CN107637859A - A kind of mixed acid for tobacco charging and its preparation method and application - Google Patents
A kind of mixed acid for tobacco charging and its preparation method and application Download PDFInfo
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- CN107637859A CN107637859A CN201711000726.5A CN201711000726A CN107637859A CN 107637859 A CN107637859 A CN 107637859A CN 201711000726 A CN201711000726 A CN 201711000726A CN 107637859 A CN107637859 A CN 107637859A
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Abstract
The present invention provides a kind of for the mixed acid of tobacco charging and its preparation and application.The mixed acid is formulated by 40~70 parts of smoked plum extractives, 1~5 part of lactic acid, 1~5 part of valeric acid, 5~10 parts of malic acid and 10~50 parts of mixed with propylene glycol, wherein, the smoked plum extractive is with 20~30 parts of dark plum dry fruits actually raw material, add 10~30 parts of light-coloured vinegars and 50~80 parts of more than 90 DEG C hot water, mixing immersion filters off sediment after 5~7 days, then filtrate is concentrated into the rufous working fluid that (20 DEG C) of relative density is 1.15~1.25g/mL at 60~80 DEG C.The mixed acid quickly removes moisture removal to 12% or so, and cigarette is made with being sprayed directly on after distilled water diluting on pipe tobacco after 45 DEG C of baking ovens are placed 4 hours.The present invention can effectively make cigarette flavor comfortably become clear, flue gas it is soft it is fine and smooth, pleasant impression is totally comfortable, natural comfort when assigning cigarette smoking.
Description
Technical field
The present invention relates to technical field of cigarette flavors, in particular to a kind of preparation of the mixed acid for tobacco charging
Methods and applications.
Background technology
Tobacco is alkaline soil plant, except bringing the pleasant feeling of fragrance to consumer during suction, is also brought to oral cavity and throat
The uncomfortable sensation such as stimulation, and by adding appropriate organic acid, the pH value of tobacco is adjusted, can effectively alleviate or remove suction
When the sense of discomfort such as stimulation, while flue gas exquisiteness can also be made soft, comfort during increase suction.
Dark plum, it is the drying almost ripe fruit of rose family apricot category plum, in existing more than the 3000 years cultivation history in China, fresh flower
Extractable essence, flower, leaf, root and benevolence can be used as medicine.Edible fruit, salt marsh or drying, or smoke into dark plum and be used as medicine, have only
Cough, antidiarrheal, the effect promoted the production of body fluid, quenched the thirst, contain guarantor necessary to the human bodies such as a variety of organic acids, vitamin, flavones and basic mineral
Strong material.8 kinds of amino acid such as threonine wherein contained and flavones etc. be highly advantageous to human body protein form with metabolic function just
Often carry out, the generation of the diseases such as angiocarpy can be prevented.
Smoked plum extractive or dark plum medicinal extract are widely used in technical field of cigarette flavors.Have been reported that and separated in dark plum
Go out more than 10 kinds of organic acid, mainly there is citric acid, malic acid, oxalic acid, glycolic, lactic acid, butanedioic acid, fumaric acid, formic acid, second
Acid, propionic acid, palmitic acid etc., total acid content about 4%-5.5%, wherein, it is most with citric acid and malic acid content, in addition, dark plum fruit
It is a variety of containing furfural, 5 hydroxymethyl furfural, 5- methyl-2-furfurals, phenmethylol, guaiacol, eugenol etc. in meat and kernel
Tobacco aroma component.
Dark plum pulp acid content is high, and normal edible acidity stimulates very much, is eaten again after ironically being soaked with vinegar, its tart flavour
With regard to it is soft a lot, moreover, the content of the organic acid of dark plum after vinegar system will increase by 2.5~3.5.
Extract obtained by the different extraction process of dark plum in cigarette flavors technology application aspect be it is different, it is main
Embody functionally different.Presently commercially available cigarette smoked plum extractive or dark plum medicinal extract (being diluted to suitable Baume degrees) PH
Value between 3.0~3.5, acid number between 15~20, effect major embodiment in cigarette can fine and smooth soft flue gas, reduce
Stimulate；And smoked plum extractive pH value made from methods described herein, between 2.0~2.5, acid number is between 50~60, except having
Fine and smooth soft flue gas, the effect stimulated is reduced, more there is the mouthfeel for assigning cigarette sweet and sour taste and light, smooth, elegant flue gas
The effect of state.
Lactic acid, scientific name Lactic acid relative density 1.2060 (25/4 DEG C), 18 DEG C of fusing point, boiling point 122 DEG C (2kPa),
Refractive index nD (20 DEG C) 1.4392, can be miscible with water, ethanol, glycerine, in tobacco application can keep tobacco humidity, remove cigarette
Impurity in grass, improve suction mouthfeel, improve tobacco class, can also neutralize nicotine nicotine, adjust tobacco pH value, reduce to human body
Oxious component, improve cigarette quality.
Valeric acid, also known as positive valeric acid；Valeric acid；Positive punching Lysimachia sikokiana acid, colourless transparent liquid, has special stink, after dilution
There is a fruity of pleasant, relative density 0.9391 (20/4 DEG C), -33.83 DEG C of fusing point, boiling point 186.05 DEG C (100kPa), 96
DEG C (3.07kPa), refractive index 1.4085, can be dissolved in 30 parts of water, be soluble in ethanol, ether, in tobacco application can significantly improve
The texture of fragrance and bright sense.
Malic acid, malic acid have 3 kinds of malic acid of L mono-, D-malic acid and DL-malic acid isomers.Naturally occurring apple
Acid is all L-type, is almost present in all fruits, density 1.595,100 DEG C of fusing point, 140 DEG C of decomposition point, specific rotatory power-
2.3 ° (8.5 grams/100 milliliters water), soluble in water, the main function in tobacco has tart flavour regulation, reduces stimulation, soft cigarette
Gas.
The content of the invention
The mesh of the present invention is to provide cigarette mixed acid that a kind of style and features are obvious, application prospect is good and preparation method thereof
And application.The preparation method is simple, cheap, applied to can effectively make cigarette smoke exquisiteness soft in medium-to-high grade cigarette
With the mouthfeel of imparting cigarette sweet and sour taste and light, smooth, elegant smoke behavior.
The present invention is achieved through the following technical solutions：A kind of mixed acid for tobacco charging, its feature exist
It is made up of in the mixed acid the raw material of following mass fraction：40~70 parts of smoked plum extractive, 1~5 part of lactic acid, valeric acid 1~5
Part, 5~10 parts of malic acid, 10~50 parts of propane diols；The gross weight number of above-mentioned substance is 100 parts；
Wherein described smoked plum extractive is with the dark plum dry fruit of 20~30 parts by weight actually raw material, and being added after being pulverized
After the light-coloured vinegar infiltration 8-15 minutes of 10~30 parts by weight, more than 90 DEG C of 40~70 parts by weight of hot-water soak 5~7 days is added
After filter, and filtrate is concentrated into the rufous obtained when relative density (20 DEG C) is 1.15~1.25g/mL at 60~80 DEG C
Working fluid.
The present invention preferably technical scheme：The mixed acid is by the material composition of following weight fraction：Smoked plum extractive
50 parts, 2.5 parts of lactic acid, 1.5 parts of valeric acid, 8 parts of malic acid, 38 parts of propane diols；
The preparation method of a kind of mixed acid for tobacco charging provided by the invention, it is characterised in that specific steps are such as
Under：
(1) preparing raw material of smoked plum extractive is prepared according to following parts by weight：Dark plum dry fruit real 20~30 parts, light-coloured vinegar 10
~30 parts, more than 90 DEG C 40~70 parts of hot water；
(2) 20~30 parts of dark plum dry fruits are pulverized in fact, causes kernel rupture, be put into controllable temperature extraction vessel, specially may be used
Temperature control stainless steel extractor, 10~30 parts of light-coloured vinegar infiltrations are added, 40~70 parts more than 90 DEG C of hot water are added after 8-15 minutes,
And keep 90 DEG C of temperatures above to soak 6~10h, then stop heating immersion 5~7 days, finally adopt the solvent portions after immersion
Sediment is filtered off with the filter membrane that aperture is 0.8 micron and obtains filtrate, and filtrate is concentrated into relative density (20 at 60~80 DEG C
DEG C) it is 1.15~1.25g/mL, gained rufous working fluid is smoked plum extractive；
(3) mixing acid starting material is weighed according to following parts by weight：Middle 40~70 parts of the smoked plum extractive prepared of step (2),
10~50 parts of 1~5 part of lactic acid, 1~5 part of valeric acid, 5~10 parts of malic acid and propane diols；It will be made first in 40~70 parts of steps (2)
Standby smoked plum extractive and 5~10 parts of malic acid are sequentially added in stirring container, and 8-12 minutes are stirred after mixing and treat that malic acid is complete
After fully dissolved, 1~5 part of lactic acid, 1~5 part of valeric acid, 10~50 parts of propane diols are sequentially added, and 2-4 hours are stirred after mixing,
Static 24-48 hours, use aperture to filter off sediment for 0.8 micron of filter membrane and obtain the filter that relative density is 1.15~1.25g/mL
Liquid is a kind of mixed acid for tobacco charging.
A kind of application of mixed acid for tobacco charging provided by the invention, it is characterised in that：Prepared above-mentioned
Mixed acid uses the distilled water diluting of 4~8 times of its weight, is sprayed directly on laryngeal spray spray on pipe tobacco, and will be sprayed with
The pipe tobacco of mixed acid is placed 2~5 hours in the drying baker that temperature is 30~50 DEG C, and moisture removal is quickly removed after taking-up to 12% left side
The right side, and cigarette is made, wherein mixed acid accounts for the 0.25~0.50% of pipe tobacco weight.
Beneficial effects of the present invention：
1. the mixed acid in the present invention is applied to effectively make cigarette smoke exquisiteness soft in medium-to-high grade cigarette, assign
The feature of the mouthfeel of cigarette sweet and sour taste and light, smooth, elegant smoke behavior, help to strengthen enterprise to core technology
Control；
2. the bulk composition of mixed acid is dark plum in the present invention, containing many beneficial this healthy compositions of people, as calcium, iron and
Several amino acids and flavones etc., the human body protein that is highly advantageous to composition are normally carried out with metabolic function, can prevent angiocarpy etc.
Generation of disease etc.；
3. the made Preparation Method of the present invention is simple, cheap, the water in smoked plum extractive can be utilized in preparation process
Divide quick dissolving malic acid, the equipment of whole preparation requirement is relatively easy, and cost is relatively low, is easy to industrialized production, has very strong
Practicality.
Embodiment
With reference to specific embodiment, the present invention is described in further detail, but embodiment is not to skill of the present invention
The restriction of art scheme.
A kind of mixed acid for tobacco charging provided by the invention, it is characterised in that be by the raw material of following mass fraction
Composition：40~70 parts of smoked plum extractive, 1~5 part of lactic acid, 1~5 part of valeric acid, 5~10 parts of malic acid, 10~50 parts of propane diols, on
The gross weight number for stating material is 100 parts.
Heretofore described smoked plum extractive is prepared in accordance with the following methods：
(1) preparing raw material of smoked plum extractive is prepared according to following parts by weight：Dark plum dry fruit real 20~30 parts, light-coloured vinegar 10
~30 parts, more than 90 DEG C 40~70 parts of hot water；
(2) 20~30 parts of dark plum dry fruits are pulverized in fact, causes kernel rupture, be put into and can add in temperature control stainless steel extractor
10~30 parts of light-coloured vinegar infiltrations, add 40~70 parts more than 90 DEG C of hot water after 8-15 minutes, and keep 90 DEG C of temperatures above leachings
6~10h is steeped, then stops heating immersion 5~7 days, the solvent portions after immersion are finally used into aperture as 0.8 micron of filter membrane
Filter off sediment and obtain filtrate, and it is 1.15~1.25g/mL that filtrate is concentrated at 60~80 DEG C to relative density (20 DEG C), institute
It is smoked plum extractive to obtain rufous working fluid.
Embodiment 1, a kind of preparation method of mixed acid for tobacco charging, it is comprised the following steps that：
(1) mixed acid preparing raw material is prepared according to following parts by weight：40 parts of prunus mume extract, 2 parts of lactic acid, 1 part of valeric acid, apple
5 parts of tartaric acid, 52 parts of propane diols；
(2) 40 parts of smoked plum extractives, 5 parts of malic acid in raw material are sequentially added in stirring container, 10 points is stirred after mixing
2 parts of lactic acid, 1 part of valeric acid and 52 parts of propane diols are sequentially added after clock after malic acid is completely dissolved, 2-4 is stirred after continuing mixing
Hour, static 24-48 hours, it is 1.15~1.25g/ to use aperture to filter off sediment to obtain relative density for 0.8 micron of filter membrane
ML filtrate is the mixed acid for being used for tobacco charging.
The mixed acid for tobacco charging prepared in embodiment 1 is used to the distilled water diluting of 6 times of its weight, according to
0.3% amount laryngeal spray spray is sprayed directly on blank pipe tobacco, and it is small that 4 are placed in the drying baker that temperature is 30~50 DEG C
When, moisture removal is quickly removed after taking-up to 12% or so and cigarette is made, contrast is carried out and smokes panel test.
Embodiment 2, a kind of preparation method of mixed acid for tobacco charging, it is comprised the following steps that：
(1) mixed acid preparing raw material is prepared according to following parts by weight：50 parts of smoked plum extractive, 3 parts of lactic acid, 2 parts of valeric acid,
39 parts of 6 parts of malic acid and propane diols；
(2) 50 parts of smoked plum extractives, 6 parts of malic acid in raw material are added sequentially in stirring container, 10 is stirred after mixing
After minute after malic acid is completely dissolved, 3 parts of lactic acid, 2 parts of valeric acids and 39 parts of propane diols are sequentially added, 2-4 is stirred after mixing
Hour, static 24-48 hours, it is 1.15~1.25g/ to use aperture to filter off sediment to obtain relative density for 0.8 micron of filter membrane
ML filtrate is the mixed acid for being used for tobacco charging.
The mixed acid for tobacco charging prepared in embodiment 2 is used to the distilled water diluting of 6 times of its weight, according to
0.3% amount laryngeal spray spray is sprayed directly on blank pipe tobacco, and it is small that 4 are placed in the drying baker that temperature is 30~50 DEG C
When, moisture removal is quickly removed after taking-up to 12% or so and cigarette is made, contrast is carried out and smokes panel test.
Embodiment 3, a kind of preparation method of mixed acid for tobacco charging, it is comprised the following steps that：
(1) mixed acid preparing raw material is prepared according to following parts by weight：60 parts of smoked plum extractive, 3 parts of lactic acid, 3 parts of valeric acid,
28 parts of 6 parts of malic acid and propane diols；
(2) 60 parts of smoked plum extractive in raw material, 6 parts of malic acid are sequentially added in stirring container, 10 points is stirred after mixing
3 parts of lactic acid, 3 parts of valeric acid, 28 parts of propane diols are sequentially added after clock after malic acid is completely dissolved, 2-4 hours are stirred after mixing,
Static 24-48 hours, use aperture to filter off sediment for 0.8 micron of filter membrane and obtain the filter that relative density is 1.15~1.25g/mL
Liquid is the mixed acid for being used for tobacco charging.
The mixed acid for tobacco charging prepared in embodiment 1 is used to the distilled water diluting of 6 times of its weight, according to
0.3% amount laryngeal spray spray is sprayed directly on blank pipe tobacco, and it is small that 4 are placed in the drying baker that temperature is 30~50 DEG C
When, moisture removal is quickly removed after taking-up to 12% or so and cigarette is made, contrast is carried out and smokes panel test.
Cigarette prepared by above three embodiment forms the group of smokeing panel test using 7 people and smoked panel test, and wherein national level is smoked panel test
Teacher 2, provincial teacher of the smokeing panel test 5, specific smoking result such as table 1：
Evaluation of effect of the table 1 in cigarette
Shown by smoking result in table 1, the mixed acid centering high-grade cigarette quality that the present invention is used for tobacco charging has carried
Rise, rich good with fragrance, flue gas is sent out thoroughly, light and full, fine and smooth soft and smooth elegant.Mouthfeel has the sour-sweet of uniqueness to relax
Suitable sense.It can be used as novel tobacco flavor.
The mixed acid for tobacco charging prepared according to the method for the present invention is carried out physical testing, its physics by applicant
Index is as follows：
| Title | Tobacco aromaticss of the present invention |
| Outward appearance | Rufous liquid |
| Fragrance | Sour-sweet fruity |
| Relative density (20/20 DEG C) | 1.1635 |
| Refraction index (20 DEG C) | 1.4126 |
| Miscible degree (25 DEG C) in ethanol | Can be miscible with the ethanol of arbitrary volume 70% |
| Acid number | 68.6 |
| Lead content (mg/kg) | ≤5.0 |
| Arsenic content (mg/kg) | ≤1.0 |
By upper table as can be seen that essence its outward appearance for preparing of the present invention, fragrance are preferable, wherein lead content and arsenic content be all
Than relatively low, meet the standard of flavouring essence for tobacco.
Claims (4)
1. a kind of mixed acid for tobacco charging, it is characterised in that the mixed acid is the raw material group by following mass fraction
Into：40~70 parts of smoked plum extractive, 1~5 part of lactic acid, 1~5 part of valeric acid, 5~10 parts of malic acid, 10~50 parts of propane diols；
Wherein described smoked plum extractive be add 10 with the dark plum dry fruit of 20~30 parts by weight actually raw material, and after being pulverized~
After the light-coloured vinegar infiltration 8-15 minutes of 30 parts by weight, mistake after more than 90 DEG C of 40~70 parts by weight of hot-water soak 5~7 days is added
Filter, and filtrate is concentrated at 60~80 DEG C to the rufous flowing obtained when relative density (20 DEG C) be 1.15~1.25g/mL
Liquid.
A kind of 2. mixed acid for tobacco charging according to claim 1, it is characterised in that the mixed acid be by with
The material composition of lower weight fraction：50 parts of smoked plum extractive, 2.5 parts of lactic acid, 1.5 parts of valeric acid, 8 parts of malic acid, 38 parts of propane diols.
3. the preparation method of a kind of mixed acid for tobacco charging, it is characterised in that comprise the following steps that：
(1) preparing raw material of smoked plum extractive is prepared according to following parts by weight：Dark plum dry fruit real 20~30 parts, light-coloured vinegar 10~30
Part, more than 90 DEG C 40~70 parts of hot water；
(2) 20~30 parts of dark plum dry fruits are pulverized in fact, causes kernel rupture, be put into controllable temperature extraction vessel, add 10~30 parts
Light-coloured vinegar is infiltrated, and 40~70 parts more than 90 DEG C of hot water is added after 8-15 minutes, and keeps 90 DEG C of temperatures above to soak 6~10h,
Then stop heating immersion 5~7 days, finally use aperture to filter off sediment for 0.8 micron of filter membrane the solvent portions after immersion
Obtain filtrate, and it is 1.15~1.25g/mL that filtrate is concentrated at 60~80 DEG C to relative density (20 DEG C), gained rufous
Working fluid is smoked plum extractive；
(3) mixing acid starting material is weighed according to following parts by weight：40~70 parts of smoked plum extractive, the lactic acid 1 prepared in step (2)
10~50 parts of~5 parts, 1~5 part of valeric acid, 5~10 parts of malic acid and propane diols；First by preparation in 40~70 parts of steps (2)
Smoked plum extractive and 5~10 parts of malic acid are sequentially added in stirring container, and 8-12 minutes are stirred after mixing and treat that malic acid is completely molten
Xie Hou, 1~5 part of lactic acid, 1~5 part of valeric acid, 10~50 parts of propane diols are sequentially added, and stirred 2-4 hours after mixing, it is static
24-48 hours, use aperture to filter off sediment for 0.8 micron of filter membrane and obtain filtrate that relative density is 1.15~1.25g/mL i.e.
For a kind of mixed acid for tobacco charging.
A kind of 4. application of mixed acid for tobacco charging, it is characterised in that：The above-mentioned mixed acid prepared is heavy using its
The distilled water diluting of 4~8 times of amount, it is sprayed directly on laryngeal spray spray on pipe tobacco, and the pipe tobacco for being sprayed with mixed acid is existed
Temperature is to be placed 2~5 hours in 30~50 DEG C of drying baker, and moisture removal is quickly removed after taking-up to 12% or so, and cigarette is made,
Wherein mixed acid accounts for the 0.25~0.50% of pipe tobacco weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711000726.5A CN107637859B (en) | 2017-10-24 | 2017-10-24 | Mixed acid for tobacco charging and preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711000726.5A CN107637859B (en) | 2017-10-24 | 2017-10-24 | Mixed acid for tobacco charging and preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107637859A true CN107637859A (en) | 2018-01-30 |
| CN107637859B CN107637859B (en) | 2023-03-21 |
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ID=61124294
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711000726.5A Active CN107637859B (en) | 2017-10-24 | 2017-10-24 | Mixed acid for tobacco charging and preparation method and application thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3095882A (en) * | 1961-08-04 | 1963-07-02 | Philip Morris Inc | Tobacco flavorants |
| CN104188086A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Method for improving smoking flavor quality of cigarettes with green plums |
| CN104522879A (en) * | 2014-11-10 | 2015-04-22 | 浙江中烟工业有限责任公司 | Tobacco flavor for improving taste quality of upper tobacco leaf group |
| CN105038984A (en) * | 2015-07-10 | 2015-11-11 | 湖北中烟工业有限责任公司 | Acid-flavor essence for softening and smoothing smoke and reducing stimulation and application thereof |
| CN106148011A (en) * | 2016-07-20 | 2016-11-23 | 湖北中烟工业有限责任公司 | The preparation method of a kind of cigarette radix valerianae extract and the application in Medicated cigarette thereof |
| CN107216947A (en) * | 2017-07-26 | 2017-09-29 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette Catechu extract |
-
2017
- 2017-10-24 CN CN201711000726.5A patent/CN107637859B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3095882A (en) * | 1961-08-04 | 1963-07-02 | Philip Morris Inc | Tobacco flavorants |
| CN104188086A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Method for improving smoking flavor quality of cigarettes with green plums |
| CN104522879A (en) * | 2014-11-10 | 2015-04-22 | 浙江中烟工业有限责任公司 | Tobacco flavor for improving taste quality of upper tobacco leaf group |
| CN105038984A (en) * | 2015-07-10 | 2015-11-11 | 湖北中烟工业有限责任公司 | Acid-flavor essence for softening and smoothing smoke and reducing stimulation and application thereof |
| CN106148011A (en) * | 2016-07-20 | 2016-11-23 | 湖北中烟工业有限责任公司 | The preparation method of a kind of cigarette radix valerianae extract and the application in Medicated cigarette thereof |
| CN107216947A (en) * | 2017-07-26 | 2017-09-29 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette Catechu extract |
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| CN107637859B (en) | 2023-03-21 |
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