CN102871212B - Method for producing paper-making reconstituted tobacco - Google Patents

Method for producing paper-making reconstituted tobacco Download PDF

Info

Publication number
CN102871212B
CN102871212B CN201210376690.1A CN201210376690A CN102871212B CN 102871212 B CN102871212 B CN 102871212B CN 201210376690 A CN201210376690 A CN 201210376690A CN 102871212 B CN102871212 B CN 102871212B
Authority
CN
China
Prior art keywords
tobacco
under
extract
lotion
essential oil
Prior art date
Application number
CN201210376690.1A
Other languages
Chinese (zh)
Other versions
CN102871212A (en
Inventor
葛少林
徐迎波
舒俊生
田振峰
佘世科
朱栋梁
徐志强
陈开波
周顺
张晓宇
张胜军
Original Assignee
安徽中烟工业有限责任公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 安徽中烟工业有限责任公司 filed Critical 安徽中烟工业有限责任公司
Priority to CN201210376690.1A priority Critical patent/CN102871212B/en
Publication of CN102871212A publication Critical patent/CN102871212A/en
Application granted granted Critical
Publication of CN102871212B publication Critical patent/CN102871212B/en

Links

Abstract

The invention discloses a method for producing paper-making reconstituted tobacco. The method comprises the following steps of extracting essential oil from a tobacco raw material through supercritical carbon dioxide fluid; obtaining the tobacco raw material which is subjected to extraction; transferring the tobacco raw material which is subjected to the extraction to a raw material extraction tank; mixing the tobacco raw material which is subjected to the extraction with tobacco stems; performing water extraction to obtain extract liquid and solid residue; concentrating the extract liquid and then adding the essential oil into the concentrated extract to obtain dip-coating liquid; preparing a film base from the solid residue by a paper-making process; and finally coating the dip-coating liquid onto the film base to obtain the reconstituted tobacco. The method is technically feasible and can be widely used for producing the paper-making reconstituted tobacco, and the product quality is easily controlled. By the method, the use ratio of the tobacco raw material can be improved, the burden of sewage discharge can be reduced, and the appearance and sensory quality of the paper-making reconstituted tobacco can be improved.

Description

A kind of manufacture method of papermaking-method reconstituted tobaccos

Technical field:

The present invention relates to a kind of manufacture method of papermaking-method reconstituted tobaccos, particularly utilize flavor component and the humectation composition of the selective raw tobacco material of supercritical fluid, to reduce the loss of this constituents in papermaking-method reconstituted tobaccos production process, improve the method for papermaking-method reconstituted tobaccos organoleptic quality and humid keeping performance.

Background technology:

Papermaking-method reconstituted tobaccos has resistance to good processability, falls the features such as burnt effect is remarkable, product quality plasticity is strong, at tobacco business, is widely used.The raw material of papermaking-method reconstituted tobaccos, through water extraction, extracts soluble component wherein at present, and extract is concentrated after purified treatment, for the lotion of reconstituted tobacco.But this technology also exists certain defect, as the water-insoluble component in tobacco is lost in slurrying and the process of manufacturing paper with pulp, wastewater treatment pressure is large, organoleptic quality reconstituted tobacco is poor, this has caused the utilization rate of raw material low, raw tobacco material resource nervous, product usage ratio is low.

Summary of the invention:

For overcoming the defect of prior art, the object of the present invention is to provide a kind of technical feasibility, product quality controllability strong, and can be widely used in the Manufacturing Method of Products that papermaking-method reconstituted tobaccos is produced.This technology is intended to improve the utilization rate of raw tobacco material, outward appearance and the aesthetic quality who reduces sewage discharge pressure, improves papermaking-method reconstituted tobaccos.

Technical solution problem of the present invention adopts following technical scheme:

A manufacture method for papermaking-method reconstituted tobaccos, carry out in accordance with the following steps:

A, the raw tobacco material that is 5~30% by moisture content are extracted thing and through stripped raw tobacco material through supercritical carbon dioxide extraction 1-4 hour, supercritical extract pressure is 200-500mPa, extraction temperature is 40-70 ℃, and entrainer is the arbitrary proportion combination of the one or both of ethanol or water;

B, will after steps A gained extract separation and purification, obtain essential oil for the preparation of lotion, described separation and purification is one or more any combination of water washing, rectifying, molecular clock method, during water washing, the ratio of extract and water is 1:1-1:10, and water washing number of times is 1-4 time; During rectifying, tower reactor temperature is 120-180 ℃, and tower top temperature is 80-140 ℃, and reflux ratio is 3-7; During molecular clock, vapo(u)rizing temperature is 40-80 ℃, rotor speed 200-300 r/min, material flow 50-80 mL/h;

C, steps A remaining raw tobacco material after supercritical carbon dioxide extraction is transferred in raw material abstraction tank with tobacco stalk raw material and is mixed by weight 1:100-100:1, according to weight ratio, add water, water addition is 4-10 times of tobacco leaf offal compound, at the temperature of 40-65 ℃, through one or many extraction, expression separation, be extracted liquid and solid-state raw material residue;

D, the extract of step C gained is carried out to centrifugation removal impurity wherein, the extract after purification is under the temperature conditions of the vacuum of 30-100mPa and 40-80 ℃, and Vacuum Concentration to the solid content weight content in concentrate reaches 30%-55%;

E, gained essential oil in step B is added in the concentrate of step D gained and is prepared into lotion, adding proportion is: the weight ratio that essential oil accounts for lotion is 0.01%-2%;

F, by the solid-state raw material residue of step C gained through solution after fibre, defibrination, adopt paper process to make sheet base, and the lotion that step e is obtained is applied on sheet base, coating weight is 35-45%;

G, the sheet base that step F gained is coated with to lotion are dried under the temperature conditions of 100-160 ℃, reconstituted tobacco.

Raw tobacco material described in steps A is flue-cured tobacco, burley tobaccos, paste hair smoke, solarization tobacco, shine one or more the arbitrary proportion mixtures in red cigarette and Turkish tobaccos.

Compared with the prior art, beneficial effect of the present invention is embodied in:

1, the present invention utilizes water-insoluble in supercritical carbon dioxide extraction reconstituted tobacco raw material to cause fragrant component, has significantly improved the utilization rate of raw material and the organoleptic quality of reconstituted tobacco.

2, the water-insoluble component of the present invention, in slurrying and the loss of manufacturing paper with pulp in process, significantly reduces the COD value of waste water, reduces wastewater treatment pressure.

3, the assorted gas that adds the reconstituted tobacco of supercritical carbon dioxide extraction thing significantly weakens, and sense organ comfort level significantly promotes.

4, the present invention utilizes the selective of supercritical carbon dioxide extraction, can realize the regulation and control to raw material chemical constituent, thereby realize the regulation and control of reconstituted tobacco chemical constituent.

Below, by the specific embodiment, the present invention is described further.

The specific embodiment:

Embodiment 1:

The Flue-cured Tobacco powder stock that is 5% by 5 kilogram of 60 above moisture content of order adds in 24L extraction kettle, under 300mPa extracting pressure, under 50 ℃ of conditions, extract 2 hours, entrainer is 70% ethanol, and supercritical carbon dioxide extraction thing obtains essential oil 3 times with the water washing of 10 times.

After supercritical extract, offal raw material mixes according to weight ratio 5:5 with offal, and adds 80 kg of water, under 60 ℃ of temperature conditions, extracts 1 hour, then it is separated with solid residue by extract to pass through squeezing, filtration, centrifugation.Extract after purification is under the temperature conditions of the vacuum of 80mPa and 60 ℃, Vacuum Concentration to the solid content weight content in concentrate reaches 50%, and the essential oil obtaining after water washing is added in concentrate and makes lotion, essential oil accounts for 0.3% of whole lotion according to weight ratio.Solid residue after water extraction, through separating after fibre, defibrination, adopts paper process to make sheet base, and lotion is applied on sheet base, it is 38% that coating weight is controlled, flash baking under the temperature conditions of 120 ℃, cuts rear adjusting moisture content to 12%, reconstituted tobacco finished product.

The made reconstituted tobacco outward appearance of this law is soft and moist, perfume quantity is high, assorted gas is few, jealous comfortable.

Embodiment 2:

The broken end of burley tobaccos that is 25% by 5 kilogram of 60 above moisture content of order adds in 24L extraction kettle, under 350mPa extracting pressure, under 50 ℃ of conditions, extracts 2 hours.In separating still, extract is 150 ℃ in tower reactor temperature, and tower top temperature is 100 ℃, rectifying supercritical fluid tobacco extracts under the rectifying condition that reflux ratio is 5, and overhead essential oil is for lotion allotment;

After supercritical extract, mix according to weight ratio 5:5 with offal at the broken end of burley tobaccos, and add 80 kg of water, under 60 ℃ of temperature conditions, extracts 1 hour, then it is separated with solid residue by extract to pass through squeezing, filtration, centrifugation.Extract after purification is under the temperature conditions of the vacuum of 80mPa and 60 ℃, Vacuum Concentration to the solid content weight content in concentrate reaches 50%, and the essential oil obtaining after rectifying is added in concentrate and configures reconstituted tobacco coating fluid, essential oil accounts for 0.1% of whole lotion according to weight ratio.Solid residue is through solution after fibre, defibrination, adopts paper process to make sheet base, and lotion is applied on sheet base, and it is 40% that coating weight is controlled, and flash baking under the temperature conditions of 120 ℃, cuts rear adjusting moisture content to 12%, reconstituted tobacco finished product.

The burley tobaccos characteristic remarkable of the reconstituted tobacco that this law is made, assorted gas significantly reduce, the residual reduction in oral cavity, flue gas concentration increase.

Embodiment 3:

The broken end of flue-cured tobacco that is 12% by 5 kilogram of 60 above moisture content of order adds in 24L extraction kettle, and the ethanol water of use 80% is entrainer, under 350mPa extracting pressure, under 50 ℃ of conditions, extracts 2 hours.In separating still, extract carries out the molecular clock of different temperatures section under the condition of rotor speed 300 r/min, material flow 70 mL/h, collects the product essential oil of 40-60 ℃ of temperature section for lotion allotment.

After supercritical extract, flue-cured tobacco offal mixes according to weight ratio 5:5 with offal, and adds 80 kg of water, under 60 ℃ of temperature conditions, extracts 1 hour, then it is separated with solid residue by extract to pass through squeezing, filtration, centrifugation.Extract after purification is under the temperature conditions of the vacuum of 80mPa and 60 ℃, Vacuum Concentration to the solid content weight content in concentrate reaches 50%, and the essential oil obtaining after rectifying is added in concentrate and configures reconstituted tobacco lotion, essential oil accounts for 0.05% of whole lotion according to weight ratio.Solid residue is through solution after fibre, defibrination, adopts paper process to make sheet base, and lotion is applied on sheet base, and it is 40% that coating weight is controlled, and flash baking under the temperature conditions of 120 ℃, cuts rear adjusting moisture content to 12%, reconstituted tobacco finished product.

Assorted gas and the excitant of the reconstituted tobacco that this law is made significantly reduces, fragrance matter improves, flue gas concentration increases.

Embodiment 4:

Except raw material is that weight ratio is the flue-cured tobacco of 9:1 and the offal mixture of Turkish tobaccos, and the essential oil that supercritical carbon dioxide extraction is obtained is added into and in concentrate, makes lotion according to weight ratio, the content that essential oil accounts for lotion is 1.5%, and other process is as embodiment 1.

The made reconstituted tobacco outward appearance of this law is soft and moist, concentration is high, and strength is dense than high, and fragrance is full.

Claims (1)

1. a manufacture method for papermaking-method reconstituted tobaccos, is characterized in that carrying out in accordance with the following steps:
The broken end of flue-cured tobacco that is 12% by 5 kilogram of 60 above moisture content of order adds in 24L extraction kettle, and the ethanol water of use 80% is entrainer, under 350MPa extracting pressure, under 50 ℃ of conditions, extracts 2 hours;
In separating still, extract carries out the molecular clock of different temperatures section under the condition of rotor speed 300r/min, material flow 70mL/h, collects the product essential oil of 40-60 ℃ of temperature section for lotion allotment;
After supercritical extract, flue-cured tobacco offal mixes according to weight ratio 5:5 with offal, and adds 80 kg of water, under 60 ℃ of temperature conditions, extracts 1 hour, then it is separated with solid residue by extract to pass through squeezing, filtration, centrifugation;
Extract after purification is under the temperature conditions of the vacuum of 80MPa and 60 ℃, Vacuum Concentration to the solid content weight content in concentrate reaches 50%, and the essential oil obtaining after rectifying is added in concentrate and configures reconstituted tobacco lotion, essential oil accounts for 0.05% of whole lotion according to weight ratio;
Solid residue is through solution after fibre, defibrination, adopts paper process to make sheet base, and lotion is applied on sheet base, and it is 40% that coating weight is controlled, and flash baking under the temperature conditions of 120 ℃, cuts rear adjusting moisture content to 12%, reconstituted tobacco finished product.
CN201210376690.1A 2012-10-08 2012-10-08 Method for producing paper-making reconstituted tobacco CN102871212B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210376690.1A CN102871212B (en) 2012-10-08 2012-10-08 Method for producing paper-making reconstituted tobacco

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201210376690.1A CN102871212B (en) 2012-10-08 2012-10-08 Method for producing paper-making reconstituted tobacco

Publications (2)

Publication Number Publication Date
CN102871212A CN102871212A (en) 2013-01-16
CN102871212B true CN102871212B (en) 2014-10-08

Family

ID=47472926

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201210376690.1A CN102871212B (en) 2012-10-08 2012-10-08 Method for producing paper-making reconstituted tobacco

Country Status (1)

Country Link
CN (1) CN102871212B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105595401A (en) * 2016-01-06 2016-05-25 云南中烟再造烟叶有限责任公司 Preparation method of non-burning low-temperature smoking tobacco shreds
WO2020002589A1 (en) * 2018-06-29 2020-01-02 Nerudia Limited A method for manufacturing reconstituted plant material

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103263078A (en) * 2013-05-23 2013-08-28 红云红河烟草(集团)有限责任公司 Method for preparing low-temperature tobacco material used for non-combustion cigarette
CN103300464B (en) * 2013-06-28 2016-02-03 湖北中烟工业有限责任公司 Blended type cigarette processing method
CN103330277A (en) * 2013-07-02 2013-10-02 云南烟草科学研究院 Method of controlling contents of nitrate and nitrite in tobacco reconstituted in papermaking method
EP2989907A4 (en) * 2013-08-27 2017-01-11 Japan Tobacco, Inc. Tobacco raw material, method for manufacturing same, and tobacco product
CN103468406B (en) * 2013-09-18 2015-10-28 浙江中烟工业有限责任公司 This Studies of The Aromatic Substances of tobacco endogenous of a kind of directed compound collecting
CN103468403B (en) * 2013-09-18 2016-01-27 浙江中烟工业有限责任公司 A kind of water extraction and supercritical CO 2extraction process method of flavor matter in directed compound collecting tobacco from tobacco material
CN103468404B (en) * 2013-09-18 2016-01-27 浙江中烟工业有限责任公司 Adopt water extraction and supercritical CO 2the compound tobacco flavor matter that extraction process extracts
CN103462206B (en) * 2013-09-18 2015-10-28 浙江中烟工业有限责任公司 A kind of reconstituted tobacco of this Studies of The Aromatic Substances of tobacco endogenous containing directed compound collecting and cigarette prepared therefrom
CN103484245B (en) * 2013-09-18 2015-10-14 浙江中烟工业有限责任公司 The one directed composite extracting method growing tobacco this Studies of The Aromatic Substances of endogenous
CN103462204B (en) * 2013-09-18 2015-06-03 浙江中烟工业有限责任公司 Reconstituted tobacco containing composite tobacco aroma substances prepared by water extraction method and supercritical CO2 extraction method and cigarette prepared of same
CN103462209A (en) * 2013-09-26 2013-12-25 云南烟草科学研究院 Method for preparing paper-making-method reconstituted tobacco with sun-cured red tobacco style characteristic
CN103829364B (en) * 2014-03-05 2016-06-29 上海烟草集团有限责任公司 A kind of salt coating fluid and the application in reconstituted tobacco thereof
CN106235375B (en) * 2016-08-30 2017-11-17 湖北中烟工业有限责任公司 A kind of method for manufacturing the suncured tabacco reconstituted tobacco for being adapted to flue-cured tobacco flavor
CN109275947A (en) * 2018-10-08 2019-01-29 浙江中烟工业有限责任公司 A kind of supercritical extract processing method suitable for heating pipe tobacco under not combustion state
CN109275946A (en) * 2018-10-08 2019-01-29 浙江中烟工业有限责任公司 A kind of dynamic extraction processing method suitable for heating pipe tobacco under not combustion state
CN109275944A (en) * 2018-10-08 2019-01-29 浙江中烟工业有限责任公司 A kind of static extracting processing method suitable for heating pipe tobacco under not combustion state

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1401751A (en) * 2002-09-13 2003-03-12 云南瑞升科技有限公司 Method for preparing pure tobacco oil
CN101695407A (en) * 2009-10-21 2010-04-21 安徽中烟工业公司 Method for producing tobacco sheets by paper making method
CN102018274A (en) * 2010-12-31 2011-04-20 云南烟草科学研究院 Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method
CN102199490A (en) * 2010-03-24 2011-09-28 郑州轻工业学院 Method for extracting neutral aroma compositions in tobacco
CN102488319A (en) * 2011-11-27 2012-06-13 中国海诚工程科技股份有限公司 Continuous extraction method and device of papermaking reconstituted tobacco
CN102488318A (en) * 2011-11-18 2012-06-13 安徽中烟工业有限责任公司 Preparation method for aired tobacco extracts and essential oil
CN102488312A (en) * 2011-11-18 2012-06-13 安徽中烟工业有限责任公司 Raw material extracting method for paper-making-method remade tobaccos.

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1401751A (en) * 2002-09-13 2003-03-12 云南瑞升科技有限公司 Method for preparing pure tobacco oil
CN101695407A (en) * 2009-10-21 2010-04-21 安徽中烟工业公司 Method for producing tobacco sheets by paper making method
CN102199490A (en) * 2010-03-24 2011-09-28 郑州轻工业学院 Method for extracting neutral aroma compositions in tobacco
CN102018274A (en) * 2010-12-31 2011-04-20 云南烟草科学研究院 Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method
CN102488318A (en) * 2011-11-18 2012-06-13 安徽中烟工业有限责任公司 Preparation method for aired tobacco extracts and essential oil
CN102488312A (en) * 2011-11-18 2012-06-13 安徽中烟工业有限责任公司 Raw material extracting method for paper-making-method remade tobaccos.
CN102488319A (en) * 2011-11-27 2012-06-13 中国海诚工程科技股份有限公司 Continuous extraction method and device of papermaking reconstituted tobacco

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105595401A (en) * 2016-01-06 2016-05-25 云南中烟再造烟叶有限责任公司 Preparation method of non-burning low-temperature smoking tobacco shreds
CN105595401B (en) * 2016-01-06 2017-01-25 云南中烟再造烟叶有限责任公司 Preparation method of non-burning low-temperature smoking tobacco shreds
WO2020002589A1 (en) * 2018-06-29 2020-01-02 Nerudia Limited A method for manufacturing reconstituted plant material

Also Published As

Publication number Publication date
CN102871212A (en) 2013-01-16

Similar Documents

Publication Publication Date Title
JP2020114244A (en) Protein-enriched tobacco-derived composition
CN102813278B (en) A kind of mixed type electronic cigarette tobacco liquid
CN102697168B (en) Additive for boosting maillard reaction of recombined tobacco leaves and method for preparing tobacco leaves by using additive
CN103584045B (en) A kind of sheep bone source mutton taste method for preparing flavoring
RU2255626C2 (en) Method of manufacturing non-smoking tobacco product
CN104531351B (en) A kind of tobacco juice for electronic smoke additive and preparation method thereof
CN104489901B (en) One grows tobacco taste tobacco juice for electronic smoke
CN104041935B (en) A kind of extracting method of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice
CN101411543B (en) Method for preparing flavoring for cigarette and use
CN103005661B (en) Mixed paper-making reconstituted tobacco as well as preparation method and application thereof
CN104213461B (en) A kind ofly be coated with cork paper body paper of uniform sticky lip and preparation method thereof
CN103054777B (en) Lignum Aquilariae Resinatum Chinese medicine shampoo and method for making thereof
RU2248166C2 (en) Method for manufacturing non-smoking tobacco products
EP2786664A1 (en) Pulp preparation method for electronic smoking set and traditional hookah
CN103584276B (en) Ambergris cigarette and ambergris spices
CN104946390A (en) Method for processing natural perfume used for electronic cigarette
US10098377B2 (en) Process and apparatus for improving raw tobacco
CN103478894A (en) Camellia extract composition with spicy fragrance and application of same to cigarettes
CN102559388A (en) Essential oil of tobaccos as well as preparation method and application thereof to cigarettes
CN102524934A (en) Reconstructed tobacco coating liquid component-component group chemical kitchen combination, coupling preparation, and coupling preparation process
CN104041936B (en) A kind of extracting method of electronic cigarette Chinese style mixing odor type style tobacco juice
CN107232638B (en) A kind of upgrading purification process of raisin extract and its application
CN101768514B (en) Alhagi sparsifolia extract and preparation method and application thereof
CN104705779B (en) A kind of processing method improving cut stem quality
CN102940309B (en) Preparation method of burley tobacco for simple and elegant fragrant cigarettes

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant