CN103421607A - Clustering material preparation with filter stick perfuming function - Google Patents
Clustering material preparation with filter stick perfuming function Download PDFInfo
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- CN103421607A CN103421607A CN2013103186050A CN201310318605A CN103421607A CN 103421607 A CN103421607 A CN 103421607A CN 2013103186050 A CN2013103186050 A CN 2013103186050A CN 201310318605 A CN201310318605 A CN 201310318605A CN 103421607 A CN103421607 A CN 103421607A
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Abstract
The invention discloses a clustering material preparation with the filter stick perfuming function, relates to an additive for tobaccos, and aims to provide the clustering material preparation which can improve the richness, fullness and expressive force of tobacco aroma, improves wetness of cigarette smoke, enables smoke to be delicate and soft, reduces the stimulus of cigarettes, increases partial sweetness, and improves the sucking durability of cigarettes. The clustering material preparation is characterized by mainly comprising the following raw material compositions: 2, 5-dimethyl pyrazine, sage clary oil, phenethyl alcohol, leaf alcohol, caproic acid, geranyl acetone, isophorone oxide, benzyl acetate, ethyl valerate, ethyl cinnamate, 2-acetyl pyrrole, and glycerol triacetate. The clustering material preparation provided by the invention can be popularized and applied in all the cigarette factories in China.
Description
Technical field
The present invention relates to the tobacco additive, particularly relate to a kind of cluster thing preparation with filter stick perfuming function.
Background technology
Along with the day by day enhancing of human consumer to smoking and health concerns, national governments are more and more stricter to the restriction of cigarette, only with a kind of unifunctional common filter stick, be difficult to meet the growth requirement of cigarette market, this just impels filter stick now to plant the future development of function to compound multiple perfuming module by list.Requirement according to market and Cigarette design, there is purpose selectively various technology organically to be combined, develop the multi-functional special filter stick with desirable lowering harm and decreasing coking or flavouring humectation effect, especially both there is the perfuming effect, there is again the sweet mellow sense of the cigarette smoke of increasing, can reduce the special filter stick of multiple harmful smoke composition, will there is fairly obvious economic benefit and important social effect simultaneously.
Summary of the invention
The purpose of this invention is to provide a kind of cluster thing preparation with filter stick perfuming function, said preparation can obviously promote rich, fullness ratio and the expressive force of cigarette cigarette perfume (or spice), increase the moist feeling of cigarette smoke, make the mellow exquisiteness of flue gas, reduce the pungency of cigarette, increase the part sugariness, improve the anti-suction of cigarette, more obvious to the low-coke tar cigarette effect.
For achieving the above object, the invention provides a kind of like this cluster thing preparation with filter stick perfuming function, it is characterized in that, the raw material of making described preparation comprises the basic raw material that the component by following weight percent forms:
(1) 2,5-dimethylpyrazine 0.04-0.14
(2) Salvia Sclare L.oil 0.007-0.012
(3) phenylethyl alcohol 0.04-0.14
(4) leaf-alcohol 0.02-0.07
(5) sour 0.04-0.14
(6) geranyl acetone 0.016-0.022
(7) oxidation isophorone 0.03-0.08
(8) jasmal 0.015-0.04
(9) Valeric acid ethylester 0.02-0.07
(10) ethyl cinnamate 0.02-0.07
(11) 2-acetyl pyrrole 0.04-0.14
(12) surplus is glycerine triacetate.
Further, the raw material of making described preparation also comprises and accounts for the vanillin food grade,1000.000000ine mesh that described basic raw material weight percent is 0.09-0.19.
Further, the raw material of making described preparation also comprises and accounts for the mentha camphor that described basic raw material weight percent is 0.09-0.19.
Further, the raw material of making described preparation also comprises and accounts for the Glacial acetic acid that described basic raw material weight percent is 0.14-0.24.
Further, the raw material of making described preparation also comprises and accounts for the dimethyl tobacco leaf ketone that described basic raw material weight percent is 0.24-0.34.
Further, the raw material of making described preparation also comprises and accounts for the ethyl acetate that described basic raw material weight percent is 0.2-0.7.
Further, the raw material of making described preparation also comprises and accounts for the acetic ester that described basic raw material weight percent is 0.2-1.2.
Further, the raw material of making described preparation also comprises and accounts for the gamma decalactone that described basic raw material weight percent is 0.09-0.19.
Further, the raw material of making described preparation also comprises and accounts for the ethyl butyrate that described basic raw material weight percent is 0.2-0.7.
The using method of the above-mentioned cluster thing preparation with filter stick perfuming function is as follows:
Formula combination by above-mentioned cluster thing preparation is prepared, and various components are added in respectively in container, stirs evenly, and, after allowing all compositions dissolve, can use.In the filter stick production process, with 0.04%(, take the glycerine triacetate amount as benchmark) addition be sprayed directly on acetate silk and get final product.
Beneficial effect:
Compared with prior art, the present invention has the following advantages:
1, the successful development of preparation of the present invention has responded State Bureau about carrying forward vigorously the call of scientific-technical progress and innovation, has complied with the researchdevelopment direction of tobacco industry lowering harm and decreasing coking, flavouring humectation technology; The present invention is keeping and is developing on the basis of intrinsic style and features and carry out the research of filter stick perfuming module, the flavouring that utilizes " cold-patch " and " the outer benefit " to combine is mended the technology such as perfume (or spice) and slowly-releasing flavouring, develops a kind of novel cluster thing preparation with filter stick perfuming functions of modules;
2, the qualification result of smokeing panel test: according to the regulation in GB5606.4-2005, the resulting preparation of embodiment 1-54 in embodiment is added in the filter stick of double happiness auspicious day (soft beautiful) cigarette group of Shenzhen Tobacco Industry Co., Ltd., contrast and smoke panel test with the double happiness auspicious day do not added (soft beautiful) cigarette group, the evaluation work of smokeing panel test is presided over by the council of smokeing panel test of Shenzhen Tobacco Industry Co., Ltd. and Shantou gold leaf reconstituted tobacco company, and smoking result is in Table 1; Through smokeing panel test, seven committee members that smoke panel test unanimously think: the adding of preparation of the present invention, can obviously promote rich, fullness ratio and the expressive force of cigarette cigarette perfume (or spice), increase the sweet mellow sense of cigarette smoke, the oral cavity aftertaste is promoted the production of body fluid, reduce the pungency of cigarette, increase the part sugariness, improve the anti-suction of cigarette, more obvious to the effect of low-coke tar cigarette;
Table 1 cigarette inner quality sensory evaluating smoking result
| Comparative run | Gloss | Fragrance | Harmony | Assorted gas | Stimulate | Pleasant impression | Add up to |
| The cigarette of perfuming preparation not | 4.0 | 26.0 | 4.5 | 9.0 | 17.0 | 20.5 | 81.0 |
| The cigarette of perfuming preparation | 4.0 | 27.0 | 4.9 | 9.5 | 17.4 | 21.5 | 84.3 |
3, success commercially: at present, preparation of the present invention is promoted the use of in Shenzhen Tobacco Industry Co., Ltd., adds double happiness auspicious day (soft beautiful) the cigarette constant product quality of said preparation, and sales volume is steadily increasing, the human consumer is well received, has obtained good economic benefit.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail, and following examples are explanation of the invention, and the present invention is not limited to following examples.
Following each embodiment all be take total amount as 100 grams, and as the basis of test, all raw materials of using in embodiment are all bought from market.
Embodiment 1
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
(1) 2,5-dimethylpyrazine, 0.04 gram
(2) Salvia Sclare L.oil 0.007 gram
(3) phenylethyl alcohol 0.04 gram
(4) leaf-alcohol 0.02 gram
(5) sour 0.04 gram
(6) geranyl acetone 0.016 gram
(7) oxidation isophorone 0.03 gram
(8) jasmal 0.015 gram
(9) Valeric acid ethylester 0.02 gram
(10) ethyl cinnamate 0.02 gram
(11) 2-acetyl pyrrole 0.04 gram
(12) surplus is glycerine triacetate.
Embodiment 2
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
(1) 2,5-dimethylpyrazine, 0.06 gram
(2) Salvia Sclare L.oil 0.008 gram
(3) phenylethyl alcohol 0.06 gram
(4) leaf-alcohol 0.03 gram
(5) sour 0.06 gram
(6) geranyl acetone 0.018 gram
(7) oxidation isophorone 0.04 gram
(8) jasmal 0.02 gram
(9) Valeric acid ethylester 0.03 gram
(10) ethyl cinnamate 0.03 gram
(11) 2-acetyl pyrrole 0.06 gram
(12) surplus is glycerine triacetate.
Embodiment 3
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
(1) 2,5-dimethylpyrazine, 0.08 gram
(2) Salvia Sclare L.oil 0.009 gram
(3) phenylethyl alcohol 0.08 gram
(4) leaf-alcohol 0.04 gram
(5) sour 0.08 gram
(6) geranyl acetone 0.019 gram
(7) oxidation isophorone 0.05 gram
(8) jasmal 0.025 gram
(9) Valeric acid ethylester 0.04 gram
(10) ethyl cinnamate 0.04 gram
(11) 2-acetyl pyrrole 0.08 gram
(12) surplus is glycerine triacetate.
Embodiment 4
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
(1) 2,5-dimethylpyrazine, 0.1 gram
(2) Salvia Sclare L.oil 0.01 gram
(3) phenylethyl alcohol 0.1 gram
(4) leaf-alcohol 0.05 gram
(5) sour 0.1 gram
(6) geranyl acetone 0.02 gram
(7) oxidation isophorone 0.06 gram
(8) jasmal 0.03 gram
(9) Valeric acid ethylester 0.05 gram
(10) ethyl cinnamate 0.05 gram
(11) 2-acetyl pyrrole 0.1 gram
(12) surplus is glycerine triacetate.
Embodiment 5
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
(1) 2,5-dimethylpyrazine, 0.12 gram
(2) Salvia Sclare L.oil 0.011 gram
(3) phenylethyl alcohol 0.12 gram
(4) leaf-alcohol 0.06 gram
(5) sour 0.12 gram
(6) geranyl acetone 0.021 gram
(7) oxidation isophorone 0.07 gram
(8) jasmal 0.035 gram
(9) Valeric acid ethylester 0.06 gram
(10) ethyl cinnamate 0.06 gram
(11) 2-acetyl pyrrole 0.12 gram
(12) surplus is glycerine triacetate.
Embodiment 6
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
(1) 2,5-dimethylpyrazine, 0.14 gram
(2) Salvia Sclare L.oil 0.012 gram
(3) phenylethyl alcohol 0.14 gram
(4) leaf-alcohol 0.07 gram
(5) sour 0.14 gram
(6) geranyl acetone 0.022 gram
(7) oxidation isophorone 0.08 gram
(8) jasmal 0.04 gram
(9) Valeric acid ethylester 0.07 gram
(10) ethyl cinnamate 0.07 gram
(11) 2-acetyl pyrrole 0.14 gram
(12) surplus is glycerine triacetate.
Embodiment 7-12
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
Add vanillin food grade,1000.000000ine mesh 0.09 gram in above-described embodiment 1, add vanillin food grade,1000.000000ine mesh 0.11 gram in above-described embodiment 2, add vanillin food grade,1000.000000ine mesh 0.13 gram in above-described embodiment 3, add vanillin food grade,1000.000000ine mesh 0.15 gram in above-described embodiment 4, add vanillin food grade,1000.000000ine mesh 0.17 gram in above-described embodiment 5, add vanillin food grade,1000.000000ine mesh 0.19 gram in above-described embodiment 6, obtain respectively embodiment 7-12.
Embodiment 13-18
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
Add mentha camphor 0.09 gram in above-described embodiment 7, add mentha camphor 0.11 gram in above-described embodiment 8, add mentha camphor 0.13 gram in above-described embodiment 9, add mentha camphor 0.15 gram in above-described embodiment 10, add mentha camphor 0.17 gram in above-described embodiment 11, add mentha camphor 0.19 gram in above-described embodiment 12, obtain respectively embodiment 13-18.
Embodiment 19-24
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
Add Glacial acetic acid 0.14 gram in above-described embodiment 13, add Glacial acetic acid 0.16 gram in above-described embodiment 14, add Glacial acetic acid 0.18 gram in above-described embodiment 15, add Glacial acetic acid 0.2 gram in above-described embodiment 16, add Glacial acetic acid 0.22 gram in above-described embodiment 17, add Glacial acetic acid 0.24 gram in above-described embodiment 18, obtain respectively embodiment 19-24.
Embodiment 25-30
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
Add dimethyl tobacco leaf ketone 0.24 gram in above-described embodiment 19, add dimethyl tobacco leaf ketone 0.26 gram in above-described embodiment 20, add dimethyl tobacco leaf ketone 0.28 gram in above-described embodiment 21, add dimethyl tobacco leaf ketone 0.3 gram in above-described embodiment 22, add dimethyl tobacco leaf ketone 0.32 gram in above-described embodiment 23, add dimethyl tobacco leaf ketone 0.34 gram in above-described embodiment 24, obtain respectively embodiment 25-30.
Embodiment 31-36
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
Add ethyl acetate 0.2 gram in above-described embodiment 25, add ethyl acetate 0.3 gram in above-described embodiment 26, add ethyl acetate 0.4 gram in above-described embodiment 27, add ethyl acetate 0.5 gram in above-described embodiment 28, add ethyl acetate 0.6 gram in above-described embodiment 29, add ethyl acetate 0.7 gram in above-described embodiment 30, obtain respectively embodiment 31-36.
Embodiment 37-42
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
Add acetic ester 0.2 gram in above-described embodiment 31, add acetic ester 0.4 gram in above-described embodiment 32, add acetic ester 0.6 gram in above-described embodiment 33, add acetic ester 0.8 gram in above-described embodiment 34, add acetic ester 1.0 grams in above-described embodiment 35, add acetic ester 1.2 grams in above-described embodiment 36, obtain respectively embodiment 37-42.
Embodiment 43-48
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
Add gamma decalactone 0.09 gram in above-described embodiment 37, add gamma decalactone 0.11 gram in above-described embodiment 38, add gamma decalactone 0.13 gram in above-described embodiment 39, add gamma decalactone 0.15 gram in above-described embodiment 40, add gamma decalactone 0.17 gram in above-described embodiment 41, add gamma decalactone 0.19 gram in above-described embodiment 42, obtain respectively embodiment 43-48.
Embodiment 49-54
A kind of cluster thing preparation with filter stick perfuming function, by following raw material, made:
Add ethyl butyrate 0.2 gram in above-described embodiment 49, add ethyl butyrate 0.3 gram in above-described embodiment 50, add ethyl butyrate 0.4 gram in above-described embodiment 51, add ethyl butyrate 0.5 gram in above-described embodiment 52, add ethyl butyrate 0.6 gram in above-described embodiment 53, add ethyl butyrate 0.7 gram in above-described embodiment 54, obtain respectively embodiment 49-54.
Claims (9)
1. the cluster thing preparation with filter stick perfuming function, is characterized in that, the raw material of making described preparation comprises the basic raw material that the component by following weight percent forms:
(1) 2,5-dimethylpyrazine 0.04-0.14
(2) Salvia Sclare L.oil 0.007-0.012
(3) phenylethyl alcohol 0.04-0.14
(4) leaf-alcohol 0.02-0.07
(5) sour 0.04-0.14
(6) geranyl acetone 0.016-0.022
(7) oxidation isophorone 0.03-0.08
(8) jasmal 0.015-0.04
(9) Valeric acid ethylester 0.02-0.07
(10) ethyl cinnamate 0.02-0.07
(11) 2-acetyl pyrrole 0.04-0.14
(12) surplus is glycerine triacetate.
2. the cluster thing preparation with filter stick perfuming function according to claim 1 is characterized in that: the raw material of making described preparation also comprises and accounts for the vanillin food grade,1000.000000ine mesh that described basic raw material weight percent is 0.09-0.19.
3. the cluster thing preparation with filter stick perfuming function according to claim 1 is characterized in that: the raw material of making described preparation also comprises and accounts for the mentha camphor that described basic raw material weight percent is 0.09-0.19.
4. the cluster thing preparation with filter stick perfuming function according to claim 1 is characterized in that: the raw material of making described preparation also comprises and accounts for the Glacial acetic acid that described basic raw material weight percent is 0.14-0.24.
5. the cluster thing preparation with filter stick perfuming function according to claim 1 is characterized in that: the raw material of making described preparation also comprises and accounts for the dimethyl tobacco leaf ketone that described basic raw material weight percent is 0.24-0.34.
6. the cluster thing preparation with filter stick perfuming function according to claim 1 is characterized in that: the raw material of making described preparation also comprises and accounts for the ethyl acetate that described basic raw material weight percent is 0.2-0.7.
7. the cluster thing preparation with filter stick perfuming function according to claim 1 is characterized in that: the raw material of making described preparation also comprises and accounts for the acetic ester that described basic raw material weight percent is 0.2-1.2.
8. the cluster thing preparation with filter stick perfuming function according to claim 1 is characterized in that: the raw material of making described preparation also comprises and accounts for the gamma decalactone that described basic raw material weight percent is 0.09-0.19.
9. the cluster thing preparation with filter stick perfuming function according to claim 1 is characterized in that: the raw material of making described preparation also comprises and accounts for the ethyl butyrate that described basic raw material weight percent is 0.2-0.7.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104498192A (en) * | 2014-12-15 | 2015-04-08 | 云南中烟工业有限责任公司 | Preparation method and application of florists chrysanthemum extract |
| WO2021046921A1 (en) * | 2019-09-12 | 2021-03-18 | 深圳雾芯科技有限公司 | Flavor composition and e-liquid containing flavor composition |
| CN113355159A (en) * | 2021-04-30 | 2021-09-07 | 深圳烟草工业有限责任公司 | Tobacco essence for increasing fresh and sweet aroma of cigarettes |
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| CN1356071A (en) * | 2000-12-04 | 2002-07-03 | 武汉卷烟厂 | Amendment with different tastes and styles for tip filter of cigarette and its preparing process |
| CN101215805A (en) * | 2008-01-07 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Cigarette perfuming agent and its preparation method and application |
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- 2013-07-26 CN CN2013103186050A patent/CN103421607A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1356071A (en) * | 2000-12-04 | 2002-07-03 | 武汉卷烟厂 | Amendment with different tastes and styles for tip filter of cigarette and its preparing process |
| CN101215805A (en) * | 2008-01-07 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Cigarette perfuming agent and its preparation method and application |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104498192A (en) * | 2014-12-15 | 2015-04-08 | 云南中烟工业有限责任公司 | Preparation method and application of florists chrysanthemum extract |
| WO2021046921A1 (en) * | 2019-09-12 | 2021-03-18 | 深圳雾芯科技有限公司 | Flavor composition and e-liquid containing flavor composition |
| CN113355159A (en) * | 2021-04-30 | 2021-09-07 | 深圳烟草工业有限责任公司 | Tobacco essence for increasing fresh and sweet aroma of cigarettes |
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Application publication date: 20131204 |