CN105199850B - A kind of preparation method and applications of tobacco aromaticss - Google Patents
A kind of preparation method and applications of tobacco aromaticss Download PDFInfo
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- CN105199850B CN105199850B CN201510667638.5A CN201510667638A CN105199850B CN 105199850 B CN105199850 B CN 105199850B CN 201510667638 A CN201510667638 A CN 201510667638A CN 105199850 B CN105199850 B CN 105199850B
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Abstract
The present invention relates to a kind of preparation method and applications of tobacco aromaticss, preparation method includes: to use Yunnan tobacco for raw material, by drying, it crushes, the water of 4 ~ 5 times of Yunnan tobacco quality amounts is added, it is heated to 80 ~ 85 DEG C of 1 ~ 1.5h of immersion, then the ethyl alcohol that quality is 6 ~ 6.5 times of Yunnan tobacco amounts is added to extract, Yunnan tobacco primary extract is obtained after concentration, it is in mass ratio that 10 ~ 30 ﹕ 1 addition progress supercritical extract into carbon dioxide supercritical extraction device obtains extract liquor by Yunnan tobacco primary extract and particulate filler, by extract liquor, xylose, phenylalanine, glycerol and pure water are that tobacco aromaticss are prepared in 50 ~ 70 ﹕, 5 ~ 7 ﹕, 1 ~ 3 ﹕, 20 ~ 50 ﹕ 2 ~ 5 progress Maillard reaction in mass ratio.Preparation method easy steps of the present invention are easily operated, supercritical extract is used in combination with Maillard reaction, extraction temperature is low, extraction time is short, the aroma component in tobacco is saved to greatest extent, by making the tobacco aromaticss note being prepared into richer after Maillard reaction, fragrance is more full strong.
Description
Technical field
The present invention relates to a kind of preparation method and applications of tobacco aromaticss, belong to tobacco aromaticss preparation technical field.
Background technique
As people gradually increase smoking with health problem attention rate, tobacco industry implements reducing tar and reducing harm in recent years
Engineering, constantly to adapt to the requirement of society, and with the continuous reduction of tar content in cigarette, fragrance component in tobacco also phase
The reduction answered needs to compensate low-coke tar cigarette fragrance.Therefore fragrance material is extracted from tobacco to low-coke tar cigarette perfume
It is an important approach that gas, which carries out effective compensation,.
Tobacco leaf has a variety of effects such as subdhing swelling and detoxicating, desinsection, pharmacy, can also produce high-grade natural perfume material, this fragrance,
It can be directly used for cigarette and perfuming tobacco thin sheet, fragrance is true to nature, naturally, enhancing cigarette perfume, reduces miscellaneous gas, improves cigarette quality, no
It is only capable of augmenting the characteristic perfume of all kinds of tobaccos, and has effects that smoke draft is fragrant, effect is adjusted considerably more than previous
The various tobacco aromaticss that perfume (or spice) uses.
Summary of the invention
The purpose of the present invention is to solve need to add fragrance in cigarette to carry out flavor compensating, existing tobacco aromaticss preparation
Complicated problem, provides that a kind of preparation method is simple, the system of the fragrance tobacco aromaticss suitable for cigarette shreds naturally true to nature
Preparation Method and its application.
The present invention adopts the following technical scheme: a kind of preparation method of tobacco aromaticss, uses Yunnan tobacco for raw material, passes through
Maillard reaction being carried out after supercritical extract, tobacco aromaticss being prepared, specific steps include:
(1) preparation of Yunnan tobacco primary extract: Yunnan tobacco is dried, and is crushed, and is obtained after crossing 10 ~ 20 meshes using alcohol extracting
Yunnan tobacco primary extract；
It (2) is in mass ratio that 10 ~ 30 ﹕ 1 are packed into after mixing to overcritical by Yunnan tobacco primary extract and particulate filler
In extractor, then volume fraction is 75% ethyl alcohol as supercritical extract entrainer and be added into entrainer tank, opens super face
Boundary's extraction equipment carry out supercritical extract, supercritical extract pressure be 23 ~ 28MPa, supercritical extract temperature be 40 ~ 50 DEG C, two
Oxidation carbon flow is 2 ~ 4L/min, and 150 ~ 300ml/min of entrainer, the supercritical extract time is 2 ~ 5h；
(3) after extracting, 5 ~ 8MPa of pressure in separating still is controlled, 35 ~ 45 DEG C of temperature, is separated, is gone out from separating still
Mouth releases extract liquor；
It (4) is in mass ratio 50 ~ 70 ﹕, 5 ~ 7 ﹕, 1 ~ 3 ﹕, 20 ~ 50 ﹕ 2 by extract liquor, xylose, phenylalanine, glycerol and pure water
~ 5 be uniformly mixed reaction solution is made；
(5) reaction solution is added into Maillard reaction tank, it is beautiful using the pH value of KOH aqueous solution adjusting reaction solution to 6 ~ 7
It is 80 ~ 100 DEG C that moral, which draws the temperature in reactor tank, is stirred continuously and carries out 3 ~ 5h of Maillard reaction, obtains tobacco aromaticss after cooling.
Further, the density of the tobacco aromaticss is 1.21 ~ 1.23g/ml.
Further, the alcohol extracting includes the following steps: for the Yunnan tobacco after sieving to be added into extractor, and matter is added
Amount is the water of 4 ~ 5 times of Yunnan tobacco amounts, is heated to 80 ~ 85 DEG C of 1 ~ 1.5h of immersion, and it is Yunnan that quality is then added into extractor
The ethyl alcohol of 6 ~ 6.5 times of tobacco leaf amounts, heating make extracting solution boil, and 3 ~ 5h of refluxing extraction, liquid cooling to be extracted is but cooled to 40 DEG C or less
When release extracting solution, after centrifugal filtration will filtrate be added concentration tank in be concentrated under reduced pressure, fluid temperature be not higher than 60 DEG C, density
To stop concentration when 1.30 ~ 1.32g/ml.
Further, the volume fraction of the ethyl alcohol is not less than 90%.
Further, the particulate filler is ceramic raschig rings, and the diameter of the ceramic raschig rings is 16 ~ 38mm.
Using the application for the tobacco aromaticss that the preparation method of tobacco spice obtains, tobacco aromaticss obtained are diluted to quality
Solution, is uniformly sprayed to volume with laryngeal spray by 0.2 ~ 0.5% dosage of pipe tobacco weight by the solution that concentration is 0.5 ~ 0.2%
In cigarette pipe tobacco, pipe tobacco is rolled into cigarette.
Preparation method easy steps of the present invention are easily operated, and supercritical extract is used in combination with Maillard reaction, extraction
Temperature is low, and extraction time is short, saves the aroma component in tobacco to greatest extent, by making to be prepared into after Maillard reaction
Tobacco aromaticss note it is richer, fragrance is more full strong.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment one:
(1) preparation of Yunnan tobacco primary extract: Yunnan tobacco is dried, and is crushed, and 10 ~ 20 meshes are crossed, and is added in extractor,
Then the water that quality is 5 times of Yunnan tobacco amounts is added, is warming up to 85 DEG C, impregnates 1h at this temperature, then adds into extractor
Entering the ethyl alcohol that quality is 6 times of Yunnan tobacco amounts, volume fraction of ethanol 90%, heating makes extracting solution boil, refluxing extraction 3h, to
Extracting solution releases extracting solution when cooling to 40 DEG C or less, and filtrate is added in concentration tank after centrifugal filtration and is concentrated under reduced pressure, liquid
Temperature is not higher than 60 DEG C, stops concentration when density is 1.32g/ml, obtains Yunnan tobacco primary extract；
(2) Yunnan tobacco primary extract and particulate filler are fitted into supercritical extract tank after mixing, Yunnan tobacco
The mass ratio of primary extract and particulate filler is 10 ﹕ 1, and particulate filler is the Raschig ring that specification is Φ 38, is then by volume fraction
75% ethyl alcohol is added as supercritical extract entrainer into entrainer tank, opens supercritical extraction unit and carries out supercritical extract,
Supercritical extract pressure is 28MPa, and supercritical extract temperature is 50 DEG C, carbon dioxide flow 4L/min, entrainer 300ml/
Min, supercritical extract time are 2h；
(3) after extracting, pressure 8MPa in separating still is controlled, temperature 45 C is separated, and is exported and is released from separating still
Extract liquor；
(4) reaction solution is prepared by proportion scale, extract liquor, xylose, phenylalanine, glycerol and pure water are in mass ratio
50:5:1:20:2 is weighed and is uniformly mixed；
(5) reaction solution of preparation is added into Maillard reaction tank, is adjusted in Maillard reaction tank with KOH aqueous solution
For pH value to 7, it is 80 DEG C that virtue, which draws the temperature in reactor tank, is stirred continuously and carries out Maillard reaction 5h, and cigarette perfume is obtained after cooling
Material.
Gained tobacco aromaticss are diluted to 80% ethanol solution to 0.5% solution, by 0.2% dosage of pipe tobacco weight
Solution is uniformly added in cigarette shreds with laryngeal spray, pipe tobacco is rolled into cigarette.It is smoked panel test and thinks the product in cigarette
Middle flavoring is obvious, so that cigarette cigarette perfume is strong, flue gas is soft, without miscellaneous gas, improves cigarette product quality.
Embodiment two:
(1) preparation of Yunnan tobacco primary extract: Yunnan tobacco is dried, and is crushed, and 10 ~ 20 meshes are crossed, and is added in extractor,
Then the water that quality is 5 times of Yunnan tobacco amounts is added, is warming up to 80 DEG C, impregnates 1h at this temperature, then adds into extractor
Entering the ethyl alcohol that quality is 6 times of Yunnan tobacco amounts, volume fraction of ethanol 95%, heating makes extracting solution boil, refluxing extraction 5h, to
Extracting solution releases extracting solution when cooling to 40 DEG C or less, and filtrate is added in concentration tank after centrifugal filtration and is concentrated under reduced pressure, liquid
Temperature is not higher than 60 DEG C, stops concentration when density is 1.30g/ml, obtains Yunnan tobacco primary extract；
(2) Yunnan tobacco primary extract and particulate filler are fitted into supercritical extract tank after mixing, Yunnan tobacco
The mass ratio of primary extract and particulate filler is 30 ﹕ 1, and particulate filler is the Raschig ring that specification is Φ 16, is then by volume fraction
75% ethyl alcohol is added as supercritical extract entrainer into entrainer tank, opens supercritical extraction unit and carries out supercritical extract,
Supercritical extract pressure is 23MPa, and supercritical extract temperature is 40 DEG C, carbon dioxide flow 2L/min, entrainer 150ml/
Min, supercritical extract time are 5h；
(3) after extracting, pressure 5MPa in separating still is controlled, 35 DEG C of temperature, is separated, exported and release from separating still
Extract liquor；
It (4) is in mass ratio that 70:7:3:50:5 is weighed and mixed by Cui Qu Ye ﹕ Mu Tang ﹕ Ben Bing An Suan ﹕ Gan You ﹕ pure water
Uniformly it is configured to reaction solution；
(5) prepared reaction solution is added into Maillard reaction tank, is adjusted in Maillard reaction tank with KOH aqueous solution
Solution ph to 6, it is 100 DEG C that virtue, which draws the temperature in reactor tank, is stirred continuously and carries out Maillard reaction 3h, obtains after cooling
Tobacco aromaticss.
Gained tobacco aromaticss are diluted to 80% ethanol solution to 0.2% solution, by 0.5% dosage of pipe tobacco weight
Solution is uniformly added in cigarette shreds with laryngeal spray, pipe tobacco is rolled into cigarette.It is smoked panel test and thinks the product in cigarette
Middle flavoring is obvious, so that cigarette cigarette perfume is strong, flue gas is soft, without miscellaneous gas, improves cigarette product quality.
Embodiment three:
(1) preparation of Yunnan tobacco primary extract: Yunnan tobacco is dried, and is crushed, and 10 ~ 20 meshes are crossed, and is added in extractor,
Then the water that quality is 5 times of Yunnan tobacco amounts is added, is warming up to 83 DEG C, impregnates 1h at this temperature, then adds into extractor
Entering the ethyl alcohol that quality is 6 times of Yunnan tobacco amounts, volume fraction of ethanol 95%, heating makes extracting solution boil, refluxing extraction 4h, to
Extracting solution releases extracting solution when cooling to 40 DEG C or less, and filtrate is added in concentration tank after centrifugal filtration and is concentrated under reduced pressure, liquid
Temperature is not higher than 60 DEG C, stops concentration when density is 1.31g/ml, obtains Yunnan tobacco primary extract；
(2) Yunnan tobacco primary extract and particulate filler are fitted into supercritical extract tank after mixing, Yunnan tobacco
The mass ratio of primary extract and particulate filler is 20 ﹕ 1, and particulate filler is the Raschig ring that specification is Φ 25, is then by volume fraction
75% ethyl alcohol is added as supercritical extract entrainer into entrainer tank, opens supercritical extraction unit and carries out supercritical extract,
Supercritical extract pressure is 25MPa, and supercritical extract temperature is 45 DEG C, carbon dioxide flow 3L/min, entrainer 200ml/
Min, supercritical extract time are 4h；
(3) after extracting, pressure 6MPa in separating still is controlled, 40 DEG C of temperature, is separated, exported and release from separating still
Extract liquor；
It (4) is in mass ratio that 60:6:2:30:3 is weighed and mixed by extract liquor, xylose, phenylalanine, glycerol and pure water
Uniformly it is configured to reaction solution；
(5) reaction solution of preparation is added into Maillard reaction tank, is adjusted in Maillard reaction tank with KOH aqueous solution
For pH value to 6.5, it is 90 DEG C that virtue, which draws the temperature in reactor tank, is stirred continuously and carries out Maillard reaction 4h, and cigarette use is obtained after cooling
Fragrance.
Gained tobacco aromaticss are diluted to 80% ethanol solution to 0.3% solution, by 0.4% dosage of pipe tobacco weight
Solution is uniformly added in cigarette shreds with laryngeal spray, pipe tobacco is rolled into cigarette.It is smoked panel test and thinks the product in cigarette
Middle flavoring is obvious, so that cigarette cigarette perfume is strong, flue gas is soft, without miscellaneous gas, improves cigarette product quality.
Claims (3)
1. a kind of preparation method of tobacco aromaticss, it is characterised in that: use Yunnan tobacco for raw material, it is laggard by supercritical extract
Tobacco aromaticss are prepared in row Maillard reaction, and specific steps include:
(1) preparation of Yunnan tobacco primary extract: Yunnan tobacco is dried, and is crushed, and is crossed after 10 ~ 20 meshes and is obtained Yunnan using alcohol extracting
Tobacco leaf primary extract, the alcohol extracting include the following steps: for the Yunnan tobacco after sieving to be added into extractor, and addition quality is cloud
4 ~ 5 times of southern tobacco leaf amount water, be heated to 80 ~ 85 DEG C of 1 ~ 1.5h of immersions, then into extractor be added quality for Yunnan tobacco 6 ~
The ethyl alcohol of 6.5 times of amounts, heating make extracting solution boil, 3 ~ 5h of refluxing extraction, releasing when liquid cooling to be extracted is but cooled to 40 DEG C or less
Filtrate is added in concentration tank after centrifugal filtration and is concentrated under reduced pressure by extracting solution, and fluid temperature is not higher than 60 DEG C, density 1.30
Stop concentration when ~ 1.32g/ml, the volume fraction of the ethyl alcohol is not less than 90%；
It (2) is in mass ratio that 10 ~ 30:1 is packed into after mixing to supercritical extract by Yunnan tobacco primary extract and particulate filler
In tank, the particulate filler is ceramic raschig rings, and the diameter of the ceramic raschig rings is 16 ~ 38mm, then using ethyl alcohol as super
Critical extraction entrainer is added into entrainer tank, opens supercritical extraction unit and carries out supercritical extract, supercritical extract pressure
Power is 23 ~ 28MPa, and supercritical extract temperature is 40 ~ 50 DEG C, and carbon dioxide flow is 2 ~ 4L/min, 150 ~ 300ml/ of entrainer
Min, supercritical extract time are 2 ~ 5h；
(3) after extracting, 5 ~ 8MPa of pressure in separating still is controlled, 35 ~ 45 DEG C of temperature, is separated, put from separating still outlet
Extract liquor out；
It (4) is in mass ratio that 50 ~ 70:5 ~ 7:1 ~ 3:20 ~ 50:2 ~ 5 are mixed by extract liquor, xylose, phenylalanine, glycerol and pure water
It closes and reaction solution is uniformly made；
(5) reaction solution is added into Maillard reaction tank, using the pH value of KOH aqueous solution adjusting reaction solution to 6 ~ 7, virtue is drawn
Temperature in reactor tank is 80 ~ 100 DEG C, is stirred continuously and carries out 3 ~ 5h of Maillard reaction, obtains tobacco aromaticss after cooling.
2. the preparation method of tobacco aromaticss as described in claim 1, it is characterised in that: the density of the tobacco aromaticss is 1.21
~1.23g/ml。
3. using the application for the tobacco aromaticss that the preparation method of the tobacco aromaticss of claim 1 obtains, it is characterised in that: will be made
Tobacco aromaticss be diluted to the solution that mass concentration is 0.5 ~ 0.2%, it is spraying with larynx by 0.2 ~ 0.5% dosage of pipe tobacco weight
Solution is uniformly sprayed in cigarette shreds by device, and pipe tobacco is rolled into cigarette.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105768203B (en) * | 2016-03-25 | 2017-07-07 | 广东省金叶科技开发有限公司 | A kind of endogenous preparation method of Studies of The Aromatic Substances tobacco particle of enhancing |
| CN106190562A (en) * | 2016-08-11 | 2016-12-07 | 无锡华海香料有限公司 | A kind of preparation method of tobacco aromatics using |
| CN106190578A (en) * | 2016-08-15 | 2016-12-07 | 河南中烟工业有限责任公司 | A kind of roasting liquorice essence, its preparation method and the application in Medicated cigarette |
| CN108251213A (en) * | 2016-12-29 | 2018-07-06 | 广州华芳烟用香精有限公司 | A kind of natural perfume material distillation and its preparation method and application |
| CN108219942A (en) * | 2018-01-08 | 2018-06-29 | 安徽中烟工业有限责任公司 | A kind of method for preparing tobacco extract using high static pressure auxiliary Maillard reactions |
| CN114983003A (en) * | 2022-06-13 | 2022-09-02 | 湖北中烟工业有限责任公司 | Preparation method and application of tobacco extract |
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| CN1415717A (en) * | 2002-11-08 | 2003-05-07 | 华宝香化科技发展（上海）有限公司 | Method for producing cigarette spicery made from extractive material of tobacco as raw material |
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Address after: 850000, Tibet autonomous region Lhasa economic and Technological Development Zone Sang Sang road investment building, No. 6 Applicant after: HUABAO FLAVOURS & FRAGRANCES CO.,LTD. Address before: 850000, Tibet autonomous region Lhasa economic and Technological Development Zone Sang Sang road investment building, No. 6 Applicant before: Huabao flavor Ltd. Address after: 850000, Tibet autonomous region Lhasa economic and Technological Development Zone Sang Sang road investment building, No. 6 Applicant after: Huabao flavor Ltd. Address before: 201821 Yecheng Road, Shanghai, No. 1299, No. Applicant before: Huabao Flavours & Fragrances Co.,Ltd |
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Address after: 850000 Tibet economic and Technological Development Zone, Lhasa Economic Development Zone, road, building Applicant after: HUABAO FLAVOURS & FRAGRANCES CO.,LTD. Address before: 850000, Tibet autonomous region Lhasa economic and Technological Development Zone Sang Sang road investment building, No. 6 Applicant before: HUABAO FLAVOURS & FRAGRANCES CO.,LTD. |
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