CN103070475A - Cigar tobacco leaf additive and production method thereof - Google Patents
Cigar tobacco leaf additive and production method thereof Download PDFInfo
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Abstract
The invention discloses a cigar tobacco leaf additive and a production method thereof. The production method of the cigar tobacco leaf additive comprises the following steps of: smashing natural plants into pulp; adding an enzyme preparation for enzymolysis and then inactivating enzyme; carrying out Maillard reaction within a temperature range of 110 to 150DEG C; distilling a reacted mixture at normal pressure to obtain a first component; heating and extracting residual slag generated by distilling with a compound solvent consisting of ethanol and water to obtain a second component; and mixing 2 to 4 parts of first component with 6 to 8 parts of second component to obtain the cigar tobacco leaf additive. According to the cigar tobacco leaf additive disclosed by the invention, the styles of cigar cigarettes are enriched and the sweet feeling of cigar flavor is added, so that the cigar cigarette is sweet and comfortable in flavor and pure and mild in smoke.
Description
Technical field
The embodiment of the invention relates to the tobacco essence field of perfumery, is specifically related to a kind of cigar tobacco additive and production method thereof that can increase cigar tobacco sweet taste and performance of keeping humidity.
Background technology
Abroad, American-European cigar is owing to the factors such as maturation of raw material advantage and process technology, and the phenomenon of part middle and high end cigar bitterness is also not obvious.
Domestic at present cigar being increased sweetly increases profit research and still is in the starting stage, can say that the technical research in this field is blank, in order to fill up this blank, promote the jealous quality of domestic cigar, make its characteristics of sucking that more are fit to Chinese Consumer's, necessary this problem is carried out application study.
For the jealous characteristics that present cigar pleasant impression is partially bitter, the oral cavity moisture feeling is inadequate, use traditional tobacco process technology and the fragrant adding technique of material can not guarantee that " Chinese style cigar " adapts to east consumer's the characteristics of sucking.Need to seek new natural plant extracts and carry out the processing of cigar, thereby make cigar have the distinctive taste of Chinese style cigar.
Summary of the invention
The object of the invention is to solve the defective of above-mentioned prior art, a kind of cigar tobacco additive and production method thereof that can increase cigar tobacco sweet taste and performance of keeping humidity is provided.
For solving above-mentioned technical problem, the present invention by the following technical solutions:
A kind of production method of cigar tobacco additive may further comprise the steps:
Natural plants is smashed pulping,
Add enzyme preparation, the amount that per 1 gram substrate adds enzyme is 500U to 1000U,
In the temperature range of 48 to 52 degree, carry out enzymolysis,
Enzymolysis is later with enzyme-deactivating,
Carry out Maillard reaction at 110 degree to the temperature range of 150 degree, the control reaction time is 55 to 65 minutes,
Reacted mixture is distilled under normal pressure, and the control temperature is 95 to 105 degree, and distillation time is 25 to 35 minutes, the cut of collecting is the volatile materials of natural plants, be the first component, the first component has fresh and sweet, pure and sweet, dense sweet, the fruit note such as sweet of natural plants
Distillation test residue is heated extraction with the double solvents that the second alcohol and water forms, the temperature of control double solvents is 78 to 82 degree, heating extraction time is 55 to 65 minutes, then concentrate, obtain second component, second component is pure and mild flue gas, increases the sweet functional component that increases profit, and the mass ratio of second alcohol and water is 1:1 in the described double solvents
First component of 2 to 4 parts (mass fraction) and the second component of 6 to 8 parts (mass fraction) are mixed, namely get the cigar tobacco additive, kind according to the cigar of finally making is different, the first component that adds is different with the ratio of second component, in the application of the cut tobacco that biases toward outer perfuming and vane type cigar, the first component ratio is slightly large; In the application that biases toward the manual cigar of this fragrant vane type of cigar and Ye Shu formula, the second component ratio is slightly large.
As optimal way of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, may further comprise the steps:
Natural plants is smashed pulping,
Add enzyme preparation, the amount that per 1 gram substrate adds enzyme is 500U to 1000U,
Under the temperature of 50 degree, carry out enzymolysis,
Enzymolysis is later with enzyme-deactivating,
Carry out Maillard reaction under the temperature of 130 degree, the control reaction time is 60 minutes,
Reacted mixture is distilled under normal pressure, and the control temperature is 100 degree, and distillation time is 30 minutes, and the cut of collecting is the volatile materials of natural plants, is the first component,
Distillation test residue is heated extraction with the double solvents that the second alcohol and water forms, the temperature of control double solvents is 80 degree, heating extraction time is 60 minutes, then concentrate, obtain second component, second component is latent perfume, increases the sweet functional component that increases profit, and the mass ratio of second alcohol and water is 1:1 in the described double solvents
3 parts of (mass fraction) first components and 7 parts of (mass fraction) second components are mixed, namely get the cigar tobacco additive.
As optimal way of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described enzyme preparation is one or more in pectase, carbohydrase, the cellulase, pectase decomposes colloid, can increase clarity of solution, carbohydrase, cellulase can decompose carbohydrate, enrich efficient monose for Maillard reaction provides.
As optimal way of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described natural plants is the natural fruit and vegetables class plant of being rich in vitamin C and vitamin E.
As optimal way of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described natural plants is one or more in Kiwi berry, tomato or the STEVIA REBAUDIANA.
As optimal way of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described natural plants is the red heart Kiwi berry.
As optimal way of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described enzyme-deactivating is the intensification deactivation, and the control temperature is 100 degree, and inactivation time is 30 minutes.
As optimal way of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, and described concentrated employing falling liquid film concentration technology, control vacuum is-0.07 to-0.088 MPa, and the control temperature is 60 to 80 degree, and cycles of concentration is 5 to 10 times.
A kind of cigar tobacco additive, described cigar tobacco additive are that described cigar tobacco comprises the by weight following component of meter by the preparation of the production method of above-mentioned cigar tobacco additive:
Isobutylaldehyde: 0.264 to 0.276 part,
Glacial acetic acid: 3.409 to 9.981 parts,
Isopentyl aldehyde: 0.838 to 0.883 part,
2 methyl butyraldehyde: 0.274 to 0.301 part,
Furfural: 6.294 to 6.808 parts,
Furfuryl alcohol: 1.666 to 3.289 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.328 to 0.876 part,
The 2-acetyl furan: 0.223 to 0.448 part,
3-methyl-2, the 5-furasndione: 2.709 to 4.241 parts,
5 methyl furfural: 1.411 to 2.123 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 0.981 to 1.075 part,
Phenylacetaldehyde: 0.412 to 0.415 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 to 0.937 part,
Furancarboxylic acid: 0.206 to 1.229 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 to 19.989 parts,
5 hydroxymethyl furfural: 45.32 to 46.724 parts,
The dextrorotation quininic acid: 0 to 19.072 part,
2 (5H)-furanones: 0 to 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0 to 0.72 part,
Methylfuroate: 0 to 1.342 part,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 0 to 1.337 part.
Effect of the present invention and advantage are as follows:
1, extraction by natural plants and on probation, constituent analysis, chemical analysis, add test, the taste signature analysis, optimization and development method to process conditions, the cigar tobacco additive that obtains from natural plants, extracting, its quality is improved, enriched the cigar style, and the sweet sense of increase cigar taste, make the cigar taste sweet, comfortable, smoke alcohol and soft, and improve cigar at process and the moisture retention that stores in the sales process, improve the interior quality score of product, further enlarge scope and the volume of production and marketing of domestic and international market consumption.
2, production method of the present invention utilizes that natural plants self contains enriches amino acid and sugar, Maillard reaction occurs, the nitrogen-containing compound that wherein is unfavorable for the cigar suction quality is transformed into micromolecular volatile ingredient, adopts again double solvents to extract the liposoluble constituent that wherein is conducive to the cigar suction quality.
3, the first component of production method of the present invention, the fragrant composition of feature head and the acid of little molecule of natural plants have been kept, guaranteed that product has that comfortable fruit is sweet, a fragrance of the fragrance of a flower, in tobacco, the pH value that acid can be regulated cigarette, make smoke pure and mild, promote the cigarette class, the fragrant head of micromolecular ester is fragrant can increase cigar thoroughly send out property; Furfural in the additive of the present invention, 6-methyl-5-hepten-2-one with refrigerant breath, have cool moisture feeling in cigarette, 5-2 methylpyrazine, 5 methyl furfural, 2-amyl furan have flavouring, increase profit, increase sweet effect.
4, production method of the present invention adds enzyme preparation, and pectase decomposes colloid, can increase clarity of solution; Carbohydrase, cellulase can decompose carbohydrate, enrich efficient monose for Maillard reaction provides; The amount that per 1 gram substrate adds enzyme is 500U to 1000U, uses minimum enzyme to obtain the fastest reaction rate.
The specific embodiment
According to one embodiment of present invention, fresh Kiwi berry is smashed pulping, add pectase, the amount that per 1 gram substrate adds pectase is 500U, under the temperature of 48 degree, carry out enzymolysis, after the enzymolysis temperature is increased to 100 degree and continues 30 minutes, finish enzyme-deactivating, then carry out Maillard reaction, the control reaction temperature is 110 degree, reaction time is 55 minutes, reacted mixture is distilled under normal pressure, and the control vapo(u)rizing temperature is 95 degree, and distillation time is 25 minutes, the cut of collecting is the volatile materials of natural plants, is the first component; Distillation test residue is heated extraction with the double solvents (mass ratio of second alcohol and water is 1:1) that the second alcohol and water forms, the temperature of control double solvents is 78 degree, heating extraction time is 55 minutes, then concentrate, described concentrated employing falling liquid film concentration technology, control vacuum is-0.07 MPa, the control temperature is 60 degree, cycles of concentration is 5 times, and the material after concentrating is second component; 2 parts of (mass fraction) first components and 6 parts of (mass fraction) second components are mixed, namely get the cigar tobacco additive.
The cigar tobacco additive is detected, comprises the by weight following component of meter:
Isobutylaldehyde: 0.264 part,
Glacial acetic acid: 3.409 parts,
Isopentyl aldehyde: 0.838 part,
2 methyl butyraldehyde: 0.274 part,
Furfural: 6.294 parts,
Furfuryl alcohol: 1.666 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.328 part,
The 2-acetyl furan: 0.223 part,
3-methyl-2, the 5-furasndione: 2.709 parts,
5 methyl furfural: 1.411 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 0.981 part,
Phenylacetaldehyde: 0.412 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 part,
Furancarboxylic acid: 0.206 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 parts,
5 hydroxymethyl furfural: 45.32 parts,
The dextrorotation quininic acid: 19.072 parts,
2 (5H)-furanones: 0.069 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0.12 part,
Methylfuroate: 0.5 part,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 0.5 part.
According to one embodiment of present invention, fresh tomato is smashed pulping, add carbohydrase, the amount that per 1 gram substrate adds carbohydrase is 1000U, in the temperature range of 52 degree, carry out enzymolysis, after the enzymolysis temperature is increased to 100 degree and continues 30 minutes, finish enzyme-deactivating, then carry out Maillard reaction in the temperature range of 150 degree, the control reaction time is 65 minutes, and reacted mixture is distilled under normal pressure, the control vapo(u)rizing temperature is 105 degree, distillation time is 35 minutes, and the cut of collecting is the volatile materials of natural plants, is the first component; Distillation test residue is heated extraction with the double solvents (mass ratio of second alcohol and water is 1:1) that the second alcohol and water forms, the temperature of control double solvents is 82 degree, heating extraction time is 65 minutes, then concentrate, described concentrated employing falling liquid film concentration technology, control vacuum is-0.088 MPa, the control temperature is 80 degree, cycles of concentration is 10 times, material after concentrated is second component, 4 parts of (mass fraction) first components and 8 parts of (mass fraction) second components are mixed, namely get the cigar tobacco additive.
The cigar tobacco additive is detected, comprises the by weight following component of meter:
Isobutylaldehyde: 0.276 part,
Glacial acetic acid: 9.981 parts,
Isopentyl aldehyde: 0.883 part,
2 methyl butyraldehyde: 0.301 part,
Furfural: 6.808 parts,
Furfuryl alcohol: 3.289 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.876 part,
The 2-acetyl furan: 0.448 part,
3-methyl-2, the 5-furasndione: 4.241 parts,
5 methyl furfural: 2.123 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 1.075 parts,
Phenylacetaldehyde: 0.415 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.937 part,
Furancarboxylic acid: 1.229 parts,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 19.989 parts,
5 hydroxymethyl furfural: 46.724 parts,
The dextrorotation quininic acid: 0.8 part,
2 (5H)-furanones: 0.269 part,
0.72 part of 2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone,
Methylfuroate: 1.34 parts,
1.337 parts of 3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone.
According to one embodiment of present invention, fresh STEVIA REBAUDIANA is smashed pulping, add pectase, carbohydrase and cellulase, the enzyme-added total amount of per 1 gram substrate is 800U, in the temperature range of 50 degree, carry out enzymolysis, after the enzymolysis temperature is increased to 100 degree and continues 30 minutes, finish enzyme-deactivating, then carry out Maillard reaction in the temperature range of 130 degree, the control reaction time is 60 minutes, and reacted mixture is distilled under normal pressure, the control vapo(u)rizing temperature is 100 degree, distillation time is 30 minutes, and the cut of collecting is the volatile materials of natural plants, is the first component; Distillation test residue is heated extraction with the double solvents (mass ratio of second alcohol and water is 1:1) that the second alcohol and water forms, the temperature of control double solvents is 80 degree, heating extraction time is 60 minutes, then concentrate, described concentrated employing falling liquid film concentration technology, control vacuum is-0.08 MPa, the control temperature is 70 degree, cycles of concentration is 8 times, material after concentrated is second component, first component of 3 parts (mass fractions) and the second component of 7 parts (mass fractions) are mixed, namely get the cigar tobacco additive.
The cigar tobacco additive is detected, comprises the by weight following component of meter:
Isobutylaldehyde: 0.265 part,
Glacial acetic acid: 5.409 parts,
Isopentyl aldehyde: 0.848 part,
2 methyl butyraldehyde: 0.284 part,
Furfural: 6.294 parts,
Furfuryl alcohol: 2.666 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.428 part,
The 2-acetyl furan: 0.323 part,
3-methyl-2, the 5-furasndione: 3.709 parts,
5 methyl furfural: 1.411 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 0.981 part,
Phenylacetaldehyde: 0.412 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 part,
Furancarboxylic acid: 0.206 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 parts,
5 hydroxymethyl furfural: 45.32 parts,
The dextrorotation quininic acid: 19.072 parts,
2 (5H)-furanones: 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0.12 part,
Methylfuroate: 0.1 part,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 0.1 part.
According to one embodiment of present invention, fresh red heart Kiwi berry is smashed pulping, add pectase, carbohydrase and cellulase, the total amount that per 1 gram substrate adds enzyme is 800U, in the temperature range of 50 degree, carry out enzymolysis, after the enzymolysis temperature is increased to 100 degree and continues 30 minutes, finish enzyme-deactivating, then carry out Maillard reaction in the temperature range of 130 degree, the control reaction time is 60 minutes, and reacted mixture is distilled under normal pressure, the control vapo(u)rizing temperature is 100 degree, distillation time is 30 minutes, and the cut of collecting is the volatile materials of natural plants, is the first component; Distillation test residue is heated extraction with the double solvents (mass ratio of second alcohol and water is 1:1) that the second alcohol and water forms, the temperature of control double solvents is 78 to 82 degree, heating extraction time is 55 to 65 minutes, then concentrate, described concentrated employing falling liquid film concentration technology, control vacuum is-0.08 MPa, the control temperature is 70 degree, cycles of concentration is 8 times, material after concentrated is second component, first component of 3 parts (mass fractions) and the second component of 7 parts (mass fractions) are mixed, namely get the cigar tobacco additive.
The cigar tobacco additive is detected, comprises the by weight following component of meter:
Isobutylaldehyde: 0.264 part,
Glacial acetic acid: 5.409 parts,
Isopentyl aldehyde: 0.838 part,
2 methyl butyraldehyde: 0.274 part,
Furfural: 6.294 parts,
Furfuryl alcohol: 2.666 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.628 part,
The 2-acetyl furan: 0.323 part,
3-methyl-2, the 5-furasndione: 2.709 parts,
5 methyl furfural: to 2.123 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: to 1.075 parts,
Phenylacetaldehyde: to 0.415 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 part,
Furancarboxylic acid: 0.206 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 parts,
5 hydroxymethyl furfural: 45.32 parts,
The dextrorotation quininic acid: 13.072 parts,
2 (5H)-furanones: 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0.62 part,
Methylfuroate: 1.342 parts,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 1.337 parts.
" embodiment " who speaks of in this manual, " another embodiment ", " embodiment ", etc., refer to specific features, structure or the characteristics described in conjunction with this embodiment and be included among at least one embodiment that the application's generality describes.A plurality of local appearance statement of the same race is not necessarily to refer to same embodiment in specification.Furthermore, when describing a specific features, structure or characteristics in conjunction with arbitrary embodiment, what advocate is to realize that in conjunction with other embodiment this feature, structure or characteristics also fall within the scope of the invention.
Although invention has been described with reference to a plurality of explanatory embodiment of the present invention here, but, should be appreciated that, those skilled in the art can design a lot of other modification and embodiments, and these are revised and embodiment will drop within the disclosed principle scope and spirit of the application.More particularly, in the scope of and claim open in the application, can carry out multiple modification and improvement to building block and/or the layout of subject combination layout.Except modification that building block and/or layout are carried out with improving, to those skilled in the art, other purposes also will be obvious.
Claims (9)
1. the production method of a cigar tobacco additive is characterized in that, may further comprise the steps:
Natural plants is smashed pulping,
Add enzyme preparation, the amount that per 1 gram substrate adds enzyme is 500U to 1000U,
In the temperature range of 48 to 52 degree, carry out enzymolysis,
Enzymolysis is later with enzyme-deactivating,
Carry out Maillard reaction at 110 degree to the temperature range of 150 degree, the control reaction time is 55 to 65 minutes,
Reacted mixture is distilled under normal pressure, the control temperature is 95 to 105 degree, and distillation time is 25 to 35 minutes, and the cut of collecting is the volatile materials of natural plants, be the first component, distillation test residue is heated extraction with the double solvents that the second alcohol and water forms, and the temperature of control double solvents is 78 to 82 degree, and heating extraction time is 55 to 65 minutes, then concentrate, obtain second component, the mass ratio of second alcohol and water is 1:1 in the described double solvents
First component of 2 to 4 parts (mass fraction) and the second component of 6 to 8 parts (mass fraction) are mixed, namely get the cigar tobacco additive.
2. the production method of described cigar tobacco additive according to claim 1 is characterized in that, may further comprise the steps:
Natural plants is smashed pulping,
Add enzyme preparation, the amount that per 1 gram substrate adds enzyme is 500U to 1000U,
Under the temperature of 50 degree, carry out enzymolysis,
Enzymolysis is later with enzyme-deactivating,
Carry out Maillard reaction under the temperature of 130 degree, the control reaction time is 60 minutes,
Reacted mixture is distilled under normal pressure, and the control temperature is 100 degree, and distillation time is 30 minutes, and the cut of collecting is the volatile materials of natural plants, is the first component,
Distillation test residue is heated extraction with the double solvents that the second alcohol and water forms, and the temperature of control double solvents is 80 degree, and heating extraction time is 60 minutes, then concentrates, and obtains second component, and the mass ratio of second alcohol and water is 1:1 in the described double solvents,
3 parts of (mass fraction) first components and 7 parts of (mass fraction) second components are mixed, namely get the cigar tobacco additive.
3. the production method of described cigar tobacco additive according to claim 1 and 2 is characterized in that, described enzyme preparation is one or more in pectase, carbohydrase, the cellulase.
4. the production method of described cigar tobacco additive according to claim 1 and 2 is characterized in that, described natural plants is the natural fruit and vegetables class plant of being rich in vitamin C and vitamin E.
5. the production method of described cigar tobacco additive according to claim 4 is characterized in that, described natural plants is one or more in Kiwi berry, tomato or the STEVIA REBAUDIANA.
6. the production method of described cigar tobacco additive according to claim 5 is characterized in that, described natural plants is the red heart Kiwi berry.
7. the production method of described cigar tobacco additive according to claim 1 and 2 is characterized in that, described enzyme-deactivating is the intensification deactivation, and the control temperature is 100 degree, and inactivation time is 30 minutes.
8. the production method of described cigar tobacco additive according to claim 1 and 2 is characterized in that, described concentrated employing falling liquid film concentration technology, and control vacuum be-0.07 to-0.088 MPa, and the control temperature is 60 to 80 to spend, and cycles of concentration is 5 to 10 times.
9. a cigar tobacco additive is characterized in that, described cigar tobacco additive is that described cigar tobacco comprises the by weight following component of meter by the preparation of the production method of the arbitrary described cigar tobacco additive of claim 1 to 8:
Isobutylaldehyde: 0.264 to 0.276 part,
Glacial acetic acid: 3.409 to 9.981 parts,
Isopentyl aldehyde: 0.838 to 0.883 part,
2 methyl butyraldehyde: 0.274 to 0.301 part,
Furfural: 6.294 to 6.808 parts,
Furfuryl alcohol: 1.666 to 3.289 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.328 to 0.876 part,
The 2-acetyl furan: 0.223 to 0.448 part,
3-methyl-2, the 5-furasndione: 2.709 to 4.241 parts,
5 methyl furfural: 1.411 to 2.123 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 0.981 to 1.075 part,
Phenylacetaldehyde: 0.412 to 0.415 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 to 0.937 part,
Furancarboxylic acid: 0.206 to 1.229 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 to 19.989 parts,
5 hydroxymethyl furfural: 45.32 to 46.724 parts,
The dextrorotation quininic acid: 0 to 19.072 part,
2 (5H)-furanones: 0 to 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0 to 0.72 part,
Methylfuroate: 0 to 1.342 part,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 0 to 1.337 part.
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| CN105029683A (en) * | 2015-06-25 | 2015-11-11 | 湖北中烟工业有限责任公司 | Method for preparing cigar tobacco leaves by virtue of compound starter fermentation |
| CN105054286A (en) * | 2015-06-25 | 2015-11-18 | 湖北中烟工业有限责任公司 | Method for preparing cigar tobacco leaves by means of fermentation effect of compounded enzyme preparation |
| CN105673016A (en) * | 2016-02-17 | 2016-06-15 | 三亚深海科学与工程研究所 | Mining machine |
| CN106723315A (en) * | 2016-12-01 | 2017-05-31 | 华宝香精股份有限公司 | A kind of preparation method of electronic cigarette raw material |
| CN112961728A (en) * | 2021-02-04 | 2021-06-15 | 中国烟草总公司海南省公司 | Method for extracting essential oil from cigar tobacco leaves |
| CN115005489A (en) * | 2022-06-21 | 2022-09-06 | 河南中烟工业有限责任公司 | Cigar-flavored electronic cigarette liquid and preparation method thereof |
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| CN105029683A (en) * | 2015-06-25 | 2015-11-11 | 湖北中烟工业有限责任公司 | Method for preparing cigar tobacco leaves by virtue of compound starter fermentation |
| CN105054286A (en) * | 2015-06-25 | 2015-11-18 | 湖北中烟工业有限责任公司 | Method for preparing cigar tobacco leaves by means of fermentation effect of compounded enzyme preparation |
| CN105673016A (en) * | 2016-02-17 | 2016-06-15 | 三亚深海科学与工程研究所 | Mining machine |
| CN106723315A (en) * | 2016-12-01 | 2017-05-31 | 华宝香精股份有限公司 | A kind of preparation method of electronic cigarette raw material |
| CN106723315B (en) * | 2016-12-01 | 2018-12-28 | 华宝香精股份有限公司 | A kind of preparation method of electronic cigarette raw material |
| CN112961728A (en) * | 2021-02-04 | 2021-06-15 | 中国烟草总公司海南省公司 | Method for extracting essential oil from cigar tobacco leaves |
| CN115005489A (en) * | 2022-06-21 | 2022-09-06 | 河南中烟工业有限责任公司 | Cigar-flavored electronic cigarette liquid and preparation method thereof |
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Effective date of registration: 20161229 Address after: 610000, Sichuan, Chengdu, Longquanyi economic and Technological Development Zone, Jackie Chan Road, Longquan, No. 2, paragraph Patentee after: CHINA TOBACCO SICHUAN INDUSTRIAL CO., LTD. Patentee after: CHONGQING CHINA TOBACCO INDUSTRIAL CO., LTD. Address before: 610000 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Patentee before: China Tobacco Chuanyu Industry Co., Ltd. |