CN107502449A - A kind of preparation method and application of rhamnoides extract Maillard reaction type tobacco aromaticss - Google Patents

A kind of preparation method and application of rhamnoides extract Maillard reaction type tobacco aromaticss Download PDF

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Publication number
CN107502449A
CN107502449A CN201710728966.0A CN201710728966A CN107502449A CN 107502449 A CN107502449 A CN 107502449A CN 201710728966 A CN201710728966 A CN 201710728966A CN 107502449 A CN107502449 A CN 107502449A
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China
Prior art keywords
preparation
maillard reaction
extract
rhamnoides
cigarette
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CN201710728966.0A
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Chinese (zh)
Inventor
郑宏伟
苏海建
马长峰
岳勇
王强
孙强
于国锋
杨景全
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China Tobacco Shandong Industrial Co Ltd
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China Tobacco Shandong Industrial Co Ltd
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Priority to CN201710728966.0A priority Critical patent/CN107502449A/en
Publication of CN107502449A publication Critical patent/CN107502449A/en
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/12—Steaming, curing, or flavouring tobacco
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/022—Refining
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/025—Recovery by solvent extraction

Abstract

The invention discloses a kind of rhamnoides extract Maillard reaction type tobacco aromaticss and preparation method and application, the preparation method of tobacco aromaticss, comprise the following steps：1）After dry fructus hippophae removes impurity, crush, cross 80 mesh sieves, it is standby；2）To step 1）In add organic solvent in obtained Seabuckthorn Fruit, extracted, obtain Seabuckthorn extraction juice；3）To step 2）In Seabuckthorn extraction juice filtered, concentrated, be made rhamnoides extract；4）With Ammonia material Maillard reaction occurs for rhamnoides extract, obtains reaction product；5）To step 4）Certain glycerine is added in obtained reaction product, produces rhamnoides extract Maillard reaction type tobacco aromaticss.The method is with strong points, extract fragrance enriches, and applied to can preferably lift cigarette flavor matter in cigarette, increases perfume quantity, increases oral cavity moisture feeling, improve pleasant impression, has the application effect for significantly improving cigarette smoking quality.

Description

A kind of preparation method and application of rhamnoides extract Maillard reaction type tobacco aromaticss
Technical field
Present invention relates particularly to a kind of preparation method of rhamnoides extract Maillard reaction type tobacco aromaticss and in cigarette blending In application, belong to cigarette meat flavor formulating technology field.
Background technology
Sea-buckthorn is that Elaeangnaceae calculates the machaka for piercing category or dungarunga, also known as vinegar willow.It is mainly distributed on NORTHWEST CHINA, China More than the ten individual provinces and regions such as north, northeast and southwest.Sea buckthorn fruit is rich in multivitamin, organic acid, flavones and trace element, has very High nutrition and medical value.Application study of the China to sea-buckthorn has made some progress, be mainly used in food, medicine, Cosmetics etc..
At present, most cigarette hippophae rhamnoides, it is raw material by simple extraction, filtering, dense mainly using sea-buckthorn Hippophae rhamnoides is prepared in the techniques such as contracting.The extract that the method obtains contains a variety of esters, carboxylic acids and polysaccharide, can reduce volume The dry sensation and excitant of cigarette flue gas, improve flue gas comfortable taste degree, and reduce the peculiar N- of the tobacco in cigarette mainstream flue gas Nitrosamine (TSNAs) total amount, but fragrance be present and not enough enrich in it, the application effect in cigarette is comparatively single, is only capable of Increase the sweet sense in oral cavity, slightly increase flue gas concentration, and in lifting cigarette flavor matter, the improvement flue gas property sent out, and assign cigarette thoroughly Deficiency in terms of characteristic flavor on basis.
Maillard reaction is condensation, dehydration, degraded and the redox that amino acid occurs with reduced sugar or carbonyls Etc. series reaction.The chemical substance that species is abundant and molecular weight is big can be produced by Maillard reaction, make whole reactant Full aroma.In addition, contain substantial amounts of fragrance matter in maillard reaction thing, and most of and cigarette perfume is coordinated, thus turn into Good tobacco aromaticss.With deepening continuously for Chinese style flue-cured tobacco type Tar work, all kinds of causes in tobacco tar are fragrant Material also has different degrees of reduction, causes that smoke is flat, fragrance is thin, and cigarette grade is had a greatly reduced quality, maillard reaction product It can be used as effective flavoring substances on low-coke tar cigarette, to strengthen the fragrance of cigarette.
Although disclose seabuckthorn fruit extract in the prior art occurs Maillard reaction with amino acid, tobacco aromaticss are prepared, However, it is necessary to add the concentrate and fructus hippophae of the extract of the spices such as fritillaria thunbergii, gynostemma pentaphylla, honeysuckle, loguat leaf and lily Extract prepares tobacco aromaticss by Maillard reaction together, to reach the purpose of submissive flue gas and abundant cigarette pleasant impression, a side Security of the combustion product for these raw materials that face adds in human body is also to be verified, on the other hand, these material mixings Maillard reaction product and fructus hippophae are entirely different, and the improvement for cigarette odor-absorbing is also entirely different.
The content of the invention
It is an object of the invention to for problem of the prior art, there is provided a kind of rhamnoides extract Maillard reaction type cigarette is fragrant Material and preparation method and application.The method is with strong points, extract fragrance enriches, applied to can preferably lift volume in cigarette Cigarette perfume makings, increase perfume quantity, increase oral cavity moisture feeling, improve pleasant impression, there is the application effect for significantly improving cigarette smoking quality.
In order to solve the above technical problems, the technical scheme is that：
A kind of preparation method of rhamnoides extract Maillard reaction type tobacco aromaticss, comprises the following steps：
1) after the fructus hippophae dried removes impurity, crush, cross 80 mesh sieves, it is standby；
2) organic solvent is added in the Seabuckthorn Fruit obtained into step 1), is extracted, obtains Seabuckthorn extraction juice；
3) Seabuckthorn extraction juice in step 2) is filtered, concentrated, rhamnoides extract is made；
4) with Ammonia material Maillard reaction occurs for rhamnoides extract, obtains reaction product；
5) certain glycerine is added in the reaction product obtained to step 4), produces rhamnoides extract Maillard reaction type cigarette Use spices.
It is that its own is deposited after harvesting because fructus hippophae contains substantial amounts of carbohydrate and amino acids from dry fructus hippophae In reactions such as complicated Mei Lade, breathings, the degree that these reactions of dried fructus hippophae are carried out is smaller, is used as raw material When, the aroma component having is more, bigger to the sense organ contribution degree of cigarette product.And the fructus hippophae dried is not easy corrupt change Matter, can guarantee that the tobacco aromaticss of preparation taste it is pure, reduce the generation of miscellaneous taste, be also convenient for buying and selling and transport.
Only it is that fragrance existing for sea-buckthorn itself is not rich enough in the cigarette prepared based on existing method as raw material from fructus hippophae Richness, the application effect in cigarette is relatively single, is only capable of increasing the sweet sense in oral cavity, slightly increases flue gas concentration, and in lifting cigarette Aroma quality, improve the flue gas property sent out and the deficiency etc. in terms of assigning cigarette characteristic flavor on basis thoroughly.
Preferably, in step 2), the organic solvent is absolute ethyl alcohol.
It is further preferred that in step 2), extract and separate is carried out using microwave-assisted extraction technique.
Microwave abstracting is to make some organic components and matrix in solid or semi-solid material using the effect of electromagnetic field Efficiently separate, and can keep analyzing a kind of separation method of the script compound state of object.
Preferably, in step 3), concentrated using the method for vacuum concentration, the sea-buckthorn for the rhamnoides extract being concentrated to give carries The content for taking thing is 70-95%.
During vacuum concentration, solvent can be made largely to evaporate at a lower temperature, save mass energy.Simultaneously as thing Material is not affected by high temperatures, and avoids the destruction and loss of thermally labile component, preferably saves the nutritional ingredient and perfume (or spice) of raw material Gas.
Preferably, in step 4), the mass percent that Ammonia material accounts for rhamnoides extract is 5-30%.
It is further preferred that in step 4), the Ammonia material is alanine, proline, valine, arginine, silk ammonia One or more in acid, phenylalanine, glutamic acid, aspartic acid, glycine or tyrosine.
Still more preferably, the Ammonia material is alanine, glutamic acid and phenylalanine in mass ratio 2:3:1 it is mixed Compound.
Preferably, in step 4), the pH value of Maillard reaction is 4-12, preferably 10-12, most preferably 10；
The temperature of reaction is 80-120 DEG C, and the time of reaction is 2-4 hours.
Maillard reaction, most preferably 10 are preferably carried out in the present invention in the basic conditions.Because in alkalescence condition Under Maillard reaction formed the presoma for being 1-deoxysome, being numerous food product fragrance, be more beneficial for obtaining more tools Dulcet composition.
It is further preferred that regulation Maillard reaction pH value material for concentrated ammonia liquor, the NaOH aqueous solution, the KOH aqueous solution, Na2HPO4The aqueous solution, Na2CO3One or more in the aqueous solution, hydrochloric acid, acetic acid, citric acid.
Preferably, in step 5), the glycerine of addition accounts for the 2-5% of reaction product weight.
The tobacco aromaticss that above-mentioned preparation method is prepared.
Application of the above-mentioned tobacco aromaticss in cigarette is prepared.
The application, specifically comprises the following steps：
1) tobacco aromaticss are added in pipe tobacco, the percentage by weight that tobacco aromaticss account for pipe tobacco is 0.02-0.10%；
2) distilled water is added into pipe tobacco, the moisture for making pipe tobacco is 19-21%；
3) pipe tobacco is sealed and stored 1-3h, is then 12-13% by shredded tobacco baking to moisture at 130-140 DEG C, obtains For making the pipe tobacco of cigarette.
Beneficial effects of the present invention are：
(1) present invention prepares Maillard reaction type spices using sea-buckthorn as sugar source, by adding amino acid, rationally control Process conditions, a small amount of flavor substance that fragrance caused by Maillard reaction and rhamnoides extract are contained in itself organically combine, mutually Set off, note is more abundant to be coordinated；
(2) the rhamnoides extract Maillard reaction type tobacco aromaticss obtained by the present invention are used in tobacco charging, can be preferable Lifting cigarette flavor matter, increase perfume quantity, increase oral cavity moisture feeling, improve pleasant impression, have significantly improve cigarette smoking quality Application effect.
(3) it is excellent to have that easy to operate, production cost is low, product aroma strength is high, reaction substrate is readily available etc. by the present invention Point, is easy to industrialized production.
Embodiment
It is noted that described further below is all exemplary, it is intended to provides further instruction to the application.It is unless another Indicate, all technologies used herein and scientific terminology are with usual with the application person of an ordinary skill in the technical field The identical meanings of understanding.
It should be noted that term used herein above is merely to describe embodiment, and be not intended to restricted root According to the illustrative embodiments of the application.As used herein, unless the context clearly indicates otherwise, otherwise singulative It is also intended to include plural form, additionally, it should be understood that, when in this manual using term "comprising" and/or " bag Include " when, it indicates existing characteristics, step, operation, device, component and/or combinations thereof.
The fructus hippophae used in the embodiment of the present invention is purchased from Yizhong (Qingdao) Industrial Co., Ltd..
Embodiment 1：
(1) after dry fructus hippophae being removed into impurity, carry out crushed the processing of 80 mesh sieves, it is standby；
(2) after adding alcohol solvent into above-mentioned Seabuckthorn Fruit, homogenized is carried out using high-speed homogenization machine, is homogenized Sea-buckthorn sample after processing；
(3) the sea-buckthorn sample after homogenized obtained by step (2) is subjected to extract and separate using microwave-assisted extraction technique, obtained Seabuckthorn extraction juice；
(4) Seabuckthorn extraction juice obtained by step (3) is filtered, after vacuum concentration processing, produces rhamnoides extract.
(5) weigh the rhamnoides extract obtained by a certain amount of step (4) to be added in container, then add rhamnoides extract weight 10% Ammonia material, is stirred；Ammonia material is alanine, glutamic acid and phenylalanine in mass ratio 2:3:1 mixing Thing.
(6) mixture obtained through step (5) is added in reactor, with acid or alkali compounds adjust pH value to 10；Acid compound is citric acid, and alkali compounds is the NaOH aqueous solution；
(7) 110 DEG C are heated to, opens cooling and reflux device, constant temperature stirs 3 hours under normal pressure, mixing speed 800 Rev/min, then stop heating, pour out reactant.
(8) by step (7) gained reactant it is filtered, be concentrated under reduced pressure after, the glycerine for adding reactant weight 5% produces Rhamnoides extract Maillard reaction type tobacco aromaticss.
Application Example:
Sea-buckthorn U.S. is drawn in the ratio that the percentage by weight of sea-buckthorn Maillard reaction type tobacco aromaticss and pipe tobacco is 0.05% Moral response type tobacco aromaticss are added in pipe tobacco, add distilled water, moisture in cut tobacco is reached 20 ± 1%, closed storage 2h, with baking Shredded tobacco baking to moisture is 12.5 ± 0.5% under the conditions of 135 DEG C by case, then manual cigarette.
Analyses Methods for Sensory Evaluation Results shows：Applied to can preferably lift cigarette flavor matter in cigarette, increase perfume quantity, increase Oral cavity moisture feeling, improve pleasant impression, there is the application effect for significantly improving cigarette smoking quality.
Embodiment 2：
(1) after dry fructus hippophae being removed into impurity, carry out crushed the processing of 80 mesh sieves, it is standby；
(2) after adding alcohol solvent into above-mentioned Seabuckthorn Fruit, homogenized is carried out using high-speed homogenization machine, is homogenized Sea-buckthorn sample after processing；
(3) the sea-buckthorn sample after homogenized obtained by step (2) is subjected to extract and separate using microwave-assisted extraction technique, obtained Seabuckthorn extraction juice；
(4) Seabuckthorn extraction juice obtained by step (3) is filtered, after vacuum concentration processing, produces rhamnoides extract.
(5) weigh the rhamnoides extract obtained by a certain amount of step (4) to be added in container, then add rhamnoides extract weight 20% Ammonia material, is stirred；Ammonia material is alanine.
(6) mixture obtained through step (5) is added in reactor, pH value is adjusted to 5 with acid or alkali compounds； Acid compound is hydrochloric acid, and alkali compounds is the NaOH aqueous solution；
(7) 90 DEG C are heated to, opens cooling and reflux device, constant temperature stirs 4 hours under normal pressure, mixing speed 800 Rev/min, then stop heating, pour out reactant.
(8) by step (7) gained reactant it is filtered, be concentrated under reduced pressure after, the glycerine for adding reactant weight 2% produces Rhamnoides extract Maillard reaction type tobacco aromaticss.
Embodiment 3：
(1) after dry fructus hippophae being removed into impurity, carry out crushed the processing of 80 mesh sieves, it is standby；
(2) after adding alcohol solvent into above-mentioned Seabuckthorn Fruit, homogenized is carried out using high-speed homogenization machine, is homogenized Sea-buckthorn sample after processing；
(3) the sea-buckthorn sample after homogenized obtained by step (2) is subjected to extract and separate using microwave-assisted extraction technique, obtained Seabuckthorn extraction juice；
(4) Seabuckthorn extraction juice obtained by step (3) is filtered, after vacuum concentration processing, produces rhamnoides extract.
(5) weigh the rhamnoides extract obtained by a certain amount of step (4) to be added in container, then add rhamnoides extract weight 5% Ammonia material, is stirred；Ammonia material is alanine.
(6) mixture obtained through step (5) is added in reactor, with acid or alkali compounds adjust pH value to 12；Acid compound is acetic acid, and alkali compounds is concentrated ammonia liquor；
(7) 120 DEG C are heated to, opens cooling and reflux device, constant temperature stirs 2 hours under normal pressure, mixing speed 800 Rev/min, then stop heating, pour out reactant.
(8) by step (7) gained reactant it is filtered, be concentrated under reduced pressure after, the glycerine for adding reactant weight 3% produces Rhamnoides extract Maillard reaction type tobacco aromaticss.
The preferred embodiment of the application is the foregoing is only, is not limited to the application, for the skill of this area For art personnel, the application can have various modifications and variations.It is all within spirit herein and principle, made any repair Change, equivalent substitution, improvement etc., should be included within the protection domain of the application.

Claims (10)

  1. A kind of 1. preparation method of rhamnoides extract Maillard reaction type tobacco aromaticss, it is characterised in that：Comprise the following steps：
    1) after the fructus hippophae dried removes impurity, crush, cross 80 mesh sieves, it is standby；
    2) organic solvent is added in the Seabuckthorn Fruit obtained into step 1), is extracted, obtains Seabuckthorn extraction juice；
    3) Seabuckthorn extraction juice in step 2) is filtered, concentrated, rhamnoides extract is made；
    4) with Ammonia material Maillard reaction occurs for rhamnoides extract, obtains reaction product；
    5) certain glycerine is added in the reaction product obtained to step 4), produces rhamnoides extract Maillard reaction type cigarette perfume Material.
  2. 2. preparation method according to claim 1, it is characterised in that：In step 2), the organic solvent is absolute ethyl alcohol；
    Preferably, in step 2), extract and separate is carried out using microwave-assisted extraction technique.
  3. 3. preparation method according to claim 1, it is characterised in that：In step 3), carried out using the method for vacuum concentration Concentration, the content of the hippophae rhamnoides for the rhamnoides extract being concentrated to give is 70-95%.
  4. 4. preparation method according to claim 1, it is characterised in that：In step 4), Ammonia material accounts for the matter of rhamnoides extract Amount percentage is 5-30%.
  5. 5. preparation method according to claim 1, it is characterised in that：In step 4), the Ammonia material is alanine, dried meat One kind or more in propylhomoserin, valine, arginine, serine, phenylalanine, glutamic acid, aspartic acid, glycine or tyrosine Kind；
    Preferably, the Ammonia material is alanine, glutamic acid and phenylalanine in mass ratio 2:3:1 mixture.
  6. 6. preparation method according to claim 1, it is characterised in that：In step 4), the pH value of Maillard reaction is 4-12, Preferably 10-12, the temperature of reaction is 80-120 DEG C, and the time of reaction is 2-4 hours；
    Preferably, the material for adjusting the pH value of Maillard reaction is concentrated ammonia liquor, the NaOH aqueous solution, the KOH aqueous solution, Na2HPO4It is water-soluble Liquid, Na2CO3One or more in the aqueous solution, hydrochloric acid, acetic acid, citric acid.
  7. 7. preparation method according to claim 1, it is characterised in that：In step 5), the glycerine of addition accounts for reaction product The 2-5% of weight.
  8. 8. the tobacco aromaticss that any preparation methods of claim 1-7 are prepared.
  9. 9. application of the tobacco aromaticss described in claim 8 in cigarette is prepared.
  10. 10. application according to claim 9, it is characterised in that：Specifically comprise the following steps：
    1) tobacco aromaticss are added in pipe tobacco, the percentage by weight that tobacco aromaticss account for pipe tobacco is 0.02-0.10%；
    2) distilled water is added into pipe tobacco, the moisture for making pipe tobacco is 19-21%；
    3) pipe tobacco is sealed and stored 1-3h, is then 12-13% by shredded tobacco baking to moisture at 130-140 DEG C, is used for Make the pipe tobacco of cigarette.
CN201710728966.0A 2017-08-23 2017-08-23 A kind of preparation method and application of rhamnoides extract Maillard reaction type tobacco aromaticss Pending CN107502449A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109207259A (en) * 2018-07-25 2019-01-15 河南中烟工业有限责任公司 It a kind of maple extract Maillard reaction tobacco aromaticss, preparation method and its does not burn the application in cigarette in heating
CN109536279A (en) * 2018-11-27 2019-03-29 湖北中烟工业有限责任公司 A method of jujube maillard reaction thing is prepared using microwave
CN109864331A (en) * 2019-04-11 2019-06-11 滁州卷烟材料厂 A kind of cigarette flavors additive and preparation method thereof
CN111004683A (en) * 2019-12-26 2020-04-14 贵州中烟工业有限责任公司 Sea-buckthorn fruit essence, production method of sea-buckthorn fruit essence and tobacco product
CN111418884A (en) * 2020-05-20 2020-07-17 云南如茨生物科技有限公司 Cigarette spice

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101469292A (en) * 2007-12-27 2009-07-01 武汉烟草(集团)有限公司 Method for mixedly extracting red date and seabuckthorn fruit for preparing spices for cigarette
CN105861152A (en) * 2016-05-27 2016-08-17 山东中烟工业有限责任公司 Tobacco flavor with sweet smoke and application
CN106244333A (en) * 2016-08-30 2016-12-21 无锡华海香料有限公司 A kind of preparation method and applications of tobacco aromatics using

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101469292A (en) * 2007-12-27 2009-07-01 武汉烟草(集团)有限公司 Method for mixedly extracting red date and seabuckthorn fruit for preparing spices for cigarette
CN105861152A (en) * 2016-05-27 2016-08-17 山东中烟工业有限责任公司 Tobacco flavor with sweet smoke and application
CN106244333A (en) * 2016-08-30 2016-12-21 无锡华海香料有限公司 A kind of preparation method and applications of tobacco aromatics using

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王永华: "《食品风味化学》", 30 June 2015, 中国轻工业出版社 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109207259A (en) * 2018-07-25 2019-01-15 河南中烟工业有限责任公司 It a kind of maple extract Maillard reaction tobacco aromaticss, preparation method and its does not burn the application in cigarette in heating
CN109207259B (en) * 2018-07-25 2022-03-25 河南中烟工业有限责任公司 Maple extract Maillard reaction tobacco flavor, preparation method and application thereof in cigarette heating without combustion
CN109536279A (en) * 2018-11-27 2019-03-29 湖北中烟工业有限责任公司 A method of jujube maillard reaction thing is prepared using microwave
CN109864331A (en) * 2019-04-11 2019-06-11 滁州卷烟材料厂 A kind of cigarette flavors additive and preparation method thereof
CN111004683A (en) * 2019-12-26 2020-04-14 贵州中烟工业有限责任公司 Sea-buckthorn fruit essence, production method of sea-buckthorn fruit essence and tobacco product
CN111418884A (en) * 2020-05-20 2020-07-17 云南如茨生物科技有限公司 Cigarette spice
CN111418884B (en) * 2020-05-20 2021-12-21 云南如茨生物科技有限公司 Cigarette spice

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Application publication date: 20171222