CN111621362A - Camellia essence for cigarette bead blasting, bead blasting prepared from camellia essence and cigarette - Google Patents
Camellia essence for cigarette bead blasting, bead blasting prepared from camellia essence and cigarette Download PDFInfo
- Publication number
- CN111621362A CN111621362A CN202010420752.9A CN202010420752A CN111621362A CN 111621362 A CN111621362 A CN 111621362A CN 202010420752 A CN202010420752 A CN 202010420752A CN 111621362 A CN111621362 A CN 111621362A
- Authority
- CN
- China
- Prior art keywords
- parts
- cigarette
- bead
- camellia
- blasting
- Prior art date
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- Pending
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 113
- 239000011324 bead Substances 0.000 title claims abstract description 111
- 235000018597 common camellia Nutrition 0.000 title claims abstract description 95
- 238000005422 blasting Methods 0.000 title claims abstract description 79
- 241000209507 Camellia Species 0.000 title claims abstract 9
- 240000001548 Camellia japonica Species 0.000 title description 88
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 45
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 30
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 claims abstract description 30
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 claims abstract description 30
- RGXWDWUGBIJHDO-UHFFFAOYSA-N ethyl decanoate Chemical compound CCCCCCCCCC(=O)OCC RGXWDWUGBIJHDO-UHFFFAOYSA-N 0.000 claims abstract description 30
- PPXUHEORWJQRHJ-UHFFFAOYSA-N ethyl isovalerate Chemical compound CCOC(=O)CC(C)C PPXUHEORWJQRHJ-UHFFFAOYSA-N 0.000 claims abstract description 30
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims abstract description 30
- MLFHJEHSLIIPHL-UHFFFAOYSA-N isoamyl acetate Chemical compound CC(C)CCOC(C)=O MLFHJEHSLIIPHL-UHFFFAOYSA-N 0.000 claims abstract description 30
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 30
- MDHYEMXUFSJLGV-UHFFFAOYSA-N phenethyl acetate Chemical compound CC(=O)OCCC1=CC=CC=C1 MDHYEMXUFSJLGV-UHFFFAOYSA-N 0.000 claims abstract description 30
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 claims abstract description 24
- GAIBLDCXCZKKJE-QRYCCKSOSA-N (-)-Germacrene D Natural products C(C)(C)[C@H]1/C=C/C(=C)CC/C=C(/C)\CC1 GAIBLDCXCZKKJE-QRYCCKSOSA-N 0.000 claims abstract description 15
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 15
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 15
- XYHKNCXZYYTLRG-UHFFFAOYSA-N 1h-imidazole-2-carbaldehyde Chemical compound O=CC1=NC=CN1 XYHKNCXZYYTLRG-UHFFFAOYSA-N 0.000 claims abstract description 15
- KVKKTLBBYFABAZ-UHFFFAOYSA-N 2-phenylethyl 2-methylbutanoate Chemical compound CCC(C)C(=O)OCCC1=CC=CC=C1 KVKKTLBBYFABAZ-UHFFFAOYSA-N 0.000 claims abstract description 15
- GWYFCOCPABKNJV-UHFFFAOYSA-M 3-Methylbutanoic acid Natural products CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 claims abstract description 15
- 235000005976 Citrus sinensis Nutrition 0.000 claims abstract description 15
- 240000002319 Citrus sinensis Species 0.000 claims abstract description 15
- GAIBLDCXCZKKJE-YZJXYJLZSA-N Germacren D Chemical compound CC(C)C/1CC\C(C)=C\CCC(=C)\C=C\1 GAIBLDCXCZKKJE-YZJXYJLZSA-N 0.000 claims abstract description 15
- 235000021314 Palmitic acid Nutrition 0.000 claims abstract description 15
- 229960002903 benzyl benzoate Drugs 0.000 claims abstract description 15
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 claims abstract description 15
- GWYFCOCPABKNJV-UHFFFAOYSA-N beta-methyl-butyric acid Natural products CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 claims abstract description 15
- OJIGFVZZEVQUNV-UHFFFAOYSA-N germacrene D Natural products CC(C)C1CCC=C(/C)CCC(=C)C=C1 OJIGFVZZEVQUNV-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229940117955 isoamyl acetate Drugs 0.000 claims abstract description 15
- GAIBLDCXCZKKJE-UHFFFAOYSA-N isogermacrene D Natural products CC(C)C1CCC(C)=CCCC(=C)C=C1 GAIBLDCXCZKKJE-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229930007744 linalool Natural products 0.000 claims abstract description 15
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000010502 orange oil Substances 0.000 claims abstract description 15
- 150000003505 terpenes Chemical class 0.000 claims abstract description 15
- 235000007586 terpenes Nutrition 0.000 claims abstract description 15
- 229930007850 β-damascenone Natural products 0.000 claims abstract description 15
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 claims abstract description 15
- WJTCHBVEUFDSIK-NWDGAFQWSA-N (2r,5s)-1-benzyl-2,5-dimethylpiperazine Chemical compound C[C@@H]1CN[C@@H](C)CN1CC1=CC=CC=C1 WJTCHBVEUFDSIK-NWDGAFQWSA-N 0.000 claims abstract description 14
- WLAMNBDJUVNPJU-UHFFFAOYSA-N 2-methylbutyric acid Chemical compound CCC(C)C(O)=O WLAMNBDJUVNPJU-UHFFFAOYSA-N 0.000 claims abstract description 14
- YYZUSRORWSJGET-UHFFFAOYSA-N octanoic acid ethyl ester Natural products CCCCCCCC(=O)OCC YYZUSRORWSJGET-UHFFFAOYSA-N 0.000 claims abstract description 14
- UAXOELSVPTZZQG-UHFFFAOYSA-N tiglic acid Natural products CC(C)=C(C)C(O)=O UAXOELSVPTZZQG-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229940073505 ethyl vanillin Drugs 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims description 48
- 239000000839 emulsion Substances 0.000 claims description 37
- UAHWPYUMFXYFJY-UHFFFAOYSA-N beta-myrcene Chemical compound CC(C)=CCCC(=C)C=C UAHWPYUMFXYFJY-UHFFFAOYSA-N 0.000 claims description 28
- TVQGDYNRXLTQAP-UHFFFAOYSA-N ethyl heptanoate Chemical compound CCCCCCC(=O)OCC TVQGDYNRXLTQAP-UHFFFAOYSA-N 0.000 claims description 28
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims description 28
- WLJVXDMOQOGPHL-UHFFFAOYSA-N phenylacetic acid Chemical compound OC(=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-UHFFFAOYSA-N 0.000 claims description 28
- NPNUFJAVOOONJE-ZIAGYGMSSA-N β-(E)-Caryophyllene Chemical compound C1CC(C)=CCCC(=C)[C@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-ZIAGYGMSSA-N 0.000 claims description 28
- 229920000858 Cyclodextrin Polymers 0.000 claims description 27
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims description 27
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 17
- 239000000661 sodium alginate Substances 0.000 claims description 17
- 235000010413 sodium alginate Nutrition 0.000 claims description 17
- 229940005550 sodium alginate Drugs 0.000 claims description 17
- 238000001723 curing Methods 0.000 claims description 16
- 238000000465 moulding Methods 0.000 claims description 16
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 15
- 239000000600 sorbitol Substances 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims description 14
- 239000005770 Eugenol Substances 0.000 claims description 14
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims description 14
- NPNUFJAVOOONJE-UHFFFAOYSA-N beta-cariophyllene Natural products C1CC(C)=CCCC(=C)C2CC(C)(C)C21 NPNUFJAVOOONJE-UHFFFAOYSA-N 0.000 claims description 14
- NPNUFJAVOOONJE-UONOGXRCSA-N caryophyllene Natural products C1CC(C)=CCCC(=C)[C@@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-UONOGXRCSA-N 0.000 claims description 14
- 238000004140 cleaning Methods 0.000 claims description 14
- 239000008367 deionised water Substances 0.000 claims description 14
- 229910021641 deionized water Inorganic materials 0.000 claims description 14
- 229960002217 eugenol Drugs 0.000 claims description 14
- 125000005456 glyceride group Chemical group 0.000 claims description 14
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 14
- 229960003424 phenylacetic acid Drugs 0.000 claims description 14
- 239000003279 phenylacetic acid Substances 0.000 claims description 14
- 239000006187 pill Substances 0.000 claims description 14
- JYVLIDXNZAXMDK-UHFFFAOYSA-N pentan-2-ol Chemical compound CCCC(C)O JYVLIDXNZAXMDK-UHFFFAOYSA-N 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 9
- 238000009740 moulding (composite fabrication) Methods 0.000 claims description 8
- 238000007605 air drying Methods 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- IAEGWXHKWJGQAZ-UHFFFAOYSA-N trimethylpyrazine Chemical compound CC1=CN=C(C)C(C)=N1 IAEGWXHKWJGQAZ-UHFFFAOYSA-N 0.000 abstract description 18
- 230000000391 smoking effect Effects 0.000 abstract description 9
- 235000009508 confectionery Nutrition 0.000 abstract description 7
- 239000003205 fragrance Substances 0.000 abstract description 7
- 239000000779 smoke Substances 0.000 abstract description 5
- 208000002193 Pain Diseases 0.000 abstract description 2
- QUMXDOLUJCHOAY-UHFFFAOYSA-N alpha-methylbenzyl acetate Natural products CC(=O)OC(C)C1=CC=CC=C1 QUMXDOLUJCHOAY-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- MTZQAGJQAFMTAQ-UHFFFAOYSA-N ethyl benzoate Chemical compound CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 description 20
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 13
- RVGRUAULSDPKGF-UHFFFAOYSA-N Poloxamer Chemical compound C1CO1.CC1CO1 RVGRUAULSDPKGF-UHFFFAOYSA-N 0.000 description 13
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 13
- 239000001768 carboxy methyl cellulose Substances 0.000 description 13
- 229960000502 poloxamer Drugs 0.000 description 13
- 229920001983 poloxamer Polymers 0.000 description 13
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 13
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 13
- 238000007493 shaping process Methods 0.000 description 12
- 238000001035 drying Methods 0.000 description 11
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical compound C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 238000000605 extraction Methods 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 4
- 241000208125 Nicotiana Species 0.000 description 4
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 4
- 229910001424 calcium ion Inorganic materials 0.000 description 4
- 239000003995 emulsifying agent Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 235000006467 Camellia japonica Nutrition 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 1
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 229920001213 Polysorbate 20 Polymers 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000011162 core material Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000011067 equilibration Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 229940041616 menthol Drugs 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 description 1
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 description 1
- 239000012745 toughening agent Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
Abstract
The invention relates to camellia essence for cigarette bead blasting, bead blasting prepared from camellia essence and cigarettes, and belongs to the technical field of cigarette essence. The essence comprises components such as camellia extract, ethyl vanillin, oak moss extract, 2-methylbutyric acid, ethyl caprylate, 2-phenylethyl 2-methylbutyrate, 2, 3, 5 trimethyl pyrazine, sweet orange oil terpene, phenylethyl acetate, caprolactone, phenethyl alcohol, isoamyl acetate, germacrene D, linalool, acetic acid, 2-amyl alcohol, palmitic acid, benzyl benzoate, ethyl isovalerate, damascenone, isovaleric acid, acetophenone, ethyl decanoate and the like. The bead blasting agent can improve the comfort of cigarette smoking, improve the sweet feeling of cigarette smoking, reduce the choking feeling in cigarette smoke, reduce the stinging feeling on the tongue surface, has good compatibility of flower fragrance and cigarette fragrance, and has higher application value and popularization significance.
Description
Technical Field
The invention belongs to the technical field of tobacco essence, and particularly relates to camellia essence for cigarette bead blasting, bead blasting prepared from camellia essence and a cigarette.
Background
The bead is a liquid fragrant bead embedded in the tobacco filter tip, which wraps liquid with different types of spices, so that a smoker can break the bead in the smoking process, and the liquid in the bead flows out of the filter stick and is fused into smoke, so that the cigarette has richer and more fragrant mouthfeel, and the smoker can obtain more comfortable experience, thereby being one of important means for perfuming and enhancing the flavor of the cigarette.
Camellia japonica Linne, Theaceae, and plant species belonging to evergreen shrubs and small trees. The existing cigarettes often have the characteristics of poor sweet feeling, poor sweet return, large smoke irritation and the like in the smoking process, although the comfort of the cigarettes can be improved by the bead-blasting cigarettes, the improvement contribution degree is limited, and no bead blasting with camellia as a main aroma characteristic raw material exists, so that the application of the camellia essence for bead blasting in the cigarettes is influenced to a certain extent.
How to overcome the defects of the prior art and enrich the satisfaction and the sweet feeling in the cigarette smoking process by using the camellia fragrance bead blasting, which is the problem to be solved in the technical field of the bead blasting for cigarettes at present.
Disclosure of Invention
The invention aims to solve the defects of the prior art and provides camellia essence for cigarette bead blasting, and bead blasting and cigarettes prepared from camellia essence.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the invention provides a camellia essence for cigarette blasting beads, which comprises the following components in parts by weight:
4.50-12.50 parts of camellia extract; 0.50-2.50 parts of ethyl vanillin; 1.15-1.35 parts of oak moss extract; 0.05-1.55 parts of 2-methylbutyric acid; 0.55-0.95 part of ethyl caprylate; 0.35-0.85 part of 2-methylbutyric acid-2-phenethyl ester; 2. 0.50-1.45 parts of 3, 5-trimethyl pyrazine; sweet orange oil terpene 0.45-1.35 weight portions; 0.15-1.25 parts of phenethyl acetate; 0.35-0.65 part of caprolactone; 0.15-0.95 parts of phenethyl alcohol; 0.50-1.05 parts of isoamyl acetate; 0.10-0.25 part of germacrene D; 0.10-0.25 part of linalool; 0.15-0.45 part of acetic acid; 0.10-0.30 part of 2-pentanol; 0.05-0.15 part of palmitic acid; 0.05-0.15 part of benzyl benzoate; 0.50-1.45 parts of ethyl isovalerate; 0.35-0.65 part of damascenone; isovaleric acid 0.10-0.25 weight portions; 0.10-0.30 part of acetophenone; 0.05-0.15 part of ethyl decanoate; 0.05-1.15 parts of ethyl heptanoate; 0.15-0.45 part of beta-caryophyllene; 0.15-0.45 part of beta-myrcene; 0.80-1.35 parts of eugenol; 0.10-0.50 parts of juniperbene; 0.10-1.05 parts of phenylacetic acid.
The preparation method of the camellia essence is to directly physically mix the components until the components are uniform.
The second aspect of the invention provides a cigarette blasting bead, and the content of the blasting bead is the camellia essence for the cigarette blasting bead.
Further, the content of the camellia essence for cigarette blasting beads in the blasting beads is preferably 5-45 mu L/bead.
Further, it is preferable that the diameter of the bead is 2.0mm to 4.5mm and the crushing pressure of the bead is 0.7kgf to 1.7 kgf.
The third aspect of the invention provides a method for preparing the cigarette blasting bead, which comprises the following steps:
step (1), preparing an emulsion: according to the weight parts, 660 parts of caprylic capric glyceride 510-;
step (2), preparing a forming liquid: according to the weight parts, 90-100 parts of deionized water, 1-3 parts of sodium alginate, 0.5-1.0 part of sorbitol, 0.1-0.3 part of cyclodextrin and 200.1-0.5 part of tween-200 are stirred together under the condition of 15-45 ℃ until the mixture is uniformly mixed to obtain a forming liquid;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid, curing and forming, cleaning, and air-drying to obtain the camellia blasting bead.
Further, it is preferable that, in the step (1), the specific conditions of stirring are: stirring at 40-80r/min for 20-30 min.
Further, it is preferable that, in the step (2), the specific conditions of stirring are: stirring at 40-80r/min for 20-30 min.
Further, it is preferable that, in the step (3), the dropping speed is 5 drops/s.
Further, in the step (3), it is preferable that the curing molding is carried out under a condition of equilibration at a temperature of 20 ℃ and a relative humidity of 60% RH for 24 hours.
The fourth aspect of the invention provides a cigarette with the cigarette blasting bead prepared by the preparation method of the cigarette blasting bead, which specifically comprises the following steps: a cigarette blasting bead is placed in the center of the cigarette filter stick to provide better smoking experience. For example, if the length of the filter stick is 25mm, the center of the cigarette bead is 12.5 mm.
The beneficial effects of the partial materials adopted by the invention are as follows:
1. sodium alginate: the main raw material of the wall material of the blasting bead is crosslinked with calcium ions to form a film, and the irreversible moisture-proof performance of the film is good;
2. calcium chloride: improving calcium ions required by film formation;
3. cyclodextrin: a filler to increase the solid solution concentration;
4. poloxamer: emulsifier, improve the surface activity of liquid;
5. sorbitol: the toughening agent has good moisture retention and can increase the toughness of the wall material;
6. sodium carboxymethylcellulose: thickening agent to increase liquid viscosity;
7. tween-20: emulsifiers, improve the surface tension of liquids;
8. caprylic capric acid glyceride: used as essential oil to prepare emulsion.
The invention adopts an interfacial film forming method to prepare the blasting beads, and the principle is that the wall material glue solution and calcium ions can generate a crosslinking reaction to form a compact film so as to realize the embedding of the core material essence. Mixing and stirring water, essence, a thickening agent, an emulsifier and calcium ions according to a certain proportion to obtain an emulsion with certain fluidity, preparing a sodium alginate wall material glue solution according to a certain proportion, dripping the emulsion into the sodium alginate solution at a certain speed through dripping equipment, curing and forming, and washing, drying and screening to obtain the bead blasting for cigarettes.
The preparation method of the camellia extract is preferably obtained by adopting a supercritical carbon dioxide extraction mode, and the extraction conditions are as follows: when the extraction flow rate is 22g/min, the extraction pressure is as follows: 275 Bar, extraction temperature: 43 ℃, extraction time: 1.5 h; but is not limited to this method.
Compared with the prior art, the invention has the beneficial effects that:
the nature and the effect of the camellia japonica are applied to the bead blasting essence for the cigarettes, the bead blasting essence for the cigarettes with the function of relieving throat discomfort is developed, the comfort of cigarette smoking can be improved through bead blasting, the sweet cigarette smoking feeling of the cigarettes is improved, the choking feeling in cigarette smoke is reduced, the stinging feeling on the tongue surface is reduced, the compatibility of the flower fragrance and the cigarette fragrance is good, and the application value and the popularization significance are high.
The invention provides a special bead blasting essence, namely camellia essence, by taking high-quality camellia with Yunnan characteristics as a raw material and combining a bead blasting technology. When the tobacco is applied to cigarettes, a tobacco brand with Yunnan characteristics can be created.
The camellia essence for blasting beads disclosed by the invention can obtain the fragrance of the camellia essence through the matching of various raw materials, and because the essential oil is not adopted as the raw material of the essence, the chemical components and the content of the camellia essence for blasting beads disclosed by the invention are fixed, the camellia essence is not influenced by external factors such as production conditions, storage environment, manufacturers and the like, and the stability of the quality of the camellia essence for blasting beads is favorably ensured.
Detailed Description
Various exemplary embodiments of the present invention will now be described in detail. It should be noted that: the relative arrangement of the components and steps, the numerical expressions and numerical values set forth in these embodiments do not limit the scope of the present invention unless specifically stated otherwise.
The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses.
Techniques, methods, and apparatus known to those of ordinary skill in the relevant art may not be discussed in detail but are intended to be part of the specification where appropriate.
In all examples shown and discussed herein, any particular value should be construed as merely illustrative, and not limiting. Thus, other examples of the exemplary embodiments may have different values.
The experimental procedures used in the examples below are conventional unless otherwise specified, the materials and reagents used therein are commercially available, and the equipment used in the experiments are well known to those skilled in the art without otherwise specified.
Example 1
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 5.00 parts of camellia extract according to parts by weight; 2.50 parts of ethyl vanillin; 1.35 parts of oak moss extract; 1.55 parts of 2-methylbutyric acid; 0.95 part of ethyl caprylate; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.45 parts of 3, 5-trimethyl pyrazine; 1.35 parts of sweet orange oil terpene; 1.25 parts of phenethyl acetate; 0.65 part of caprolactone; 0.55 part of phenethyl alcohol; 0.55 part of isoamyl acetate; 1.25 parts of octalactone; 0.25 part of germacrene D; 0.25 part of linalool; 0.45 part of acetic acid; 0.25 part of 2-pentanol; 0.15 part of palmitic acid; 0.15 part of benzyl benzoate; 1.45 parts of ethyl isovalerate; 0.60 part of damascenone and 0.25 part of isovaleric acid; 0.30 part of acetophenone; 0.15 part of ethyl decanoate; 1.05 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.45 part of beta-myrcene; 0.45 part of 2-furan ethyl benzoate; 1.35 parts of eugenol; 0.50 parts of juniperbene; 1.00 part of phenylacetic acid.
Preparing an emulsion: according to the weight portion, 660 portions of caprylic capric glyceride, 2 portions of anhydrous calcium chloride, 0.8 portion of sodium carboxymethylcellulose, 0.5 portion of cyclodextrin, 3.5 portions of poloxamer and 220 portions of camellia essence are stirred together for 25min at the rotating speed of 60r/min under the condition of 40 ℃ until the components are uniformly mixed, and the emulsion is obtained.
Preparing a forming liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together at the temperature of 30 ℃ and the rotating speed of 60r/min for 25min until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/S by using dripping equipment, balancing for 24h at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the camellia blasting bead S1.
And (3) placing the camellia essence puffed bead S1 into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia puffed bead cigarette C1.
Example 2
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 6.50 parts of camellia extract according to parts by weight; 1.00 part of ethyl vanillin; 1.20 parts of oak moss extract; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl caprylate; 0.45 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.75 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.65; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of octalactone; 0.15 part of germacrene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-amyl alcohol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.95 part of ethyl heptanoate; 0.20 part of beta-caryophyllene; 0.25 part of beta-myrcene; 0.30 part of 2-furan ethyl benzoate; 0.90 part of eugenol; 0.15 parts of juniperbene; 0.30 part of phenylacetic acid.
Preparing an emulsion: according to the weight parts, 550 parts of caprylic/capric glyceride, 2 parts of anhydrous calcium chloride, 1 part of sodium carboxymethylcellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 240 parts of camellia essence are stirred together at 40-80r/min for 20-30min under the condition of 40 ℃ until the components are uniformly mixed, so as to obtain an emulsion;
preparing a forming liquid: according to the weight parts, 95 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, so as to obtain a forming liquid;
and (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/S by using dripping equipment, balancing for 24h at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the camellia blasting bead S2.
And (3) placing the camellia essence puffed bead S2 into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia puffed bead cigarette C2.
Example 3
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 8.50 parts of camellia extract according to parts by weight; 1.50 parts of ethyl vanillin; 1.25 parts of oak moss extract; 1.05 parts of 2-methylbutyric acid; 0.75 part of ethyl caprylate; 0.65 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.15 parts of 3, 5-trimethyl pyrazine; 1.05 parts of sweet orange oil terpene; 1.05 parts of phenethyl acetate; 0.50 part of caprolactone; 0.75 part of phenethyl alcohol; 0.90 part of isoamyl acetate; 1.05 parts of octalactone; 0.20 part of germacrene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-amyl alcohol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 1.05 parts of ethyl isovalerate; 0.55 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.05-0.95 part of ethyl heptanoate; 0.35 part of beta-caryophyllene; 0.35 part of beta-myrcene; 0.40 part of 2-furan ethyl benzoate; 1.20 parts of eugenol; 0.40 parts of juniperbene; 0.95 part of phenylacetic acid.
Preparing an emulsion: according to the weight parts, 600 parts of caprylic capric glyceride, 2 parts of anhydrous calcium chloride, 1 part of sodium carboxymethylcellulose, 0.5 part of cyclodextrin, 3 parts of poloxamer and 245 parts of camellia essence are stirred together at the temperature of 40 ℃ at the rotating speed of 60r/min for 25min until the components are uniformly mixed, and the emulsion is obtained.
Preparing a forming liquid: according to the weight parts, 95 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, so as to obtain a forming liquid;
and (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/S by using dripping equipment, balancing for 24h at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the camellia blasting bead S3.
And (3) placing the camellia essence puffed bead S3 into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia puffed bead cigarette C3.
Example 4
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 12 parts of camellia extract according to parts by weight; 2.25 parts of ethyl vanillin; 1.25 parts of oak moss extract; 1.45 parts of 2-methylbutyric acid; 0.90 part of ethyl caprylate; 0.80 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.40 parts of 3, 5-trimethyl pyrazine; 1.30 parts of sweet orange oil terpene; 1.20 parts of phenethyl acetate; 0.60 part of caprolactone; 0.90 part of phenethyl alcohol; 1.00 part of isoamyl acetate; 1.25 parts of octalactone; 0.20 part of germacrene D; 0.20 part of linalool; 0.40 part of acetic acid; 0.25 part of 2-pentanol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 1.40 parts of ethyl isovalerate; 0.60 part of damascenone; 0.20 part of isovaleric acid; 0.25 part of acetophenone; 0.10 part of ethyl decanoate; 1.10 parts of ethyl heptanoate; 0.40 part of beta-caryophyllene; 0.40 part of beta-myrcene; 0.40 part of 2-furan ethyl benzoate; 1.30 parts of eugenol; 0.45 part of juniperbene; 1.00 part of phenylacetic acid.
Preparing an emulsion: according to the weight parts, 610 parts of caprylic capric glyceride, 2 parts of anhydrous calcium chloride, 1 part of sodium carboxymethylcellulose, 0.5 part of cyclodextrin, 3 parts of poloxamer and 255 parts of camellia essence are stirred together at the temperature of 40 ℃ and the rotating speed of 60r/min for 25min until the components are uniformly mixed, and the emulsion is obtained.
Preparing a forming liquid: according to the weight parts, 95 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together for 25min at the rotating speed of 60r/min at the temperature of 30 ℃ until the mixture is uniformly mixed, so as to obtain a forming liquid;
and (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/S by using dripping equipment, balancing for 24h at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the camellia blasting bead S4.
And (3) placing the camellia essence puffed bead S4 into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia puffed bead cigarette C4.
Example 5
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 4.50 parts of camellia extract according to parts by weight; 0.50 part of ethyl vanillin; 1.15 parts of oak moss extract; 0.05 part of 2-methylbutyric acid; 0.55 part of ethyl caprylate; 0.35 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.50 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.45; 0.15 part of phenethyl acetate; 0.35 part of caprolactone; 0.15 part of phenethyl alcohol; 0.50 part of isoamyl acetate; 0.10 part of germacrene D; 0.10 part of linalool; 0.15 part of acetic acid; 0.10 part of 2-pentanol; 0.05 part of palmitic acid; 0.05 part of benzyl benzoate; 0.50 part of ethyl isovalerate; 0.35 part of damascenone; 0.10 part of isovaleric acid; 0.10 part of acetophenone; 0.05 part of ethyl decanoate; 0.05 part of ethyl heptanoate; 0.15 part of beta-caryophyllene; 0.15 part of beta-myrcene; 0.80 part of eugenol; 0.10 parts of juniperbene; 0.10 part of phenylacetic acid.
Preparing an emulsion: according to the weight parts, 510 parts of caprylic capric glyceride, 1 part of anhydrous calcium chloride, 0.5 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 2 parts of poloxamer and 220 parts of camellia essence are stirred together at the temperature of 30 ℃ and the rotating speed of 40r/min for 20min until the components are uniformly mixed to obtain emulsion;
preparing a forming liquid: according to the weight parts, 90 parts of deionized water, 1 part of sodium alginate, 0.5 part of sorbitol, 0.1 part of cyclodextrin and 200.1 parts of tween-200 are stirred together for 20min at the rotating speed of 40r/min under the condition of 15 ℃ until the mixture is uniformly mixed, so as to obtain a forming liquid;
and (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/S by using dripping equipment, balancing at the temperature of 20 ℃ and the relative humidity of 60% RH for 24 hours, curing and molding, cleaning, and air-drying to obtain the camellia blasting bead S11.
And (3) placing the camellia essence puffed bead S11 into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia puffed bead cigarette C11.
Example 6
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 12.50 parts of camellia extract according to parts by weight; 2.50 parts of ethyl vanillin; 1.35 parts of oak moss extract; 1.55 parts of 2-methylbutyric acid; 0.95 part of ethyl caprylate; 0.85 part of 2-methyl butyric acid-2-phenethyl ester; 2. 1.45 parts of 3, 5-trimethyl pyrazine; 1.35 parts of sweet orange oil terpene; 1.25 parts of phenethyl acetate; 0.65 part of caprolactone; 0.95 part of phenethyl alcohol; 1.05 parts of isoamyl acetate; 0.25 part of germacrene D; 0.25 part of linalool; 0.45 part of acetic acid; 0.30 part of 2-pentanol; 0.15 part of palmitic acid; 0.15 part of benzyl benzoate; 1.45 parts of ethyl isovalerate; 0.65 part of damascenone; 0.25 part of isovaleric acid; 0.30 part of acetophenone; 0.15 part of ethyl decanoate; 1.15 parts of ethyl heptanoate; 0.45 part of beta-caryophyllene; 0.45 part of beta-myrcene; 1.35 parts of eugenol; 0.50 parts of juniperbene; 1.05 parts of phenylacetic acid.
Preparing an emulsion: according to the weight parts, 660 parts of caprylic capric glyceride, 3 parts of anhydrous calcium chloride, 1.5 parts of sodium carboxymethylcellulose, 1.00 part of cyclodextrin, 5 parts of poloxamer and 260 parts of camellia essence are stirred together at the temperature of 50 ℃ and the rotating speed of 80r/min for 30min until the components are uniformly mixed to obtain emulsion;
preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 3 parts of sodium alginate, 1.0 part of sorbitol, 0.3 part of cyclodextrin and 200.5 parts of tween-200 are stirred together for 30min at the rotating speed of 80r/min at the temperature of 45 ℃ until the mixture is uniformly mixed, so as to obtain a forming liquid;
and (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/S by using dripping equipment, balancing at the temperature of 20 ℃ and the relative humidity of 60% RH for 24 hours, curing and molding, cleaning, and air-drying to obtain the camellia blasting bead S12.
And (3) placing the camellia essence puffed bead S12 into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia puffed bead cigarette C12.
Comparative example 1
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 1.00 parts of ethyl vanillin by weight; 1.20 parts of oak moss extract; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl caprylate; 0.45 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.75 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.65; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of octalactone; 0.15 part of germacrene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-amyl alcohol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.95 part of ethyl heptanoate; 0.20 part of beta-caryophyllene; 0.25 part of beta-myrcene; 0.30 part of 2-furan ethyl benzoate; 0.90 part of eugenol; 0.15 parts of juniperbene; 0.30 part of phenylacetic acid.
Preparing an emulsion: according to the weight portion, 660 portions of caprylic capric glyceride, 2 portions of anhydrous calcium chloride, 1.0 portion of sodium carboxymethylcellulose, 0.5 portion of cyclodextrin, 3.5 portions of poloxamer and 210 portions of camellia essence are stirred together at the temperature of 40 ℃ and the rotating speed of 60r/min for 25min until the components are uniformly mixed.
Preparing a forming liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together at the temperature of 30 ℃ and the rotating speed of 60r/min for 25min until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: and uniformly dripping the emulsion into the forming liquid through dripping equipment at a dripping speed of 5 drops/S, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and forming, cleaning, and drying to obtain the popping S5.
And placing the flavor S5 bead blasting into a cigarette filter stick, and receiving a cigarette sample to obtain the bead blasting cigarette C5.
Comparative example 2
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 6.50 parts of camellia extract according to parts by weight; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl caprylate; 0.45 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.75 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.65; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of octalactone; 0.15 part of germacrene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-amyl alcohol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.95 part of ethyl heptanoate; 0.20 part of beta-caryophyllene; 0.25 part of beta-myrcene; 0.30 part of 2-furan ethyl benzoate; 0.90 part of eugenol; 0.15 parts of juniperbene; 0.30 part of phenylacetic acid.
Preparing an emulsion: according to the weight portion, 660 portions of caprylic capric glyceride, 2 portions of anhydrous calcium chloride, 1.0 portion of sodium carboxymethylcellulose, 0.5 portion of cyclodextrin, 3.5 portions of poloxamer and 210 portions of camellia essence are stirred together at the temperature of 40 ℃ and the rotating speed of 60r/min for 25min until the components are uniformly mixed.
Preparing a forming liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together at the temperature of 30 ℃ and the rotating speed of 60r/min for 25min until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: uniformly dripping the emulsion into the molding liquid at a dripping speed of 5 drops/S by using dripping equipment, balancing for 24h at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and molding, cleaning, and drying to obtain the camellia blasting bead S6.
And (3) putting the camellia essence S6 bead blasting into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia bead blasting cigarette C6.
Comparative example 3
The essence for the cigarette bead blasting comprises the following components in parts by weight: 6.50 parts of rose extract according to parts by weight; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl caprylate; 0.45 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.75 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.65; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of octalactone; 0.15 part of germacrene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-amyl alcohol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.95 part of ethyl heptanoate; 0.20 part of beta-caryophyllene; 0.25 part of beta-myrcene; 0.30 part of 2-furan ethyl benzoate; 0.90 part of eugenol; 0.15 parts of juniperbene; 0.30 part of phenylacetic acid.
Preparing an emulsion: according to the weight parts, 660 parts of caprylic capric glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethylcellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 210 parts of essence are stirred together at the temperature of 40 ℃ at the rotating speed of 60r/min for 25min until the components are uniformly mixed.
Preparing a forming liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together at the temperature of 30 ℃ and the rotating speed of 60r/min for 25min until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: and uniformly dripping the emulsion into the forming liquid through dripping equipment at a dripping speed of 5 drops/S, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and forming, cleaning, and drying to obtain the popping S7.
And (4) placing the S7 exploded beads into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia exploded bead cigarette C7.
Comparative example 4
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 6.50 parts of camellia extract according to parts by weight; 1.25 parts of levorotatory menthol; 0.45 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.75 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.65; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of octalactone; 0.15 part of germacrene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-amyl alcohol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.95 part of ethyl heptanoate; 0.20 part of beta-caryophyllene; 0.25 part of beta-myrcene; 0.30 part of 2-furan ethyl benzoate; 0.90 part of eugenol; 0.15 parts of juniperbene; 0.30 part of phenylacetic acid.
Preparing an emulsion: according to the weight portion, 660 portions of caprylic capric glyceride, 2 portions of anhydrous calcium chloride, 1.0 portion of sodium carboxymethylcellulose, 0.5 portion of cyclodextrin, 3.5 portions of poloxamer and 210 portions of camellia essence are stirred together at the temperature of 40 ℃ and the rotating speed of 60r/min for 25min until the components are uniformly mixed.
Preparing a forming liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together at the temperature of 30 ℃ and the rotating speed of 60r/min for 25min until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: and uniformly dripping the emulsion into the forming liquid through dripping equipment at a dripping speed of 5 drops/S, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and forming, cleaning, and drying to obtain the popping S8.
And (4) placing the S8 exploded beads into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia exploded bead cigarette C8.
Comparative example 5
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: 3.00 parts of camellia extract according to parts by weight; 0.25 part of ethyl vanillin; 1.00 part of oak moss extract; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl caprylate; 0.45 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.75 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.65; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of octalactone; 0.15 part of germacrene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-amyl alcohol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.95 part of ethyl heptanoate; 0.20 part of beta-caryophyllene; 0.25 part of beta-myrcene; 0.30 part of 2-furan ethyl benzoate; 0.90 part of eugenol; 0.15 parts of juniperbene; 0.30 part of phenylacetic acid.
Preparing an emulsion: according to the weight portion, 660 portions of caprylic capric glyceride, 2 portions of anhydrous calcium chloride, 1.0 portion of sodium carboxymethylcellulose, 0.5 portion of cyclodextrin, 3.5 portions of poloxamer and 210 portions of camellia essence are stirred together at the temperature of 40 ℃ and the rotating speed of 60r/min for 25min until the components are uniformly mixed.
Preparing a forming liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together at the temperature of 30 ℃ and the rotating speed of 60r/min for 25min until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: and uniformly dripping the emulsion into the forming liquid through dripping equipment at a dripping speed of 5 drops/S, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and forming, cleaning, and drying to obtain the popping S9.
And (4) placing the S9 exploded beads into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia exploded bead cigarette C9.
Comparative example 6
The camellia essence for the cigarette bead blasting comprises the following components in parts by weight: according to the parts by weight, 15.00 parts of camellia extract; 3.00 parts of ethyl vanillin; 1.50 parts of oak moss extract; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl caprylate; 0.45 part of 2-methyl butyric acid-2-phenethyl ester; 2. 0.75 part of 3, 5 parts of trimethyl pyrazine; sweet orange oil terpene 0.65; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of octalactone; 0.15 part of germacrene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-amyl alcohol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.95 part of ethyl heptanoate; 0.20 part of beta-caryophyllene; 0.25 part of beta-myrcene; 0.30 part of 2-furan ethyl benzoate; 0.90 part of eugenol; 0.15 parts of juniperbene; 0.30 part of phenylacetic acid.
Preparing an emulsion: according to the weight portion, 660 portions of caprylic capric glyceride, 2 portions of anhydrous calcium chloride, 1.0 portion of sodium carboxymethylcellulose, 0.5 portion of cyclodextrin, 3.5 portions of poloxamer and 210 portions of camellia essence are stirred together at the temperature of 40 ℃ and the rotating speed of 60r/min for 25min until the components are uniformly mixed.
Preparing a forming liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 200.3 parts of tween-200 are stirred together at the temperature of 30 ℃ and the rotating speed of 60r/min for 25min until the mixture is uniformly mixed, and the forming liquid is obtained.
And (3) shaping the dropping pills: and uniformly dripping the emulsion into the forming liquid through dripping equipment at a dripping speed of 5 drops/S, balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH, curing and forming, cleaning, and drying to obtain the popping S10.
And (4) placing the S10 exploded beads into a cigarette filter stick, and connecting a cigarette sample to obtain the camellia exploded bead cigarette C10.
The samples of the camellia essence bead-exploded cigarette C1-C12 and the blank (without essence bead-exploded) cigarette are subjected to smoking evaluation according to a Chinese cigarette evaluation method, and the results are detailed in Table 1.
TABLE 1
From the above review results, it can be seen that: compared with the blank cigarette, the sensory quality of the C5-C10 is slightly reduced, all indexes are basically leveled or reduced, and although the fragrance amount and the sweet feeling of partial exploded beads are obviously increased, the problems of reduced penetrability and fineness and the like occur. The C1-C4, C11 and C12 have stable quality, not only well solve the problems of reduced penetrability and fineness and the like of the C5-C10 camellia essence bead-exploded cigarettes which do not accord with the protection range of the invention, but also further improve the aroma quality of the cigarettes, further increase the aroma quantity, further increase the sweet and moist smoke and penetrability caused by the aroma of the camellia, make the aftertaste more comfortable and increase the aftersweet. Meanwhile, the degree of significance of camellia blasting beads and the smoker preference degree are both improved, the sensory quality score is improved by more than 2 points, and the camellia blasting bead has important practical value
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (10)
1. The camellia essence for the cigarette bead blasting is characterized by comprising the following components in parts by weight:
4.50-12.50 parts of camellia extract; 0.50-2.50 parts of ethyl vanillin; 1.15-1.35 parts of oak moss extract; 0.05-1.55 parts of 2-methylbutyric acid; 0.55-0.95 part of ethyl caprylate; 0.35-0.85 part of 2-methylbutyric acid-2-phenethyl ester; 2. 0.50-1.45 parts of 3, 5-trimethyl pyrazine; sweet orange oil terpene 0.45-1.35 weight portions; 0.15-1.25 parts of phenethyl acetate; 0.35-0.65 part of caprolactone; 0.15-0.95 parts of phenethyl alcohol; 0.50-1.05 parts of isoamyl acetate; 0.10-0.25 part of germacrene D; 0.10-0.25 part of linalool; 0.15-0.45 part of acetic acid; 0.10-0.30 part of 2-pentanol; 0.05-0.15 part of palmitic acid; 0.05-0.15 part of benzyl benzoate; 0.50-1.45 parts of ethyl isovalerate; 0.35-0.65 part of damascenone; isovaleric acid 0.10-0.25 weight portions; 0.10-0.30 part of acetophenone; 0.05-0.15 part of ethyl decanoate; 0.05-1.15 parts of ethyl heptanoate; 0.15-0.45 part of beta-caryophyllene; 0.15-0.45 part of beta-myrcene; 0.80-1.35 parts of eugenol; 0.10-0.50 parts of juniperbene; 0.10-1.05 parts of phenylacetic acid.
2. A cigarette blasting bead, characterized in that the content of the blasting bead is the camellia essence for cigarette blasting bead of claim 1.
3. The cigarette blasting bead according to claim 2, wherein the content of camellia essence for cigarette blasting bead in the blasting bead is 5-45 μ L/bead.
4. The cigarette popping bead of claim 2, wherein said popping bead has a diameter gauge of 2.0mm to 4.5mm and a bead breaking pressure of 0.7kgf to 1.7 kgf.
5. The method for preparing the cigarette blasting bead according to any one of claims 2 to 4, characterized by comprising the following steps:
step (1), preparing an emulsion: according to the weight parts, 660 parts of caprylic capric glyceride 510-;
step (2), preparing a forming liquid: according to the weight parts, 90-100 parts of deionized water, 1-3 parts of sodium alginate, 0.5-1.0 part of sorbitol, 0.1-0.3 part of cyclodextrin and 200.1-0.5 part of tween-200 are stirred together under the condition of 15-45 ℃ until the mixture is uniformly mixed to obtain a forming liquid;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid, curing and forming, cleaning, and air-drying to obtain the camellia blasting bead.
6. The method for preparing the cigarette blasting bead according to the claim 5, wherein in the step (1), the specific stirring conditions are as follows: stirring at 40-80r/min for 20-30 min.
7. The method for preparing the cigarette blasting bead according to the claim 5, wherein in the step (2), the specific stirring conditions are as follows: stirring at 40-80r/min for 20-30 min.
8. The method for producing cigarette blasting beads according to claim 5, wherein in the step (3), the dropping speed is 5 drops/s.
9. The method for producing cigarette blasting beads according to claim 5, wherein in the step (3), the conditions for curing and molding are equilibrium at 20 ℃ and 60% RH for 24 hours.
10. A cigarette containing the cigarette blasting beads prepared by the preparation method of the cigarette blasting beads according to any one of claims 5 to 9 is characterized in that one cigarette blasting bead is placed in the center of a cigarette filter stick.
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| CN112048389A (en) * | 2020-09-07 | 2020-12-08 | 泛亚（武汉）食品科技有限公司 | Tea-flavored mint compound essence suitable for bead blasting for cigarettes and preparation method thereof |
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