CN110839945A - Preparation method and application of colorless caramel spice - Google Patents
Preparation method and application of colorless caramel spice Download PDFInfo
- Publication number
- CN110839945A CN110839945A CN201911353761.4A CN201911353761A CN110839945A CN 110839945 A CN110839945 A CN 110839945A CN 201911353761 A CN201911353761 A CN 201911353761A CN 110839945 A CN110839945 A CN 110839945A
- Authority
- CN
- China
- Prior art keywords
- caramel
- colorless
- colorless caramel
- aroma
- preparing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
Abstract
The invention belongs to the technical field of tobacco flavors, and particularly relates to a preparation method and application of a colorless caramel flavor. The colorless caramel essence is prepared by preparing caramel essence liquid by microwave method, adding ethanol, distilling under reduced pressure, and collecting colorless caramel essence. The colorless caramel aroma can be applied to filter stick tows, aroma lines or tobacco shreds, and caramel-like characteristic aroma is given to the smoke while the aesthetic feeling of the appearance is ensured, so that the smoke irritation is reduced, the aftertaste of the oral cavity is improved, and the sweet and moist feeling of the oral cavity is increased. The method is simple to operate, easy to meet the manufacturing conditions, good in stability, economical, applicable and suitable for popularization and application.
Description
Technical Field
The invention belongs to the technical field of tobacco flavors, and particularly relates to a preparation method and application of a colorless caramel flavor.
Background
Caramel or caramel pigment is used as a food additive with functions of color matching, flavor blending and seasoning, and is widely applied to the food fields of candies, biscuits, beverages, seasonings and the like. From the current research situation of caramelized pigments, most of caramelized reaction application researches are mainly focused on the color attribute, namely, the pigment product which is matched with the target color matching product and has higher color yield, better stability and guaranteed safety is obtained, and the aroma attribute is less applied. The caramelization reaction is closely related to tobacco, and because the tobacco leaves contain more monosaccharide, disaccharide and oligosaccharide after being prepared, and exogenous sugar serving as a tobacco flavor modifier is also added into tobacco material liquid in a large amount, the caramelization reaction is widely existed in the cigarette processing and burning processes. For example, the important aroma components in cigarette smoke, such as 5-methylfurfural, furfural, furfuryl alcohol, furanone, DDMP and the like, are very typical caramelization reaction products. Theoretically, the caramelization reaction spice has certain innovation and feasibility for supplementing the aroma style of the cigarette product.
At present, in the cigarette consumption market, cigarette filter sticks with different types and different flavors appear, but the appearance color of the filter stick is always white as the basic tone. Cigarette filter sticks with altered appearance colors are difficult for consumers to accept. The colorless caramel-flavored filter stick prepared by the invention endows caramel flavor to smoke during suction on the premise of ensuring no color change, so that the smoke is softer. Meanwhile, the cigarette has the functions of increasing aroma and supplementing fragrance for cigarette products with reduced tar and harm.
Disclosure of Invention
In order to make up for the defects of the prior art, the invention provides the colorless caramel aroma spice which can endow caramel aroma to the cigarette filter stick under the condition of ensuring that the filter stick is not discolored, so that the aroma is improved to be rich, and the sweet and moist feeling of the oral cavity is increased.
The technical scheme of the invention is realized as follows:
a preparation method of colorless caramel spice comprises the following steps:
(1) preparing sugar solution from sugar and solvent;
(2) adding an alkaline compound into the sugar solution obtained in the step (1) to adjust the pH value to obtain a reaction solution;
(3) carrying out microwave reflux heating on the reaction solution in the step (2) to obtain caramel essence, and refrigerating and standing until layering;
(4) and (4) taking the upper layer liquid of the caramel essence liquid after standing in the step (3), adding absolute ethyl alcohol, mixing, and then placing in a reduced pressure distillation device to collect fractions, namely the colorless caramel essence.
The mass ratio of the sugar to the solvent in the step (1) is 1 (2-5), and the sugar is glucose, fructose, lactose, ribose, deoxyribose, maltose or compound sugar; the solvent is propylene glycol or water or a mixed solution of the propylene glycol and the water.
In the step (2), the alkaline compound is sodium carbonate, sodium bicarbonate, potassium hydroxide or sodium hydroxide, and the pH value is 9-11.
The temperature of the microwave reflux heating in the step (3) is 80-90 ℃, the microwave power is 400-600W, and the heating time is 0.5-1.5 h.
The time for cooling and standing in the step (3) is 24-48h, and the temperature is 1-5 ℃.
The mass ratio of the upper layer liquid to the absolute ethyl alcohol in the step (4) is 1 (1-2).
The reduced pressure distillation conditions in the step (4) are as follows: the temperature is 60-80 ℃, the time is 0.5-1.5h, and the pressure is 90kPa-100 kPa.
The prepared colorless caramel fragrance is applied to preparing colorless caramel fragrance cigarettes, and the colorless caramel fragrance is added into filter stick tows according to the application amount of 1-2 mu L/mm to prepare colorless caramel fragrance cigarette filter sticks.
And soaking the filter stick fragrant threads with colorless caramel fragrant spices to prepare colorless caramel fragrant cigarette filter sticks.
Adding colorless caramel aroma into tobacco shreds at an application amount of 1-10wt% for preparing colorless caramel cigarette.
The invention has the following beneficial effects:
1. the caramel essence liquid with high color ratio is quickly prepared by a microwave method, and the colorless distillate liquid is quickly collected by reducing the pressure and the boiling point of the solvent by a reduced pressure distillation method, wherein the distillate liquid contains the aroma components of the caramel essence, such as: and fragrance components such as furfuryl alcohol and ethyl cyclopentenolone. The problem that the traditional caramel spice is heavily colored is solved, the attractiveness of the cigarette filter stick is guaranteed, the characteristic flavor of caramel aroma is given to smoke, the sweet and moist feeling of the oral cavity is increased, and the irritation and aftertaste of the smoke are improved. Simultaneously, the cigarette has the functions of increasing aroma and supplementing fragrance for cigarette products with reduced tar and harm.
2. The invention combines microwave preparation of caramel spice, further shortens the preparation time. The preparation method has the advantages of easy satisfaction of preparation conditions, simple operation and easy popularization and application.
3. The colorless caramel spice prepared by the invention has high safety, is not only limited to be applied to cigarettes, but also can be widely applied to the industries of food and health care products, has the functions of enhancing and supplementing fragrance, endows characteristic flavor and ensures the attractiveness of products.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts.
Fig. 1 is a total ion flow diagram of example 1.
Fig. 2 is a total ion flow diagram of example 2.
Figure 3 is the total ion flow diagram of example 3.
Fig. 4 is the total ion flow diagram of example 4.
Fig. 5 is the total ion flow diagram of example 5.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without inventive effort based on the embodiments of the present invention, are within the scope of the present invention.
Example 1
The preparation method of the colorless caramel spice of the embodiment comprises the following steps:
(1) mixing lactose and water according to a mass ratio of 1: 2 preparing sugar solution;
(2) adding sodium carbonate into the sugar solution obtained in the step (1) to adjust the pH value to 10 to obtain a reaction solution;
(3) carrying out microwave reflux heating on the reaction solution obtained in the step (2) for 0.5h at 80 ℃ under the condition of 400W to obtain caramel essence;
(4) standing and refrigerating the caramel essence obtained in the step (3) for 24 hours at the temperature of 2 ℃;
(5) taking the fragrant liquid subjected to standing and refrigeration in the step (4), and mixing the upper liquid and absolute ethyl alcohol according to a mass ratio of 1: 2, mixing, distilling at 60 ℃ under 100kPa for 0.5h, and collecting the distillate, wherein the distillate is the colorless caramel essence.
The colorless caramel aroma of this example was used to prepare colorless caramel aroma cigarettes: adding the prepared colorless caramel spice into tobacco shreds at an application amount of 5%.
Example 2
The preparation method of the colorless caramel spice of the embodiment comprises the following steps:
(1) mixing glucose and water according to a mass ratio of 1: 1 sugar solution prepared;
(2) adding sodium bicarbonate into the sugar solution obtained in the step (1) to adjust the pH value to 10 to obtain a reaction solution;
(3) carrying out microwave reflux heating on the reaction solution obtained in the step (2) for 0.5h at the temperature of 90 ℃ and the power of 600W to obtain caramel essence;
(4) standing and refrigerating the caramel essence obtained in the step (3) for 24 hours at the temperature of 2 ℃;
(5) taking the fragrant liquid subjected to standing and refrigeration in the step (4), and mixing the upper liquid and absolute ethyl alcohol according to a mass ratio of 1: 1, mixing, distilling at 80 ℃ under 100kPa for 0.5h, and collecting the distillate, namely the color caramel essence.
The colorless caramel aroma of this example was used to prepare colorless caramel aroma cigarettes: the colorless caramel aroma prepared in this example was added to the tobacco shreds at an application rate of 5%.
Example 3
The preparation method of the colorless caramel spice of the embodiment comprises the following steps:
(1) mixing fructose, water and propylene glycol according to a mass ratio of 1: 1: 1 sugar solution prepared;
(2) adding sodium bicarbonate into the sugar solution obtained in the step (1) to adjust the pH value to 11 to obtain a reaction solution;
(3) carrying out microwave reflux heating on the reaction solution obtained in the step (2) for 1.5h at the temperature of 90 ℃ and under the condition of 600W to obtain caramel essence;
(4) standing and refrigerating the caramel essence obtained in the step (3) for 24 hours at the temperature of 2 ℃;
(5) taking the fragrant liquid subjected to standing and refrigeration in the step (4), and mixing the upper liquid and absolute ethyl alcohol according to a mass ratio of 1: 2, mixing, distilling at 80 ℃ under 100kPa for 0.5h, and collecting the distillate, namely the color caramel essence.
Preparing a colorless caramel fragrance cigarette filter stick by using the colorless caramel fragrance spice of the embodiment: the colorless caramel aroma prepared in this example was added to the filter tow at an application rate of 1 μ L/mm.
Example 4
The preparation method of the colorless caramel spice of the embodiment comprises the following steps:
(1) mixing glucose and water according to a mass ratio of 1: 1 sugar solution prepared;
(2) adding sodium bicarbonate into the sugar solution obtained in the step (1) to adjust the pH value to 10 to obtain a reaction solution;
(3) carrying out microwave reflux heating on the reaction solution obtained in the step (2) for 1h at 85 ℃ under the condition of 400W to obtain caramel essence;
(4) standing and refrigerating the caramel essence obtained in the step (3) for 24 hours at the temperature of 2 ℃;
(5) taking the fragrant liquid subjected to standing and refrigeration in the step (4), and mixing the upper liquid and absolute ethyl alcohol according to a mass ratio of 1: 1, mixing, distilling at 60 ℃ under 90kPa for 0.5h, and collecting the distillate, namely the color caramel essence.
Preparing a colorless caramel fragrance cigarette filter stick by using the colorless caramel fragrance spice of the embodiment: the colorless caramel aroma prepared in this example was added to the filter tow at an application rate of 1 μ L/mm.
Example 5
The preparation method and the application research of the colorless caramel perfume of the embodiment comprise the following steps:
(1) mixing glucose, fructose, lactose and water according to a mass ratio of 1: 1: 1: 3 preparing sugar solution;
(2) adding sodium bicarbonate into the sugar solution obtained in the step (1) to adjust the pH value to 10 to obtain a reaction solution;
(3) carrying out microwave reflux heating on the reaction solution obtained in the step (2) for 1h at 85 ℃ under the condition of 600W to obtain caramel essence;
(4) standing and refrigerating the caramel essence obtained in the step (3) for 48 hours at the temperature of 5 ℃;
(5) taking the fragrant liquid subjected to standing and refrigeration in the step (4), and mixing the upper liquid and absolute ethyl alcohol according to a mass ratio of 1: 1, mixing, distilling at 80 ℃ under 100kPa for 1.5h, and collecting the distillate, namely the color caramel essence.
Preparing a colorless caramel fragrance cigarette filter stick by using the colorless caramel fragrance spice of the embodiment: the colorless caramel aroma prepared in this example was added to the filter tow at an application rate of 2 μ L/mm.
Examples of the effects of the invention
The cigarettes of the colorless caramel-flavored filter sticks prepared in examples 1-5 were equilibrated for 48 hours in an environment of 65% relative humidity and 22 ± 2 ℃, and the cigarettes without any treatment were used as a control. 5 smokers were selected for smoking. The result of smoke panel test shows that after the colorless caramel fragrance filter stick cigarette is smoked, the irritation of the throat is reduced, the aftertaste is obviously improved, the sweet feeling of the oral cavity is enhanced, and meanwhile, the smoke gas emits the caramel fragrance. The specific results of the smoking are shown in tables 1 and 2 below.
The cigarettes of the colorless caramel fragrance filter stick prepared in the five examples are used as an experimental group, and the cigarettes without any treatment are used as a color difference standard, and the same section is selected for color difference comparison analysis. The specific analysis results are shown in table 3 below:
TABLE 1 colorless caramel incense filter stick cigarette evaluation table
TABLE 2 evaluation of cigarettes with colorless caramel aroma
TABLE 3 color difference analysis of colorless caramel essence applied to filter stick
TABLE 4 results of the intrinsic flavour components of the colourless caramel flavour
The results show that: on the premise of not changing the natural color of the cigarette filter stick, the cigarette filter stick gives the characteristic style of caramel aroma to the smoke, reduces the irritation of the smoke, improves the aftertaste of the oral cavity, increases the sweet and moist feeling of the oral cavity, and has the functions of increasing the aroma and supplementing the aroma to the cigarette.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. The preparation method of the colorless caramel spice is characterized by comprising the following steps:
(1) preparing sugar solution from sugar and solvent;
(2) adding an alkaline compound into the sugar solution obtained in the step (1) to adjust the pH value to obtain a reaction solution;
(3) carrying out microwave reflux heating on the reaction solution in the step (2) to obtain caramel essence, and refrigerating and standing until layering;
(4) and (4) taking the upper layer liquid of the caramel essence liquid after standing in the step (3), adding absolute ethyl alcohol, mixing, and then placing in a reduced pressure distillation device to collect fractions, namely the colorless caramel essence.
2. The method of preparing a colorless caramel aroma according to claim 1, wherein: the mass ratio of the sugar to the solvent in the step (1) is 1 (2-5), and the sugar is glucose, fructose, lactose, ribose, deoxyribose, maltose or compound sugar; the solvent is propylene glycol or water or a mixed solution of the propylene glycol and the water.
3. The method of preparing a colorless caramel aroma according to claim 1, wherein: in the step (2), the alkaline compound is sodium carbonate, sodium bicarbonate, potassium hydroxide or sodium hydroxide, and the pH value is 9-11.
4. The method of preparing a colorless caramel aroma according to claim 1, wherein: the temperature of the microwave reflux heating in the step (3) is 80-90 ℃, the microwave power is 400-600W, and the heating time is 0.5-1.5 h.
5. The method of preparing a colorless caramel aroma according to claim 4, wherein: the time for cooling and standing in the step (3) is 24-48h, and the temperature is 1-5 ℃.
6. The method of preparing a colorless caramel aroma according to claim 1, wherein: the mass ratio of the upper layer liquid to the absolute ethyl alcohol in the step (4) is 1 (1-2).
7. The process for the preparation of a colorless caramel flavor according to claim 6, wherein the distillation under reduced pressure in step (4) is carried out under the following conditions: the temperature is 60-80 ℃, the time is 0.5-1.5h, and the pressure is 90kPa-100 kPa.
8. Use of a colourless caramel flavour prepared according to any one of claims 1 to 7 in the preparation of a colourless caramel flavour cigarette, characterised in that: adding the colorless caramel aroma perfume into the filter stick tows according to the application amount of 1-2 mu L/mm to prepare the colorless caramel aroma cigarette filter stick.
9. Use according to claim 8, characterized in that: and soaking the filter stick fragrant threads with colorless caramel fragrant spices to prepare colorless caramel fragrant cigarette filter sticks.
10. Use according to claim 8, characterized in that: adding colorless caramel aroma into tobacco shreds at an application amount of 1-10wt% for preparing colorless caramel cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911353761.4A CN110839945B (en) | 2019-12-25 | 2019-12-25 | Preparation method and application of colorless caramel spice |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911353761.4A CN110839945B (en) | 2019-12-25 | 2019-12-25 | Preparation method and application of colorless caramel spice |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110839945A true CN110839945A (en) | 2020-02-28 |
| CN110839945B CN110839945B (en) | 2021-07-30 |
Family
ID=69610811
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911353761.4A Active CN110839945B (en) | 2019-12-25 | 2019-12-25 | Preparation method and application of colorless caramel spice |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110839945B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111254014A (en) * | 2020-03-05 | 2020-06-09 | 四川中烟工业有限责任公司 | Caramel aroma spice, preparation method and application method thereof |
| CN111588073A (en) * | 2020-03-05 | 2020-08-28 | 四川中烟工业有限责任公司 | Burnt sweet-fragrance electronic cigarette tobacco tar, preparation method and application method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101619173A (en) * | 2009-07-29 | 2010-01-06 | 华南理工大学 | Method for simultaneously preparing caramel pigment and aromatiser for edible safety beverage |
| KR20120026917A (en) * | 2010-09-10 | 2012-03-20 | 주식회사 케이티앤지 | Cigarette paper using tobacco fibers and cigarette including the same |
| CN106947596A (en) * | 2017-04-12 | 2017-07-14 | 安徽中烟工业有限责任公司 | A kind of cigarette preparation method of maltose caramel spices |
| CN107011696A (en) * | 2017-05-26 | 2017-08-04 | 陕西科技大学 | A kind of common caramel colorant of salt tolerance and its preparation method and application |
| CN108948784A (en) * | 2018-08-23 | 2018-12-07 | 湖南汇升生物科技有限公司 | A kind of caramel pigment production technology |
-
2019
- 2019-12-25 CN CN201911353761.4A patent/CN110839945B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101619173A (en) * | 2009-07-29 | 2010-01-06 | 华南理工大学 | Method for simultaneously preparing caramel pigment and aromatiser for edible safety beverage |
| KR20120026917A (en) * | 2010-09-10 | 2012-03-20 | 주식회사 케이티앤지 | Cigarette paper using tobacco fibers and cigarette including the same |
| CN106947596A (en) * | 2017-04-12 | 2017-07-14 | 安徽中烟工业有限责任公司 | A kind of cigarette preparation method of maltose caramel spices |
| CN107011696A (en) * | 2017-05-26 | 2017-08-04 | 陕西科技大学 | A kind of common caramel colorant of salt tolerance and its preparation method and application |
| CN108948784A (en) * | 2018-08-23 | 2018-12-07 | 湖南汇升生物科技有限公司 | A kind of caramel pigment production technology |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111254014A (en) * | 2020-03-05 | 2020-06-09 | 四川中烟工业有限责任公司 | Caramel aroma spice, preparation method and application method thereof |
| CN111588073A (en) * | 2020-03-05 | 2020-08-28 | 四川中烟工业有限责任公司 | Burnt sweet-fragrance electronic cigarette tobacco tar, preparation method and application method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110839945B (en) | 2021-07-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101565652B (en) | Fruity type flue-cured tobacco essence and applications thereof | |
| CN107125803B (en) | A kind of electronic cigarette tobacco tar and preparation method thereof | |
| CN103923747B (en) | Essence on cigarette tissue | |
| CN110846133A (en) | Cigarette caramel spice under negative pressure condition and preparation method thereof | |
| CN110699183A (en) | Tobacco essence with spicy fragrance | |
| CN110839945B (en) | Preparation method and application of colorless caramel spice | |
| CN101633864A (en) | Apple-flavored essence for tobacco, preparation method and application thereof | |
| CN108504454B (en) | Preparation method of improved cigarette tailing spice and application of improved cigarette tailing spice in cigarettes | |
| CN110584214B (en) | Composite fragrant essence for low-temperature cigarettes and application thereof | |
| CN111073945A (en) | Peptide Maillard intermediate, preparation method and application thereof | |
| CN110423647A (en) | A kind of tea essence and its preparation method and application | |
| CN104745304A (en) | Maillard reaction product prepared by taking rose, pomegranate and fermented glutinous rice as raw materials and application thereof in cigarette | |
| KR20130002109A (en) | Method for manufacturing cartridge solution composite of electronic non-smoking cigarette and cartridge solution composite of electronic non-smoking cigarette manufactured by this | |
| CN103462212A (en) | Method for improving quality of tobacco leaves by adding enzyme preparation, glucose and citric acid | |
| CN105831797B (en) | A kind of cabo particle and its application for being applied to prepare buccal cigarette | |
| CN103070475A (en) | Cigar tobacco leaf additive and production method thereof | |
| CN107325886A (en) | The preparation method and applications of aspartic acid maillard reaction thing | |
| CN105029683A (en) | Method for preparing cigar tobacco leaves by virtue of compound starter fermentation | |
| CN106701324B (en) | Method for extracting tomato essence for cigarettes step by using kaoliang spirit as solvent | |
| CN110643428A (en) | Lemon and vanilla compound aroma type perfume essence and application thereof | |
| CN105029684A (en) | Method for preparing cigar tobacco leaves by virtue of compound amino acid fermentation | |
| CN104068465A (en) | Method for making strong-flavor buccal cigarette | |
| CN112980580A (en) | Maillard reaction spice and preparation method and application thereof | |
| CN111187666A (en) | Burnt flavor essence for cigarettes and application thereof | |
| CN109864331A (en) | A kind of cigarette flavors additive and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |