CN103070475B - Cigar tobacco leaf additive and production method thereof - Google Patents
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Abstract
The invention discloses a cigar tobacco leaf additive and a production method thereof. The production method of the cigar tobacco leaf additive comprises the following steps of: smashing natural plants into pulp; adding an enzyme preparation for enzymolysis and then inactivating enzyme; carrying out Maillard reaction within a temperature range of 110 to 150DEG C; distilling a reacted mixture at normal pressure to obtain a first component; heating and extracting residual slag generated by distilling with a compound solvent consisting of ethanol and water to obtain a second component; and mixing 2 to 4 parts of first component with 6 to 8 parts of second component to obtain the cigar tobacco leaf additive. According to the cigar tobacco leaf additive disclosed by the invention, the styles of cigar cigarettes are enriched and the sweet feeling of cigar flavor is added, so that the cigar cigarette is sweet and comfortable in flavor and pure and mild in smoke.
Description
Technical field
The embodiment of the present invention relates to tobacco essence field of perfumery, is specifically related to a kind of cigar tobacco additive and the production method thereof that can increase cigar tobacco sweet taste and performance of keeping humidity.
Background technology
Abroad, American-European cigar is due to the factor such as maturation of raw material advantage and process technology, and the phenomenon of part middle and high end cigar bitterness is also not obvious.
Domestic research the sweet increasing profit of cigar increasing at present is still in the starting stage, can say in the technical research in this field it is blank, blank in order to fill up this, promote the jealous quality of domestic cigar, what make it more be applicable to Chinese Consumer's sucks feature, necessaryly carries out application study to this problem.
The jealous feature partially bitter for current cigar pleasant impression, oral cavity moisture feeling is inadequate, using traditional tobacco processing techniques and the fragrant adding technique of material can not ensure, " Chinese style cigar " adapt to east consumer sucks feature.Need to find the process that new natural plant extracts carries out cigar, thus make cigar have the distinctive taste of Chinese style cigar.
Summary of the invention
The object of the invention is to the defect solving above-mentioned prior art, a kind of cigar tobacco additive and the production method thereof that can increase cigar tobacco sweet taste and performance of keeping humidity are provided.
For solving above-mentioned technical problem, the present invention by the following technical solutions:
A production method for cigar tobacco additive, comprises the following steps:
Natural plants is smashed pulping,
Add enzyme preparation, the amount that every 1 gram of substrate adds enzyme is 500U to 1000U,
Enzymolysis is carried out in the temperature range of 48 to 52 degree,
By enzyme-deactivating after enzymolysis,
In the temperature range of 110 degree to 150 degree, carry out Maillard reaction, controlling the reaction time is 55 to 65 minutes,
Distilled at ambient pressure by reacted mixture, control temperature is 95 to 105 degree, and distillation time is 25 to 35 minutes, the cut collected is the volatile materials of natural plants, be the first component, the first component has fresh and sweet, pure and sweet, dense sweet, the fruit note such as sweet of natural plants
The double solvents that distillation test residue second alcohol and water forms is carried out heating extract, the temperature controlling double solvents is 78 to 82 degree, heating extraction time is 55 to 65 minutes, then concentrate, obtain second component, second component is alcohol and flue gas, the sweet functional component increasing profit of increasing, and in described double solvents, the mass ratio of second alcohol and water is 1:1
First component of 2 to 4 parts (mass fractions) and the second component of 6 to 8 parts (mass fractions) are mixed, obtain cigar tobacco additive, different according to the kind of the cigar finally made, the first component added is different with the ratio of second component, in the application of the cut tobacco and vane type cigar that bias toward outer perfuming, the first component ratio is slightly large; In the application of the manual cigar of vane type and Ye Shu formula biasing toward this perfume (or spice) of cigar, second component ratio is slightly large.
As preferred embodiment of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, comprise the following steps:
Natural plants is smashed pulping,
Add enzyme preparation, the amount that every 1 gram of substrate adds enzyme is 500U to 1000U,
Enzymolysis is carried out at the temperature of 50 degree,
By enzyme-deactivating after enzymolysis,
At the temperature of 130 degree, carry out Maillard reaction, controlling the reaction time is 60 minutes,
Distilled at ambient pressure by reacted mixture, control temperature is 100 degree, and distillation time is 30 minutes, and the cut collected is the volatile materials of natural plants, is the first component,
The double solvents that distillation test residue second alcohol and water forms is carried out heating extract, the temperature controlling double solvents is 80 degree, heating extraction time is 60 minutes, then concentrate, obtain second component, second component is functional component that is fragrant, that increase sweet increasing profit of diving, and in described double solvents, the mass ratio of second alcohol and water is 1:1
By 3 parts (mass fractions) first component and 7 parts of (mass fraction) second components mix, obtain cigar tobacco additive.
As preferred embodiment of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described enzyme preparation is one or more in pectase, carbohydrase, cellulase, pectase decomposes colloid, can increase clarity of solution, carbohydrase, cellulase can decompose carbohydrate, for Maillard reaction provides abundant efficient monose.
As preferred embodiment of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described natural plants is the natural fruit and vegetables class plant of being rich in vitamin C and vitamin E.
As preferred embodiment of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described natural plants is one or more in Kiwi berry, tomato or STEVIA REBAUDIANA.
As preferred embodiment of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described natural plants is red heart Kiwi berry.
As preferred embodiment of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described enzyme-deactivating is intensification deactivation, and control temperature is 100 degree, and inactivation time is 30 minutes.
As preferred embodiment of the present invention, in the production method of above-mentioned cigar tobacco additive, preferably, described concentrated employing falling film concentration technique, controlling vacuum is-0.07 to-0.088 MPa, and control temperature is 60 to 80 degree, and cycles of concentration is 5 to 10 times.
A kind of cigar tobacco additive, described cigar tobacco additive is prepared by the production method of above-mentioned cigar tobacco additive, and described cigar tobacco comprises the following component counted by weight:
Isobutylaldehyde: 0.264 to 0.276 part,
Glacial acetic acid: 3.409 to 9.981 parts,
Isopentyl aldehyde: 0.838 to 0.883 part,
2 methyl butyraldehyde: 0.274 to 0.301 part,
Furfural: 6.294 to 6.808 parts,
Furfuryl alcohol: 1.666 to 3.289 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.328 to 0.876 part,
2-acetyl furan: 0.223 to 0.448 part,
3-methyl-2,5-furasndione: 2.709 to 4.241 parts,
5 methyl furfural: 1.411 to 2.123 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 0.981 to 1.075 part,
Phenylacetaldehyde: 0.412 to 0.415 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 to 0.937 part,
Furancarboxylic acid: 0.206 to 1.229 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 to 19.989 parts,
5 hydroxymethyl furfural: 45.32 to 46.724 parts,
Dextrorotation quininic acid: 0 to 19.072 part,
2 (5H)-furanones: 0 to 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0 to 0.72 part,
Methylfuroate: 0 to 1.342 part,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 0 to 1.337 part.
Effect of the present invention and advantage as follows:
1, by the extraction of natural plants and on probation, constituent analysis, chemical analysis, add test, taste profile is analyzed, to optimization and the development method of process conditions, obtain the cigar tobacco additive extracted from natural plants, its quality is improved, enrich cigar style, and increase the sweet sense of cigar taste, make cigar taste sweet, comfortable, smoke alcohol and soft, and improve the moisture retention of cigar in process and storage sales process, improve the interior quality score of product, the scope of further expansion domestic and international market consumption and volume of production and marketing.
What 2, production method of the present invention utilized natural plants self to contain enriches amino acid and sugar, there is Maillard reaction, to wherein be unfavorable for that the nitrogen-containing compound of cigar suction quality is transformed into micromolecular volatile ingredient, then adopt double solvents to extract the liposoluble constituent being wherein conducive to cigar suction quality.
3, the first component of production method of the present invention, remain the fragrant composition of feature head and the Small molecular acid of natural plants, ensure that product has that comfortable fruit is sweet, the fragrant fragrance of the head of the fragrance of a flower, in tobacco, acid can regulate the pH value of cigarette, make smoke alcohol and, promote cigarette class, what the fragrant head perfume of micromolecular ester can increase cigar sends out property thoroughly; Furfural in additive of the present invention, 6-methyl-5-hepten-2-one, with refrigerant breath, have cool moisture feeling, 5-2 methylpyrazine, 5 methyl furfural, 2-amyl furan in cigarette, has flavouring, increases profit, increases sweet effect.
4, production method of the present invention, adds enzyme preparation, and pectase decomposes colloid, can increase clarity of solution; Carbohydrase, cellulase can decompose carbohydrate, for Maillard reaction provides abundant efficient monose; The amount that every 1 gram of substrate adds enzyme is 500U to 1000U, uses minimum enzyme to obtain the fastest reaction rate.
Detailed description of the invention
According to one embodiment of present invention, fresh Kiwi berry is smashed pulping, add pectase, the amount that every 1 gram of substrate adds pectase is 500U, enzymolysis is carried out at the temperature of 48 degree, after enzymolysis, temperature is increased to 100 degree and continues 30 minutes, complete enzyme-deactivating, then carry out Maillard reaction, controlling reaction temperature is 110 degree, reaction time is 55 minutes, distilled at ambient pressure by reacted mixture, controlling vapo(u)rizing temperature is 95 degree, and distillation time is 25 minutes, the cut collected is the volatile materials of natural plants, is the first component; The double solvents (mass ratio of second alcohol and water is 1:1) that distillation test residue second alcohol and water forms is carried out heating extract, the temperature controlling double solvents is 78 degree, heating extraction time is 55 minutes, then concentrate, described concentrated employing falling film concentration technique, controlling vacuum is-0.07 MPa, and control temperature is 60 degree, cycles of concentration is 5 times, and the material after concentrated is second component; By 2 parts (mass fractions) first component and 6 parts of (mass fraction) second components mix, obtain cigar tobacco additive.
Cigar tobacco additive is detected, comprises the following component counted by weight:
Isobutylaldehyde: 0.264 part,
Glacial acetic acid: 3.409 parts,
Isopentyl aldehyde: 0.838 part,
2 methyl butyraldehyde: 0.274 part,
Furfural: 6.294 parts,
Furfuryl alcohol: 1.666 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.328 part,
2-acetyl furan: 0.223 part,
3-methyl-2,5-furasndione: 2.709 parts,
5 methyl furfural: 1.411 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 0.981 part,
Phenylacetaldehyde: 0.412 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 part,
Furancarboxylic acid: 0.206 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 parts,
5 hydroxymethyl furfural: 45.32 parts,
Dextrorotation quininic acid: 19.072 parts,
2 (5H)-furanones: 0.069 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0.12 part,
Methylfuroate: 0.5 part,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 0.5 part.
According to one embodiment of present invention, fresh tomato is smashed pulping, add carbohydrase, the amount that every 1 gram of substrate adds carbohydrase is 1000U, enzymolysis is carried out in the temperature range of 52 degree, after enzymolysis, temperature is increased to 100 degree and continues 30 minutes, complete enzyme-deactivating, then in the temperature range of 150 degree, Maillard reaction is carried out, controlling the reaction time is 65 minutes, reacted mixture is distilled at ambient pressure, controlling vapo(u)rizing temperature is 105 degree, distillation time is 35 minutes, the cut collected is the volatile materials of natural plants, be the first component, the double solvents (mass ratio of second alcohol and water is 1:1) that distillation test residue second alcohol and water forms is carried out heating extract, the temperature controlling double solvents is 82 degree, heating extraction time is 65 minutes, then concentrate, described concentrated employing falling film concentration technique, controlling vacuum is-0.088 MPa, control temperature is 80 degree, cycles of concentration is 10 times, material after concentrated is second component, by 4 parts (mass fractions) first component and 8 parts of (mass fraction) second components mix, obtain cigar tobacco additive.
Cigar tobacco additive is detected, comprises the following component counted by weight:
Isobutylaldehyde: 0.276 part,
Glacial acetic acid: 9.981 parts,
Isopentyl aldehyde: 0.883 part,
2 methyl butyraldehyde: 0.301 part,
Furfural: 6.808 parts,
Furfuryl alcohol: 3.289 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.876 part,
2-acetyl furan: 0.448 part,
3-methyl-2,5-furasndione: 4.241 parts,
5 methyl furfural: 2.123 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 1.075 parts,
Phenylacetaldehyde: 0.415 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.937 part,
Furancarboxylic acid: 1.229 parts,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 19.989 parts,
5 hydroxymethyl furfural: 46.724 parts,
Dextrorotation quininic acid: 0.8 part,
2 (5H)-furanones: 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone 0.72 part,
Methylfuroate: 1.34 parts,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone 1.337 parts.
According to one embodiment of present invention, fresh STEVIA REBAUDIANA is smashed pulping, add pectase, carbohydrase and cellulase, the enzyme-added total amount of every 1 gram of substrate is 800U, enzymolysis is carried out in the temperature range of 50 degree, after enzymolysis, temperature is increased to 100 degree and continues 30 minutes, complete enzyme-deactivating, then in the temperature range of 130 degree, Maillard reaction is carried out, controlling the reaction time is 60 minutes, reacted mixture is distilled at ambient pressure, controlling vapo(u)rizing temperature is 100 degree, distillation time is 30 minutes, the cut collected is the volatile materials of natural plants, be the first component, the double solvents (mass ratio of second alcohol and water is 1:1) that distillation test residue second alcohol and water forms is carried out heating extract, the temperature controlling double solvents is 80 degree, heating extraction time is 60 minutes, then concentrate, described concentrated employing falling film concentration technique, controlling vacuum is-0.08 MPa, control temperature is 70 degree, cycles of concentration is 8 times, material after concentrated is second component, first component of 3 parts (mass fractions) and the second component of 7 parts (mass fractions) are mixed, obtains cigar tobacco additive.
Cigar tobacco additive is detected, comprises the following component counted by weight:
Isobutylaldehyde: 0.265 part,
Glacial acetic acid: 5.409 parts,
Isopentyl aldehyde: 0.848 part,
2 methyl butyraldehyde: 0.284 part,
Furfural: 6.294 parts,
Furfuryl alcohol: 2.666 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.428 part,
2-acetyl furan: 0.323 part,
3-methyl-2,5-furasndione: 3.709 parts,
5 methyl furfural: 1.411 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 0.981 part,
Phenylacetaldehyde: 0.412 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 part,
Furancarboxylic acid: 0.206 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 parts,
5 hydroxymethyl furfural: 45.32 parts,
Dextrorotation quininic acid: 19.072 parts,
2 (5H)-furanones: 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0.12 part,
Methylfuroate: 0.1 part,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 0.1 part.
According to one embodiment of present invention, fresh red heart Kiwi berry is smashed pulping, add pectase, carbohydrase and cellulase, the total amount that every 1 gram of substrate adds enzyme is 800U, enzymolysis is carried out in the temperature range of 50 degree, after enzymolysis, temperature is increased to 100 degree and continues 30 minutes, complete enzyme-deactivating, then in the temperature range of 130 degree, Maillard reaction is carried out, controlling the reaction time is 60 minutes, reacted mixture is distilled at ambient pressure, controlling vapo(u)rizing temperature is 100 degree, distillation time is 30 minutes, the cut collected is the volatile materials of natural plants, be the first component, the double solvents (mass ratio of second alcohol and water is 1:1) that distillation test residue second alcohol and water forms is carried out heating extract, the temperature controlling double solvents is 78 to 82 degree, heating extraction time is 55 to 65 minutes, then concentrate, described concentrated employing falling film concentration technique, controlling vacuum is-0.08 MPa, control temperature is 70 degree, cycles of concentration is 8 times, material after concentrated is second component, first component of 3 parts (mass fractions) and the second component of 7 parts (mass fractions) are mixed, obtains cigar tobacco additive.
Cigar tobacco additive is detected, comprises the following component counted by weight:
Isobutylaldehyde: 0.264 part,
Glacial acetic acid: 5.409 parts,
Isopentyl aldehyde: 0.838 part,
2 methyl butyraldehyde: 0.274 part,
Furfural: 6.294 parts,
Furfuryl alcohol: 2.666 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.628 part,
2-acetyl furan: 0.323 part,
3-methyl-2,5-furasndione: 2.709 parts,
5 methyl furfural: to 2.123 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: to 1.075 parts,
Phenylacetaldehyde: to 0.415 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 part,
Furancarboxylic acid: 0.206 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 parts,
5 hydroxymethyl furfural: 45.32 parts,
Dextrorotation quininic acid: 13.072 parts,
2 (5H)-furanones: 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0.62 part,
Methylfuroate: 1.342 parts,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 1.337 parts.
Spoken of in this manual " embodiment ", " another embodiment ", " embodiment ", etc., refer to the specific features, structure or the feature that describe in conjunction with this embodiment and be included at least one embodiment of the application's generality description.Multiple place occurs that statement of the same race is not necessarily refer to same embodiment in the description.Furthermore, when describing specific features, structure or a feature in conjunction with any embodiment, what advocate is also fall within the scope of the invention to realize this feature, structure or feature in conjunction with other embodiments.
Although with reference to multiple explanatory embodiment of the present invention, invention has been described here, but, should be appreciated that, those skilled in the art can design a lot of other amendment and embodiment, these amendments and embodiment will drop within spirit disclosed in the present application and spirit.More particularly, in the scope of and claim open in the application, multiple modification and improvement can be carried out to the building block of subject combination layout and/or layout.Except the modification of carrying out building block and/or layout is with except improvement, to those skilled in the art, other purposes also will be obvious.
Claims (6)
1. a production method for cigar tobacco additive, is characterized in that, comprises the following steps:
The natural plants being rich in vitamin C and vitamin E is smashed pulping, and described natural plants is one or more in Kiwi berry, tomato or STEVIA REBAUDIANA;
Add enzyme preparation, the amount that every 1 gram of substrate adds enzyme is 500U to 1000U, and described enzyme preparation is one or more in pectase, carbohydrase, cellulase;
Enzymolysis is carried out in the temperature range of 48 to 52 degree,
By enzyme-deactivating after enzymolysis,
In the temperature range of 110 degree to 150 degree, carry out Maillard reaction, controlling the reaction time is 55 to 65 minutes,
Distilled at ambient pressure by reacted mixture, control temperature is 95 to 105 degree, and distillation time is 25 to 35 minutes, and the cut collected is the volatile materials of natural plants, is the first component,
The double solvents that distillation test residue second alcohol and water forms is carried out heating extract, the temperature controlling double solvents is 78 to 82 degree, and heating extraction time is 55 to 65 minutes, then concentrate, obtain second component, in described double solvents, the mass ratio of second alcohol and water is 1:1
First component of 2 to 4 mass parts and the second component of 6 to 8 mass parts are mixed, obtains cigar tobacco additive.
2. the production method of cigar tobacco additive according to claim 1, is characterized in that, comprise the following steps:
Natural plants is smashed pulping,
Add enzyme preparation, the amount that every 1 gram of substrate adds enzyme is 500U to 1000U,
Enzymolysis is carried out at the temperature of 50 degree,
By enzyme-deactivating after enzymolysis,
At the temperature of 130 degree, carry out Maillard reaction, controlling the reaction time is 60 minutes, is distilled at ambient pressure by reacted mixture, control temperature is 100 degree, and distillation time is 30 minutes, and the cut collected is the volatile materials of natural plants, be the first component
The double solvents that distillation test residue second alcohol and water forms is carried out heating extract, the temperature controlling double solvents is 80 degree, and heating extraction time is 60 minutes, and then concentrate, obtain second component, in described double solvents, the mass ratio of second alcohol and water is 1:1,
3 mass parts first components and 7 mass parts second components are mixed, obtains cigar tobacco additive.
3. the production method of cigar tobacco additive according to claim 1, it is characterized in that, described natural plants is red heart Kiwi berry.
4. the production method of cigar tobacco additive according to claim 1 or 2, it is characterized in that, described enzyme-deactivating is intensification deactivation, and control temperature is 100 degree, and inactivation time is 30 minutes.
5. the production method of cigar tobacco additive according to claim 1 or 2, is characterized in that, described concentrated employing falling film concentration technique, and controlling vacuum be-0.07 to-0.088 MPa, and control temperature is 60 to 80 to spend, and cycles of concentration is 5 to 10 times.
6. a cigar tobacco additive, is characterized in that, described cigar tobacco additive is prepared by the production method of the arbitrary described cigar tobacco additive of claim 1 to 5, and described cigar tobacco additive comprises the following component counted by weight:
Isobutylaldehyde: 0.264 to 0.276 part,
Glacial acetic acid: 3.409 to 9.981 parts,
Isopentyl aldehyde: 0.838 to 0.883 part,
2 methyl butyraldehyde: 0.274 to 0.301 part,
Furfural: 6.294 to 6.808 parts,
Furfuryl alcohol: 1.666 to 3.289 parts,
2-cyclopentene-Isosorbide-5-Nitrae-diketone: 0.328 to 0.876 part,
2-acetyl furan: 0.223 to 0.448 part,
3-methyl-2,5-furasndione: 2.709 to 4.241 parts,
5 methyl furfural: 1.411 to 2.123 parts,
2,4-dihydroxy-2,5-dimethyl-3 (2H)-furans-3-ketone: 0.981 to 1.075 part,
Phenylacetaldehyde: 0.412 to 0.415 part,
4-hydroxyl-2,5-dimethyl-3 (2H) furanone: 0.358 to 0.937 part,
Furancarboxylic acid: 0.206 to 1.229 part,
2,3-dihydro-3,5-dihydroxy-6-methyl-4 (4H)-pyrans-4-ketone: 12.974 to 19.989 parts,
5 hydroxymethyl furfural: 45.32 to 46.724 parts,
Dextrorotation quininic acid: 0 to 19.072 part,
2 (5H)-furanones: 0 to 0.269 part,
2,3-dihydro-5-hydroxyl-6-methyl-4H-pyrans-4-ketone: 0 to 0.72 part,
Methylfuroate: 0 to 1.342 part,
3,5-dihydroxy-2-methyl-4H-pyrans-4-ketone: 0 to 1.337 part.
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| CN105029683B (en) * | 2015-06-25 | 2017-07-21 | 湖北中烟工业有限责任公司 | The method that cigar tobacco is prepared using composite ferment fermentation |
| CN105054286B (en) * | 2015-06-25 | 2017-01-11 | 湖北中烟工业有限责任公司 | Method for preparing cigar tobacco leaves by means of fermentation effect of compounded enzyme preparation |
| CN105673016B (en) * | 2016-02-17 | 2018-09-11 | 三亚深海科学与工程研究所 | A kind of collecting machine |
| CN106723315B (en) * | 2016-12-01 | 2018-12-28 | 华宝香精股份有限公司 | A kind of preparation method of electronic cigarette raw material |
| CN112961728A (en) * | 2021-02-04 | 2021-06-15 | 中国烟草总公司海南省公司 | Method for extracting essential oil from cigar tobacco leaves |
| CN115005489B (en) * | 2022-06-21 | 2023-06-20 | 河南中烟工业有限责任公司 | Cigar-flavored electronic cigarette liquid and preparation method thereof |
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| CN1594521A (en) * | 2004-07-04 | 2005-03-16 | 云南烟草科学研究院 | Method for preparing reactive mixture flavor and its use in tobacco |
| CN1875794A (en) * | 2006-07-04 | 2006-12-13 | 云南瑞升烟草技术（集团）有限公司 | Functional addictive for cigarette and preparation method thereof |
| CN101416775A (en) * | 2007-10-26 | 2009-04-29 | 武汉烟草(集团)有限公司 | Tomato gradual extraction and integrated utilization method in cigarette |
| CN101292776A (en) * | 2008-06-23 | 2008-10-29 | 中国烟草总公司郑州烟草研究院 | Orally taken tobacco |
| CN101731748A (en) * | 2008-11-05 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for extracting Dendranthema indium leaves and application of extractive thereof in cigarettes |
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Effective date of registration: 20161229 Address after: 610000, Sichuan, Chengdu, Longquanyi economic and Technological Development Zone, Jackie Chan Road, Longquan, No. 2, paragraph Patentee after: CHINA TOBACCO SICHUAN INDUSTRIAL CO., LTD. Patentee after: CHONGQING CHINA TOBACCO INDUSTRIAL CO., LTD. Address before: 610000 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Patentee before: China Tobacco Chuanyu Industry Co., Ltd. |