CN104041936B - A kind of extracting method of electronic cigarette Chinese style mixing odor type style tobacco juice - Google Patents
A kind of extracting method of electronic cigarette Chinese style mixing odor type style tobacco juice Download PDFInfo
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- CN104041936B CN104041936B CN201410249613.9A CN201410249613A CN104041936B CN 104041936 B CN104041936 B CN 104041936B CN 201410249613 A CN201410249613 A CN 201410249613A CN 104041936 B CN104041936 B CN 104041936B
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Abstract
The invention discloses the extracting method of a kind of electronic cigarette Chinese style mixing odor type style tobacco juice, the Nicotiana tabacum L. of flue-cured tobacco, burley tobaccos and Turkish tobaccos, tobacco shred or offal mixing, add at least one in cigarette feed liquid or cocoa powder, Radix Glycyrrhizae, Mel, black currant extract, divide temperature section dry distilling said mixture, collect fraction.The fraction that this inventive method is collected can use directly as tobacco juice for electronic smoke, also can add essence spice for cigarette or the edible essence spice with special flavor, with abundant tobacco juice for electronic smoke style.This inventive method is collected electronic cigarette liquid and is possessed style and features and the taste being similar to Chinese style blended type cigarette, and the sweet pungent appetizing having again dry in the sun cigarette of the gentleness of existing VIRGINIA and pleasant impression are pure.
Description
Technical field
The present invention relates to the extracting method of a kind of tobacco juice for electronic smoke, the extraction side of a kind of electronic cigarette Chinese style mixing odor type style tobacco juice
Method.
Background technology
There is extremely complex chemistry, physical change in Medicated cigarette during burning, cigarette mainstream flue gas composition is extremely complex, cigarette
The compound identified in gas just has kind more than 5000, there is harmful and/or poisonous component in these compounds.
Along with the countries in the world control to Medicated cigarette, tobacco business will face many difficulties.Owing to smoking property of cigarette person has and depends on sucking Medicated cigarette
Lai Xing, mandatory successful quitting rate is the lowest, and therefore novel tobacco goods arise at the historic moment as the transition product of smoking cessation.
Electronic cigarette is the one in novel tobacco goods, and electronic cigarette has another name called virtual medicated cigarette, electronic cigarette, is mainly used in smoking cessation and replaces
For medicated cigarette.It has with particularly for tobacco items as outward appearance, also like medicated cigarette the same can sucking-off cigarette, sucking-off taste with sensation come.It is a kind of logical
Cross electronics heater means and transmit the electronic installation of nicotine to respiratory system.Therefore tobacco juice formula is to affect electronic cigarette taste profile
Deciding factor, is directly connected to the Consumer acceptance of product.Owing to electronic cigarette is to make electronic cigarette liquid mist by electronics heating
Changing, and Medicated cigarette is to produce flue gas by burning tobacco, both are essentially different, but electronic cigarette smoker always wishes electronic cigarette
There is " taste " of medicated cigarette, and without hope there is " evil " of medicated cigarette.
The extraction of existing liquid tobacco juice is usually through CO2Supercritical extraction or by Nicotiana tabacum L. through one or more levels dry distilling process
After add the materials such as essence again, modulate the tobacco juice of required taste, Chinese patent CN1742636A discloses a kind of nuisanceless liquid
The production technology of body note cigarette, tobacco shred processes through dehydrating kettle, the second retort, the 3rd retort etc., and retorting step herein is multiple
Miscellaneous, it is difficult to operation, and after 430 DEG C of dry distilling, tobacco shred the most carbonization, after 555 DEG C, tobacco shred seriously carbonization,
After carbonization, tobacco shred is only as garbage, and tobacco shred is when glowing, and the temperature of combustion cone is at 400～550 DEG C, in the middle part of side-stream smoke
The content that the content of point harmful components is higher than in main flume.After dry distilling, fraction needs other substance to make
Use for electronic cigarette liquid, be unfavorable for industrialized production.Utilizing Maillard reaction is well known in the prior art to prepare flavouring essence for tobacco,
But Maillard reaction is combined with dry distilling the electronic cigarette liquid that can directly use of preparation and there is techniques below problem: Maillard reaction
Temperature relatively low, and the temperature of dry distilling is of a relatively high, if carrying out according to the temperature needed for unified Maillard reaction, tobacco juice carries
Take insufficient, react according to the temperature of dry distilling if unified, Maillard reaction may produce impurity, the most poisonous
Material, so not being unified in the extracting method of electronic cigarette mixed type style tobacco juice by Maillard reaction and dry distilling in prior art
In.
Summary of the invention
It is an object of the invention to provide the extracting method of a kind of electronic cigarette Chinese style mixing odor type style tobacco juice, what the method obtained carries
Take liquid and directly as the tobacco juice of electronic cigarette, and the suction taste of hybrid cigarette can be remained.
For reaching above-mentioned technical purpose, the present invention is achieved through the following technical solutions:
The extracting method of a kind of electronic cigarette Chinese style mixing odor type style tobacco juice, specifically includes following steps:
The Nicotiana tabacum L. of flue-cured tobacco, burley tobaccos and Turkish tobaccos, tobacco shred or offal mixing, add cigarette feed liquid or cocoa powder, Radix Glycyrrhizae, Mel,
At least one in black currant extract, point temperature section dry distilling said mixture, collect fraction.
The extracting method of a kind of electronic cigarette Chinese style mixing odor type style tobacco juice, comprises the following steps:
1) flue-cured tobacco 10-15 part, burley tobaccos 5-10 part and Nicotiana tabacum L., tobacco shred or the offal of Turkish tobaccos 3-5 part, cigarette is with feed liquid 1-5 part
Or at least one in the cocoa powder of 0.01-5 part, Radix Glycyrrhizae, Mel or black currant extract loads dry distilling tank；
2) heating dry distilling tank is to 60-120 DEG C (preferably 80 DEG C), insulation 0.5-2h (preferably 1h)；
3) after, temperature is increased to 180-240 DEG C (preferably 220 DEG C), keeps 0.5-2h (preferably 1h)；
4) fraction is collected after reaction terminates.
The solvent of above-mentioned collection fraction is followed successively by ethanol, water, propylene glycol, glycerol.
The fraction of above-mentioned collection both can be individually directly as the tobacco juice of electronic cigarette, it is also possible to make after the fraction mixing collected five kinds
For the tobacco juice of electronic cigarette, the mouthfeel of combination is more rich.
Tobacco juice obtained by said extracted method and the application in electronic cigarette of this tobacco juice.
The invention has the beneficial effects as follows: the fraction that this inventive method is collected can use directly as the tobacco juice of electronic cigarette, this cigarette
Liquid remains the suction taste of hybrid cigarette, also can add essence spice for cigarette or the edible essence spice with special flavor, with rich
Electron rich cigarette tobacco juice style.The electronic cigarette liquid that the method is extracted possesses style and features and the taste being similar to international blended type cigarette,
The sweet pungent appetizing having again dry in the sun cigarette of the gentleness of existing VIRGINIA and pleasant impression are pure.
The inventive method achieves the dry distilling of lower temperature, it is to avoid the carbonization of tobacco shred, and reduce in flue gas of knowing clearly and be harmful to into
The content divided, is effectively combined the extraction of tobacco juice with Maillard reaction, both ensure that effective extraction of tobacco juice dry distilling, has made cigarette simultaneously
Additive in liquid is directly appended in tobacco juice, need not remix, save step, reduce cost after individually producing.
Detailed description of the invention
Embodiment 1
By Burley Tobacco in Hubei Province 20g, Sichuan burley tobaccos 15g, Xinjiang cigarette 10g, Yunnan Flue-cured Tobacco 10g, Hunan Flue-cured Tobacco 20g,
Shandong flue-cured tobacco 10g and Guizhou Flue-cured Tobacco 15g adds dry distilling tank；
Add 1g cigarette feed liquid；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained at 110 DEG C, constant temperature time 0.5h；
Rise high-temperature, be maintained at 220 DEG C, constant temperature time 2h；
Fraction is collected successively with ethanol, water, propylene glycol.
Embodiment 2
By Burley Tobacco in Hubei Province 20g, Sichuan burley tobaccos 15g, Xinjiang cigarette 10g, Yunnan Flue-cured Tobacco 10g, Hunan Flue-cured Tobacco 20g,
Shandong flue-cured tobacco 10g and Guizhou Flue-cured Tobacco 15g adds dry distilling tank；
Add the Mel of 1g；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained at 80 DEG C, constant temperature time 1h；
Rise high-temperature, be maintained at 180 DEG C, constant temperature time 0.5h；
Fraction is collected successively with ethanol, water, propylene glycol.
Embodiment 3
Just Burley Tobacco in Hubei Province 20g, Sichuan burley tobaccos 15g, Xinjiang cigarette 10g, Yunnan Flue-cured Tobacco 10g, Hunan Flue-cured Tobacco 20g,
Shandong flue-cured tobacco 10g and Guizhou Flue-cured Tobacco 15g adds dry distilling tank；
Add 0.5g cocoa powder, 1.5g Radix Glycyrrhizae；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained at 100 DEG C, constant temperature time 0.5h；
Rise high-temperature, be maintained at 240 DEG C, constant temperature time 1h；
Fraction is collected successively with ethanol, water, propylene glycol, glycerol.
Embodiment 4
Weigh cigarette finished product tobacco shred 80g, wherein Guizhou Flue-cured Tobacco 40g, Sichuan burley tobaccos 26.7g and Xinjiang cigarette 13.3g；
Add 0.5g black currant extract, 1.5g Radix Glycyrrhizae；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained at 100 DEG C, constant temperature time 0.5h；
Rise high-temperature, be maintained at 240 DEG C, constant temperature time 2h；
Fraction is collected successively with ethanol, water, propylene glycol, glycerol.
The detailed description of the invention of the present invention is described although above-mentioned in conjunction with the embodiments, but not to scope
Limiting, one of ordinary skill in the art should be understood that, on the basis of technical scheme, those skilled in the art need not
Pay various amendments or deformation that creative work can make still within protection scope of the present invention.
Claims (7)
1. an electronic cigarette extracting method for Chinese style mixing odor type style tobacco juice,
It is characterized in that, comprise the following steps:
(1) flue-cured tobacco 10-15 part, burley tobaccos 5-10 part and Nicotiana tabacum L., tobacco shred or the offal of Turkish tobaccos 3-5 part, at least one in feed liquid 1-5 part or the cocoa powder of 0.01-5 part, Radix Glycyrrhizae, Mel, black currant extract of cigarette loads dry distilling tank；
(2) when using at least one in the cocoa powder of 0.01-5 part, Radix Glycyrrhizae, Mel, black currant extract: heating dry distilling tank, to 60-120 DEG C, is incubated 0.5-2h；When using cigarette with feed liquid 1-5 part: heating dry distilling tank, to 60-80 DEG C, is incubated 0.5-2h；
(3) when using at least one in the cocoa powder of 0.01-5 part, Radix Glycyrrhizae, Mel, black currant extract: afterwards temperature is increased to 180-240 DEG C, 0.5-2h is kept；When using cigarette with feed liquid 1-5 part: heating dry distilling tank, to 180-220 DEG C, keeps 0.5-2h；
(4) fraction is collected after reaction terminates.
2. the extracting method as described in claim 1, it is characterised in that described step 4) collect fraction solvent be followed successively by ethanol, water, propylene glycol, glycerol.
3. extracting method as claimed in claim 1, it is characterised in that described step 2) in heating dry distilling tank to 80 DEG C.
4. the extracting method as described in claim 1, it is characterised in that described step 3) in temperature be increased to 220 DEG C.
5. the extracting method as described in claim 1, it is characterised in that described step 2), 3) in insulation 1h.
6. the tobacco juice that the extracting method as described in claim 1-5 is arbitrary obtains.
7. the application in electronic cigarette of the tobacco juice as described in claim 6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410249613.9A CN104041936B (en) | 2014-06-06 | 2014-06-06 | A kind of extracting method of electronic cigarette Chinese style mixing odor type style tobacco juice |
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| CN201410249613.9A CN104041936B (en) | 2014-06-06 | 2014-06-06 | A kind of extracting method of electronic cigarette Chinese style mixing odor type style tobacco juice |
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| CN104041936A CN104041936A (en) | 2014-09-17 |
| CN104041936B true CN104041936B (en) | 2016-08-24 |
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Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104498184A (en) * | 2014-11-20 | 2015-04-08 | 湖北中烟工业有限责任公司 | Preparation method for tobacco flavor by utilizing fragrant honey in Maillard reaction |
| CN104585860B (en) * | 2015-01-15 | 2016-11-30 | 中国烟草总公司郑州烟草研究院 | There is the preparation method of the tobacco juice for electronic smoke of the fragrant feature of baking |
| CN104783323B (en) * | 2015-05-14 | 2016-08-17 | 安徽中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke containing Dry distillated flavor |
| CN105011355B (en) * | 2015-06-05 | 2016-07-06 | 浙江中烟工业有限责任公司 | A kind of essential oil of tobaccos and extracting method thereof and application |
| CN104921287B (en) * | 2015-06-05 | 2016-09-28 | 浙江中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke |
| CN104983064B (en) * | 2015-06-05 | 2016-06-01 | 浙江中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke and its preparation method |
| CN105559145A (en) * | 2015-12-17 | 2016-05-11 | 立场电子科技发展（上海）有限公司 | E-cigarette flavor and preparation method thereof |
| CN105595411B (en) * | 2016-02-01 | 2017-05-17 | 湖北中烟工业有限责任公司 | Method for preparing tobacco-characteristic-taste tobacco flavor material and electronic cigarette fluid containing tobacco flavor material |
| CN105725265A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Device and method for preparing tobacco source basic cigarette flavor material for novel tobacco products |
| CN108142978A (en) * | 2018-01-02 | 2018-06-12 | 四川三联新材料有限公司 | A kind of perfume material for the fragrant section of cigarette production of not burning for the heating of pipe tobacco style and preparation method thereof |
| CN108185512A (en) * | 2018-01-02 | 2018-06-22 | 四川三联新材料有限公司 | A kind of perfume material for the fragrant section of cigarette production of not burning for mixed type heating and preparation method thereof |
| CN108185510A (en) * | 2018-01-02 | 2018-06-22 | 四川三联新材料有限公司 | A kind of perfume material for the fragrant section of cigarette production of not burning for fire-cured tobacco type heating and preparation method thereof |
| CN110279163A (en) * | 2019-08-06 | 2019-09-27 | 四川三联新材料有限公司 | Fragrance dose for heating cigarette smoke section of not burning and its preparation method and application and heating are not burnt cigarette |
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| US5235992A (en) * | 1991-06-28 | 1993-08-17 | R. J. Reynolds Tobacco Company | Processes for producing flavor substances from tobacco and smoking articles made therewith |
| CN1742636A (en) * | 2004-09-02 | 2006-03-08 | 邹宝安 | Technology for producing pollution-free liquid cigarette |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4150677A (en) * | 1977-01-24 | 1979-04-24 | Philip Morris Incorporated | Treatment of tobacco |
| US5235992A (en) * | 1991-06-28 | 1993-08-17 | R. J. Reynolds Tobacco Company | Processes for producing flavor substances from tobacco and smoking articles made therewith |
| CN1742636A (en) * | 2004-09-02 | 2006-03-08 | 邹宝安 | Technology for producing pollution-free liquid cigarette |
| CN101061888A (en) * | 2006-04-27 | 2007-10-31 | 湖南中烟工业公司 | High-temperature dry distillation thermal cracking device and cracking method |
| CN102048238A (en) * | 2009-11-03 | 2011-05-11 | 程露 | Preparation method for liquid cigarette |
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Inventor after: Wang Jun Inventor after: Liu Xiaoqian Inventor after: Liu Shimin Inventor after: Zhou Shilu Inventor after: Lin Jiansheng Inventor before: Wang Jun Inventor before: Liu Xiaoqian Inventor before: Liu Shimin Inventor before: Zhou Shilu |
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Free format text: CORRECT: INVENTOR; FROM: WANG JUN LIU XIAOQIAN LIU SHIMIN ZHOU SHILU TO: WANG JUN LIU XIAOQIAN LIU SHIMIN ZHOU SHILU LIN JIANSHENG |
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