CN109007956A - A kind of preparation method and purposes of cigarette fruit solid fragrance - Google Patents
A kind of preparation method and purposes of cigarette fruit solid fragrance Download PDFInfo
- Publication number
- CN109007956A CN109007956A CN201810554371.2A CN201810554371A CN109007956A CN 109007956 A CN109007956 A CN 109007956A CN 201810554371 A CN201810554371 A CN 201810554371A CN 109007956 A CN109007956 A CN 109007956A
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- China
- Prior art keywords
- cigarette
- insoluble matter
- fruit
- solid fragrance
- preparation
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a kind of cigarette preparation method of fruit solid fragrance, steps are as follows: (1) by fruit flooding, separates leaching liquor and insoluble matter；(2) substrate is made in the insoluble matter that step (1) obtains；(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum is concentrated that step (1) obtains to get arriving cigarette fruit solid fragrance.The invention also discloses cigarette made from the preparation method with fruit solid fragrance for the purposes in tobacco product.
Description
Technical field
The invention belongs to cigarette solid spice technical fields, are specifically related to a kind of preparation of cigarette fruit solid fragrance
Method and purposes.
Background technique
It is the reconstruction that is process with paper technology using offal and offal as raw material with paper process production reconstituted tobacco
Tobacco leaf, production method are to be soaked in water, extract after mixing offal and offal, separate insoluble matter and soluble matter leaching liquor, no
Molten object is used to slurrying, and manufactures paper with pulp into substrate, after the concentration modulation of soluble matter leaching liquor, immerses in substrate or is coated on substrate, or
It is extraction separation after offal and offal are used corresponding solvent soaking respectively, the resulting insoluble matter mixed pulp of difference, upper paper machine
Substrate is manufactured paper with pulp into, resulting soluble matter leaching liquor concentration adjustment is made coating fluid, is applied on substrate.The production technology is letter
Tobacco material is regulated and controled and is recombinated by single ground, is had no special other function or is inhaled taste.Due to the particularity of raw material, lead to this
Body flue gas is thin, single, not strong with the compatibility of tobacco leaf in use, and the effect modified along making up is unobvious.In the past
Mainly improved by manually adding fragrance.With the emergence of new cigarette material, according to different trade mark cigarette
Style and the difference for inhaling taste, targetedly the suitable raw material of selection is combined collocation, it has also become papermaking-method reconstituted tobaccos are raw
Conventional technical means in production.
Summary of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of cigarette fruit solid fragrance and its preparation
Methods and applications, with increase cigarette fragrance and it is jealous, reduce xylon gas and pungent sense, to promote integrated sensory's product of cigarette
Matter.
The purpose of the present invention is achieved by the following technical programs.
Unless otherwise indicated, percentage of the present invention is mass percent.
The first aspect of the present invention discloses a kind of preparation method of cigarette fruit solid fragrance, step are as follows:
(1) by fruit flooding, leaching liquor and insoluble matter are separated；
(2) substrate is made in the insoluble matter that step (1) obtains；
(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum is concentrated that step (1) obtains, i.e.,
Obtain the cigarette fruit solid fragrance.
Preferably, the fruit is loquat, cumquat, jujube, plum, pears, plum, apricot, apple, fig, grape, lemon
Lemon, peach, pineapple, hawthorn, dried orange peel, shaddock, sweet orange, orange, pomegranate, blueberry, green plum, pawpaw, pear cv nanguo, Chinese grooseberry, Hami
One of melon, mulberries, blackcurrant, lichee or numerous compositions.
Preferably, the mass ratio of the fruit and water of step (1) is 1:8~1:15, and ultrasound extraction, the time is 20~60 points
Clock.
Preferably, the step of substrate is made in insoluble matter by step (2) are as follows:
1. the mixture of insoluble matter or insoluble matter and waste/hypo-tobacco leaf is added 5~10 times of water rettings of its quality, and pectin is added
Enzyme, amylase and cellulase carry out catalytic degradation；The mass ratio of the insoluble matter and waste/hypo-tobacco leaf is 10:90-90:10.
2. again 1. 1~10% wood fibre of insoluble matter or insoluble matter and waste/hypo-tobacco leaf gross mass is added to step
Mixed pulp is carried out in obtained mixture, is manufactured paper with pulp using conventional paper process and substrate is made.After roll paper, cutting, drying, system
Obtain cigarette fruit solid fragrance.
Preferably, the dosage of the pectase, amylase and cellulase accounts for the insoluble matter or insoluble matter respectively and gives up
The percentage of hypo-tobacco leaf gross mass are as follows: pectase 0.03%~0.1%, amylase 0.1%~0.6%, cellulase 0.5%~
1%；Hydrolysis temperature is 30 DEG C~60 DEG C；The catalytic degradation time 1~4 hour.
Second aspect of the present invention discloses cigarette made from any of the above-described preparation method and is used for fruit solid fragrance
Purposes in tobacco product.
Preferably, the cigarette is used separately as pipe tobacco with fruit solid fragrance or is used in mixed way with common pipe tobacco.
Preferably, when cigarette fruit solid fragrance and common pipe tobacco are used in mixed way, the adding proportion of fruit solid fragrance is 1
~55wt%.
Compared with the existing technology, the invention has the following advantages that
1, the present invention takes full advantage of the effective component and fragrance matter of fruit extract, and passes through catalytic degradation processing pair
Pectin and protein etc. carry out fully degraded in insoluble matter, produce a large amount of Maillard reaction precursor.Improve the solid
Adaptability and compatibility of the fragrance in cigarette composition can sufficiently promote the suction of cigarette made of the cigarette fruit solid fragrance
Quality achievees the purpose that partly or entirely to substitute tobacco leaf.
2, cigarette of the invention is used for cigarette products with fruit solid fragrance, and the style and features of tobacco product can be enhanced, make
Fragrance is more abundant, enhances fresh and sweet note and sense of promoting the production of body fluid, flue gas is finer and smoother, soft, preferably improves the integrated sensory of cigarette
Quality.It has been surprisingly found that, this can reduce the content of harmful substance with fruit solid fragrance for cigarette products, and especially tar contains
Amount reduces obvious；Water content obviously increases simultaneously.
3, the fruit solid used in the present invention can reduce the demand to wood fibre, therefore the pumping with cigarette reconstituted tobacco
Inhale comparison, can the bad breath such as substantially reduced woody odor, while also solving the problems, such as and cigarette enterprise contention raw material.
4, cigarette of the invention extends the use scope of fruit with fruit solid fragrance, enriches the fragrance type of cigarette,
Can preferably meet the needs of cigarette product specializes.
5, the shortage problem that material is inevitably encountered in cigarette product, causes product quality to fluctuate.The present invention
Production of cigarettes raw material is enriched, alleviates the problem of raw tobacco material shortage to a certain extent, and then can achieve stable prod and match
The purpose of side.
Specific embodiment
The present invention is described in further detail combined with specific embodiments below, but embodiment is not to skill of the present invention
The restriction of art scheme.Unless otherwise indicated, percentage of the present invention is mass percent.
Embodiment 1
Mass parts: 3 portions of loquats, 1 portion of sweet orange, 2 portions of apples, 1 portion of jujube are chosen, by raw material after mixing using water as leaching liquor
Ultrasound extraction 30 minutes, solid-to-liquid ratio 1:10.Isolated leaching liquor and insoluble matter after extraction.Leaching liquor is true through low temperature
It is spare after empty concentration, by insoluble matter plus the water retting of 5 times of quality, then be separately added by insoluble matter gross mass 0.03% fruit
The catalyzing enzymes such as glue enzyme, 0.6% amylase, 0.5% cellulase, catalytic degradation temperature are 30 DEG C, are stirred 2 hours.Then
Wood fibre is added by 2% mass ratio of insoluble matter gross mass again and carries out slurrying, then manufactures paper with pulp into substrate.Leaching liquor is uniform
In dip-coating to above-mentioned substrate, after roll paper, cutting, drying, cigarette fruit solid fragrance is made.Individually chopping and volume can be made
The tobacco products such as cigarette can also be mixed and made into tobacco product with pipe tobacco.
Cigarette process of the cigarette with fruit solid fragrance routinely rolls into cigarette through flavoring, volume job contract skill.It is commented through sense organ
Inhale, overall process can obviously experience sucks cigarette habit continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet tea
Moisture feeling is good, overall comfort is good, and the ash rate tobacco ash content to burn is white.By cigarette with fruit solid fragrance in varing proportions with cigarette
Silk is mixed with tobacco product, can embody above-mentioned sensory effects in various degree.
Cigarette is mixed with 8wt% ratio with pipe tobacco with fruit solid fragrance, cigarette is rolled into through flavoring, volume job contract skill, orders
Entitled No. 1 cigarette.On same production line, control cigarette is rolled by identical cigarette process, control sample is that cigarette water is not added
The normal cigarette of fruit solid spice.Then by national standard, " tobacco of GB/T16447~1996 and tobacco product adjust the atmosphere with test
Environment " adjust cigarette sample moisture content be 12%, by panel of expert of smokeing panel test by " the cigarette sense organ technology of GB5606.4~1996 is wanted
Ask " regulation carry out cigarette sensory evaluating smoking.Smoking result is shown in Table 1；Specific sense organ marking is shown in Table 2, table 3；According to GB 5606.5-
2005 pairs of cigarette carry out flue gas conventional detection, and testing result is shown in Table 4.
Embodiment 2
Choose mass parts: 3 parts of plums, 1 portion of cumquat, 2 portions of shaddocks, 1 portion of apricot, 3 portions of pomegranates, by raw material after mixing with water
For leaching liquor ultrasound extraction 20 minutes, solid-to-liquid ratio 1:8, isolated leaching liquor and insoluble matter after extraction.Leaching liquor
It is spare after cryogenic vacuum concentration, by insoluble matter and waste/hypo-tobacco leaf (mass ratio of insoluble matter and waste/hypo-tobacco leaf is 1:1) plus 7
Times water impregnates again, then by insoluble matter and waste/hypo-tobacco leaf gross mass be separately added into 0.15% pectase, 0.3% amylase,
The catalyzing enzymes such as 0.8% cellulase, catalytic degradation temperature are 50 DEG C, are stirred 3 hours.Insoluble matter is pressed after mixed pulp again and is given up
The mass ratio of hypo-tobacco leaf gross mass 4% is added wood fibre and carries out slurrying, then manufactures paper with pulp into substrate.The uniform dip-coating of leaching liquor is arrived
On above-mentioned substrate, after roll paper, cutting, drying, cigarette fruit solid fragrance is made.Individually chopping and the cigarettes such as cigarette can be made
Straw-made articles can also be mixed and made into tobacco product with pipe tobacco.
Cigarette process of the cigarette with fruit solid fragrance routinely rolls into cigarette through flavoring, volume job contract skill.It is commented through sense organ
Inhale, overall process can obviously experience sucks cigarette habit continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet tea
Moisture feeling is good, overall comfort is good, and the ash rate tobacco ash content to burn is white.By cigarette with fruit solid fragrance in varing proportions with cigarette
Silk is mixed with tobacco product, can embody above-mentioned sensory effects in various degree.
Cigarette is mixed with 6wt% ratio with pipe tobacco with fruit solid fragrance, cigarette is rolled into through flavoring, volume job contract skill, orders
Entitled No. 2 cigarettes.On same production line, control cigarette is rolled by identical cigarette process, control sample is that cigarette water is not added
The normal cigarette of fruit solid spice.Then by national standard, " tobacco of GB/T16447~1996 and tobacco product adjust the atmosphere with test
Environment " adjust cigarette sample moisture content be 12%, by panel of expert of smokeing panel test by " the cigarette sense organ technology of GB5606.4~1996 is wanted
Ask " regulation carry out cigarette sensory evaluating smoking.Smoking result is shown in Table 1；Specific sense organ marking is shown in Table 2, table 3；According to GB 5606.5-
2005 pairs of cigarette carry out flue gas conventional detection, and testing result is shown in Table 4.
Embodiment 3
Choose mass parts: 2 portions of hawthorn, 1 part of blueberry, 2 portions of pawpaws, 2 parts of mulberries, 1 part of dried orange peel, by raw material after mixing with
Water is that leaching liquor ultrasound extracts 40 minutes, solid-to-liquid ratio 1:15, isolated leaching liquor and insoluble matter after extraction.Extraction
Liquid is spare after cryogenic vacuum concentration, by insoluble matter and waste/hypo-tobacco leaf (mass ratio of insoluble matter and waste/hypo-tobacco leaf is 2:1)
Add 10 times of water to impregnate again, then is separately added into 0.1% pectase, 0.3% starch by insoluble matter and waste/hypo-tobacco leaf gross mass
Enzyme, 1% the catalyzing enzymes such as cellulase, catalytic degradation temperature is 60 DEG C, is stirred 4 hours.After mixed pulp again by insoluble matter and
The mass ratio of waste/hypo-tobacco leaf gross mass 6% is added wood fibre and carries out slurrying, then manufactures paper with pulp into substrate.By the uniform dip-coating of leaching liquor
Onto above-mentioned substrate, after roll paper, cutting, drying, cigarette fruit solid fragrance is made.Individually chopping and cigarette can be made etc.
Tobacco product can also be mixed and made into tobacco product with pipe tobacco.
Cigarette process of the cigarette with fruit solid fragrance routinely rolls into cigarette through flavoring, volume job contract skill.It is commented through sense organ
Inhale, overall process can obviously experience sucks cigarette habit continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet tea
Moisture feeling is good, overall comfort is good, and the ash rate tobacco ash content to burn is white.By cigarette with fruit solid fragrance in varing proportions with cigarette
Silk is mixed with tobacco product, can embody above-mentioned sensory effects in various degree.
Cigarette is mixed with 8wt% ratio with pipe tobacco with fruit solid fragrance, cigarette is rolled into through flavoring, volume job contract skill, orders
Entitled No. 3 cigarettes.On same production line, control cigarette is rolled by identical cigarette process, control sample is that cigarette water is not added
The normal cigarette of fruit solid spice.Then by national standard, " tobacco of GB/T16447~1996 and tobacco product adjust the atmosphere with test
Environment " adjust cigarette sample moisture content be 12%, by panel of expert of smokeing panel test by " the cigarette sense organ technology of GB5606.4~1996 is wanted
Ask " regulation carry out cigarette sensory evaluating smoking.Smoking result is shown in Table 1；Specific sense organ marking is shown in Table 2, table 3；According to GB 5606.5-
2005 pairs of cigarette carry out flue gas conventional detection, and testing result is shown in Table 4.
1 cigarette sensory evaluating smoking's result of table
2 sensory evaluation of table marking table
3 suction evaluation table of table
4 flue gas conventional analysis result of table
Show that the cigarette of preparation is added in cigarette with fruit solid fragrance by the smoking result in table 1- table 3, sample cigarette
Smoke panel test point higher than control sample 0.5 point or more.Compared with control sample, the comfort mean height 0.6 of sample cigarette divides or so, cigarette
Gas feature mean height 0.4 divides or so, more than sweet taste mean height 0.5 divides in taste style, tart flavour mean height 0.2 or so.Therefore originally
The cigarette of invention is added in cigarette with fruit solid fragrance can be obviously improved cigarette perfume, coordinate flue gas, increase the sweet sense of flue gas, reduce
Cigarette smoke irritation, the effect for improving user throat comfort, can increase the richness and sophistication of cigarette perfume, have preferable
Cigarette application effect.As shown in Table 4, compared with control sample, the cigarette of the invention cigarette main flue of fruit solid fragrance is added
Total granules, smoking nicotine and CO decrease in gas, and especially tar content is substantially reduced, and averagely have dropped
It is more than 0.80mg/ branch.Flue gas moisture obviously increases simultaneously, averagely increases 0.4mg/ branch or so.
Claims (8)
1. a kind of cigarette preparation method of fruit solid fragrance, which is characterized in that step are as follows:
(1) by fruit flooding, leaching liquor and insoluble matter are separated；
(2) substrate is made in the insoluble matter that step (1) obtains；
(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum is concentrated that step (1) obtains to get arriving
Cigarette fruit solid fragrance.
2. preparation method according to claim 1, which is characterized in that the fruit be loquat, cumquat, jujube, plum, pears,
Plum, apricot, apple, fig, grape, lemon, peach, pineapple, hawthorn, dried orange peel, shaddock, sweet orange, orange, pomegranate, blueberry, blueness
One of plum, pawpaw, pear cv nanguo, Chinese grooseberry, "Hami" melon, mulberries, blackcurrant, lichee or numerous compositions.
3. preparation method according to claim 1, which is characterized in that the fruit dry product of step (1) and the mass ratio of water are
1:8~1:15, ultrasound extraction, time are 20~40 minutes.
4. preparation method according to claim 1, which is characterized in that the step of substrate is made in insoluble matter by step (2) are as follows:
1. the mixture of insoluble matter or insoluble matter and waste/hypo-tobacco leaf is added into 5~10 times of water rettings of its quality, and be added pectase,
Amylase and cellulase carry out catalytic degradation；
2. 1~10% wood fibre of insoluble matter or insoluble matter and waste/hypo-tobacco leaf gross mass is added to step again 1. to obtain
Mixture in carry out mixed pulp, manufactured paper with pulp using conventional paper process and substrate be made.
5. the preparation method according to claim 4, which is characterized in that the use of the pectase, amylase and cellulase
Amount accounts for the percentage of the mixture gross mass of the insoluble matter or insoluble matter and waste/hypo-tobacco leaf respectively are as follows: and pectase 0.03%~
0.1%, amylase 0.1%~0.6%, cellulase 0.5%~1%；Hydrolysis temperature is 30 DEG C~60 DEG C；The catalytic degradation time
1~4 hour.
6. cigarette made from a kind of -5 any preparation methods according to claim 1 is used for tobacco product with fruit solid fragrance
In purposes.
7. purposes according to claim 6, which is characterized in that the cigarette fruit solid fragrance makes separately as pipe tobacco
It is used in mixed way with or with common pipe tobacco.
8. purposes according to claim 7, which is characterized in that cigarette is used in mixed way with fruit solid fragrance and common pipe tobacco
When, the ratio of fruit solid fragrance is 1~55wt%.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554371.2A CN109007956A (en) | 2018-06-01 | 2018-06-01 | A kind of preparation method and purposes of cigarette fruit solid fragrance |
| CN201910181089.9A CN109691684A (en) | 2018-06-01 | 2019-03-11 | The preparation method and its purposes in tobacco product of a kind of fragrance |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554371.2A CN109007956A (en) | 2018-06-01 | 2018-06-01 | A kind of preparation method and purposes of cigarette fruit solid fragrance |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109007956A true CN109007956A (en) | 2018-12-18 |
Family
ID=64611925
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810554371.2A Pending CN109007956A (en) | 2018-06-01 | 2018-06-01 | A kind of preparation method and purposes of cigarette fruit solid fragrance |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109007956A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110150727A (en) * | 2019-05-05 | 2019-08-23 | 贵州中烟工业有限责任公司 | A kind of fragrant preparation of sections method of dried orange peel odor type plant production suitable for heating the cigarette that do not burn |
-
2018
- 2018-06-01 CN CN201810554371.2A patent/CN109007956A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110150727A (en) * | 2019-05-05 | 2019-08-23 | 贵州中烟工业有限责任公司 | A kind of fragrant preparation of sections method of dried orange peel odor type plant production suitable for heating the cigarette that do not burn |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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Application publication date: 20181218 |