion；
(2) soak is extracted with the triacetyl glycerine of 0.9 times of the soak volume, extraction temperature is less than 10 DEG C, extraction
It is 5h to take the time, is stood after the completion of extraction, removes top aqueous layer, is concentrated under reduced pressure, is concentrated under reduced pressure to triacetyl glycerine layer
1/2 to original volume obtains solution A；
(3) the immersion slag is immersed in the complex enzyme for hydrolyzing liquid of 5 times of its quality, in the complex enzyme for hydrolyzing liquid, by quality
Percentages, the content of each component are：Cellulase 0.8%, pectase 0.8%, citric acid 15%, vitamin C 6%, acetic acid 4%, its
The sum of Yu Weishui, each component percentage is 100%.The temperature that complex enzyme for hydrolyzing liquid is kept in immersion process is 50~55 DEG C, compound
The enzymolysis time of enzyme hydrolyzate is 48h, liquid and Production With Residue of Enzymatic Hydrolysis after separation of solid and liquid is digested after the completion of immersion, after the enzymolysis liquid into
Row is concentrated under reduced pressure, and be concentrated under reduced pressure into original volume 1/2 obtains solution B；
(4) by the Production With Residue of Enzymatic Hydrolysis carry out microwave radiation exaraction, extractant be malic acid/potassium sorbate ethanol solution, the apple
In the ethanol solution of tartaric acid/potassium sorbate, the mass fraction of malic acid and potassium sorbate is respectively 16%, 8%.Microwave Extraction solid-liquid
Than for 1:15, Extracting temperature is 70 DEG C, microwave power 900W, extraction time 5min；Separation of solid and liquid after the completion of extraction, collection liquid
Mutually it is concentrated under reduced pressure, be concentrated under reduced pressure into original volume 1/4 obtains solution C；
(5) by the solution A, solution B and solution C according to mass ratio 1:1:1 mixes, that is, obtains the iris extract.
Embodiment 5
A kind of iris extract that can reduce heavy metal Pb in cigarette smoke, Cd contents and tar content, the iris extraction
The preparation process of thing includes：
(1) fresh iris leaf is mashed, adds the matter of 80~90 DEG C of immersion 28h of deionized water, deionized water and fresh iris leaf
Amount is than being 6:1, separation of solid and liquid obtains soak and immersion slag after the completion of immersion；
(2) soak is extracted with the triacetyl glycerine of 0.9 times of the soak volume, extraction temperature is less than 10 DEG C, extraction
It is 5h to take the time, is stood after the completion of extraction, removes top aqueous layer, is concentrated under reduced pressure, is concentrated under reduced pressure to triacetyl glycerine layer
1/2 to original volume obtains solution A；
(3) the immersion slag is immersed in the complex enzyme for hydrolyzing liquid of 6 times of its quality, in the complex enzyme for hydrolyzing liquid, by quality
Percentages, the content of each component are：Cellulase 0.8%, pectase 0.8%, citric acid 17%, vitamin C 8%, acetic acid 5%, its
The sum of Yu Weishui, each component percentage is 100%.The temperature that complex enzyme for hydrolyzing liquid is kept in immersion process is 50~55 DEG C, compound
The enzymolysis time of enzyme hydrolyzate is 48h, liquid and Production With Residue of Enzymatic Hydrolysis after separation of solid and liquid is digested after the completion of immersion, after the enzymolysis liquid into
Row is concentrated under reduced pressure, and be concentrated under reduced pressure into original volume 1/3 obtains solution B；
(4) by the Production With Residue of Enzymatic Hydrolysis carry out microwave radiation exaraction, extractant be malic acid/potassium sorbate ethanol solution, the apple
In the ethanol solution of tartaric acid/potassium sorbate, the mass fraction of malic acid and potassium sorbate is respectively 16%, 10%.Microwave Extraction is consolidated
Liquor ratio is 1:12, Extracting temperature is 80 DEG C, microwave power 800W, extraction time 10min；Separation of solid and liquid after the completion of extraction, is received
Liquid collecting is mutually concentrated under reduced pressure, and be concentrated under reduced pressure into original volume 1/5 obtains solution C；
(5) by the solution A, solution B and solution C according to mass ratio 1:1:1 mixes, that is, obtains the iris extract.
Comparative example 1
A kind of iris extract, preparation method step and embodiment 2 are identical, it is differed only in：It is compound in the step (3)
By mass percentage, the content of each component is enzyme hydrolyzate：Cellulase 0.6%, pectase 0.6%, remaining is water, each component
The sum of percentage is 100%.Do not include citric acid, vitamin C and acetic acid.Other step parameters and method are same as Example 2 complete
It is exactly the same, iris extract is finally made.
Comparative example 2
A kind of iris extract, preparation method step and embodiment 2 are identical, it is differed only in：In the step (4), extraction
Agent is using the absolute ethyl alcohol with the ethanol solution equivalent of malic acid/potassium sorbate.Other step parameters and method and 2 phase of embodiment
With identical, iris extract is finally made.
Embodiment 6
Iris extract made from above-described embodiment 1~5 and comparative example 1~2 is uniformly sprayed in cigarette shreds and made respectively
Into cigarette, the additive amount of iris extract is the 0.3% of pipe tobacco weight.Above-described embodiment 1~5 and the institute of comparative example 1~2 will be contained
The cigarette for stating iris extract lights test in test equipment, while is used as blank by the use of the common cigarette without iris extract
Control group lights test in test equipment, collects the smog after the filtering of mouth rod respectively and is detected contrast, detects flue gas
Middle heavy metal Pb, Cd contents and tar content, the results are shown in Table 1.
The pipe tobacco of embodiment 1~5, comparative example 1~2 and cigarette used in control group is selected from a batch of pipe tobacco, ensures cigarette
The source of silk is identical.
Table 1
As shown in table 1, from embodiment 1~5 and blank control group, the pipe tobacco containing iris extract of the present invention is made
Cigarette, heavy metal in flue gas Pb, Cd content and the tar content ratio discharged in regular combustion process do not include institute of the present invention
The cigarette that the pipe tobacco of iris extract is made is stated to be remarkably decreased.Comparative example 2 and comparative example 1 are understood, in complex enzyme for hydrolyzing liquid
Middle addition citric acid, vitamin C and acetic acid help to improve enzymolysis, and a large amount of beneficiating ingredients dissolve in iris extract after enzymolysis
In, showing as the removal to heavy metal in flue gas Pb, Cd and tar has facilitation.Comparative example 2 and comparative example 2 can
Know, using the ethanol solution of malic acid/potassium sorbate as Microwave Extraction liquor ratio merely using ethanol as obtained by extracting solution
Iris extract has more excellent removal effect to heavy metal in flue gas Pb, Cd and tar.
Technical solution provided by the present invention is described in detail above, for those of ordinary skill in the art,
According to the thought of the embodiment of the present invention, there will be changes in specific embodiments and applications, in conclusion this theory
Bright book content should not be construed as limiting the invention.
Claims (10)
1. a kind of iris extract, it is characterised in that preparation process includes：
(1) fresh iris leaf is mashed, adds 80~90 DEG C of immersion more than 24h of deionized water, separation of solid and liquid obtains after the completion of immersion
Obtain soak and immersion slag；
(2) soak is extracted with triacetyl glycerine, extraction temperature is less than 10 DEG C, is stood after the completion of extraction, removes top
Water layer, is concentrated under reduced pressure triacetyl glycerine layer, obtains solution A；
(3) by it is described immersion slag be immersed in complex enzyme for hydrolyzing liquid, the complex enzyme for hydrolyzing liquid include cellulase, pectase,
Citric acid, vitamin C, acetic acid and water, the temperature that complex enzyme for hydrolyzing liquid is kept in immersion process is 50~55 DEG C, after the completion of immersion
Liquid and Production With Residue of Enzymatic Hydrolysis after separation of solid and liquid is digested, liquid is concentrated under reduced pressure after the enzymolysis, obtains solution B；
(4) Production With Residue of Enzymatic Hydrolysis is subjected to microwave radiation exaraction, extractant is the ethanol solution of malic acid/potassium sorbate, has been extracted
Into rear separation of solid and liquid, collection liquid is mutually concentrated under reduced pressure, and obtains solution C；
(5) solution A, solution B and solution C are mixed, that is, obtains the iris extract.
A kind of 2. iris extract according to claim 1, it is characterised in that in the step (1), deionized water and new
The mass ratio of fresh iris leaf is 4~6:1.
3. a kind of iris extract according to claim 1, it is characterised in that in the step (2), three acetic acid used is sweet
The volume of grease is 0.8~1 times of soak volume to be extracted, and extraction time >=5h, triacetyl glycerine layer is concentrated under reduced pressure into
The 1/3~1/2 of original volume.
4. a kind of iris extract according to claim 1, it is characterised in that in the complex enzyme for hydrolyzing liquid, by quality
Percentages, the content of each component are：Cellulase 0.5%~0.8%, pectase 0.5%~0.8%, citric acid 12%~17%, dimension
Raw element C6%~8%, acetic acid 1%~5%, remaining is that the sum of water, each component percentage is 100%.
A kind of 5. iris extract according to claim 4, it is characterised in that in the step (3), the complex enzyme water
The liquid of solution liquid and immersion slag consolidates mass ratio as 4~6:1, the enzymolysis time of complex enzyme for hydrolyzing liquid is more than 48h, is concentrated under reduced pressure into original
The 1/3~1/2 of volume obtains solution B.
A kind of 6. iris extract according to claim 1, it is characterised in that the ethanol of the malic acid/potassium sorbate
In solution, the mass fraction of malic acid and potassium sorbate is 13%~16%, 5%~10%.
7. a kind of iris extract according to claim 1, it is characterised in that the parameter of the microwave radiation exaraction is：
Microwave Extraction solid-to-liquid ratio is 1:10~15, Extracting temperature is 60~80 DEG C, and microwave power is 800~1000W, extraction time 5~
10min；1/5~1/4 that original volume is concentrated under reduced pressure into the step (4) obtains solution C.
A kind of 8. iris extract according to claim 1, it is characterised in that in the step (5), solution A, solution B
With solution C according to mass ratio 1:1:1 mixes.
9. such as application of the claim 1~8 any one of them iris extract in cigarette, it is characterised in that by the kite
Tail extract is uniformly added in cigarette shreds, then the pipe tobacco for being sprayed with iris extract is made cigarette finished product.
10. application of a kind of iris extract according to claim 9 in cigarette, it is characterised in that the iris carries
The additive amount for taking thing is the 0.2 ~ 0.3% of pipe tobacco weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711338919.1A CN108004023B (en) | 2017-12-14 | 2017-12-14 | Iris extract and application thereof in cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711338919.1A CN108004023B (en) | 2017-12-14 | 2017-12-14 | Iris extract and application thereof in cigarettes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108004023A true CN108004023A (en) | 2018-05-08 |
| CN108004023B CN108004023B (en) | 2021-04-16 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108587818A (en) * | 2018-05-30 | 2018-09-28 | 陆爱明 | Peony seed oil bacteriostatic skin-care perfumed soap and preparation method thereof |
| CN110655985A (en) * | 2019-08-23 | 2020-01-07 | 广东中烟工业有限责任公司 | Spices with Chinese flue-cured tobacco characteristic aroma and heating non-combustible cigarette prepared from spices |
| CN112956733A (en) * | 2021-02-07 | 2021-06-15 | 无锡华叶生物科技有限公司 | Preparation method of iris root isolate for cigarettes |
| CN116161647A (en) * | 2023-03-15 | 2023-05-26 | 云南师范大学 | Preparation method of sorbic acid carbon quantum dots |
| CN116173170A (en) * | 2023-02-22 | 2023-05-30 | 河北一品制药股份有限公司 | A pharmaceutical composition for treating respiratory diseases, and its preparation method |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60186269A (en) * | 1984-12-28 | 1985-09-21 | 日本たばこ産業株式会社 | Improvement in tobacco smoking taste |
| CN1348725A (en) * | 2000-10-16 | 2002-05-15 | 北京倍和德营养制品科技发展有限公司 | Filter tip capable of eliminating free radical in cigarette fume and its making process |
| CN101016288A (en) * | 2007-03-06 | 2007-08-15 | 川渝中烟工业公司 | Method of stabilizing bioactivity of flavones substance |
| CN101461560A (en) * | 2008-01-29 | 2009-06-24 | 延吉烟悦科技有限公司 | Fire-cured tobacco type low-coke tar cigarette and technique for preparing the same |
| CN103305342A (en) * | 2013-06-28 | 2013-09-18 | 湖北中烟工业有限责任公司 | Casing flavor for expanded cut tobacco |
| CN104818120A (en) * | 2015-04-29 | 2015-08-05 | 湖北中烟工业有限责任公司 | Cigarette black plum extract and preparation method thereof |
| CN104886761A (en) * | 2015-05-14 | 2015-09-09 | 湖北中烟工业有限责任公司 | Flavored essence for increasing cigarette sour and sweet note |
| CN105132172A (en) * | 2015-08-28 | 2015-12-09 | 安徽中烟工业有限责任公司 | Method for preparing orris root flavonoid matter for tobaccos from orris roots |
| CN106701325A (en) * | 2017-03-08 | 2017-05-24 | 湖北中烟工业有限责任公司 | Apricot extract for tobaccos and preparation method of apricot extract |
-
2017
- 2017-12-14 CN CN201711338919.1A patent/CN108004023B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60186269A (en) * | 1984-12-28 | 1985-09-21 | 日本たばこ産業株式会社 | Improvement in tobacco smoking taste |
| CN1348725A (en) * | 2000-10-16 | 2002-05-15 | 北京倍和德营养制品科技发展有限公司 | Filter tip capable of eliminating free radical in cigarette fume and its making process |
| CN101016288A (en) * | 2007-03-06 | 2007-08-15 | 川渝中烟工业公司 | Method of stabilizing bioactivity of flavones substance |
| CN101461560A (en) * | 2008-01-29 | 2009-06-24 | 延吉烟悦科技有限公司 | Fire-cured tobacco type low-coke tar cigarette and technique for preparing the same |
| CN103305342A (en) * | 2013-06-28 | 2013-09-18 | 湖北中烟工业有限责任公司 | Casing flavor for expanded cut tobacco |
| CN104818120A (en) * | 2015-04-29 | 2015-08-05 | 湖北中烟工业有限责任公司 | Cigarette black plum extract and preparation method thereof |
| CN104886761A (en) * | 2015-05-14 | 2015-09-09 | 湖北中烟工业有限责任公司 | Flavored essence for increasing cigarette sour and sweet note |
| CN105132172A (en) * | 2015-08-28 | 2015-12-09 | 安徽中烟工业有限责任公司 | Method for preparing orris root flavonoid matter for tobaccos from orris roots |
| CN106701325A (en) * | 2017-03-08 | 2017-05-24 | 湖北中烟工业有限责任公司 | Apricot extract for tobaccos and preparation method of apricot extract |
Non-Patent Citations (5)
| Title |
|---|
| 张岩蕾: "《卷烟降焦工程》", 31 October 2000, 北京：中国轻工业出版社 * |
| 张晶等: "《中药化学》", 30 April 2015, 北京：中国农业大学出版社 * |
| 朱善元: "《基础生物化学》", 31 March 2007, 北京：中国环境科学出版社 * |
| 李晓等: "中草药萃取液在卷烟中的减害作用研究 ", 《河南农业科学》 * |
| 黄天辉等: "茉莉花茶提取物降低卷烟气中有害成分的研究 ", 《安徽农业科学》 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108587818A (en) * | 2018-05-30 | 2018-09-28 | 陆爱明 | Peony seed oil bacteriostatic skin-care perfumed soap and preparation method thereof |
| CN110655985A (en) * | 2019-08-23 | 2020-01-07 | 广东中烟工业有限责任公司 | Spices with Chinese flue-cured tobacco characteristic aroma and heating non-combustible cigarette prepared from spices |
| CN112956733A (en) * | 2021-02-07 | 2021-06-15 | 无锡华叶生物科技有限公司 | Preparation method of iris root isolate for cigarettes |
| CN116173170A (en) * | 2023-02-22 | 2023-05-30 | 河北一品制药股份有限公司 | A pharmaceutical composition for treating respiratory diseases, and its preparation method |
| CN116173170B (en) * | 2023-02-22 | 2023-11-24 | 河北一品制药股份有限公司 | A pharmaceutical composition for treating respiratory diseases, and its preparation method |
| CN116161647A (en) * | 2023-03-15 | 2023-05-26 | 云南师范大学 | Preparation method of sorbic acid carbon quantum dots |
| CN116161647B (en) * | 2023-03-15 | 2024-05-14 | 云南师范大学 | Preparation method of sorbic acid carbon quantum dots |
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