CN101129216A - Tobacco component additive agent for compensating aroma to low tar cigarette - Google Patents
Tobacco component additive agent for compensating aroma to low tar cigarette Download PDFInfo
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- CN101129216A CN101129216A CNA2007101897207A CN200710189720A CN101129216A CN 101129216 A CN101129216 A CN 101129216A CN A2007101897207 A CNA2007101897207 A CN A2007101897207A CN 200710189720 A CN200710189720 A CN 200710189720A CN 101129216 A CN101129216 A CN 101129216A
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Abstract
The invention discloses a tobacco component additive to compensate the perfume of low-tar cigarette, which comprises the following parts: 0. 1-2kg tobacco extract, 0-10g furfural, 1-5g 5-methyl-furfural, 1-10g 3-ethyl-2-hydroxy-cyclopentene-1-ketone, 1-10g hexadecyl methyl ester, 1-10g solanestone, 0-10g kiwi fruit lactone dihydroxide, 1-10g calicotone, 1-20g hugebean alkatrientone, 0-10g pyridine, 0-10g 2-methyl-pyridine, 0-100g acetic acid, 0-10g propionic acid, 0-10g benzene carbonic acid, 0-100g benzene carbonic acid, wherein the weight of the raw materials is 1-4 times as diluent. The invention uses tobacco extract and tobacco perfume material as raw material to improve the perfume content of low-tar cigarette, which has good harmonization with tobacco under convenient preparing method and wide resource of raw material.
Description
Technical field
The present invention relates to the tobacco manufacture field, relate to a kind of tobacco component additive agent concretely fragrance compensation for low-coke tar cigarette.Add this additive in tobacco leaf, pipe tobacco or the auxilliary material by using, can compensate the loss of aroma of low-coke tar cigarette effectively at low-coke tar cigarette.
Technical background
Along with the growing interest to the cigarette consumer health, the research and development of low-coke tar cigarette product and production and sales are inexorable trends of tobacco business development.But meanwhile, cigarette also descends aspect jealous to some extent at perfume (or spice), and it is comparatively outstanding that the compensating aroma problem has seemed, and is especially all the more so for China's Virginian-type cigarette accounts for tobacco business more than 95%.Therefore, endeavour to explore the compensating aroma problem of low tar Virginian-type cigarette, study practicable compensation technique measure, most important for the development of Chinese style cigarette.
Ventilation dilution (Dweyer R.W., et al.Beitr.Tabakforsch.Int.1999,18:205.Jing Y., C., et al.Beitr.Tabakforsch.Int.2005,21:280.) and the lengthening filter stick (Fielding S., et al.Mutation 1989,214:147) be present cigarette the most frequently used burnt measure falls.Yet; these fall the minimizing (Jing Yanqiu of the cigarette main flow grain phase flavor component that burnt measure can cause usually; Xian Kefa. Chinese tobacco journal 1999; (02): 1.) research (Gori G.B.Science (Washington DC) 1976; 194 (4271): 1243.) show; adopt ventilation dilution and the cigarette main flow grain minimizing of flavor component mutually that Jiao causes falls in measure such as the filter stick that extends; can compensate by the method for adding the tobacco aroma component, thereby reach the purpose of compensating aroma of low tar cigarette.
Summary of the invention
Purpose of the present invention just be based on present employing ventilation dilution with lengthening filter stick etc. measure fall Jiao cause cigarette main flow grain mutually flavor component reduce, the problem that smoke is thin out, fragrance is not enough and provide a kind of can add in low-coke tar cigarette raw material or the auxilliary material can be to the tobacco component additive agent of fragrance compensation for low-coke tar cigarette, the interpolation by this additive can reach the purpose to fragrance compensation for low-coke tar cigarette.
Characteristics of the present invention are that with tobacco extract and tobacco flavor matter be primary raw material, obviously improve the perfume quantity of low-coke tar cigarette, and good with the fragrant harmony of cigarette, and raw material sources are wide, easy to prepare simultaneously.
Tobacco component additive agent to fragrance compensation for low-coke tar cigarette of the present invention comprises the raw material of following weight ratio, wherein: tobacco extract 0.1-2 kilogram, furfural 0-10 gram, 5-methyl-furfural 1-5 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 1-10 gram, methyl palmitate 1-10 gram, eggplant Buddhist nun ketone 1-10 gram, dihydroactinidiolide 0-10 gram, damascenone 1-10 gram, Megastigmatrienone 1-20 gram, pyridine 0-10 gram, 2-methyl-pyridine 0-10 gram, acetate 0-100 gram, propionic acid 0-10 gram, benzoic acid 0-10 gram, hexadecylic acid 0-100 gram, and above-mentioned raw materials weight sum 1-4 diluent doubly.
Described diluent is ethanol or triacetyl glycerine.
Tobacco extract described in the present invention be in the tobacco leaf from types such as flue-cured tobacco, suncured tabacco, burley tobaccos, Turkish tobaccos any one or two or more tobacco leaf through in extract and obtain, its extracting method can adopt supercritical fluid CO
2Extracting, also can adopt alcohol extract, can also adopt extracted by ether, also can be two or more extraction that combines of said extracted method.
Specifically, described supercritical fluid CO
2Method comprises the steps: that with tobacco leaf be raw material, with supercritical CO
2Fluid is an extractant, extracting pressure 20-30MPa, and extraction temperature 35-50 ℃, entrainer is the 20-30% absolute ethyl alcohol, separating pressure 5-8MPa, separation temperature 55-70 ℃, disengaging time 1-3h, final gained is tobacco extract.
Described alcohol extract method comprises the steps: to get tobacco leaf 1000 grams and is raw material, adds the ethanol 2000-4000mL of 90-100%, extracts 2h under 60-80 ℃ of condition, repeats to extract once; Extract concentrates removes ethanol, and final gained is tobacco extract.
Described extracted by ether method comprises the steps: to get tobacco leaf 1000 grams and is raw material, adds ether 2000-5000mL, and refluxing extraction 2h under 40-60 ℃ condition repeats once, and extract is removed ether through concentrating, and final gained is tobacco extract.
The extracting method that described ethanol and extracted by ether combine comprises the steps: to get tobacco leaf 1000 grams and is raw material, adds the ethanol 2000-4000mL of 70-95%, extracts 2h under 60-80 ℃ condition, repeats to extract once; Extract gets CE after concentrating and removing ethanol; Crude extract filters through the ether dissolution of 400-1000mL, and filtrate concentrating removed ether, and final gained is tobacco extract.
The raw material that can also comprise the following weight ratio in the additive of the present invention: neophytadiene 10-500 gram.
The additive that the feedstock production of above-mentioned weight ratio forms is 100 kilograms of amounts that tobacco feeding is required.
Additive of the present invention is mended the fragrant additive time spent as per 100 kilograms of raw tobacco materials, and the raw material of its optimum ratio (weight ratio) is: tobacco extract 0.1-2 kilogram, 5-methyl-furfural 1-5 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 1-10 gram, methyl palmitate 1-10 gram, eggplant Buddhist nun ketone 1-10 gram damascenone 1-10 gram, Megastigmatrienone 1-20 gram.
Additive of the present invention is mended the fragrant additive time spent as dark obbbin, and the raw material of its optimum ratio (weight ratio) is: tobacco extract 0.1-2 kilogram, furfural 0-10 gram, 5-methyl-furfural 1-5 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 1-10 gram, methyl palmitate 1-10 gram, eggplant Buddhist nun ketone 1-10 gram, damascenone 1-10 gram, Megastigmatrienone 1-20 gram, 2-picoline 0-10 gram, hexadecylic acid 0-100 gram.
Cigarette after adopting additive of the present invention to fragrance compensation for low-coke tar cigarette is compared with the prior art low-coke tar cigarette, and its beneficial effect is as follows:
1. get low-coke tar cigarette blade double centner, 0.5 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2 grams, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2 grams, damascenone 2 grams, Megastigmatrienone 3 grams, 2-methyl-pyridine 1 gram, acetate 10 grams, hexadecylic acid 10 grams are added in reinforced link with 2 kilograms of ethanol dilution backs, and other link is with normal cigarette process.Low-coke tar cigarette after the processing is compared with contrast cigarette, and sensory evaluating smoking's perfume quantity obviously increases, and main flume grain phase flavor component total amount can increase by 11%.
2. 1 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2, damascenone 2 grams, Megastigmatrienone 3 grams, 2-methyl-pyridine 1 gram, acetate 10 grams, hexadecylic acid 10 grams are added on the dark colour obbbin all the other same normal process with the amount of weight ratio 2% after with 4 kilograms of ethanol dilutions.The low-coke tar cigarette of handling compared with the control, sensory evaluating smoking's perfume quantity obviously increases.
3. get low-coke tar cigarette baking back pipe tobacco double centner, 0.5 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2, damascenone 2 grams, Megastigmatrienone 3 grams, acetate 10 grams, hexadecylic acid 10 grams are added in the perfuming link with 2 kilograms of ethanol dilution backs.All the other same normal process.The low-coke tar cigarette of handling compared with the control, sensory evaluating smoking's perfume quantity obviously increases, main flume grain phase flavor component total amount can increase by 13%.
4. 1 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2 grams, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2 grams, damascenone 2 grams, Megastigmatrienone 3 grams, 2-methyl-pyridine 1 gram, acetate 10 grams, hexadecylic acid 10 grams are added in the filter tip all the other same normal process with the amount of weight ratio 5% after with 4 kilograms of triacetyl glycerines dilutions.The low-coke tar cigarette of handling compared with the control, sensory evaluating smoking's perfume quantity obviously increases.
Embodiment
The present invention is further described below with reference to embodiment, but does not limit the present invention.
Embodiment 1
Get low-coke tar cigarette blade double centner, 0.5 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2 grams, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2 grams, damascenone 2 grams, Megastigmatrienone 3 grams, 2-methyl-pyridine 1 gram, acetate 10 grams, hexadecylic acid 10 grams are added in reinforced link with 2 kilograms of ethanol dilution backs, and other links are with normal cigarette process.
Embodiment 2
Get low-coke tar cigarette baking back pipe tobacco double centner, 0.5 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2, damascenone 2 grams, Megastigmatrienone 3 grams, acetate 10 grams, hexadecylic acid 10 grams are added in the perfuming link with 2 kilograms of ethanol dilution backs.All the other same normal process.
Embodiment 3
1 kilogram of tobacco extract, furfural 2 grams, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2 grams, damascenone 2 grams, Megastigmatrienone 3 grams, 2-methyl-pyridine 1 gram, acetate 10 grams, hexadecylic acid 10 grams are added on the dark colour obbbin with the amount of 4 kilograms of ethanol dilution backs with weight ratio 2%.All the other same normal process.
Embodiment 4
1 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2 grams, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2, damascenone 2 grams, Megastigmatrienone 3 grams, 2-methyl-pyridine 1 gram, acetate 10 grams, hexadecylic acid 10 grams are added in the filter tip with the amount of 4 kilograms of triacetyl glycerine dilution backs with weight ratio 5%.All the other same normal process.
Embodiment 5
1 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2 grams, damascenone 2 grams, dihydroactinidiolide 3 grams, Megastigmatrienone 3 grams, 2-methyl-pyridine 1 gram, pyridine 2 grams, benzoic acid 3 grams, propionic acid 1 gram, hexadecylic acid 10 grams are added on the dark colour obbbin with the amount of 4 kilograms of ethanol dilution backs with weight ratio 2%.All the other same normal process.
Embodiment 6
Get low-coke tar cigarette blade double centner, with 0.5 kilogram of tobacco extract, 5-methyl-furfural 1 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 2 grams, methyl palmitate 2 grams, eggplant Buddhist nun ketone 2 grams, damascenone 2 grams, Megastigmatrienone 3 grams, 2-methyl-pyridine 1 gram, pyridine 3 grams, benzoic acid 3 grams, propionic acid 10 grams, acetate 10 grams, hexadecylic acid 10 grams, neophytadiene 20 grams, add in reinforced link with 2 kilograms of ethanol dilution backs, other links are with normal cigarette process.
Claims (9)
1. tobacco component additive agent to fragrance compensation for low-coke tar cigarette, it is characterized in that: this additive comprises the raw material of following weight ratio, wherein: tobacco extract 0.1-2 kilogram, furfural 0-10 gram, 5-methyl-furfural 1-5 gram, 3-ethyl-2-hydroxyl-2-cyclopentene-1-ketone 1-10 gram, methyl palmitate 1-10 gram, eggplant Buddhist nun ketone 1-10 gram, dihydroactinidiolide 0-10 gram, damascenone 1-10 gram, Megastigmatrienone 1-20 gram, pyridine 0-10 gram, 2-methyl-pyridine 0-10 gram, acetate 0-100 gram, propionic acid 0-10 gram, benzoic acid 0-10 gram, hexadecylic acid 0-100 gram, and above-mentioned raw materials weight sum 1-4 diluent doubly.
2. the tobacco component additive agent to fragrance compensation for low-coke tar cigarette according to claim 1 is characterized in that: described tobacco extract be in the tobacco leaf from types such as flue-cured tobacco, suncured tabacco, burley tobaccos, Turkish tobaccos any one or two or more tobacco leaf through in extract and obtain.
3. the tobacco component additive agent to fragrance compensation for low-coke tar cigarette according to claim 1 and 2 is characterized in that: described tobacco extract can adopt supercritical fluid CO
2Extracting, also can adopt alcohol extract, can also adopt extracted by ether, also can be two or more extraction that combines of said extracted method.
4. the tobacco component additive agent to fragrance compensation for low-coke tar cigarette according to claim 3 is characterized in that: described tobacco extract is to adopt supercritical fluid CO
2Method is prepared from, and it comprises the steps: that with tobacco leaf be raw material, with supercritical CO
2Fluid is an extractant, extracting pressure 20-30MPa, and extraction temperature 35-50 ℃, entrainer is the 20-30% absolute ethyl alcohol, separating pressure 5-8MPa, separation temperature 55-70 ℃, disengaging time 1-3h, final gained is tobacco extract.
5. the tobacco component additive agent to fragrance compensation for low-coke tar cigarette according to claim 3, it is characterized in that: described tobacco extract is to adopt the alcohol extract method to be prepared from, it comprises the steps: to get tobacco leaf 1000 grams and is raw material, the ethanol 2000-4000mL that adds 90-100%, under 60-80 ℃ of condition, extract 2h, repeat to extract once; Extract concentrates removes ethanol, and final gained is tobacco extract.
6. the tobacco component additive agent to fragrance compensation for low-coke tar cigarette according to claim 3, it is characterized in that: described tobacco extract is to adopt the extracted by ether method to be prepared from, it comprises the steps: to get tobacco leaf 1000 grams and is raw material, add ether 2000-5000mL, refluxing extraction 2h under 40-60 ℃ condition, repeat once, extract is removed ether through concentrating, and final gained is tobacco extract.
7. the tobacco component additive agent to fragrance compensation for low-coke tar cigarette according to claim 3, it is characterized in that: the described tobacco extract of stating is that the extracting method that adopts ethanol and extracted by ether to combine is prepared from, it comprises the steps: to get tobacco leaf 1000 grams and is raw material, the ethanol 2000-4000mL that adds 70-95%, under 60-80 ℃ condition, extract 2h, repeat to extract once; Extract gets CE after concentrating and removing ethanol; Crude extract filters through the ether dissolution of 400-1000mL, and filtrate concentrating removed ether, and final gained is tobacco extract.
8. the tobacco component additive agent to fragrance compensation for low-coke tar cigarette according to claim 1 is characterized in that: the raw material that can also comprise the following weight ratio in the described additive: neophytadiene 10-500 gram.
9. the tobacco component additive agent to fragrance compensation for low-coke tar cigarette according to claim 1 is characterized in that: described diluent is ethanol or triacetyl glycerine.
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| CNB2007101897207A CN100542438C (en) | 2007-09-29 | 2007-09-29 | A kind of tobacco component additive agent to fragrance compensation for low-coke tar cigarette |
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| CNB2007101897207A CN100542438C (en) | 2007-09-29 | 2007-09-29 | A kind of tobacco component additive agent to fragrance compensation for low-coke tar cigarette |
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| CN100542438C CN100542438C (en) | 2009-09-23 |
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Cited By (13)
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| CN101301111B (en) * | 2008-06-30 | 2010-06-02 | 中国烟草总公司郑州烟草研究院 | Additive agent for perfuming tobacco thin sheet |
| CN102174773A (en) * | 2010-12-30 | 2011-09-07 | 任军林 | Spice additive for concealing and improving peculiar smell of deep-color tipping paper |
| CN102199490A (en) * | 2010-03-24 | 2011-09-28 | 郑州轻工业学院 | Method for extracting neutral aroma compositions in tobacco |
| RU2443315C1 (en) * | 2011-01-27 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| CN102413722A (en) * | 2009-04-29 | 2012-04-11 | 英美烟草(投资)有限公司 | Treated tobacco |
| WO2012148996A1 (en) * | 2011-04-27 | 2012-11-01 | R. J. Reynolds Tobacco Company | Tobacco-derived components and materials |
| CN101926506B (en) * | 2009-06-19 | 2012-11-21 | 李文博 | Application of neophytadiene being taken as cigarette additive |
| CN103052328A (en) * | 2010-07-19 | 2013-04-17 | 英美烟草(投资)有限公司 | Cellulosic material such as tobacco comprising one or more smoke diluents |
| CN103387876A (en) * | 2013-08-07 | 2013-11-13 | 湖北中烟工业有限责任公司 | Low-tar cigarette flavoring essence with organic acids |
| CN104031741A (en) * | 2014-06-13 | 2014-09-10 | 广西中烟工业有限责任公司 | Preparation method for maillard reaction production particles of tobacco leaf extract |
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| CN105199850A (en) * | 2015-10-16 | 2015-12-30 | 华宝食用香精香料（上海）有限公司 | Preparation method and application of tobacco flavor |
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- 2007-09-29 CN CNB2007101897207A patent/CN100542438C/en active Active
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| CN101301111B (en) * | 2008-06-30 | 2010-06-02 | 中国烟草总公司郑州烟草研究院 | Additive agent for perfuming tobacco thin sheet |
| CN102413722A (en) * | 2009-04-29 | 2012-04-11 | 英美烟草(投资)有限公司 | Treated tobacco |
| CN101926506B (en) * | 2009-06-19 | 2012-11-21 | 李文博 | Application of neophytadiene being taken as cigarette additive |
| CN102199490A (en) * | 2010-03-24 | 2011-09-28 | 郑州轻工业学院 | Method for extracting neutral aroma compositions in tobacco |
| CN102199490B (en) * | 2010-03-24 | 2012-11-21 | 郑州轻工业学院 | Method for extracting neutral aroma compositions in tobacco |
| US8758561B2 (en) | 2010-07-19 | 2014-06-24 | British American Tobacco (Investments) Limited | Cellulosic material |
| CN103052328A (en) * | 2010-07-19 | 2013-04-17 | 英美烟草(投资)有限公司 | Cellulosic material such as tobacco comprising one or more smoke diluents |
| CN103052328B (en) * | 2010-07-19 | 2015-12-09 | 英美烟草(投资)有限公司 | Comprise the cellulosic material of one or more flue gas dilution agent, as tobacco |
| CN102174773A (en) * | 2010-12-30 | 2011-09-07 | 任军林 | Spice additive for concealing and improving peculiar smell of deep-color tipping paper |
| CN102174773B (en) * | 2010-12-30 | 2014-06-04 | 任军林 | Spice additive for concealing and improving peculiar smell of deep-color tipping paper |
| RU2443315C1 (en) * | 2011-01-27 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| WO2012148996A1 (en) * | 2011-04-27 | 2012-11-01 | R. J. Reynolds Tobacco Company | Tobacco-derived components and materials |
| US9254001B2 (en) | 2011-04-27 | 2016-02-09 | R.J. Reynolds Tobacco Company | Tobacco-derived components and materials |
| EP3545775A1 (en) * | 2011-04-27 | 2019-10-02 | R. J. Reynolds Tobacco Company | Method of extracting and isolating compounds from plants of the nicotiana species useful as flavor material |
| US10595554B2 (en) | 2011-04-27 | 2020-03-24 | R.J. Reynolds Tobacco Company | Tobacco-derived components and materials |
| CN103387876A (en) * | 2013-08-07 | 2013-11-13 | 湖北中烟工业有限责任公司 | Low-tar cigarette flavoring essence with organic acids |
| CN104031741A (en) * | 2014-06-13 | 2014-09-10 | 广西中烟工业有限责任公司 | Preparation method for maillard reaction production particles of tobacco leaf extract |
| CN104031741B (en) * | 2014-06-13 | 2018-03-20 | 广西中烟工业有限责任公司 | A kind of preparation method of the maillard reaction product particle of leaf tobacco extract |
| CN104323419A (en) * | 2014-09-03 | 2015-02-04 | 湖南中烟工业有限责任公司 | Application of pyridine zinc complex in tobacco product |
| CN104323419B (en) * | 2014-09-03 | 2016-07-13 | 湖南中烟工业有限责任公司 | The application in tobacco product of the pyridine Zn complex |
| CN105199850A (en) * | 2015-10-16 | 2015-12-30 | 华宝食用香精香料（上海）有限公司 | Preparation method and application of tobacco flavor |
| CN105199850B (en) * | 2015-10-16 | 2019-07-09 | 华宝香精股份有限公司 | A kind of preparation method and applications of tobacco aromaticss |
| CN108968134A (en) * | 2018-06-08 | 2018-12-11 | 李华 | A kind of composition for substituting conventional cigarette and helping to give up smoking |
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