CN102174773B - Spice additive for concealing and improving peculiar smell of deep-color tipping paper - Google Patents

Spice additive for concealing and improving peculiar smell of deep-color tipping paper Download PDF

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CN102174773B
CN102174773B CN201010613331.4A CN201010613331A CN102174773B CN 102174773 B CN102174773 B CN 102174773B CN 201010613331 A CN201010613331 A CN 201010613331A CN 102174773 B CN102174773 B CN 102174773B
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oil
extracts
volatile
additive
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CN102174773A (en
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任军林
杨卫军
李轩
邓宝安
曹稳
左满兴
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China Tobacco Shaanxi Industrial Co Ltd
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任军林
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Abstract

The invention relates to a spice additive for concealing and improving peculiar smell of deep-color tipping paper. The additive consists of faint scent type tobacco extracts, phenethyl alcohol, Zimbabwe tobacco extracts, rhodinol, tree moss absolute oil, cinnamyl alcohol part supercritical extraction baical skullcap root volatile oil, eugenol, honeysuckle flower volatile oil, decyl alcohol, schizandra volatile components, terpineol, mosla dianthera volatile oil, ethyl pelargonate, geranyl formate parts, undecylenic aldenyde, citronellyl acetate, furfuryl alcohol parts, phenyl acetaldehyde dimethyl acetal, geranium oil, passion flower extracts, 5-methyl furfural, dihydro actinidiolide, phenyl ethyl acetate, carrot extracts and bergamot aldehyde which serve as raw materials. In the additive, the tobacco extracts, tobacco flavor substances and plant extracts are used as main raw materials and are comprehensively compatible with various monomers and plate spices; the peculiar smell of the deep-color tipping paper is obviously concealed and improved; and the additive is well coordinated with cigarettes; the tree moss absolute oil has a cigarette incense coordinating function; and the carrot extracts have the function of improving cigarette incense and concealing ink miscellaneous gas.

Description

A kind of perfume additive of covering the dark tipping paper peculiar smell of improvement
Technical field
The present invention relates to a kind of perfume additive of covering the dark tipping paper peculiar smell of improvement.
Background technology
The single use valerian oil of prior art volatile ingredient, tamarind volatile oil flavor component, means of supercritical extraction root of large-flowered skullcap qin volatile oil, volatile honeysuckle oil, lophatherum gracile volatile oil dihydroactinidiolide, fructus schisandrae volatile ingredient and the former spices of the Mosla dianthera volatility wet goods gas of mixing is covered, although these perfume materials of single use can be covered assorted gas in various degree, but band is served new aesthetic quality's defect again simultaneously, as perfume quantity diminishes, smoke is thin out, and flue gas concentration diminishes etc.
Summary of the invention
In order to overcome the defect of prior art, the object of this invention is to provide extensive, easy to prepare, good with cigarette harmony and the improvement of a kind of raw material sources dark contact paper peculiar smell effective cover the perfume additive of improveing dark tipping paper peculiar smell.
To achieve these goals, the technical solution used in the present invention is:
A kind of perfume additive of covering the dark contact of improvement paper peculiar smell, its special character is: its raw material is by delicate fragrance type tobacco extract, benzyl carbinol, Zimbabwe's tobacco extract, rhodinol, tree moss absolute, cinnamic alcohol, means of supercritical extraction root of large-flowered skullcap volatile oil, eugenol, volatile honeysuckle oil, decyl alcohol, the volatile ingredient of fructus schisandrae, terpinol, Mosla dianthera volatile oil, ethyl pelargonate, geranyl formate part, undecylene aldehyde, citronellyl acetate, furfuryl alcohol, phenylacetaldehyde dimethyl acetal, geranium oil, Passion flower P.E, 5 methyl furfural, dihydroactinidiolide, phenethyl acetate, carrot, bergamot aldehyde composition.
Weight proportion between above-mentioned raw materials is as follows:
Delicate fragrance type tobacco extract 1.0-3.0 part, benzyl carbinol 2.5-5.5 part, Zimbabwe tobacco extract 1.5-2.1 part, rhodinol 0.6-1.0 part, tree moss absolute 0.05-0.1 part cinnamic alcohol 0.7-1.0 part, means of supercritical extraction root of large-flowered skullcap volatile oil 0.05-0.1 part, eugenol 0.8-1.6 part, volatile honeysuckle oil 0.05-0.1 part, decyl alcohol 0.1-0.3 part, volatile ingredient 0.03-0.05 part of fructus schisandrae, terpinol 0.5-1.5 part, Mosla dianthera volatile oil 0.02-0.04 part, ethyl pelargonate 5.0-7.0 part, geranyl formate 0.42-0.62 part, undecylene aldehyde 0.01-0.02 part, citronellyl acetate 3.0-5.0 part, furfuryl alcohol 4.0-7.0 part, phenylacetaldehyde dimethyl acetal 2.0-4.0 part, geranium oil 0.4-0.8 part, Passion flower P.E 3.0-6.0 part, 5 methyl furfural 0.5-1.5 part.
The present invention is take tobacco extract, tobacco flavor matter and plant extracts as main raw material, comprehensive compatibility various of monomer and plate spices, obviously cover the dark tipping paper peculiar smell of improvement, and good with cigarette harmony, wherein " tree moss absolute " has the cigarette of coordination Xiang Gong energy, and carrot extract is improved cigarette perfume and covers the assorted airway dysfunction of ink.
The specific embodiment
Embodiment 1:
Carrot is dried to abrasive dust, add 10 times of benzinums, add extraction heat 2 hours, separate solvent gained extract and be carrot extract, then take after following 26 kinds of raw materials according to following weight ratio, wherein 1.0 parts of delicate fragrance type tobacco extracts, 2.5 parts of benzyl carbinols, 1.5 parts of Zimbabwe's tobacco extracts, 0.6 part of rhodinol, 0.05 part of tree moss absolute, 0.7 part of cinnamic alcohol, 0.05 part of means of supercritical extraction root of large-flowered skullcap volatile oil, 0.8 part of eugenol, 0.05 part of volatile honeysuckle oil, 0.1 part of decyl alcohol, 0.03 part of the volatile ingredient of fructus schisandrae, 0.5 part of terpinol, 0.02 part of Mosla dianthera volatile oil, 5.0 parts of ethyl pelargonates, 0.42 part of geranyl formate, 0.01 part of undecylene aldehyde, 3.0 parts of citronellyl acetates, 4.0 parts of furfuryl alcohols, 2.0 parts of phenylacetaldehyde dimethyl acetals, 0.4 part of geranium oil, 3.0 parts of Passion flower P.Es, 0.5 part of 5 methyl furfural, 0.05 part of dihydroactinidiolide, 0.5 part of phenethyl acetate, 10.0 parts of carrot extracts, 1.0 parts of bergamot aldehydes.
Add the ethanol of 2:1 and mixed with propylene glycol liquid to be supplemented to 100 parts said mixture, obtain liquid perfume additive.
By above-mentioned perfume additive routinely program roll into cigarette, sense organ is inhaled and is commented result to show: obviously improve fragrance matter, do not change the odor type that does not add this perfume additive and make cigarette, and the soft exquisiteness of fragrance, free from extraneous odour, flue gas concentration is high, harmony is good.
Embodiment 2:
Carrot is dried to abrasive dust, add 10 times of benzinums, add extraction heat 2 hours, separate solvent gained extract and be carrot extract, then take after following 26 kinds of raw materials according to following weight ratio, wherein 3.0 parts of delicate fragrance type tobacco extracts, 5.5 parts of benzyl carbinols, 2.1 parts of Zimbabwe's tobacco extracts, 1.0 parts of rhodinols, 0.1 part of tree moss absolute, 1.0 parts of cinnamic alcohols, 0.1 part of means of supercritical extraction root of large-flowered skullcap volatile oil, 1.6 parts of eugenols, 0.1 part of volatile honeysuckle oil, 0.3 part of decyl alcohol, 0.05 part of the volatile ingredient of fructus schisandrae, 1.5 parts of terpinols, 0.04 part of Mosla dianthera volatile oil, 7.0 parts of ethyl pelargonates, 0.62 part of geranyl formate, 0.02 part of undecylene aldehyde, 5.0 parts of citronellyl acetates, 7.0 parts of furfuryl alcohols, 4.0 parts of phenylacetaldehyde dimethyl acetals, 0.8 part of geranium oil, 6.0 parts of Passion flower P.Es, 1.5 parts of 5 methyl furfurals, 0.1 part of dihydroactinidiolide, 1.5 parts of phenethyl acetates, 15.0 parts of carrot extracts, 3.0 parts of bergamot aldehydes.
Add the ethanol of 2:1 and mixed with propylene glycol liquid to be supplemented to 100 parts, the liquid perfume additive obtaining said mixture.
By above-mentioned perfume additive routinely program roll into cigarette, sense organ is inhaled and is commented result to show: obviously improve fragrance matter, do not change the odor type that does not add this perfume additive and make cigarette, and the soft exquisiteness of fragrance, free from extraneous odour, flue gas concentration is high, harmony is good.
Embodiment 3
Carrot is dried to abrasive dust, add 10 times of benzinums, add extraction heat 2 hours, separate solvent gained extract and be carrot extract, then take following 26 kinds of raw materials according to following weight ratio, wherein 2.0 parts of delicate fragrance type tobacco extracts, 3.5 parts of benzyl carbinols, 1.8 parts of Zimbabwe's tobacco extracts, 0.8 part of rhodinol, 0.08 part of tree moss absolute, 0.85 part of cinnamic alcohol, 0.08 part of means of supercritical extraction root of large-flowered skullcap volatile oil, 1.2 parts of eugenols, 0.08 part of volatile honeysuckle oil, 0.2 part of decyl alcohol, 0.04 part of the volatile ingredient of fructus schisandrae, 1.0 parts of terpinols, 0.03 part of Mosla dianthera volatile oil, 6.0 parts of ethyl pelargonates, 0.52 part of geranyl formate, 0.15 part of undecylene aldehyde, 4.0 parts of citronellyl acetates, 5.5 parts of furfuryl alcohols, 3.0 parts of phenylacetaldehyde dimethyl acetals, 0.6 part of geranium oil, 4.5 parts of Passion flower P.Es, 1.0 parts of 5 methyl furfurals, 0.08 part of dihydroactinidiolide, 1.0 parts of phenethyl acetates, 12.0 parts of carrot extracts, 2.0 parts of bergamot aldehydes.
Add the ethanol of 2:1 and mixed with propylene glycol liquid to be supplemented to 100 parts, the liquid perfume additive obtaining said mixture.
By above-mentioned perfume additive routinely program roll into cigarette, sense organ is inhaled and is commented result to show: obviously improve fragrance matter, do not change the odor type that does not add this perfume additive and make cigarette, and the soft exquisiteness of fragrance, free from extraneous odour, flue gas concentration is high, harmony is good.
For the actual effect of check perfume additive application of the present invention, in the situation that outward appearance, raw material are consistent, roll with same ventilation dilution mouth rod containing sample cigarette and the blank sample cigarette of this additive, by 80 parts of survey consumers impression of smokeing panel test, specific as follows:
Table 1 cigarette odor-absorbing investigation summary sheet
Figure 254162DEST_PATH_IMAGE002
Solicit by market suggestion, draw to draw a conclusion:
1, the odor type style of two groups of samples is basically identical.
2, the cigarette sample that adds this kind of spices can embody the fragrance of tobacco itself, and without ink taste, flue gas concentration is moderate, and oral cavity is totally comfortable, and it is better that entirety is inhaled taste.
Detect fume indication and the harmful components of two groups of samples by contrast, two groups of samples have been carried out to flue gas inspection, cigarette smoke index is specific as follows: table 2
Sample Tarry matters in smoke amount Nicotine content in smoke Nitric oxide amount
Containing additive cigarette 11.8mg 1.10 mg 12.5 mg
Blank cigarette 11.6 mg 1.08 mg 12.6 mg
Detect through contrast, the cigarette sample tarry matters in smoke amount, nicotine content in smoke, the CO content that add this kind of spices are more not obvious than changing with control sample, and difference is in 5%.

Claims (2)

1. a perfume additive of covering the dark contact of improvement paper peculiar smell, is characterized in that the weight proportion between described raw material: delicate fragrance type tobacco extract 1.0-3.0 part, benzyl carbinol 2.5-5.5 part, Zimbabwe tobacco extract 1.5-2.1 part, rhodinol 0.6-1.0 part, tree moss absolute 0.05-0.1 part, cinnamic alcohol 0.7-1.0 part, means of supercritical extraction root of large-flowered skullcap volatile oil 0.05-0.1 part, eugenol 0.8-1.6 part, volatile honeysuckle oil 0.05-0.1 part, decyl alcohol 0.1-0.3 part, volatile ingredient 0.03-0.05 part of fructus schisandrae, terpinol 0.5-1.5 part, Mosla dianthera volatile oil 0.02-0.04 part, ethyl pelargonate 5.0-7.0 part, geranyl formate 0.42-0.62 part, undecylene aldehyde 0.01-0.02 part, citronellyl acetate 3.0-5.0 part, furfuryl alcohol 4.0-7.0 part, phenylacetaldehyde dimethyl acetal 2.0-4.0 part, geranium oil 0.4-0.8 part, Passion flower P.E 3.0-6.0 part, 5 methyl furfural 0.5-1.5 part, dihydroactinidiolide 0.05-0.1 part, phenethyl acetate 0.5-1.5 part, carrot extract 10.0-15.0 part, bergamot aldehyde 1.0-3.0 part.
2. the perfume additive of covering the dark contact of improvement paper peculiar smell according to claim 1, it is characterized in that: described raw material weight proportioning is: 2.0 parts of delicate fragrance type tobacco extracts, 3.5 parts of benzyl carbinols, 1.8 parts of Zimbabwe's tobacco extracts, 0.8 part of rhodinol, 0.08 part of tree moss absolute, 0.85 part of cinnamic alcohol, 0.08 part of means of supercritical extraction root of large-flowered skullcap volatile oil, 1.2 parts of eugenols, 0.08 part of volatile honeysuckle oil, 0.2 part of decyl alcohol, 0.04 part of the volatile ingredient of fructus schisandrae, 1.0 parts of terpinols, 0.03 part of Mosla dianthera volatile oil, 6.0 parts of ethyl pelargonates, 0.52 part of geranyl formate, 0.15 part of undecylene aldehyde, 4.0 parts of citronellyl acetates, 5.5 parts of furfuryl alcohols, 3.0 parts of phenylacetaldehyde dimethyl acetals, 0.6 part of geranium oil, 4.5 parts of Passion flower P.Es, 1.0 parts of 5 methyl furfurals, 0.08 part of dihydroactinidiolide, 1.0 parts of phenethyl acetates, 12.0 parts of carrot extracts, 2.0 parts of bergamot aldehydes.
CN201010613331.4A 2010-12-30 2010-12-30 Spice additive for concealing and improving peculiar smell of deep-color tipping paper Active CN102174773B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103468408B (en) * 2013-09-24 2014-10-15 无锡华海香料有限公司 Preparation method of tree moss extract
CN104928975A (en) * 2015-05-28 2015-09-23 安徽顺彤包装材料有限公司 Faint scent type inner lining paper for cigarette

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1994164A (en) * 2006-12-13 2007-07-11 云南瑞升烟草技术(集团)有限公司 Acetate plasticizer for improving smoking property of cigarette and method for preparing same
CN101129220A (en) * 2007-09-29 2008-02-27 中国烟草总公司郑州烟草研究院 Tobacco flavor compensating agent used for low tar filter tip rod and uses thereof
CN101129216A (en) * 2007-09-29 2008-02-27 中国烟草总公司郑州烟草研究院 Tobacco component additive agent for compensating aroma to low tar cigarette

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1994164A (en) * 2006-12-13 2007-07-11 云南瑞升烟草技术(集团)有限公司 Acetate plasticizer for improving smoking property of cigarette and method for preparing same
CN101129220A (en) * 2007-09-29 2008-02-27 中国烟草总公司郑州烟草研究院 Tobacco flavor compensating agent used for low tar filter tip rod and uses thereof
CN101129216A (en) * 2007-09-29 2008-02-27 中国烟草总公司郑州烟草研究院 Tobacco component additive agent for compensating aroma to low tar cigarette

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Effective date of registration: 20160126

Address after: Shaanxi city of Xi'an province high tech Zone Fenghui Road No. 38

Patentee after: China Tobacco Shaanxi Industrial Co.,Ltd.

Address before: 710065 Shaanxi city of Xi'an province Fenghui Road No. 38 Crystal Island

Patentee before: Ren Junlin