CN113355159A - Tobacco essence for increasing fresh and sweet aroma of cigarettes - Google Patents

Tobacco essence for increasing fresh and sweet aroma of cigarettes Download PDF

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Publication number
CN113355159A
CN113355159A CN202110487494.0A CN202110487494A CN113355159A CN 113355159 A CN113355159 A CN 113355159A CN 202110487494 A CN202110487494 A CN 202110487494A CN 113355159 A CN113355159 A CN 113355159A
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China
Prior art keywords
cigarettes
tobacco
fresh
percent
sweet
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CN202110487494.0A
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Chinese (zh)
Inventor
陈武林
刘晓晖
吕乔
孙海峰
畅晓渊
王奕
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Shenzhen Tobacco Industry Co Ltd
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Shenzhen Tobacco Industry Co Ltd
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Priority to CN202110487494.0A priority Critical patent/CN113355159A/en
Publication of CN113355159A publication Critical patent/CN113355159A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • C11B9/0015Aliphatic compounds containing oxygen as the only heteroatom
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

A tobacco essence for increasing the sweet fragrance of cigarette. The tobacco essence comprises the following components in percentage by mass: vanillin 0.03-0.08%; 0.006-0.016% of 2, 5-dimethyl pyrazine; 0.1-0.35% of methyl laurate; 0.01 to 0.06 percent of clary sage oil; 0.04-0.14% of phenethyl alcohol; 0.06-0.16% of dimethyl tobacco ketone; 0.06-0.16% of B-damascone; 0.015-0.04% of furanone; geranylacetone 0.006-0.016%; linalool 0.05-0.1%; 0.01 to 0.06 percent of benzyl acetate; 0.3 to 0.8 percent of ethyl acetate; 0.1 to 0.35 percent of ethyl caproate; the balance being propylene glycol. The tobacco essence is added into the cigarettes, so that the richness, fullness and expressive force of the cigarette fragrance of the cigarettes can be obviously improved, the fresh and sweet aroma of the cigarette smoke can be obviously increased, the smoke is soft, smooth and fine, the irritation of the cigarettes is reduced, the smoking resistance of the cigarettes is improved, and the effect on low-tar cigarettes is more obvious.

Description

Tobacco essence for increasing fresh and sweet aroma of cigarettes
Technical Field
The invention relates to the technical field of tobacco, in particular to tobacco essence for increasing the fresh and sweet aroma of cigarettes.
Background
The cigarette is a special commodity, the main purpose of smoking the cigarette by consumers is to feel the aroma and strength of smoke, and the aroma style and smoking taste of the smoke are important product attributes of the cigarette and are also important concerns that smokers are faithful to cigarette brands. When the cigarette is smoked, the sweet fragrance can bring comfort and pleasure to consumers. The tobacco has sweet taste when burning, and the sweet taste is divided into fresh sweet taste, normal sweet taste and burnt sweet taste, but the sweet taste of the smoke is weaker. In order to highlight the cigarette flavor style characteristics and eliminate the unpleasant tastes such as bitterness, dryness, astringency and the like caused by the reasons of tobacco leaves, cigarette product developers often add some essence with fresh and sweet fragrance when blending the fragrance of cigarettes, so as to increase the sweet feeling of the cigarettes, reduce the stimulation and make the aftertaste comfortable. The tobacco flavor is an indispensable additive component in the production process of tobacco products, has the advantages of perfecting the aroma style characteristics of the products and covering bad smell, and is regarded as one of key core technologies influencing the sensory quality of the cigarette products.
Under a new trend, Shenzhen tobacco industry Limited liability company constantly focuses on the research and development direction of Chinese style cigarette products and technologies in the national tobacco industry, responds to the call of the State office, vigorously advances technological progress and innovation, develops the research on fresh and sweet aroma on the basis of maintaining and developing the inherent style characteristics around the style of the 'elegant natural aroma' characteristic product, and develops the essence capable of obviously increasing the fresh and sweet aroma of the cigarette. After the essence is added into cigarette products, the richness, fullness and expressive force of cigarette fragrance can be obviously improved, the sweet feeling of cigarette smoke is increased, the smoke is soft, soft and fine, the irritation of the cigarette is reduced, the fresh and sweet taste of the smoke is increased, the smoking resistance of the cigarette is improved, the effect on low-tar cigarettes is more obvious, the product quality is stable, and good economic benefits are obtained.
Disclosure of Invention
The invention aims to solve the technical problem of providing the tobacco essence for increasing the fresh and sweet aroma of cigarettes.
In order to solve the technical problems, the invention adopts the following technical scheme: the tobacco essence for increasing the fresh and sweet aroma of the cigarettes is characterized by comprising the following components in percentage by mass:
vanillin 0.03-0.08%;
0.006-0.016% of 2, 5-dimethyl pyrazine;
0.1-0.35% of methyl laurate;
0.01 to 0.06 percent of clary sage oil;
0.04-0.14% of phenethyl alcohol;
0.06-0.16% of dimethyl tobacco ketone;
0.06-0.16% of B-damascone;
0.015-0.04% of furanone;
geranylacetone 0.006-0.016%;
linalool 0.05-0.1%;
0.01 to 0.06 percent of benzyl acetate;
0.3 to 0.8 percent of ethyl acetate;
0.1 to 0.35 percent of ethyl caproate;
the balance being propylene glycol.
In some embodiments, the essence for tobacco further comprises the following components in percentage by mass: 0.06-0.16 of tea spirane.
In some embodiments, the essence for tobacco further comprises the following components in percentage by mass: 0.005-0.1 of gamma decalactone.
In some embodiments, the essence for tobacco further comprises the following components in percentage by mass: 0.1-0.35 of ethyl butyrate.
In some embodiments, the essence for tobacco further comprises the following components in percentage by mass: 0.004-0.014 of Lieberdang extract.
In some embodiments, the essence for tobacco further comprises the following components in percentage by mass: 0.04-0.14 of ethyl phenylacetate.
The essence for tobacco can at least achieve the following beneficial effects: the essence for the cigarettes comprises the following components in percentage by mass: vanillin 0.03-0.08%; 0.006-0.016% of 2, 5-dimethyl pyrazine; 0.1-0.35% of methyl laurate; 0.01 to 0.06 percent of clary sage oil; 0.04-0.14% of phenethyl alcohol; 0.06-0.16% of dimethyl tobacco ketone; 0.06-0.16% of B-damascone; 0.015-0.04% of furanone; geranylacetone 0.006-0.016%; linalool 0.05-0.1%; 0.01 to 0.06 percent of benzyl acetate; 0.3 to 0.8 percent of ethyl acetate; 0.1 to 0.35 percent of ethyl caproate; the balance being propylene glycol. The essence for cigarettes is added into cigarettes, so that the richness, fullness and expressive force of cigarette fragrance of the cigarettes can be obviously improved, the fresh and sweet aroma of cigarette smoke can be obviously increased, the smoke is soft and fine, the irritation of the cigarettes is reduced, the smoking resistance of the cigarettes is improved, and the effect of low-tar cigarettes is more obvious.
Detailed Description
In order to facilitate an understanding of the invention, a more complete description of the invention is provided below. The following are typical examples of the invention. The invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention.
Each of the following examples 1-36 was based on a total of 100 grams. The components of the embodiments 1 to 36 are respectively added into a container, stirred evenly and dissolved to obtain the corresponding essence for tobacco.
Example 1
The tobacco essence for increasing the fresh and sweet aroma of the cigarettes comprises the following components:
0.03 g of vanillin;
0.006 g of 2, 5-dimethyl pyrazine;
0.1 g of methyl laurate;
0.01 g of clary sage oil;
0.04 g of phenethyl alcohol;
0.06 g of dimethyl tobacco ketone;
0.06 g of B-damascone;
0.015 g of furanone;
geranylacetone 0.006 g;
linalool 0.05 g;
benzyl acetate 0.01 g;
ethyl acetate 0.3 g;
0.1 g of ethyl caproate;
the balance being propylene glycol.
Example 2
The tobacco essence for increasing the fresh and sweet aroma of the cigarettes comprises the following components:
vanillin 0.04 g;
0.008 g of 2, 5-dimethyl pyrazine;
0.15 g of methyl laurate;
0.02 g of clary sage oil;
0.06 g of phenethyl alcohol;
0.08 g of dimethyl tobacco ketone;
0.08 g of beta-damascone;
0.02 g of furanone;
geranylacetone 0.008 g;
linalool 0.06 g;
benzyl acetate 0.02 g;
ethyl acetate 0.4 g;
0.15 g of ethyl caproate;
the balance being propylene glycol.
Example 3
The tobacco essence for increasing the fresh and sweet aroma of the cigarettes comprises the following components:
0.05 g of vanillin;
0.01 g of 2, 5-dimethyl pyrazine;
0.2 g of methyl laurate;
0.03 g of clary sage oil;
0.08 g of phenethyl alcohol;
0.1 g of dimethyl tobacco ketone;
0.1 g of B-damascone;
0.025 g of furanone;
geranylacetone 0.01 g;
linalool 0.07 g;
benzyl acetate 0.03 g;
ethyl acetate 0.5 g;
0.2 g of ethyl caproate;
the balance being propylene glycol.
Example 4
The tobacco essence for increasing the fresh and sweet aroma of the cigarettes comprises the following components:
0.06 g of vanillin;
0.012 g of 2, 5-dimethyl pyrazine;
0.25 g of methyl laurate;
0.04 g of clary sage oil;
0.1 g of phenethyl alcohol;
0.12 g of dimethyl tobacco ketone;
0.12 g of B-damascone;
0.03 g of furanone;
geranylacetone 0.012 g;
linalool 0.08 g;
benzyl acetate 0.04 g;
ethyl acetate 0.6 g;
0.25 g of ethyl caproate;
the balance being propylene glycol.
Example 5
The tobacco essence for increasing the fresh and sweet aroma of the cigarettes comprises the following components:
0.07 g of vanillin;
0.014 g of 2, 5-dimethyl pyrazine;
0.3 g of methyl laurate;
0.05 g of clary sage oil;
0.12 g of phenethyl alcohol;
0.14 g of dimethyl tobacco ketone;
0.14 g of B-damascone;
0.035 g of furanone;
geranylacetone 0.014 g;
linalool 0.09 g;
benzyl acetate 0.05 g;
ethyl acetate 0.7 g;
0.3 g of ethyl caproate;
the balance being propylene glycol.
Example 6
The tobacco essence for increasing the fresh and sweet aroma of the cigarettes comprises the following components:
0.08 g of vanillin;
0.016 g of 2, 5-dimethyl pyrazine;
0.35 g of methyl laurate;
0.06 g of clary sage oil;
0.14 g of phenethyl alcohol;
0.16 g of dimethyl tobacco ketone;
0.16 g of B-damascone;
0.04 g of furanone;
geranylacetone 0.016 g;
linalool 0.1 g;
benzyl acetate 0.06 g;
ethyl acetate 0.8 g;
0.35 g of ethyl caproate;
the balance being propylene glycol.
Examples 7 to 12
Examples 7 to 12 were each constructed by adding 0.06 g of theaxiangspirane to example 1, 0.08 g of theaxiangspirane to example 2, 0.1 g of theaxiangspirane to example 3, 0.12 g of theaxiangspirane to example 4, 0.14 g of theaxiangspirane to example 5, and 0.16 g of theaxiangspirane to example 6. Taking example 7 as an example, adding 0.06 g of theaxiangspirane to example 1 means that 0.06 g of theaxiangspirane is added to example 1, and simultaneously, 0.06 g of propylene glycol is correspondingly reduced, so that the total mass is maintained at 100 g.
Examples 13 to 18
Examples 13 to 18 were each constructed by adding 0.005 g of propiolactone to example 7, 0.006 g of propiolactone to example 8, 0.007 g of propiolactone to example 9, 0.008 g of propiolactone to example 10, 0.009 g of propiolactone to example 11, and 0.010 g of propiolactone to example 12. It should be noted that, taking example 13 as an example, adding 0.005 g of propane-decalactone in the above example 7 means that 0.005 g of propane-decalactone is added on the basis of example 7, and simultaneously, 0.005 g of propylene glycol is correspondingly reduced, so as to maintain the total mass at 100 g.
Examples 19 to 24
Examples 19 to 24 were each constructed by adding 0.1 g of ethyl butyrate to the above example 13, 0.15 g of ethyl butyrate to the above example 14, 0.20 g of ethyl butyrate to the above example 15, 0.25 g of ethyl butyrate to the above example 16, 0.30 g of ethyl butyrate to the above example 17, and 0.35 g of ethyl butyrate to the above example 18. In example 19, 0.1 g of ethyl butyrate was added in example 13, which means that 0.1 g of propane-decalactone was added in addition to example 13, and simultaneously, 0.1 g of propylene glycol was correspondingly reduced, so that the total mass was maintained at 100 g.
Examples 25 to 30
Examples 25 to 30 were prepared by adding 0.004 g of hebeth extract in example 19, 0.006 g of hebeth extract in example 20, 0.008 g of hebeth extract in example 21, 0.010 g of hebeth extract in example 22, 0.012 g of hebeth extract in example 23, and 0.014 g of hebeth extract in example 24, respectively. It should be noted that, taking example 25 as an example, adding 0.004 g of leber extract in the above example 19 means that 0.004 g of leber extract is added on the basis of example 19, and simultaneously, 0.004 g of propylene glycol is correspondingly reduced, so that the total mass is maintained at 100 g.
Examples 31 to 36
Examples 31 to 36 were each constructed by adding 0.04 g of ethyl phenylacetate to example 25, 0.06 g of ethyl phenylacetate to example 26, 0.08 g of ethyl phenylacetate to example 27, 0.10 g of ethyl phenylacetate to example 28, 0.12 g of ethyl phenylacetate to example 29, and 0.14 g of ethyl phenylacetate to example 30. It should be noted that, taking example 31 as an example, adding 0.04 g of ethyl phenylacetate in the above example 25 means that 0.04 g of ethyl phenylacetate is added on the basis of example 25, and simultaneously, 0.04 g of propylene glycol is correspondingly reduced, so that the total mass is maintained at 100 g.
Verification test
In the process of cigarette flavoring production, the tobacco essences provided in the above examples 1 to 36 were respectively directly sprayed on the tobacco shreds of the double happiness day brand at an addition amount of 0.8% to obtain 36 different types of fresh and sweet tobacco shreds, and then the 36 different types of fresh and sweet tobacco shreds were respectively made into 36 different types of fresh and sweet cigarettes for evaluation and identification. Through the evaluation and identification of Shenzhen tobacco industry Limited liability company smoking committee according to GB5606.4-2005 national standard, it is agreed that the fresh and sweet cigarette obviously improves the richness, fullness and expressive force of cigarette fragrance, increases the sweet and soft feeling of cigarette smoke, promotes the secretion of saliva or body fluid in oral cavity, reduces the irritation of cigarette, increases the fresh and sweet note and improves the smoking resistance of cigarette.
Taking the tobacco essence provided in example 33 as an example, the tobacco essence provided in example 33 is directly sprayed on the tobacco shreds of the double happiness and happiness day brand in an adding amount of 0.8% to obtain corresponding fresh and sweet tobacco shreds, and the fresh and sweet tobacco shreds are made into corresponding fresh and sweet cigarettes for evaluation and identification, and the results are shown in table 1 below.
TABLE 1 cigarette intrinsic quality evaluation results
Contrast item Gloss of Fragrance Tuning by hand Miscellaneous qi Stimulation of Aftertaste Total up to
Cigarette without essence for cigarette 5.0 27.0 4.5 11.0 17.0 21.0 85.5
Cigarette with tobacco essence 5.0 28.0 5.0 11.0 17.5 22.0 88.5
Remarking: the evaluation is carried out according to GB5606.4-2005 national standard, and the evaluation result is the average value of scores of 7 judges
While the embodiments of the present invention have been described, the present invention is not limited to the above embodiments, which are only illustrative and not restrictive, and those skilled in the art can make various modifications without departing from the spirit and scope of the invention as defined in the appended claims.

Claims (6)

1. The tobacco essence for increasing the fresh and sweet aroma of cigarettes is characterized by comprising the following components in percentage by mass:
vanillin 0.03-0.08%;
0.006-0.016% of 2, 5-dimethyl pyrazine;
0.1-0.35% of methyl laurate;
0.01 to 0.06 percent of clary sage oil;
0.04-0.14% of phenethyl alcohol;
0.06-0.16% of dimethyl tobacco ketone;
0.06-0.16% of B-damascone;
0.015-0.04% of furanone;
geranylacetone 0.006-0.016%;
linalool 0.05-0.1%;
0.01 to 0.06 percent of benzyl acetate;
0.3 to 0.8 percent of ethyl acetate;
0.1 to 0.35 percent of ethyl caproate;
the balance being propylene glycol.
2. The tobacco flavor for increasing the fresh and sweet aroma of cigarettes according to claim 1, which is characterized by further comprising the following components in percentage by mass:
0.06-0.16 of tea spirane.
3. The tobacco flavor for increasing the fresh and sweet aroma of cigarettes according to claim 2, which is characterized by further comprising the following components in percentage by mass:
0.005-0.1 of gamma decalactone.
4. The tobacco flavor for increasing the fresh and sweet aroma of cigarettes according to claim 3, which is characterized by further comprising the following components in percentage by mass:
0.1-0.35 of ethyl butyrate.
5. The tobacco flavor for increasing the fresh and sweet aroma of cigarettes according to claim 4, wherein the tobacco flavor further comprises the following components in percentage by mass:
0.004-0.014 of Lieberdang extract.
6. The tobacco flavor for increasing the fresh and sweet aroma of cigarettes according to claim 5, which is characterized by further comprising the following components in percentage by mass:
0.04-0.14 of ethyl phenylacetate.
CN202110487494.0A 2021-04-30 2021-04-30 Tobacco essence for increasing fresh and sweet aroma of cigarettes Pending CN113355159A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115216363A (en) * 2022-08-25 2022-10-21 云南中烟工业有限责任公司 Essence formula for increasing cigarette fragrance and improving smoke quality
CN115261136A (en) * 2022-08-25 2022-11-01 云南中烟工业有限责任公司 Fresh and sweet rhyme base module, preparation method thereof and application thereof in cigarettes

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CN104544553A (en) * 2014-12-31 2015-04-29 贵州中烟工业有限责任公司 Fen-flavor electronic tobacco liquid
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115216363A (en) * 2022-08-25 2022-10-21 云南中烟工业有限责任公司 Essence formula for increasing cigarette fragrance and improving smoke quality
CN115261136A (en) * 2022-08-25 2022-11-01 云南中烟工业有限责任公司 Fresh and sweet rhyme base module, preparation method thereof and application thereof in cigarettes
CN115216363B (en) * 2022-08-25 2023-10-27 云南中烟工业有限责任公司 Essence formula for increasing aroma of cigarettes and improving smoke quality

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