CN111635825A - Snow mountain liquorice essence for cigarette bead blasting, bead blasting prepared from snow mountain liquorice essence and cigarette - Google Patents
Snow mountain liquorice essence for cigarette bead blasting, bead blasting prepared from snow mountain liquorice essence and cigarette Download PDFInfo
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- CN111635825A CN111635825A CN202010421733.8A CN202010421733A CN111635825A CN 111635825 A CN111635825 A CN 111635825A CN 202010421733 A CN202010421733 A CN 202010421733A CN 111635825 A CN111635825 A CN 111635825A
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- parts
- cigarette
- ethyl
- essence
- bead
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 107
- 239000011324 bead Substances 0.000 title claims abstract description 86
- 238000005422 blasting Methods 0.000 title claims abstract description 73
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 title claims abstract description 71
- 244000303040 Glycyrrhiza glabra Species 0.000 title claims abstract description 71
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 title claims abstract description 61
- 235000011477 liquorice Nutrition 0.000 title claims abstract description 61
- XUPYJHCZDLZNFP-UHFFFAOYSA-N butyl butanoate Chemical compound CCCCOC(=O)CCC XUPYJHCZDLZNFP-UHFFFAOYSA-N 0.000 claims abstract description 28
- RGXWDWUGBIJHDO-UHFFFAOYSA-N ethyl decanoate Chemical compound CCCCCCCCCC(=O)OCC RGXWDWUGBIJHDO-UHFFFAOYSA-N 0.000 claims abstract description 28
- TVQGDYNRXLTQAP-UHFFFAOYSA-N ethyl heptanoate Chemical compound CCCCCCC(=O)OCC TVQGDYNRXLTQAP-UHFFFAOYSA-N 0.000 claims abstract description 28
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 claims abstract description 28
- MLFHJEHSLIIPHL-UHFFFAOYSA-N isoamyl acetate Chemical compound CC(C)CCOC(C)=O MLFHJEHSLIIPHL-UHFFFAOYSA-N 0.000 claims abstract description 28
- MDHYEMXUFSJLGV-UHFFFAOYSA-N phenethyl acetate Chemical compound CC(=O)OCCC1=CC=CC=C1 MDHYEMXUFSJLGV-UHFFFAOYSA-N 0.000 claims abstract description 28
- NPNUFJAVOOONJE-ZIAGYGMSSA-N β-(E)-Caryophyllene Chemical compound C1CC(C)=CCCC(=C)[C@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-ZIAGYGMSSA-N 0.000 claims abstract description 28
- XYHKNCXZYYTLRG-UHFFFAOYSA-N 1h-imidazole-2-carbaldehyde Chemical compound O=CC1=NC=CN1 XYHKNCXZYYTLRG-UHFFFAOYSA-N 0.000 claims abstract description 14
- KVKKTLBBYFABAZ-UHFFFAOYSA-N 2-phenylethyl 2-methylbutanoate Chemical compound CCC(C)C(=O)OCCC1=CC=CC=C1 KVKKTLBBYFABAZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- GWYFCOCPABKNJV-UHFFFAOYSA-M 3-Methylbutanoic acid Natural products CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 claims abstract description 14
- 235000005976 Citrus sinensis Nutrition 0.000 claims abstract description 14
- 240000002319 Citrus sinensis Species 0.000 claims abstract description 14
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 claims abstract description 14
- NPNUFJAVOOONJE-UHFFFAOYSA-N beta-cariophyllene Natural products C1CC(C)=CCCC(=C)C2CC(C)(C)C21 NPNUFJAVOOONJE-UHFFFAOYSA-N 0.000 claims abstract description 14
- GWYFCOCPABKNJV-UHFFFAOYSA-N beta-methyl-butyric acid Natural products CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 claims abstract description 14
- NPNUFJAVOOONJE-UONOGXRCSA-N caryophyllene Natural products C1CC(C)=CCCC(=C)[C@@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-UONOGXRCSA-N 0.000 claims abstract description 14
- 229940093503 ethyl maltol Drugs 0.000 claims abstract description 14
- 229940073505 ethyl vanillin Drugs 0.000 claims abstract description 14
- 229940117955 isoamyl acetate Drugs 0.000 claims abstract description 14
- 239000010502 orange oil Substances 0.000 claims abstract description 14
- 150000003505 terpenes Chemical class 0.000 claims abstract description 14
- 235000007586 terpenes Nutrition 0.000 claims abstract description 14
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 claims abstract description 14
- 235000009008 Eriobotrya japonica Nutrition 0.000 claims abstract description 13
- 241000287420 Pyrus x nivalis Species 0.000 claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 claims abstract description 4
- 244000061508 Eriobotrya japonica Species 0.000 claims abstract 2
- 239000007788 liquid Substances 0.000 claims description 42
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 39
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 39
- 239000000839 emulsion Substances 0.000 claims description 38
- 238000009740 moulding (composite fabrication) Methods 0.000 claims description 30
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 claims description 26
- ULDHMXUKGWMISQ-UHFFFAOYSA-N carvone Chemical compound CC(=C)C1CC=C(C)C(=O)C1 ULDHMXUKGWMISQ-UHFFFAOYSA-N 0.000 claims description 26
- NVEQFIOZRFFVFW-RGCMKSIDSA-N caryophyllene oxide Chemical compound C=C1CC[C@H]2O[C@]2(C)CC[C@H]2C(C)(C)C[C@@H]21 NVEQFIOZRFFVFW-RGCMKSIDSA-N 0.000 claims description 26
- PPXUHEORWJQRHJ-UHFFFAOYSA-N ethyl isovalerate Chemical compound CCOC(=O)CC(C)C PPXUHEORWJQRHJ-UHFFFAOYSA-N 0.000 claims description 26
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims description 26
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 26
- 238000000465 moulding Methods 0.000 claims description 26
- WLJVXDMOQOGPHL-UHFFFAOYSA-N phenylacetic acid Chemical compound OC(=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-UHFFFAOYSA-N 0.000 claims description 26
- 229920000858 Cyclodextrin Polymers 0.000 claims description 25
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims description 25
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 17
- 239000000661 sodium alginate Substances 0.000 claims description 17
- 235000010413 sodium alginate Nutrition 0.000 claims description 17
- 229940005550 sodium alginate Drugs 0.000 claims description 17
- 238000001035 drying Methods 0.000 claims description 16
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 15
- 238000001723 curing Methods 0.000 claims description 15
- 239000000600 sorbitol Substances 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 239000008367 deionised water Substances 0.000 claims description 14
- 229910021641 deionized water Inorganic materials 0.000 claims description 14
- NZGWDASTMWDZIW-MRVPVSSYSA-N (+)-pulegone Chemical compound C[C@@H]1CCC(=C(C)C)C(=O)C1 NZGWDASTMWDZIW-MRVPVSSYSA-N 0.000 claims description 13
- WJTCHBVEUFDSIK-NWDGAFQWSA-N (2r,5s)-1-benzyl-2,5-dimethylpiperazine Chemical compound C[C@@H]1CN[C@@H](C)CN1CC1=CC=CC=C1 WJTCHBVEUFDSIK-NWDGAFQWSA-N 0.000 claims description 13
- WLAMNBDJUVNPJU-UHFFFAOYSA-N 2-methylbutyric acid Chemical compound CCC(C)C(O)=O WLAMNBDJUVNPJU-UHFFFAOYSA-N 0.000 claims description 13
- NVEQFIOZRFFVFW-UHFFFAOYSA-N 9-epi-beta-caryophyllene oxide Natural products C=C1CCC2OC2(C)CCC2C(C)(C)CC21 NVEQFIOZRFFVFW-UHFFFAOYSA-N 0.000 claims description 13
- 239000005973 Carvone Substances 0.000 claims description 13
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims description 13
- 239000005770 Eugenol Substances 0.000 claims description 13
- 235000021314 Palmitic acid Nutrition 0.000 claims description 13
- 235000004347 Perilla Nutrition 0.000 claims description 13
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims description 13
- NZGWDASTMWDZIW-UHFFFAOYSA-N Pulegone Natural products CC1CCC(=C(C)C)C(=O)C1 NZGWDASTMWDZIW-UHFFFAOYSA-N 0.000 claims description 13
- USMNOWBWPHYOEA-UHFFFAOYSA-N alpha-thujone Natural products CC1C(=O)CC2(C(C)C)C1C2 USMNOWBWPHYOEA-UHFFFAOYSA-N 0.000 claims description 13
- 229960002903 benzyl benzoate Drugs 0.000 claims description 13
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 claims description 13
- RSYBQKUNBFFNDO-UHFFFAOYSA-N caryophyllene oxide Natural products CC1(C)CC2C(=C)CCC3OC3(C)CCC12C RSYBQKUNBFFNDO-UHFFFAOYSA-N 0.000 claims description 13
- 238000004140 cleaning Methods 0.000 claims description 13
- 229960002217 eugenol Drugs 0.000 claims description 13
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 13
- YYZUSRORWSJGET-UHFFFAOYSA-N octanoic acid ethyl ester Natural products CCCCCCCC(=O)OCC YYZUSRORWSJGET-UHFFFAOYSA-N 0.000 claims description 13
- 229930007459 p-menth-8-en-3-one Natural products 0.000 claims description 13
- 229960003424 phenylacetic acid Drugs 0.000 claims description 13
- 239000003279 phenylacetic acid Substances 0.000 claims description 13
- 239000006187 pill Substances 0.000 claims description 13
- UAXOELSVPTZZQG-UHFFFAOYSA-N tiglic acid Natural products CC(C)=C(C)C(O)=O UAXOELSVPTZZQG-UHFFFAOYSA-N 0.000 claims description 13
- 229930007850 β-damascenone Natural products 0.000 claims description 13
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 11
- RVGRUAULSDPKGF-UHFFFAOYSA-N Poloxamer Chemical compound C1CO1.CC1CO1 RVGRUAULSDPKGF-UHFFFAOYSA-N 0.000 claims description 11
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 11
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 11
- 229960000502 poloxamer Drugs 0.000 claims description 11
- 229920001983 poloxamer Polymers 0.000 claims description 11
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 11
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 11
- 125000005456 glyceride group Chemical group 0.000 claims description 10
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- 238000007605 air drying Methods 0.000 claims description 2
- 240000008917 Glycyrrhiza uralensis Species 0.000 claims 2
- 235000000554 Glycyrrhiza uralensis Nutrition 0.000 claims 2
- 244000124853 Perilla frutescens Species 0.000 claims 1
- 230000000391 smoking effect Effects 0.000 abstract description 8
- 235000009508 confectionery Nutrition 0.000 abstract description 7
- 239000000779 smoke Substances 0.000 abstract description 6
- IAEGWXHKWJGQAZ-UHFFFAOYSA-N trimethylpyrazine Chemical compound CC1=CN=C(C)C(C)=N1 IAEGWXHKWJGQAZ-UHFFFAOYSA-N 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 5
- 244000061176 Nicotiana tabacum Species 0.000 abstract description 3
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 3
- 239000000686 essence Substances 0.000 abstract 6
- 210000001124 body fluid Anatomy 0.000 abstract 1
- 239000010839 body fluid Substances 0.000 abstract 1
- 230000001737 promoting effect Effects 0.000 abstract 1
- MTZQAGJQAFMTAQ-UHFFFAOYSA-N ethyl benzoate Chemical compound CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 description 22
- 241000229722 Perilla <angiosperm> Species 0.000 description 12
- 239000000203 mixture Substances 0.000 description 12
- 241001092070 Eriobotrya Species 0.000 description 11
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical compound C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 11
- 241000801118 Lepidium Species 0.000 description 11
- 238000007493 shaping process Methods 0.000 description 11
- 239000000463 material Substances 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- 235000001453 Glycyrrhiza echinata Nutrition 0.000 description 6
- 235000017382 Glycyrrhiza lepidota Nutrition 0.000 description 6
- 229940010454 licorice Drugs 0.000 description 6
- 238000000605 extraction Methods 0.000 description 5
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 4
- 229910001424 calcium ion Inorganic materials 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 235000017443 Hedysarum boreale Nutrition 0.000 description 3
- 235000007858 Hedysarum occidentale Nutrition 0.000 description 3
- 239000003995 emulsifying agent Substances 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 239000001947 glycyrrhiza glabra rhizome/root Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 230000007547 defect Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- 239000001606 7-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2S,3R,4R,5R,6S)-3,4,5-trihydroxy-6-methyloxan-2-yl]oxyoxan-2-yl]oxy-5-hydroxy-2-(4-hydroxyphenyl)chroman-4-one Substances 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010016952 Food poisoning Diseases 0.000 description 1
- 208000019331 Foodborne disease Diseases 0.000 description 1
- 241001071795 Gentiana Species 0.000 description 1
- 241000501743 Gentiana macrophylla Species 0.000 description 1
- 241000207923 Lamiaceae Species 0.000 description 1
- 206010068319 Oropharyngeal pain Diseases 0.000 description 1
- 240000005373 Panax quinquefolius Species 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 229920001213 Polysorbate 20 Polymers 0.000 description 1
- 244000046146 Pueraria lobata Species 0.000 description 1
- 235000010575 Pueraria lobata Nutrition 0.000 description 1
- 208000019790 abdominal distention Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 239000011162 core material Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 201000006549 dyspepsia Diseases 0.000 description 1
- 238000011067 equilibration Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- DFPMSGMNTNDNHN-ZPHOTFPESA-N naringin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1O[C@H]1[C@H](OC=2C=C3O[C@@H](CC(=O)C3=C(O)C=2)C=2C=CC(O)=CC=2)O[C@H](CO)[C@@H](O)[C@@H]1O DFPMSGMNTNDNHN-ZPHOTFPESA-N 0.000 description 1
- 229940052490 naringin Drugs 0.000 description 1
- 229930019673 naringin Natural products 0.000 description 1
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 description 1
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 description 1
- 230000001007 puffing effect Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Abstract
The invention relates to a snow mountain liquorice essence for cigarette bead blasting, and bead blasting and cigarettes prepared from the essence, and belongs to the technical field of tobacco essences. The radix glycyrrhizae essence comprises radix glycyrrhizae extract, loquat extract, snow pear extract, ethyl vanillin, perillaseed, 2-methylbutyric acid-2-phenethyl ester, 2, 3, 5 trimethyl pyrazine, sweet orange oil terpene, phenethyl acetate, caprolactone, ethyl maltol, isoamyl acetate, isovaleric acid, butyl butyrate, ethyl decanoate, ethyl heptanoate, beta-caryophyllene and other components. The invention applies the nature and the effect of the radix glycyrrhizae from the snow mountain to the bead blasting essence for the cigarette, develops the bead blasting essence for the cigarette with the function of relieving the uncomfortable feeling of the throat, improves the comfort of cigarette smoking, promotes the sweet and moist feeling of cigarette smoking, reduces the chocking feeling in the cigarette smoke, achieves the effect of promoting the production of body fluid, and has higher application value and popularization significance.
Description
Technical Field
The invention belongs to the technical field of tobacco essence, and particularly relates to a snow mountain liquorice essence for cigarette bead blasting, and bead blasting and cigarettes prepared from the essence.
Background
Xueshan Licorice root, which is the dried root and stem of Gentiana pseudolaricis of Labiatae, is distributed mainly in the northwest of Yunnan province and the southwest of Sichuan province. Gentiana macrophylla, also known as Rough Tokyo, Licorice root, Shang Licorice root, American ginseng, Bai Yuan Shen, Bai Xuan Shen, perennial herb, is a tonifying Chinese herbal medicine. Sweet and bitter in taste and cool in nature, and has the effects of clearing away heat and toxic materials, regulating qi and strengthening spleen. It is often used for treating dyspepsia, abdominal distention, and sore throat, and relieving food poisoning.
The existing cigarettes often have the characteristics of poor sweet feeling, poor sweet return, large smoke irritation and the like in the smoking process, although the comfort of the cigarettes can be improved by the bead-blasting cigarettes, the improvement contribution degree is limited, and the bead blasting using the Xueshan liquorice as the main characteristic fragrance raw material is not available, so that the application of the Xueshan liquorice essence for bead blasting in the cigarettes is influenced to a certain extent.
Therefore, how to overcome the defects of the prior art and enrich the satisfaction and the sweet feeling of the cigarette in the smoking process by using the flavor of the radix glycyrrhizae preparata in the snow mountain is a problem to be solved in the technical field of the bead puffing of the cigarette at present.
Disclosure of Invention
The invention aims to solve the defects of the prior art and provides a Xueshan liquorice essence for cigarette bead blasting, and a bead blasting and a cigarette prepared from the essence.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight:
4.50-13.50 parts of a snow mountain liquorice extract; 2.00-4.50 parts of loquat extract; 2.25-5.25 parts of snow pear extract; 0.50-2.50 parts of ethyl vanillin; 1.15-1.35 parts of perilla seed; 0.05-2.55 parts of 2-methylbutyric acid; 0.45-0.85 part of 2-methylbutyric acid-2-phenethyl ester; 2. 0.50-1.50 parts of 3, 5-trimethyl pyrazine; sweet orange oil terpene 0.45-1.75 weight portions; 0.15-1.15 parts of phenethyl acetate; 0.35-0.75 parts of caprolactone; 0.15-0.60 part of ethyl maltol; 0.50-1.10 parts of isoamyl acetate; isovaleric acid 0.10-0.30 weight portions; 0.50-1.35 parts of butyl butyrate; 0.05-0.15 part of ethyl decanoate; 0.05-1.35 parts of ethyl heptanoate; 0.15-0.45 part of beta-caryophyllene; 0.80-1.35 parts of eugenol; 0.60-1.10 parts of caryophyllene oxide; 0.10-1.25 parts of phenylacetic acid; 0.30-0.55 part of pulegone; 0.10-0.25 part of carvone; 0.15-0.45 part of acetic acid; 0.20-0.50 part of ethyl acetate; 0.05-0.15 part of palmitic acid; 0.55-0.95 part of ethyl caprylate; 0.05-0.15 part of benzyl benzoate; 0.50-1.50 parts of ethyl isovalerate; 0.35-0.75 part of damascenone.
The preparation method of the Xueshan licorice essence is to directly and physically mix the components until the components are uniform.
The invention also provides a cigarette bead, and the content of the bead is the snow mountain liquorice essence for the cigarette bead.
Further, preferably, the content of the essence of the glycyrrhiza glabra in the blasting beads is 5-45 mu L/granule.
The invention also provides a preparation method of the cigarette blasting bead, which comprises the following steps:
step (1), preparing an emulsion: according to the weight parts, 610 parts of caprylic/capric glyceride 490-42, 1-3 parts of anhydrous calcium chloride, 0.5-1.5 parts of sodium carboxymethylcellulose, 0.05-1.00 part of cyclodextrin, 2-5 parts of poloxamer and 270 parts of radix glycyrrhizae essence 230-30 are stirred together at the temperature of 30-50 ℃ and the rotating speed of 40-80r/min for 20-30min to obtain emulsion;
step (2), preparing a forming liquid: according to the weight parts, 90-110 parts of deionized water, 1-3 parts of sodium alginate, 0.5-1.0 part of sorbitol, 0.1-0.3 part of cyclodextrin and 200.1-0.5 part of tween-200 are stirred together for 20-30min at the rotating speed of 40-80r/min under the condition of 15-45 ℃ to obtain a molding liquid;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid at a dripping speed of 5-7 drops/s through dripping equipment, curing and forming, cleaning and drying to obtain the cigarette blasting beads.
Further, in the step (3), it is preferable that the curing molding is carried out under a condition of equilibration at a temperature of 20 ℃ and a relative humidity of 60% RH for 24 hours.
Further, in the step (3), the drying method is preferably air drying.
Further, it is preferable that, in the step (3), the diameter of the produced cigarette bead is 2.0mm to 4.5mm, and the crushing pressure is 0.7kgf to 1.7 kgf.
The invention further provides a cigarette containing the cigarette blasting bead.
Further, it is preferred that a cigarette popping bead is placed in the center of the cigarette filter to provide a better smoking experience. For example, if the length of the filter stick is 25mm, the center of the cigarette bead is 12.5 mm.
The preparation method of the radix glycyrrhizae extract, the loquat extract and the snow pear extract is preferably obtained by adopting a supercritical carbon dioxide extraction mode, and the extraction conditions are as follows: extraction flow rate: 17 g/min, extraction pressure: 250 Bar, extraction temperature: extraction time at 51 ℃: 2 h; but is not limited to this method.
The invention adopts an interfacial film forming method to prepare the blasting beads, and the principle is that the wall material glue solution and calcium ions can generate a crosslinking reaction to form a compact film so as to realize the embedding of the core material essence. Mixing and stirring water, essence, a thickening agent, an emulsifier and calcium ions according to a certain proportion to obtain an emulsion with certain fluidity, preparing a sodium alginate wall material glue solution according to a certain proportion, dripping the emulsion into the sodium alginate solution at a certain speed through dripping equipment, curing and forming, and washing, drying and screening to obtain the bead blasting for cigarettes.
The invention adopts part of materials with the following functions: 1. sodium alginate: the main raw material of the wall material of the blasting bead is crosslinked with calcium ions to form a film, and the irreversible moisture-proof performance of the film is good; 2. calcium chloride: improving calcium ions required by film formation; 3. cyclodextrin: a filler to increase the solid solution concentration; 4. poloxamer: emulsifier, improve the surface activity of liquid; 5. sorbitol: the toughening agent has good moisture retention and can increase the toughness of the wall material; 6. sodium carboxymethylcellulose: thickening agent to increase liquid viscosity; 7. tween-20: emulsifiers, improve the surface tension of liquids; 8. caprylic capric acid glyceride: used as essential oil to prepare emulsion.
Compared with the prior art, the invention has the beneficial effects that:
the invention applies the nature and the effect of the radix glycyrrhizae from the snow mountain to the bead blasting essence for the cigarette, develops the bead blasting essence for the cigarette with the function of relieving the uncomfortable feeling of the throat, improves the comfort of cigarette smoking, promotes the sweet feeling of cigarette smoking, increases the feeling of smoke moistening, reduces the irritating feeling and the irritating feeling of entering the throat in the cigarette smoke, and has higher application value and popularization significance.
The invention applies the extract of the plant with Yunnan characteristics, namely the extract of the snow mountain liquorice, to cigarettes in an exploded bead form, and creates a tobacco brand with Yunnan characteristics. The snow mountain licorice essence for bead blasting can obtain the fragrance of the snow mountain licorice essence through the matching of various raw materials, and because essential oil is not adopted as the raw material of the essence, the chemical components and the content of the snow mountain licorice essence for bead blasting are fixed, the snow mountain licorice essence is not influenced by external factors such as production conditions, storage environment, manufacturers and the like, and the stability of the quality of the snow mountain licorice essence for bead blasting is favorably ensured.
Detailed Description
The present invention will be described in further detail with reference to examples.
It will be appreciated by those skilled in the art that the following examples are illustrative of the invention only and should not be taken as limiting the scope of the invention. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The materials or equipment used are not indicated by manufacturers, and all are conventional products available by purchase.
Example 1
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 4.50 parts of a snow mountain liquorice extract according to parts by weight; 2.00 parts of loquat extract; 2.25 parts of snow pear extract; 0.50 part of ethyl vanillin; 1.15 parts of perilla pepperweed; 0.05 part of 2-methylbutyric acid; 0.45 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.50 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.45; 0.15 part of phenethyl acetate; 0.35 part of caprolactone; 0.15 part of ethyl maltol; 0.50 part of isoamyl acetate; 0.50 part of octalactone; 0.10 part of isovaleric acid; 0.50 part of butyl butyrate; 0.05 part of ethyl decanoate; 0.05 part of ethyl heptanoate; 0.15 part of beta-caryophyllene; 0.20 part of 2-furan ethyl benzoate; 0.80 part of eugenol; 0.60 part of caryophyllene oxide; 0.10 part of phenylacetic acid and 0.30 part of pulegone; 0.10 part of carvone; 0.15 part of acetic acid; 0.20 part of ethyl acetate; 0.05 part of palmitic acid; 0.55 part of ethyl caprylate; 0.05 part of benzyl benzoate; 0.50 part of ethyl isovalerate; 0.35 part of damascenone.
Preparing an emulsion: according to the weight portion, 90 portions of deionized water, 1 portion of sodium alginate, 0.5 portion of sorbitol, 0.1 portion of cyclodextrin and 200.1 portions of tween-200 are stirred together for 20min at the rotating speed of 40r/min under the condition of 15 ℃ until the mixture is uniformly mixed, and the emulsion is obtained.
Preparing a forming liquid: according to the parts by weight, 90 parts of deionized water, 1 part of sodium alginate, 0.5 part of sorbitol, 0.1 part of cyclodextrin and 200.1 parts of tween-200 are stirred together for 20min at the rotating speed of 40r/min under the condition of 15 ℃ until the components are uniformly mixed, so as to obtain the molding liquid.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the Xueshan liquorice popping X1.
And placing the Xueshan liquorice essence bead blasting X1 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice bead blasting cigarette C1.
Example 2
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 13.50 parts of a snow mountain liquorice extract according to parts by weight; 4.50 parts of loquat extract; 5.25 parts of snow pear extract; 2.50 parts of ethyl vanillin; 1.35 parts of perilla pepperweed; 2.55 parts of 2-methylbutyric acid; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.50 parts of 3, 5-trimethyl pyrazine; 1.75 parts of sweet orange oil terpene; 1.15 parts of phenethyl acetate; 0.75 part of caprolactone; 0.60 part of ethyl maltol; 1.10 parts of isoamyl acetate; 1.50 parts of octalactone; 0.30 part of isovaleric acid; 1.35 parts of butyl butyrate; 0.15 part of ethyl decanoate; 1.35 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.55 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 1.10 parts of caryophyllene oxide; 1.25 parts of phenylacetic acid and 0.55 part of pulegone; 0.25 part of carvone; 0.45 part of acetic acid; 0.50 part of ethyl acetate; 0.15 part of palmitic acid; 0.95 part of ethyl caprylate; 0.15 part of benzyl benzoate; 1.50 parts of ethyl isovalerate; 0.75 part of damascenone.
Preparing an emulsion: according to the weight parts, 610 parts of caprylic capric glyceride, 3 parts of anhydrous calcium chloride, 1.5 parts of sodium carboxymethylcellulose, 1.00 part of cyclodextrin, 5 parts of poloxamer and 270 parts of radix glycyrrhizae uralensis essence are stirred together at the temperature of 50 ℃ at the rotating speed of 80r/min for 30min until the materials are uniformly mixed to obtain an emulsion;
preparing a forming liquid: according to the weight parts, 110 parts of deionized water, 3 parts of sodium alginate, 1.0 part of sorbitol, 0.3 part of cyclodextrin and 200.5 parts of tween-200 are stirred together for 30min at the rotating speed of 80r/min at the temperature of 45 ℃ until the mixture is uniformly mixed, so as to obtain a forming liquid;
and (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 7 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the Xueshan liquorice popping X2.
And placing the Xueshan liquorice essence bead blasting X2 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice bead blasting cigarette C2.
Example 3
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 6.50 parts of a snow mountain liquorice extract according to parts by weight; 3.20 parts of loquat extract; 3.35 parts of snow pear extract; 1.15 parts of ethyl vanillin; 1.25 parts of perilla pepperweed; 1.35 parts of 2-methylbutyric acid; 0.60 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.00 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.85 weight portions; 0.25 part of phenethyl acetate; 0.45 part of caprolactone; 0.25 part of ethyl maltol; 0.75 part of isoamyl acetate; 0.90 part of octalactone; 0.20 part of isovaleric acid; 0.70 part of butyl butyrate; 0.10 part of ethyl decanoate; 0.55 part of ethyl heptanoate; 0.25 part of beta-caryophyllene; 0.35 part of 2-furan ethyl benzoate; 0.95 part of eugenol; 0.75 part of caryophyllene oxide; 0.55 part of phenylacetic acid and 0.35 part of pulegone; 0.15 part of carvone; 0.25 part of acetic acid; 0.35 part of ethyl acetate; 0.10 part of palmitic acid; 0.70 part of ethyl caprylate; 0.10 part of benzyl benzoate; 0.75 part of ethyl isovalerate; 0.45 part of damascenone.
Preparing an emulsion: according to the weight parts, 550 parts of caprylic/capric glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethylcellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 250 parts of radix glycyrrhizae essence are stirred together at 40 ℃ at the rotating speed of 60r/min for 25min until the components are uniformly mixed, and the emulsion is obtained.
Preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 6 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the Xueshan liquorice popping X3.
And placing the Xueshan liquorice essence bead blasting X3 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice bead blasting cigarette C3.
Example 4
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 12.50 parts of a snow mountain liquorice extract according to parts by weight; 3.50 parts of loquat extract; 4.75 parts of snow pear extract; 1.85 parts of ethyl vanillin; 1.30 parts of perilla pepperweed; 2.35 parts of 2-methylbutyric acid; 0.80 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.25 parts of 3, 5-trimethyl pyrazine; 1.55 parts of sweet orange oil terpene; 1.00 part of phenethyl acetate; 0.60 part of caprolactone; 0.45 part of ethyl maltol; 0.95 part of isoamyl acetate; 1.35 parts of octalactone; 0.20 part of isovaleric acid; 1.15 parts of butyl butyrate; 0.10 part of ethyl decanoate; 1.05 parts of ethyl heptanoate; 0.40 part of beta-caryophyllene; 0.45 part of 2-furan ethyl benzoate; 1.20 parts of eugenol; 0.90 part of caryophyllene oxide; 1.05 parts of phenylacetic acid and 0.45 part of pulegone; 0.20 part of carvone; 0.35 part of acetic acid; 0.40 part of ethyl acetate; 0.10 part of palmitic acid; 0.75 part of ethyl caprylate; 0.10 part of benzyl benzoate; 1.20 parts of ethyl isovalerate; 0.60 part of damascenone.
Preparing an emulsion: according to the weight parts, 550 parts of caprylic/capric glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethylcellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 250 parts of radix glycyrrhizae essence are stirred together at 40 ℃ at the rotating speed of 60r/min for 25min until the components are uniformly mixed, and the emulsion is obtained.
Preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the Xueshan liquorice popping X4.
And placing the Xueshan liquorice essence bead blasting X4 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice bead blasting cigarette C4.
Comparative example 1
The essence for the cigarette bead blasting comprises the following components in parts by weight: 4.50 parts of loquat extract according to parts by weight; 5.25 parts of snow pear extract; 2.50 parts of ethyl vanillin; 1.35 parts of perilla pepperweed; 2.55 parts of 2-methylbutyric acid; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.50 parts of 3, 5-trimethyl pyrazine; 1.75 parts of sweet orange oil terpene; 1.15 parts of phenethyl acetate; 0.75 part of caprolactone; 0.60 part of ethyl maltol; 1.10 parts of isoamyl acetate; 1.50 parts of octalactone; 0.30 part of isovaleric acid; 1.35 parts of butyl butyrate; 0.15 part of ethyl decanoate; 1.35 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.55 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 1.10 parts of caryophyllene oxide; 1.25 parts of phenylacetic acid and 0.55 part of pulegone; 0.25 part of carvone; 0.45 part of acetic acid; 0.50 part of ethyl acetate; 0.15 part of palmitic acid; 0.95 part of ethyl caprylate; 0.15 part of benzyl benzoate; 1.50 parts of ethyl isovalerate; 0.75 part of damascenone.
Preparing an emulsion: according to the weight parts, 510 parts of caprylic/capric glyceride, 2 parts of anhydrous calcium chloride, 1 part of sodium carboxymethylcellulose, 0.5 part of cyclodextrin, 2.5 parts of poloxamer and 220 parts of essence are stirred together at the temperature of 40 ℃ at the rotating speed of 60r/min for 25min to obtain an emulsion;
preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60 percent RH, curing and molding, cleaning, and drying to obtain the bead X5.
And placing the blasting bead X5 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice blasting bead cigarette C5.
Comparative example 2
The essence for the cigarette bead blasting comprises the following components in parts by weight: 13.50 parts of a snow mountain liquorice extract according to parts by weight; 5.25 parts of snow pear extract; 2.50 parts of ethyl vanillin; 1.35 parts of perilla pepperweed; 2.55 parts of 2-methylbutyric acid; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.50 parts of 3, 5-trimethyl pyrazine; 1.75 parts of sweet orange oil terpene; 1.15 parts of phenethyl acetate; 0.75 part of caprolactone; 0.60 part of ethyl maltol; 1.10 parts of isoamyl acetate; 1.50 parts of octalactone; 0.30 part of isovaleric acid; 1.35 parts of butyl butyrate; 0.15 part of ethyl decanoate; 1.35 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.55 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 1.10 parts of caryophyllene oxide; 1.25 parts of phenylacetic acid and 0.55 part of pulegone; 0.25 part of carvone; 0.45 part of acetic acid; 0.50 part of ethyl acetate; 0.15 part of palmitic acid; 0.95 part of ethyl caprylate; 0.15 part of benzyl benzoate; 1.50 parts of ethyl isovalerate; 0.75 part of damascenone.
Preparing an emulsion: according to the weight parts, 490 parts of caprylic/capric glyceride, 1 part of anhydrous calcium chloride, 0.5 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 2 parts of poloxamer and 280 parts of essence are stirred together at 40 ℃ and the rotating speed of 60r/min for 25min to obtain the emulsion.
Preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60 percent RH, curing and molding, cleaning, and drying to obtain the bead X6.
And placing the blasting bead X6 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice blasting bead cigarette C6.
Comparative example 3
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 13.50 parts of a snow mountain liquorice extract according to parts by weight; 4.50 parts of loquat extract; 2.50 parts of ethyl vanillin; 1.35 parts of perilla pepperweed; 2.55 parts of 2-methylbutyric acid; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.50 parts of 3, 5-trimethyl pyrazine; 1.75 parts of sweet orange oil terpene; 1.15 parts of phenethyl acetate; 0.75 part of caprolactone; 0.60 part of ethyl maltol; 1.10 parts of isoamyl acetate; 1.50 parts of octalactone; 0.30 part of isovaleric acid; 1.35 parts of butyl butyrate; 0.15 part of ethyl decanoate; 1.35 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.55 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 1.10 parts of caryophyllene oxide; 1.25 parts of phenylacetic acid and 0.55 part of pulegone; 0.25 part of carvone; 0.45 part of acetic acid; 0.50 part of ethyl acetate; 0.15 part of palmitic acid; 0.95 part of ethyl caprylate; 0.15 part of benzyl benzoate; 1.50 parts of ethyl isovalerate; 0.75 part of damascenone.
Preparing an emulsion: according to the weight parts, 490 parts of caprylic capric glyceride, 1 part of anhydrous calcium chloride, 0.5 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 2 parts of poloxamer and 280 parts of radix glycyrrhizae uralensis essence are stirred together at 40 ℃ and the rotating speed of 60r/min for 25min to obtain the emulsion.
Preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the Xueshan liquorice popping X7.
And placing the Xueshan liquorice essence bead blasting X7 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice bead blasting cigarette C7.
Comparative example 4
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 13.50 parts of kudzu root extract according to parts by weight; 4.50 parts of loquat extract; 5.25 parts of snow pear extract; 2.50 parts of ethyl vanillin; 1.35 parts of perilla pepperweed; 2.55 parts of 2-methylbutyric acid; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.50 parts of 3, 5-trimethyl pyrazine; 1.75 parts of sweet orange oil terpene; 1.15 parts of phenethyl acetate; 0.75 part of caprolactone; 0.60 part of ethyl maltol; 1.10 parts of isoamyl acetate; 1.50 parts of octalactone; 0.30 part of isovaleric acid; 1.35 parts of butyl butyrate; 0.15 part of ethyl decanoate; 1.35 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.55 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 1.10 parts of caryophyllene oxide; 1.25 parts of phenylacetic acid and 0.55 part of pulegone; 0.25 part of carvone; 0.45 part of acetic acid; 0.50 part of ethyl acetate; 0.15 part of palmitic acid; 0.95 part of ethyl caprylate; 0.15 part of benzyl benzoate; 1.50 parts of ethyl isovalerate; 0.75 part of damascenone.
Preparing an emulsion: according to the weight parts, 490 parts of caprylic capric glyceride, 1 part of anhydrous calcium chloride, 0.5 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 2 parts of poloxamer and 280 parts of radix glycyrrhizae uralensis essence are stirred together at 40 ℃ and the rotating speed of 60r/min for 25min to obtain the emulsion.
Preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60 percent RH, curing and molding, cleaning, and drying to obtain the bead X8.
And placing the bead blasting X8 into a cigarette filter stick, and receiving a cigarette sample to obtain the bead blasting cigarette C8.
Comparative example 5
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 13.50 parts of a snow mountain liquorice extract according to parts by weight; 9.75 parts of naringin; 2.50 parts of ethyl vanillin; 1.35 parts of perilla pepperweed; 2.55 parts of 2-methylbutyric acid; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.50 parts of 3, 5-trimethyl pyrazine; 1.75 parts of sweet orange oil terpene; 1.15 parts of phenethyl acetate; 0.75 part of caprolactone; 0.60 part of ethyl maltol; 1.10 parts of isoamyl acetate; 1.50 parts of octalactone; 0.30 part of isovaleric acid; 1.35 parts of butyl butyrate; 0.15 part of ethyl decanoate; 1.35 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.55 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 1.10 parts of caryophyllene oxide; 1.25 parts of phenylacetic acid and 0.55 part of pulegone; 0.25 part of carvone; 0.45 part of acetic acid; 0.50 part of ethyl acetate; 0.15 part of palmitic acid; 0.95 part of ethyl caprylate; 0.15 part of benzyl benzoate; 1.50 parts of ethyl isovalerate; preparing 0.75 part of damascenone emulsion: according to the weight parts, 490 parts of caprylic capric glyceride, 1 part of anhydrous calcium chloride, 0.5 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 2 parts of poloxamer and 280 parts of radix glycyrrhizae uralensis essence are stirred together at 40 ℃ and the rotating speed of 60r/min for 25min to obtain the emulsion.
Preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the Xueshan liquorice popping X9.
And placing the Xueshan liquorice essence bead blasting X9 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice bead blasting cigarette C9.
Comparative example 6
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 3.00 parts of a snow mountain liquorice extract according to parts by weight; 1.50 parts of loquat extract; 2.00 parts of snow pear extract; 2.50 parts of ethyl vanillin; 1.35 parts of perilla pepperweed; 2.55 parts of 2-methylbutyric acid; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.50 parts of 3, 5-trimethyl pyrazine; 1.75 parts of sweet orange oil terpene; 1.15 parts of phenethyl acetate; 0.75 part of caprolactone; 0.60 part of ethyl maltol; 1.10 parts of isoamyl acetate; 1.50 parts of octalactone; 0.30 part of isovaleric acid; 1.35 parts of butyl butyrate; 0.15 part of ethyl decanoate; 1.35 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.55 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 1.10 parts of caryophyllene oxide; 1.25 parts of phenylacetic acid and 0.55 part of pulegone; 0.25 part of carvone; 0.45 part of acetic acid; 0.50 part of ethyl acetate; 0.15 part of palmitic acid; 0.95 part of ethyl caprylate; 0.15 part of benzyl benzoate; 1.50 parts of ethyl isovalerate; 0.75 part of damascenone.
Preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the Xueshan liquorice popping X10.
And placing the Xueshan liquorice essence bead blasting X10 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice bead blasting cigarette C10.
Comparative example 7
The snow mountain liquorice essence for cigarette bead blasting comprises the following components in parts by weight: 15.00 parts of a snow mountain liquorice extract; 5.00 parts of loquat extract; 6.00 parts of snow pear extract; 2.50 parts of ethyl vanillin; 1.35 parts of perilla pepperweed; 2.55 parts of 2-methylbutyric acid; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.50 parts of 3, 5-trimethyl pyrazine; 1.75 parts of sweet orange oil terpene; 1.15 parts of phenethyl acetate; 0.75 part of caprolactone; 0.60 part of ethyl maltol; 1.10 parts of isoamyl acetate; 1.50 parts of octalactone; 0.30 part of isovaleric acid; 1.35 parts of butyl butyrate; 0.15 part of ethyl decanoate; 1.35 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.55 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 1.10 parts of caryophyllene oxide; 1.25 parts of phenylacetic acid and 0.55 part of pulegone; 0.25 part of carvone; 0.45 part of acetic acid; 0.50 part of ethyl acetate; 0.15 part of palmitic acid; 0.95 part of ethyl caprylate; 0.15 part of benzyl benzoate; 1.50 parts of ethyl isovalerate; 0.75 part of damascenone.
Preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/s by using dripping equipment, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the Xueshan liquorice popping X11.
And placing the Xueshan liquorice essence bead blasting X11 into a cigarette filter stick, and receiving a cigarette sample to obtain the Xueshan liquorice bead blasting cigarette C11.
Smoking evaluation is carried out on the cigarette samples of the Xueshan liquorice essence bead-exploded cigarettes C1-C11 and the cigarettes filled with blanks (without essence bead-exploded cigarettes) according to Chinese cigarette evaluation standards, and the results are detailed in Table 1.
TABLE 1
From the above review results, it can be seen that: the C1-C4 has stable quality, not only well solves the problems of reduced penetrability and fineness and the like of the Xueshan liquorice bead-blown cigarette which does not conform to the protection range of C5-C11 of the invention, but also further improves the aroma quality of the cigarette, further increases the aroma amount, further increases the sweetness and penetrability of the smoke, and ensures that the smoke is more exquisite and the aftertaste is more comfortable. Meanwhile, the obvious degree of the radix glycyrrhizae decrepitation in the snow mountain and the preference degree of smokers are both improved, the sensory quality score is improved by more than 2.4 points, and the method has important practical value. Compared with the blank cigarettes, the C5-C11 has the advantages that various indexes are slightly reduced, and the problems of reduced penetrability, fineness and the like of partial cigarettes are solved although the fragrance amount and the sweet return feeling are obviously increased.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (9)
1. The snow mountain liquorice essence for cigarette bead blasting is characterized by comprising the following components in parts by weight:
4.50-13.50 parts of a snow mountain liquorice extract; 2.00-4.50 parts of loquat extract; 2.25-5.25 parts of snow pear extract; 0.50-2.50 parts of ethyl vanillin; 1.15-1.35 parts of perilla seed; 0.05-2.55 parts of 2-methylbutyric acid; 0.45-0.85 part of 2-methylbutyric acid-2-phenethyl ester; 2. 0.50-1.50 parts of 3, 5-trimethyl pyrazine; sweet orange oil terpene 0.45-1.75 weight portions; 0.15-1.15 parts of phenethyl acetate; 0.35-0.75 parts of caprolactone; 0.15-0.60 part of ethyl maltol; 0.50-1.10 parts of isoamyl acetate; isovaleric acid 0.10-0.30 weight portions; 0.50-1.35 parts of butyl butyrate; 0.05-0.15 part of ethyl decanoate; 0.05-1.35 parts of ethyl heptanoate; 0.15-0.45 part of beta-caryophyllene; 0.80-1.35 parts of eugenol; 0.60-1.10 parts of caryophyllene oxide; 0.10-1.25 parts of phenylacetic acid; 0.30-0.55 part of pulegone; 0.10-0.25 part of carvone; 0.15-0.45 part of acetic acid; 0.20-0.50 part of ethyl acetate; 0.05-0.15 part of palmitic acid; 0.55-0.95 part of ethyl caprylate; 0.05-0.15 part of benzyl benzoate; 0.50-1.50 parts of ethyl isovalerate; 0.35-0.75 part of damascenone.
2. A cigarette blasting bead, characterized in that the content of the blasting bead is the essence of the glycyrrhiza uralensis for the cigarette blasting bead of claim 1.
3. The cigarette blasting bead according to claim 2, wherein the content of the glycyrrhiza uralensis essence in the blasting bead is 5-45 μ L per bead.
4. The method of producing the cigarette blasting bead of claim 2, comprising the steps of:
step (1), preparing an emulsion: according to the weight parts, 610 parts of caprylic/capric glyceride 490-42, 1-3 parts of anhydrous calcium chloride, 0.5-1.5 parts of sodium carboxymethylcellulose, 0.05-1.00 part of cyclodextrin, 2-5 parts of poloxamer and 270 parts of radix glycyrrhizae essence 230-30 are stirred together at the temperature of 30-50 ℃ and the rotating speed of 40-80r/min for 20-30min to obtain emulsion;
step (2), preparing a forming liquid: according to the weight parts, 90-110 parts of deionized water, 1-3 parts of sodium alginate, 0.5-1.0 part of sorbitol, 0.1-0.3 part of cyclodextrin and 200.1-0.5 part of tween-200 are stirred together for 20-30min at the rotating speed of 40-80r/min under the condition of 15-45 ℃ to obtain a molding liquid;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid at a dripping speed of 5-7 drops/s through dripping equipment, curing and forming, cleaning and drying to obtain the cigarette blasting beads.
5. The method for producing the cigarette blasting bead according to claim 4, wherein in the step (3), the curing and forming conditions are an equilibrium temperature of 20 ℃ and a relative humidity of 60% RH for 24 hours.
6. The method for preparing cigarette blasting beads according to claim 4, wherein in the step (3), the drying manner is air drying.
7. The method for producing cigarette blasting beads according to claim 4, wherein in the step (3), the produced cigarette blasting beads have a diameter of 2.0mm to 4.5mm and a crushing pressure of 0.7kgf to 1.7 kgf.
8. A cigarette comprising the cigarette popping bead of claim 2 or 3.
9. The cigarette of claim 8, wherein one cigarette bead is inserted into the center of the cigarette filter.
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Application publication date: 20200908 |