CN109868184A - A kind of Radix Glycyrrhizae cigarette quick-fried pearl essence and its application in cigarette - Google Patents
A kind of Radix Glycyrrhizae cigarette quick-fried pearl essence and its application in cigarette Download PDFInfo
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- CN109868184A CN109868184A CN201910099121.9A CN201910099121A CN109868184A CN 109868184 A CN109868184 A CN 109868184A CN 201910099121 A CN201910099121 A CN 201910099121A CN 109868184 A CN109868184 A CN 109868184A
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- radix glycyrrhizae
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Abstract
The invention discloses a kind of Radix Glycyrrhizae cigarettes to apply with quick-fried pearl essence and its in cigarette.With quick-fried pearl essence by licorice, Siraitia grosvenorii, Ethyl vanillin, methyl cinnamate, geraniol, 2,3,5- trimethylpyrazines, vanillic aldehyde, methyl maltol and Xin Kui acid glyceride are composed Radix Glycyrrhizae cigarette of the invention.Using the essence can Radix Glycyrrhizae cigarette processed with quick-fried pearl, the quick-fried pearl filter stick of Radix Glycyrrhizae cigarette and the quick-fried pearl cigarette of Radix Glycyrrhizae.The quick-fried pearl cigarette of Radix Glycyrrhizae bakes fragrant and sweet, improvement with abundant cigarette and takes out food mouthfeel, reduces cigarette stimulation, the sweet sense of increase flue gas and cover miscellaneous gas with good effect, has learning value and application prospect.
Description
Technical field
The invention belongs to cigarette filter rod production technical fields, and in particular to the quick-fried pearl essence of a kind of Radix Glycyrrhizae and its in cigarette
Using.
Technical background
Radix Glycyrrhizae (Glycyrrhiza uralensis Fisch.) is the plant of pulse family Glycyrrhiza, be widely used in medicine,
Food, cosmetics, tobacco and animal husbandry etc..It is widely applied and is potentially worth, scientific research personnel, scholar, doctor in face of it
The people in each field such as teacher and peasant are also more and more deep to its understanding and research.Radix Glycyrrhizae has good moistening lung, cough-relieving, dispels
Phlegm function.
Chinese medicine thinks that Radix Glycyrrhizae has the effect of invigorating middle warmer and replenishing QI, relieving spasm to stop pain, moistening lung to arrest cough, purging fire for removing toxin, coordinating the drug actions of a prescription, is
" state old " in medicine, is one of most common Chinese medicinal material, and most of Traditional Chinese medicinal prescription has all been arranged in pairs or groups Radix Glycyrrhizae, so-called " ten sides nine
Grass ", especially because its sweet taste can cover the toil taste of other medicinal materials, use more in TCM Pediatrics prescription.
A kind of new technology of " quick-fried pearl is assigned fragrant " as perfuming cigarette is strong to some table perfume (or spice) fragrance to show cigarette characteristic wind again
The fragrance of lattice carries out " cladding ", not volatile, crushes quick-fried pearl in suction, can experience the fragrance of distinctive style fragrance with
Mouthfeel is perfuming cigarette to volatile and grade can show that the flavoring of the fragrance of cigarette distinctive style has special effect again
A kind of innovative technology has widened the application range of cigarette flavors, enriches the distinctive style of cigarette, improves the product of smoking property of cigarette
Matter.
Summary of the invention
It is an object of that present invention to provide a kind of quick-fried pearl essence of Radix Glycyrrhizae with Radix Glycyrrhizae distinctive style, are used for the quick-fried pearl of cigarette filter rod
In, the quick-fried pearl filter stick of Radix Glycyrrhizae is made, is produced into the quick-fried pearl cigarette of Radix Glycyrrhizae, the distinctive style of horn of plenty cigarette provides important material base
With important academic application value and application prospect, special requisition this patent.
A kind of cigarette provided by the present invention is constituted and (is calculated in mass percent) with the quick-fried pearl essence of Radix Glycyrrhizae by following components:
1. the licorice of 8.0-14.0%；
2. the Fructus Monordicae extract of 2.0-7.0%；
3. the Ethyl vanillin of 0.4-0.5%；
4. the methyl cinnamate of 0.4-1.1%；
5. the geraniol of 0.1-0.4%；
6. the 2 of 1.1-2.0%, 3,5- trimethylpyrazines；
7. the vanillic aldehyde of 0.6-1.0%；
8. the methyl maltol of 0.1-1.0%；
9. surplus is pungent certain herbaceous plants with big flowers acid glyceride.
The licorice is the ethanol extract of Radix Glycyrrhizae；
The pungent certain herbaceous plants with big flowers acid glycerol vinegar is the product of the fatty acid containing 8-12 carbochain and glycerine esterification.
The licorice, is prepared with following steps:
1. Radix Glycyrrhizae is cut into pieces shape, in the round-bottomed baked bottle of 2000 milliliters of merging；
2. the ethanol solution of mass fraction (Radix Glycyrrhizae: 95% ethanol water=1:7) is added into the Radix Glycyrrhizae bottle of step 1.,
It is heated to reflux on about 100 DEG C of water-bath 4 hours；
3. extracting solution 2. is filtered, filtrate is concentrated under reduced pressure under conditions of 50 DEG C, 55Kpa into paste, and no distillate evaporates
Out, extract obtained is licorice.
The quick-fried pearl essence of the Radix Glycyrrhizae cigarette, the licorice that optimization formula is 1. 11.0%；2. 4.0% Siraitia grosvenorii；
3. 4.3% Ethyl vanillin；4. 0.8% methyl cinnamate；5. 0.25% geraniol；6. the 2 of 1.5%, 3,5- front threes
Base pyrazine；7. 0.7% vanillic aldehyde；8. 0.5% methyl maltol；9. 76.95% pungent certain herbaceous plants with big flowers acid glyceride.
The mouthfeel of the formula of the quick-fried pearl essence of different Radix Glycyrrhizae cigarettes, expression is different.The not same feeling can be modulated according to different formulas
The quick-fried pearl essence for seeing characteristic, manufactures the cigarette of different sensory characteristics, meets different consumer demands.
The Radix Glycyrrhizae cigarette is to be with quick-fried pearl with quick-fried pearl, the cigarette with Radix Glycyrrhizae cigarette prepared by the quick-fried pearl essence of Radix Glycyrrhizae with quick-fried pearl
Prepared essence is coated in the quick-fried pearl of a sealing by finger with high molecular material, quick-fried at one kind with the circular quick-fried pearl of sealing
The diameter of pearl is 2-4 millimeters, and essence carrying capacity is 20-25 microlitres/in quick-fried pearl,
As a kind of quick-fried pearl diameter of preparation is 3.5 millimeters, weight is 28 milligrams/, essence volume carrying capacity is 22 in quick-fried pearl
Microlitre/.
Application of the quick-fried pearl of Radix Glycyrrhizae in cigarette, is to be placed in Radix Glycyrrhizae cigarette among cigarette filter rod with quick-fried pearl, Radix Glycyrrhizae is made
Quick-fried pearl cigarette.
The Radix Glycyrrhizae cigarette developed in the present invention has significantly abundant cigarette perfume, improvement mouthfeel, enhancing flue gas sweet with quick-fried pearl
Degree reduces stimulation and covers the effect of miscellaneous gas.
In short, the present invention provides a kind of Radix Glycyrrhizae cigarette quick-fried pearl essence, the distinctive distinctive style of cigarette Radix Glycyrrhizae is shown, to rich
The cigarette perfume of rich cigarette improves to take out and eats mouthfeel, reduces cigarette stimulation, increases the sweet sense of flue gas and cover miscellaneous gas with effect well
Fruit has a good application prospect.
Specific embodiment
Below with reference to example, the present invention will be further described.
The preparation process of quick-fried pearl of cigarette described in example is introduced first.
Cigarette mainly uses shunting with the technology that quick-fried pearl produces -- and drop method preparation technique is produced in liquid, i.e., using cold
But the shearing force cutting rubber column gel column that oil liquidates, completes quick-fried droplet system.Using the different cooling oil of two incident angles in solenoid
Shearing force is formed, by the wall material and the cutting of core liquid during lower drop, condenses balling-up by the effect of surface tension in cooling oil,
It deoiled, dried, being sieved etc. after programs, quick-fried pearl is made.
Licorice used in following examples, is prepared with following methods:
1. the Radix Glycyrrhizae purchased in the market is cut into 200 grams of sheet, it is placed in 2000 milliliters of round-bottomed baked bottle, adds 1500 grams
95% ethanol solution is heated to reflux 4 hours on 100 DEG C of water-bath, and cooling filters out extracting solution, and filtrate is in 50 DEG C, 55Kpa
Under conditions of be concentrated under reduced pressure at paste, no distillate distillates, obtain 28 grams of extract be licorices.
2. other raw materials used in example are such as: Siraitia grosvenorii, Ethyl vanillin, methyl cinnamate, geraniol, 2,3,5- front threes
Base pyrazine, vanillic aldehyde, methyl maltol, pungent certain herbaceous plants with big flowers acid glyceride are purchased in fragrance in the market.
Embodiment 1
Radix Glycyrrhizae cigarette in this example is composed of the following components with quick-fried pearl essence: 8% licorice；2.0% Siraitia grosvenorii；
0.4% Ethyl vanillin；0.4% methyl cinnamate；0.1% geraniol；The 2 of 1.1%, 3,5- trimethylpyrazines；0.6% chinese cymbidium
Element；0.1% methyl maltol and 87.3% pungent certain herbaceous plants with big flowers acid glyceride, the amount of each component is calculated in mass percent.
It is 3.5 millimeters that the quick-fried pearl essence of this Radix Glycyrrhizae, which is prepared into diameter, and essence volume carrying capacity is 22 microlitres/in quick-fried pearl,
As a kind of quick-fried pearl diameter of preparation is 3.5 millimeters, weight is 26 milligrams/, essence volume carrying capacity is 22 in quick-fried pearl
Microlitre/, as Radix Glycyrrhizae cigarette are with quick-fried pearl.
Radix Glycyrrhizae cigarette is placed in filter stick center with quick-fried pearl by filter-stick forming device, is made an addition in cigarette filter rod, quick-fried pearl position is
Among filter stick, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick, is Radix Glycyrrhizae cigarette after cigarette cigarette sample with quick-fried pearl cigarette.
To Radix Glycyrrhizae cigarette with quick-fried pearl cigarette, by 11 judging panel members of the sensory evaluation committee, to the sample and blank sample
Carry out control evaluation, the results showed that there is abundant cigarette to bake distinctive style that is fragrant and sweet, highlighting cigarette glycyrrhizin moisture feeling, reduce
It stimulates, cover that miscellaneous gas, to increase the sense of flue gas smoothness, pleasant impression comfortable.But flue gas shows slightly elegant.
With blank sample comparative analysis, three qualifieds of flue gas.
Embodiment 2
Radix Glycyrrhizae cigarette in this example is composed of the following components with quick-fried pearl essence: 14% licorice；7.0% Siraitia grosvenorii；
0.5% Ethyl vanillin；1.1% methyl cinnamate；0.4% geraniol；The 2 of 2.0%, 3,5- trimethylpyrazines；1.0% chinese cymbidium
Element；1.0% methyl maltol and 73.0% pungent certain herbaceous plants with big flowers acid glyceride, the amount of each component is calculated in mass percent.
It is 3.5 millimeters that the quick-fried pearl essence of this Radix Glycyrrhizae, which is prepared into diameter, and essence carrying capacity is 22 microlitres/in quick-fried pearl,
As a kind of quick-fried pearl diameter of preparation is 3.5 millimeters, weight is 26 milligrams/, essence volume carrying capacity is 22 in quick-fried pearl
Microlitre/, as Radix Glycyrrhizae cigarette are with quick-fried pearl.
Radix Glycyrrhizae cigarette is placed in filter stick center with quick-fried pearl by filter-stick forming device, is made an addition in cigarette filter rod, quick-fried pearl position is
Among filter stick, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick, is Radix Glycyrrhizae cigarette after cigarette cigarette sample with quick-fried pearl cigarette.
To Radix Glycyrrhizae cigarette with quick-fried pearl cigarette, by 11 judging panel members of the sensory evaluation committee, to the sample and blank sample
Carry out control evaluation, the results showed that there is abundant cigarette to bake distinctive style that is fragrant and sweet, highlighting cigarette glycyrrhizin moisture feeling, reduce
It stimulates, cover that miscellaneous gas, to increase the sense of flue gas smoothness, pleasant impression comfortable.But characteristic shaddock is fragrant and sweet slightly to influence cigarette perfume, drops cigarette perfume slightly
It is low.
With blank sample comparative analysis, three qualifieds of flue gas.
Embodiment 3
Radix Glycyrrhizae cigarette in this example is composed of the following components with quick-fried pearl essence: 11.0% licorice；4.0% sieve
Chinese fruit；4.3% Ethyl vanillin；0.8% methyl cinnamate；0.25% geraniol；The 2 of 1.5%, 3,5- trimethyl pyrroles
Piperazine；0.7% vanillic aldehyde；0.5% methyl maltol；76.95% pungent certain herbaceous plants with big flowers acid glyceride, the amount of each component is with quality percentage
Number meter.
It is 3.5 millimeters that the quick-fried pearl essence of this Radix Glycyrrhizae, which is prepared into diameter, and essence carrying capacity is 22 microlitres/in quick-fried pearl,
As a kind of quick-fried pearl diameter of preparation is 3.5 millimeters, weight is 26 milligrams/, essence volume carrying capacity is 22 in quick-fried pearl
Microlitre/, as Radix Glycyrrhizae cigarette are with quick-fried pearl.
Radix Glycyrrhizae cigarette is placed in filter stick center with quick-fried pearl by filter-stick forming device, is made an addition in cigarette filter rod, quick-fried pearl position is
Among filter stick, every cigarette adds a quick-fried pearl, as quick-fried pearl filter stick, is Radix Glycyrrhizae cigarette after cigarette cigarette sample with quick-fried pearl cigarette.
To Radix Glycyrrhizae cigarette with quick-fried pearl cigarette, by 11 judging panel members of the sensory evaluation committee, to the sample and blank sample
Carry out control evaluation, the results showed that there is abundant cigarette to bake distinctive style that is fragrant and sweet, highlighting cigarette glycyrrhizin moisture feeling, reduce
It stimulates, cover that miscellaneous gas, to increase the sense of flue gas smoothness, pleasant impression comfortable, highlight cigarette distinctive style.
With blank sample comparative analysis, three qualifieds of flue gas.
Examples detailed above knot shows: the dosage of licorice and 2,3, if the dosage of 5- trimethylpyrazine is less, although
Have cigarette abundant and bake distinctive style fragrant and sweet, that cigarette glycyrrhizin moisture feeling can be highlighted, there is preferable suction comfort, but
Flue gas is elegant, does not concentrate；If the dosage of licorice and 2, the dosage of 3,5- trimethylpyrazines increases to such as example 2, though
It so shows the distinctive style of Radix Glycyrrhizae, but slightly presses fragrant, cover cigarette perfume fragrance；In example 3, when the dosage of licorice and 2,
When the dosage of 3,5- trimethylpyrazines is moderate, when the dosage of other each fragrance is also moderate, to showing cigarette distinctive style and raising
The comfort level of cigarette smoking has the effect of.
Claims (9)
1. a kind of quick-fried pearl essence of Radix Glycyrrhizae cigarette, which is characterized in that be calculated in mass percent, be made of following components:
1. the licorice of 8.0-14.0%；
2. the Fructus Monordicae extract of 2.0-7.0%；
3. the Ethyl vanillin of 0.4-0.5%；
4. the methyl cinnamate of 0.4-1.1%；
5. the geraniol of 0.1-0.4%；
6. the 2 of 1.1-2.0%, 3,5- trimethylpyrazines；
7. the vanillic aldehyde of 0.6-1.0%；
8. the methyl maltol of 0.1-1.0%；
9. surplus is pungent certain herbaceous plants with big flowers acid glyceride.
2. the quick-fried pearl essence of Radix Glycyrrhizae cigarette as described in claim 1, which is characterized in that be calculated in mass percent, by following components
It constitutes: 11.0% licorice；4.0% Siraitia grosvenorii；4.3% Ethyl vanillin；0.8% methyl cinnamate；
0.25% geraniol；The 2 of 1.5%, 3,5- trimethylpyrazines；0.7% vanillic aldehyde；0.5% methyl maltol；
76.95% pungent certain herbaceous plants with big flowers acid glyceride.
3. the quick-fried pearl essence of Radix Glycyrrhizae cigarette as described in claim 1, which is characterized in that the licorice is the ethyl alcohol of Radix Glycyrrhizae
Extract.
4. the quick-fried pearl essence of Radix Glycyrrhizae cigarette as described in claim 1, which is characterized in that the pungent certain herbaceous plants with big flowers acid glycerol vinegar is to contain 8-12
The fatty acid of a carbochain and the product of glycerine esterification.
5. the quick-fried pearl essence of Radix Glycyrrhizae cigarette as described in claim 1, which is characterized in that the licorice, with following steps
Preparation:
1. Radix Glycyrrhizae is cut into pieces shape, in the round-bottomed baked bottle of 2000 milliliters of merging；
It is Radix Glycyrrhizae: 95% ethanol water=1:7 ethanol solution that 2. mass fraction ratio, which is added, into the Radix Glycyrrhizae bottle of step 1.,
It is heated to reflux on about 100 DEG C of water-bath 4 hours；
3. extracting solution 2. is filtered, filtrate is concentrated under reduced pressure under conditions of 50 DEG C, 55Kpa into paste, and no distillate distillates, institute
Obtaining extract is licorice.
6. Radix Glycyrrhizae cigarette Radix Glycyrrhizae cigarette prepared by quick-fried pearl essence is with quick-fried pearl as described in claim 1-5 is any, it is characterised in that quick-fried
The diameter of pearl is 2-4 millimeters, and essence carrying capacity is 20-25 microlitres/in quick-fried pearl.
7. Radix Glycyrrhizae cigarette as claimed in claim 6 is with quick-fried pearl, it is characterised in that the quick-fried pearl diameter of liquorice essence is 3.5 millimeters, in quick-fried pearl
Essence volume carrying capacity is 22 microlitres/, and weight is 26 milligrams/.
8. application of the Radix Glycyrrhizae cigarette as claimed in claim 7 with quick-fried pearl in cigarette, it is characterised in that, Radix Glycyrrhizae cigarette is added with quick-fried pearl
In filter stick.
9. application of the Radix Glycyrrhizae cigarette as claimed in claim 8 with quick-fried pearl in cigarette, it is characterised in that, Radix Glycyrrhizae cigarette is located at filter with quick-fried pearl
Among stick, a quick-fried pearl is added in every cigarette filter.
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Cited By (3)
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| CN110720658A (en) * | 2019-11-18 | 2020-01-24 | 湖北中烟工业有限责任公司 | Preparation method of acacia flower extract for tobacco bead blasting |
| CN111227297A (en) * | 2020-03-25 | 2020-06-05 | 中国烟草总公司郑州烟草研究院 | Spice composition for blasting beads capable of highlighting baking aroma characteristics of cigarettes, blasting bead aroma base module, blasting beads and cigarettes |
| CN111635825A (en) * | 2020-05-18 | 2020-09-08 | 云南中烟工业有限责任公司 | Snow mountain liquorice essence for cigarette bead blasting, bead blasting prepared from snow mountain liquorice essence and cigarette |
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| Publication number | Priority date | Publication date | Assignee | Title |
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