CN103462205A - Reconstructed tobacco leaves containing basic incense substances in tobaccos prepared by water extraction method and ethanol extraction method and cigarettes produced by reconstructed tobacco leaves - Google Patents
Reconstructed tobacco leaves containing basic incense substances in tobaccos prepared by water extraction method and ethanol extraction method and cigarettes produced by reconstructed tobacco leaves Download PDFInfo
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Abstract
The invention relates to reconstructed tobacco leaves containing basic incense substances in tobaccos prepared by a water extraction method and an ethanol extraction method. The reconstructed tobacco leaves are prepared by adding the basic incense substances in the tobaccos into reconstructed tobacco leaf base slices; the adding amount of the basic incense substances in the tobaccos is 0.5-1.5 times as much as the weight of the reconstructed tobacco leaf base slices; the basic incense substances in the tobaccos are composed of polarity aroma substances prepared by mixing the water extraction method and moderate-polarity and weak-polarity aroma substances prepared by the ethanol extraction method; the mass ratio formula of the polarity aroma substances to the moderate-polarity and weak-polarity aroma substances is 100 to (0.1-5). According to the reconstructed tobacco leaves, used tobacco raw materials are wastes including small-grain tobacco powder, tobacco ash or tobacco stems and the like generated in a processing process of the tobacco leaves, cut tobaccos or the tobaccos; the wastes are changed into valuable things so as to reduce pollution to the environment; according to the reconstructed tobacco leaves, the sensory quality is improved, the aroma amount is increased, the fragrance is improved, the natural tobacco aroma is set off, the dry feeling of smoke is reduced, the body fluid production feeling of the smoke is enhanced and the smoking comfort level is improved.
Description
Technical field
The present invention relates to Field of Tobacco, relate in particular to the reconstituted tobacco of this Studies of The Aromatic Substances in a kind of tobacco made containing water extraction and ethanol extraction method and by the cigarette of its manufacture.
Background technology
Chemical composition in tobacco is numerous.Since 20 century 70s, due to the development of analysis and testing technology, the chemical composition in tobacco constantly is found.Shi Hongzhi etc. 2011 report, in the tobacco leaf through identifying, chemical composition has 4992 kinds, and wherein relevant to tobacco flavor have more than 700 kinds.In tobacco, in the molecule of flavor matter, contain-OH ,-CO ,-NH and-SH etc. is specific causes fragrant functional group, with different irritating, produces different fragrance can to people's sense of smell.According to the difference of fragrance matter functional group, tobacco flavor material can be divided into alcohols, acids, ketone, ester class and terpene etc.Mostly tobacco flavor material is secondary metabolite, therefore also can be divided into according to fragrance precursor substance in secondary metabolism the classifications such as carotenoid, phenylalanine degradation product, the western cypress alkanes of class degradation product, mailland reaction product.
Can produce the approximately leftover bits and pieces such as waster tobacco of 25 % in the Bian of tobacco receipts and production process can not use, and is regarded garbage disposal more, also causes the significant wastage of natural resources when to environment, bringing pollution.The recent domestic that utilizes for leftover bits and pieces such as waster tobaccos has risen the reconstituted tobacco method.Reconstituted tobacco, be called again reconstituted tobacoo, it is that to utilize discarded offal, tobacco leaf fragment, offal etc. be raw material, through lixiviate, concentrated, separation, making beating, defibrination, manufacture paper with pulp, oven dry, perfuming process process, make the natural tobacco sheet of function admirable, as the cigarette filler, be back to production of cigarettes.
Reconstituted tobacco can lose a part of this Studies of The Aromatic Substances of tobacco in process, and needing to add a certain amount of tobacco endogenous spices increase reconstituted tobacco fragrance fragrance, improves smoke, reduces xylon gas and pungent sense.The crucial aroma component that contains organic acid, alcohols, carbonyl class, phenols, terpenes, carbohydrate, amino acids in the tobaccos such as neophytadiene, nicotine, solanone, damascenone, geranyl acetone, Megastigmatrienone, alpha, beta-lonone, benzaldehyde, phenmethylol, dihydroactinidiolide in waster tobacco, illustrate in waster tobacco and contain the important aroma component of a large amount of tobaccos, can be used as the source of tobacco essence.
Have at present the waster tobacco water is extracted, concentrates, water extracting liquid is added in reconstituted tobacco to the fragrance fragrance that improves reconstituted tobacco.It is water that water extraction is used solvent, leaching process good economy performance, safe, strong operability, and the water-soluble flavor matters such as carbohydrate, amino acids, phenols in tobacco leaf are had to extraction effect preferably, can improve the fragrance of reconstituted tobacco.But in tobacco, exist the crucial aroma component such as organic acid, terpenes, alcohols of a large amount of Semi-polarities and low pole to adopt its extraction effect of water extraction often poor, still there is the shortcoming of fragrance deficiency in the reconstituted tobacco that only adds water extracting liquid.
Ethanol is organic solvent commonly used, nontoxic, and in fields such as chemical industry, medicine, biologies, application is very extensive.Ethanol has dissolubility preferably for the material of Semi-polarity and low pole.In in tobacco, in fragrance ingredient, be Semi-polarity or low pole compound mostly, the solubility in ethanol is very large, thereby is particularly suitable for adopting alcohol extract.With ethanol extraction method extracted tobacco flavor matter from tobacco, the important aroma component contained in the essential oil that extraction obtains all obtains much bigger on composition or relative percentage composition than traditional water extraction extraction, this essential oil is used for to the assorted gas that perfuming cigarette can obviously change the fragrance of tobacco and suppress tobacco.The product that adopts gas chromatograph and GC-MS to obtain alcohol extract analyzes to find it is mainly wherein Semi-polarity and low pole compound, and has comprised many important and suctions cigarette and distinguish the flavor of the aroma component of substantial connection is arranged.
Document and patent report in the tobacco leaf the main extracting method of aroma component water extraction, alcohol extracting method, supercritical extraction, molecularly distilled etc. are arranged.Its document and Patent are as follows:
The pertinent literature of the extraction of tobacco mainly concentrates on essential oil of tobaccos, alkaloid and Salanesol etc. at present.The technique that Gao Hongjian etc. (2011) extract essential oil of tobaccos to steam distillation is studied.Experiment be take the essential oil of tobaccos yield as index, investigates distillation time, solid-liquid ratio, NaCl concentration, soak time four factors and steam distillation is extracted to the impact of essential oil of tobaccos yield, by experiment of single factor and orthogonal experiment, extraction process is optimized.The technique that Yang Jun etc. (2012) extract the essential oil of tobaccos crude extract to ultrasonic secondary solvent method is studied. and the essential oil of tobaccos crude extract yield of take is index, investigates ultrasonic time, ultrasonic power, solid-liquid ratio, 4 factors of soak time and reciprocation thereof and ultrasonic secondary solvent method is extracted to impact and the optimum process condition of essential oil of tobaccos crude extract yield.Liang Jinfeng etc. be take the low order tobacco and are set up a kind of method of rapid extraction nicotine as raw material, adopt supercritical ultrasonics technology, the way of distillation and Nicotine Extraction with Microwave, utilize spectrophotometer method to measure nicotine content, study respectively the impact of different ethanol concentration, different time, different feed liquid comparison tobacco smoke alkaloid extracted amount by single factor experiment, compared the pluses and minuses of three kinds of extraction methods simultaneously.Liu Wei etc. (2011) have investigated respectively three kinds of extracting methods by different test methods, and take content that the RP-HPLC method measures Salanesol as investigating index, optimize optimum extraction process; Result shows Salanesol optimum extraction process in tobacco extract: potassium hydroxide methanol solution extracts the acetone cold-maceration.
Chinese patent (201110248504.1) " method that tobacco is extracted continuously ".This patent characteristic is that tobacco powder is broken into particle diameter and is no less than 20 purpose powder, add and be equivalent to tobacco volume 10-30 aqueous medium doubly, regulate the pH value to 9-13, and carry out ultrasonic pretreatment, ultrasonic power is no less than 20kHz, ultrasonic pretreatment time is no less than 20 minutes, obtains ultrasonic pretreatment fluid, more further extraction nicotine, hemicellulose, lignin, cellulose.Although the method extraction of substance is comparatively thorough, but operation is comparatively complicated, more assorted this Studies of The Aromatic Substances that is not suitable for reconstituted tobacco of extraction of substance adds, and the introducing of more material simultaneously can destroy the fragrance of tobacco equally, and abstraction process is single, this Studies of The Aromatic Substances extracts the specificity shortcoming.
Chinese patent (201110183851.0) " a kind of preparation method of tobacco extract granules ".The preparation method who it is characterized in that a kind of tobacco extract granules, first get tobacco leaf and/or offal and by its chopping, water or ethanol or ether are solvent extraction, obtain tobacco extract through sedimentation and filtration, being concentrated into relative density 1.00-1.30 again and controlling temperature is 20～40 ℃, obtains tobacco and extracts concentrate or tobacco extract, then β-cyclodextrin in mass ratio: flavouring essence for tobacco is 1～3:1, flavouring essence for tobacco and β-cyclodextrin are carried out to inclusion, the inclusion time is 1/5～3 hour, obtain spices and Benexate Hydrochloride, again spices and Benexate Hydrochloride and tobacco are extracted to the common spray-drying of concentrate and obtain the tobacco spray dried powder, be added into subsequently in cigarette to increase tobacco flavor, this has invented single employing water, alcohol or ether are as extracting reagent, yet the beta-schardinger dextrin-of follow-up interpolation is the parent of the dried particles moulding of just auxiliary person's character material only, lack the mediation of nonpolar person's character material, it is not obvious that thereby the mouthfeel aspect of tobacco promotes.
Chinese patent (200910027400) " a kind of preparation method of tobacco extract and application thereof ".The preparation method of described tobacco extract, take tobacco as raw material, through enzymolysis, ultrasonic wave extraction, filtration, chromatographic column separation, reduced pressure concentration step, makes tobacco extract; Described tobacco extract dissolves with the ethanol of concentration 80%, adopts the atomizing type spray to be added in pipe tobacco.The comparatively loaded down with trivial details very difficult large-scale industrial production of this invention step, and the spices extracted becomes singlely, can not well meet the mouthfeel demand of reproducing pipe tobacco.
Summary of the invention
In order to solve above-mentioned technical problem, purpose of the present invention is to provide the reconstituted tobacco of this Studies of The Aromatic Substances in a kind of tobacco made containing water extraction and ethanol extraction method.The reduction of the fragrance of this reconstituted tobacco and lifting aspect are with the obvious advantage, the single extraction and add this Studies of The Aromatic Substances technology of comparing, and the defects such as the suction flavor that has solved reconstituted tobacco is uncomfortable, harsh feeling and dry sensation, greatly promote the mouthfeel of reconstituted tobacco.Another object of the present invention is to provide a kind of cigarette that adopts this reconstituted tobacco to manufacture.
In order to realize above-mentioned purpose, the present invention has adopted following technical scheme:
The reconstituted tobacco of this Studies of The Aromatic Substances in a kind of tobacco made containing water extraction and ethanol extraction method, this reconstituted tobacco adds this Studies of The Aromatic Substances in tobacco and makes in the reconstituted tobacco substrate, the 1:0.5 that in described tobacco, the addition of this Studies of The Aromatic Substances is reconstituted tobacco substrate weight～1.5 times; The Semi-polarity that the polarity flavor matter that in described tobacco, this Studies of The Aromatic Substances is made by water extraction makes with ethanol extraction method and weak level property flavor matter mix and form, and described polarity flavor matter and Semi-polarity and weak grade of property flavor matter fill a prescription 100: 0.1～5 according to mass ratio.
As preferably, described polarity flavor matter and Semi-polarity and weak level property flavor matter are according to mass ratio formula 100: 2～3.
As preferably, the preparation method of the polarity flavor matter of described water extraction is as follows: water extraction, and 30～70 ℃ of 3～9 times of water gagings extract 0.5～2 hour for tobacco material, extract 1～3 time, and it is 1.1～1.3g/mL that extract is concentrated into density.
As preferably, the preparation method of the Semi-polarity of described alcohol extract and weak level property flavor matter is as follows: in ethanol extraction method, concentration of alcohol is 60%～90%, the ethanol consumption is 4～8 times of amounts, extracting temperature is 40～70 ℃, extraction time is 1～2 hour, extract 1～2 time, it is 1.1～1.3 mg/mL that extract is concentrated into density.
As preferably, described tobacco material is one or more mixing in offal, cigarette ash, tobacco fragment, offal or other tobacco wastes that the particle that produces in tobacco leaf, pipe tobacco or tobacco processing course is tiny.
The present invention realizes second above-mentioned purpose, and the present invention adopts following technical scheme:
A kind of cigarette, above-mentioned reconstituted tobacco for the tobacco leaf picking of this cigarette.
In view of at present, the modulation of reconstituted tobacco and tobacco extract thereof is mainly manifested on some not enough composition and carries out suitable supplementing, and total and natural baccy there is gap for the modulation way of this fragrant component of tobacco.The present invention adopts method and the application in the tobacco product perfuming thereof of endogenous flavor matter in directed compound extraction tobacco from tobacco of water extraction and ethanol extraction method by a kind of, comprise and adopt water extraction directed polarity flavor matter and ethanol extraction method directed Semi-polarity that extracts from tobacco of extracting from tobacco, the composite extracting method of low pole flavor matter, again according to a certain percentage by polarity flavor matter and Semi-polarity, the low pole flavor matter is allocated, then its composite spices that causes is sprayed in reconstituted tobacco, promote the quality of reconstituted tobacco, increase perfume quantity, carry and raise note, set off nature cigarette perfume (or spice), reduce the flue gas drying sense, strengthen the flue gas sense of promoting the production of body fluid, improve the cigarette comfort level.
The present invention has following beneficial effect:
1. tobacco material used herein is tiny offal, cigarette ash or the offal the like waste of particle produced in tobacco leaf, pipe tobacco or tobacco processing course, and " turning waste into wealth " reduced the pollution to environment;
2. the present invention is by the method for water extraction and the directed compound extraction flavor matter of ethanol extraction method, and orientation extracts tobacco endogenous flavor matter compoundly from tobacco;
3. the present invention is by carrying out the proper proportion allotment to tobacco water extracting liquid and alcohol extract concentrate, its composite spices that causes is added in the tobacco products such as reconstituted tobacco, promote organoleptic quality, increase perfume quantity, carry and raise note, set off nature cigarette perfume (or spice), reduce the flue gas drying sense, strengthen flue gas promote the production of body fluid sense, improve and aspirate comfort level.
The accompanying drawing explanation
Fig. 1 is 80% alcohol extract concentrate GC-MS analysis chart.
Fig. 2 is water extracting liquid GC-MS analysis chart.
The specific embodiment
As previously mentioned, according to the disclosed content in front, one of skill in the art can apply the present invention to greatest extent.It should be pointed out that the present invention aims to provide the directed composite extracting method of middle flavor matter and uses thereof that grows tobacco.The following specific embodiment partly provide be enough to confirm described tobacco in after the directed composite extracting method and uses thereof of flavor matter, those skilled in the art are according to the routine techniques of perfuming cigarette purposes, can expect the directed composite extracting method of flavor matter in tobacco of the present invention fully can be used in above-mentioned field and can realize expectation function, therefore the following examples can help the present invention of those skilled in the art's comprehend, but do not limit the present invention in any way.
Embodiment 0:
Get useless time cigarette ash 40kg and stir and extract 1 hour with 40 ℃, 280L water, filter, it is 1.2g/mL that extract is concentrated into density, gets water extracting liquid 10000 g, is added in 10 kg reconstituted tobacco substrates, in contrast sample sets.
Embodiment 1:
Get useless time cigarette ash 40kg and stir and extract 1 hour with 50 ℃, 200L water, filter, it is 1.2g/mL that extract is concentrated into density, and water extracting liquid is standby; Get useless 50 ℃ of 40L80% ethanol of time cigarette ash 10kg, extraction time is 2 hours, extracts 2 times, and it is 1.2 g/mL that extract is concentrated into density; Get water extracting liquid 10000 g and alcohol extract concentrate 300 g, both are added into after mixing in 10 kg reconstituted tobaccos, pass through the sensory evaluating smoking, compare fragrance degree of sending out, bright sense are slightly good thoroughly with the control sample group, show slightly some fragrant and sweet senses, flue gas has certain continuous sense, and concentration is medium+, there is superficial puncture in oral cavity, slightly puckery mouthful of pleasant impression.
Embodiment 2:
Get useless time cigarette ash 40kg and stir and extract 1 hour with 40 ℃, 200L water, extract 2 times, filter, it is 1.2g/mL that extract is concentrated into density, and water extracting liquid is standby; Get useless 70 ℃ of 80L60% ethanol of time cigarette ash 10kg, extraction time is 1 hour, extracts 1 time, and it is 1.2 g/mL that extract is concentrated into density; Get water extracting liquid 10000 g and alcohol extract concentrate 200 g, both are added into after mixing in 10 kg reconstituted tobaccos, pass through the sensory evaluating smoking, compare the saturating Fa Dulve of fragrance with the control sample group good, flue gas concentration is medium+, still fine and smooth, still agglomerating, there is superficial puncture in oral cavity, show slightly xylon gas, slightly puckery mouthful of pleasant impression.
Embodiment 3:
Get useless time cigarette ash 30kg and stir and extract 1 hour with 70 ℃, 210L water, extract 2 times, filter, it is 1.2g/mL that extract is concentrated into density, gets the 10kg offal and extracts 1 hour with 70 ℃, 45L water, filters, it is 1.2g/mL that extract is concentrated into density, then by cigarette ash and offal concentrate, merges standby; Get 70 ℃ of 60L90% ethanol for waster tobacco 10kg, extraction time is 2 hours, extracts 2 times, and it is 1.1 g/mL that extract is concentrated into density; Get water extracting liquid 10000 g and alcohol extract concentrate 300 g, both are added into after mixing in 10 kg reconstituted tobaccos, pass through the sensory evaluating smoking, comparing fragrance with the control sample group still sends out thoroughly, still bright, fragrant and sweetly slightly manifest, certain abundant sense is arranged, flue gas is soft exquisiteness still, slightly there is superficial puncture in oral cavity, and assorted gas shows slightly, the slightly stagnant tongue of pleasant impression, slightly residual, show slightly sweet.
Embodiment 4:
Get waster tobacco 40kg and stir and extract 2 hours with 60 ℃, 320L water, extract 2 times, filter, it is 1.2g/mL that extract is concentrated into density, and concentrate is standby; Get useless 70 ℃ of 70L60% ethanol of time cigarette ash 10kg, extraction time is 1.5 hours, extracts 2 times, and it is 1.2 g/mL that extract is concentrated into density; Get water extracting liquid 10000 g and alcohol extract concentrate 500 g, both are added into after mixing in 10 kg reconstituted tobaccos, pass through the sensory evaluating smoking, comparing fragrance with the control sample group sends out thoroughly, bright, fragrant and sweetly slightly manifest, certain abundant sense is arranged, flue gas is soft exquisiteness still, slightly there is superficial puncture in oral cavity, and assorted gas shows slightly, the slightly stagnant tongue of pleasant impression, slightly residual, show slightly sweet.
Embodiment 5:
80% alcohol extract concentrate GC-MS analyzes: get 2mL sample and 4mL dichloromethane extraction, and vibration, ultrasonic, stratification, take off the stillness of night, and 5000rpm is centrifugal, and membrane filtration is got the 1ml sample introduction.Instrument: Agilent GC/MS, its gas chromatogram as shown in Figure 1.
In 80% ethanol sample, aroma component content is as following table:
Contain a large amount of tobacco flavor matters in the alcohol extract concentrate, wherein the component contents such as organic acid, ketone, ester class, alcohols are higher.
Embodiment 6:
Water extracting liquid GC-MS analyzes: get 2mL sample and 4mL dichloromethane extraction, and vibration, ultrasonic, stratification, take off the stillness of night, and 5000rpm is centrifugal, and membrane filtration is got the 1ml sample introduction.Instrument: Agilent GC/MS, its gas chromatogram as shown in Figure 2.From the GC-MS collection of illustrative plates, in water extracting liquid, volatile aroma component content is extremely low.
Claims (6)
1. the reconstituted tobacco of this Studies of The Aromatic Substances in the tobacco made containing water extraction and ethanol extraction method, it is characterized in that: this reconstituted tobacco adds this Studies of The Aromatic Substances in tobacco and makes in the reconstituted tobacco substrate, the 1:0.5 that in described tobacco, the addition of this Studies of The Aromatic Substances is reconstituted tobacco substrate weight ~ 1.5 times; The Semi-polarity that the polarity flavor matter that in described tobacco, this Studies of The Aromatic Substances is made by water extraction makes with ethanol extraction method and weak level property flavor matter mix and form, and described polarity flavor matter and Semi-polarity and weak grade of property flavor matter fill a prescription 100: 0.1 ~ 5 according to mass ratio.
2. the reconstituted tobacco of this Studies of The Aromatic Substances in a kind of tobacco made containing water extraction and ethanol extraction method according to claim 1, it is characterized in that: polarity flavor matter and Semi-polarity and weak level property flavor matter fill a prescription 100: 2 ~ 3 according to mass ratio.
3. the reconstituted tobacco of this Studies of The Aromatic Substances in a kind of tobacco made containing water extraction and ethanol extraction method according to claim 1 and 2, the preparation method of polarity flavor matter who it is characterized in that water extraction is as follows: water extraction, tobacco material extracts 0.5 ~ 2 hour with 30 ~ 70 ℃ of 3 ~ 9 times of water gagings, extract 1 ~ 3 time, it is 1.1 ~ 1.3g/mL that extract is concentrated into density.
4. the reconstituted tobacco of this Studies of The Aromatic Substances in a kind of tobacco made containing water extraction and ethanol extraction method according to claim 1 and 2, the preparation method who it is characterized in that the Semi-polarity of alcohol extract and weak level property flavor matter is as follows: in ethanol extraction method, concentration of alcohol is 60% ~ 90%, the ethanol consumption is 4 ~ 8 times of amounts, extracting temperature is 40 ~ 70 ℃, extraction time is 1 ~ 2 hour, extract 1 ~ 2 time, it is 1.1 ~ 1.3 mg/mL that extract is concentrated into density.
5. the reconstituted tobacco of this Studies of The Aromatic Substances in a kind of tobacco made containing water extraction and ethanol extraction method according to claim 1 and 2 is characterized in that: tobacco material is one or more mixing in offal, cigarette ash, tobacco fragment, offal or other tobacco wastes that the particle that produces in tobacco leaf, pipe tobacco or tobacco processing course is tiny.
6. a cigarette, is characterized in that: the tobacco leaf picking of this cigarette reconstituted tobacco claimed in claim 1.
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| CN103478892A (en) * | 2013-09-18 | 2014-01-01 | 浙江中烟工业有限责任公司 | Intrinsic tobacco aroma substance directionally and compositely extracted from tobacco raw material by water extraction method and ethanol extraction method |
| CN104026725A (en) * | 2014-06-17 | 2014-09-10 | 江苏中烟工业有限责任公司 | Method for improving luster of reconstituted tobacco in paper-making process |
| CN104450186A (en) * | 2014-10-29 | 2015-03-25 | 山东中烟工业有限责任公司 | Method for preparing tobacco herbal fragrant substance for cigarette solution of electronic cigarette |
| CN104738809A (en) * | 2015-02-11 | 2015-07-01 | 云南香颂科技有限公司 | Preparation method for tobacco extract and application of tobacco extract in cigarettes |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1565286A (en) * | 2003-06-13 | 2005-01-19 | 广东省金叶烟草薄片技术开发有限公司 | Tobacco leaf remaking process using tobacco peduncle and tobacco fragment as material through paper making method |
| CN101708063A (en) * | 2009-12-23 | 2010-05-19 | 湖南中烟工业有限责任公司 | Method for concentrating extraction liquid in production of tobacco sheet by papermaking process |
| CN102018274A (en) * | 2010-12-31 | 2011-04-20 | 云南烟草科学研究院 | Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method |
-
2013
- 2013-09-18 CN CN201310429115.8A patent/CN103462205B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1565286A (en) * | 2003-06-13 | 2005-01-19 | 广东省金叶烟草薄片技术开发有限公司 | Tobacco leaf remaking process using tobacco peduncle and tobacco fragment as material through paper making method |
| CN101708063A (en) * | 2009-12-23 | 2010-05-19 | 湖南中烟工业有限责任公司 | Method for concentrating extraction liquid in production of tobacco sheet by papermaking process |
| CN102018274A (en) * | 2010-12-31 | 2011-04-20 | 云南烟草科学研究院 | Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method |
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| CN103478892A (en) * | 2013-09-18 | 2014-01-01 | 浙江中烟工业有限责任公司 | Intrinsic tobacco aroma substance directionally and compositely extracted from tobacco raw material by water extraction method and ethanol extraction method |
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| CN104450186B (en) * | 2014-10-29 | 2017-04-19 | 山东中烟工业有限责任公司 | Method for preparing tobacco herbal fragrant substance for cigarette solution of electronic cigarette |
| CN104757704A (en) * | 2014-12-31 | 2015-07-08 | 贵州中烟工业有限责任公司 | Preparation method for tobacco extract and composition with the tobacco extract |
| CN104757704B (en) * | 2014-12-31 | 2019-06-07 | 贵州中烟工业有限责任公司 | A kind of preparation method of tobacco extract and composition containing the tobacco extract |
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| CN104939305A (en) * | 2015-05-20 | 2015-09-30 | 湖南中烟工业有限责任公司 | Tobacco extract and electronic cigarette liquid |
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| CN106213569A (en) * | 2016-08-02 | 2016-12-14 | 上海烟草集团有限责任公司 | A kind of method for concentration of papermaking-method reconstituted tobaccos extracting solution |
| CN106562467A (en) * | 2016-11-02 | 2017-04-19 | 浙江泽源植物科技有限公司 | Tobacco/non-tobacco slice composite coating processing method |
| CN109090683A (en) * | 2018-07-19 | 2018-12-28 | 中烟施伟策（云南）再造烟叶有限公司 | A kind of preparation method of high-nicotine type reconstituted tobacco |
| CN111544923A (en) * | 2020-05-08 | 2020-08-18 | 河北瑞龙生物科技有限公司 | Preparation method of snow pear extract for cigarettes |
| CN111544923B (en) * | 2020-05-08 | 2021-12-10 | 河北瑞龙生物科技有限公司 | Preparation method of snow pear extract for cigarettes |
| EP4205566A4 (en) * | 2021-04-29 | 2024-04-10 | KT&G Corporation | Tobacco extract sheet, method for manufacturing same, and smoking article comprising same |
| CN115708591A (en) * | 2022-12-15 | 2023-02-24 | 云南中烟新材料科技有限公司 | Cigarette flavoring method |
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