CN111254015A - Pu' er tea essence bead for cigarettes and preparation method thereof - Google Patents
Pu' er tea essence bead for cigarettes and preparation method thereof Download PDFInfo
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- CN111254015A CN111254015A CN202010202494.7A CN202010202494A CN111254015A CN 111254015 A CN111254015 A CN 111254015A CN 202010202494 A CN202010202494 A CN 202010202494A CN 111254015 A CN111254015 A CN 111254015A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 16
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- ROTNQFPVXVZSRL-UHFFFAOYSA-N 4,4,6-trimethyl-7-oxabicyclo[4.1.0]heptan-2-one Chemical compound C1C(C)(C)CC(=O)C2OC21C ROTNQFPVXVZSRL-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000006468 Thea sinensis Nutrition 0.000 claims abstract description 12
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- 125000005456 glyceride group Chemical group 0.000 claims abstract description 12
- 229940094952 green tea extract Drugs 0.000 claims abstract description 12
- 235000020688 green tea extract Nutrition 0.000 claims abstract description 12
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000009740 moulding (composite fabrication) Methods 0.000 claims description 38
- 239000000839 emulsion Substances 0.000 claims description 30
- 239000007788 liquid Substances 0.000 claims description 30
- 229920000858 Cyclodextrin Polymers 0.000 claims description 19
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000008367 deionised water Substances 0.000 claims description 18
- 229910021641 deionized water Inorganic materials 0.000 claims description 18
- 238000001035 drying Methods 0.000 claims description 15
- 239000011248 coating agent Substances 0.000 claims description 14
- 238000000576 coating method Methods 0.000 claims description 14
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 13
- 238000004043 dyeing Methods 0.000 claims description 13
- 239000000661 sodium alginate Substances 0.000 claims description 13
- 235000010413 sodium alginate Nutrition 0.000 claims description 13
- 229940005550 sodium alginate Drugs 0.000 claims description 13
- 238000004140 cleaning Methods 0.000 claims description 11
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 10
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 10
- RVGRUAULSDPKGF-UHFFFAOYSA-N Poloxamer Chemical compound C1CO1.CC1CO1 RVGRUAULSDPKGF-UHFFFAOYSA-N 0.000 claims description 10
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 10
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 10
- 238000001723 curing Methods 0.000 claims description 10
- 229960000502 poloxamer Drugs 0.000 claims description 10
- 229920001983 poloxamer Polymers 0.000 claims description 10
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 10
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 10
- 239000000600 sorbitol Substances 0.000 claims description 10
- SGHZXLIDFTYFHQ-UHFFFAOYSA-L Brilliant Blue Chemical compound [Na+].[Na+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=2C(=CC=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S([O-])(=O)=O)=C1 SGHZXLIDFTYFHQ-UHFFFAOYSA-L 0.000 claims description 8
- 235000005979 Citrus limon Nutrition 0.000 claims description 8
- 244000131522 Citrus pyriformis Species 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 239000006187 pill Substances 0.000 claims description 6
- 238000007605 air drying Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 238000005422 blasting Methods 0.000 abstract description 23
- 235000013616 tea Nutrition 0.000 abstract description 19
- 230000000391 smoking effect Effects 0.000 abstract description 12
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- 239000002360 explosive Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 11
- 239000000243 solution Substances 0.000 description 11
- 239000000463 material Substances 0.000 description 10
- 239000000779 smoke Substances 0.000 description 10
- 239000003205 fragrance Substances 0.000 description 8
- 230000008569 process Effects 0.000 description 7
- 230000001953 sensory effect Effects 0.000 description 6
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 5
- 229910001424 calcium ion Inorganic materials 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 4
- 206010013911 Dysgeusia Diseases 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000003995 emulsifying agent Substances 0.000 description 3
- 239000003292 glue Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
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- 229920000136 polysorbate Polymers 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- 206010019114 Hand fracture Diseases 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 239000011162 core material Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
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- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
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- 239000002344 surface layer Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 239000012745 toughening agent Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to a Pu' er tea essence bead for cigarettes and a preparation method thereof, belonging to the technical field of bead blasting for cigarettes. The Pu' er tea essence in the puffed bead comprises the following components in percentage by mass: 10-25% of Pu' er green tea extract; 5% -10% of Pu' er black tea extract; 1% -3% of leaf alcohol; 0.5 to 1.5 percent of isophorone oxide; geranylacetone 1% -2.5%; solanesone 0.5% -1.5%; 56.5 to 82 percent of caprylic capric glyceride. The invention is added into the filter tip, when in smoking, the invention has strong explosive power, good penetrability, rich and balanced, rich tea aroma and tobacco aroma are natural, the tea aroma enters the throat softly, the tobacco aroma is full, the residual aroma is remained in the mouth, the invention brings rich sense of relaxation, comfort and satisfaction to consumers, is similar to tea cigarette, but is superior to tea cigarette, and is easy to popularize and apply.
Description
Technical Field
The invention belongs to the technical field of bead blasting for cigarettes, and particularly relates to a Pu' er tea essence bead blasting for cigarettes and a preparation method thereof.
Background
The bead is a liquid fragrant bead embedded in the tobacco filter tip, which wraps the liquid of different types of spices, so that a smoker can break the bead in the smoking process and the liquid in the bead flows out, so that the taste of the cigarette is richer and more fragrant, the smoker can obtain more comfortable experience, and the bead is one of important means for perfuming and enhancing the flavor of the cigarette.
The tea cigarette is a smoldering non-tobacco product which is processed by a process of replacing tobacco leaves with tea leaves as raw materials and preparing cigarettes, and in the smoking process, although the faint scent of the tea leaves is kept, in the smoldering process, miscellaneous gas generated by burning after the tea leaves and burning substances are mixed, influences the smoking experience.
Therefore, how to overcome the defects of the prior art and enrich the satisfaction and the sweetness in the smoking process of cigarettes by using tea aroma bead blasting is a problem to be solved in the technical field of bead blasting for cigarettes at present.
Disclosure of Invention
The invention aims to solve the defects of the prior art and provides a Pu' er tea essence bead for cigarettes and a preparation method thereof.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the Pu' er tea essence bead blasting for the cigarettes comprises the following components in percentage by mass:
10-25% of Pu' er green tea extract; 5% -10% of Pu' er black tea extract; 1% -3% of leaf alcohol; 0.5 to 1.5 percent of isophorone oxide; geranylacetone 1% -2.5%; solanesone 0.5% -1.5%; 56.5 to 82 percent of caprylic capric glyceride.
Further, preferably, the diameter specification of the Pu' er tea essence bead is 2.9mm-3.1mm, the content is 11.5 +/-1.0 mg/granule, the crushing pressure is 0.7kg-1.7kg, and the color is green.
Further, preferably, the Pu' er tea essence in the bead blasting comprises the following components in percentage by mass:
18% of Pu' er green tea extract; 6% of Pu' er black tea extract; 1.5% of leaf alcohol; 0.7 percent of isophorone oxide; geranylacetone 1.2%; solanesone 0.6%; 72% of caprylic/capric glyceride.
The invention also provides a preparation method of the Pu' er tea essence bead for the cigarettes, which comprises the following steps:
step (1), preparing an emulsion: according to the weight portion, 80-100 portions of deionized water, 3-5 portions of anhydrous calcium chloride, 0.5-1 portion of sodium carboxymethylcellulose, 0.05-1 portion of cyclodextrin, 1-5 portions of poloxamer and 300 portions of Pu' er tea essence are stirred together until the components are uniformly mixed to obtain emulsion;
step (2), preparing a forming liquid: according to the parts by weight, 80-100 parts of deionized water, 1-3 parts of sodium alginate, 0.5-1 part of sorbitol, 0.1-0.3 part of cyclodextrin and 800.1-0.3 part of tween-0.3 part are stirred together until the mixture is uniformly mixed to obtain a forming liquid;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning, drying, coating and dyeing to obtain the Pu' er tea puffed beads.
Further, it is preferable to coat and dye with an aqueous solution containing 0.24% by mass of lemon yellow and 0.04% by mass of brilliant blue.
Further, it is preferable that the drying method is air drying.
The invention adopts an interfacial film formation method to prepare the blasting beads, which is also called a chemical film formation method, and the principle is that the wall material glue solution and calcium ions can generate a crosslinking reaction to form a compact film so as to realize the embedding of the core material essence. Mixing and stirring water, essence, a thickening agent, an emulsifier and calcium ions according to a certain proportion to obtain an emulsion with certain fluidity, preparing a sodium alginate wall material glue solution according to a certain proportion, dripping the emulsion into the sodium alginate solution at a certain speed through dripping equipment, curing and forming, and washing, drying and screening to obtain the bead blasting for cigarettes.
The preparation method comprises the following steps:
1. and (4) getting qualified raw and auxiliary materials.
2. Preparation:
① preparing liquid and emulsion, sequentially adding the materials according to the process proportion, dissolving completely, stirring uniformly, refining without insoluble substances and bubbles, and controlling the temperature and viscosity.
② the shaping liquid is prepared by weighing the materials according to the process proportion, dispersing and adding, dissolving completely, stirring evenly, pumping vacuum to make the solution clear and transparent without bubbles, and controlling the viscosity and temperature of the wall material glue solution.
3. And (3) dropwise adding the emulsion into the forming liquid dropwise through a dropwise adding device, ensuring that the forming liquid rotates, avoiding adhesion, and crosslinking calcium ions in the emulsion and sodium alginate in the forming liquid to form a film to obtain the blasting beads.
4. And (4) cleaning, namely cleaning the forming liquid on the surface layer of the blasting bead to avoid adhesion.
5. And (3) air-drying, drying the cleaned exploded beads, flatly laying the dried exploded beads in a balance chamber for balancing for 24 hours at the temperature of 20 ℃ and the relative humidity of 60% RH after certain fluidity is achieved.
6. Coating, balancing the stable bead blasting, coating and dyeing, and ensuring uniform and consistent color.
Compared with the prior art, the invention has the beneficial effects that:
the plant extract with Yunnan characteristics is applied to cigarettes in an exploded bead mode, and a tobacco brand with Yunnan characteristics is created. The bead-blasting flavoring is a flavoring mode with high heat in the current cigarettes, and the Pu ' er tea is a famous and special product in Yunnan, is famous for ' high and durable aroma, unique aroma type and strong and mellow taste ', and is deeply favored by the broad masses. The invention provides a special bead blasting essence, namely Pu 'er tea essence, by taking high-quality Pu' er tea as a raw material and combining a bead blasting technology.
The beneficial effects of the partial materials adopted by the invention are as follows: 1. sodium alginate: the main raw material of the wall material of the blasting bead is crosslinked with calcium ions to form a film, and the irreversible moisture-proof performance of the film is good; 2. calcium chloride: improving calcium ions required by film formation; 3. cyclodextrin: a filler to increase the solid solution concentration; 4. poloxamer: emulsifier, improve the surface activity of liquid; 5. sorbitol: the toughening agent has good moisture retention and can increase the toughness of the wall material; 6. sodium carboxymethylcellulose: thickening agent to increase liquid viscosity; 7. edible pigment: lemon yellow and brilliant blue, beautify appearance, increase the recognition degree of the exploded bead, facilitate distinguishing; 8. tween-80: emulsifier, improve liquid surface tension 9. caprylic capric acid glyceride: used as essential oil to prepare emulsion.
The preparation method ensures the stability of the bead blasting product, and enables the bead blasting to have broken hand feeling and broken sound. The prepared puffed beads are placed into a filter stick to prepare a cigarette, after smoking evaluation, the sensory quality score of the cigarette is improved by 1-2 minutes, the smoke permeability is good, rich and balanced, the full-bodied tea aroma and the tobacco original aroma are natural, the cigarette enters the throat and is soft, the cigarette aroma is full, the residual aroma is left in the mouth, and the full-bodied relaxation feeling, the comfort feeling and the satisfaction feeling are brought to a consumer, and the cigarette is similar to tea cigarette but is superior to the tea cigarette.
Drawings
FIG. 1 is a flow chart of a production process of Pu' er tea essence bead blasting for cigarettes.
Detailed Description
The present invention will be described in further detail with reference to examples.
It will be appreciated by those skilled in the art that the following examples are illustrative of the invention only and should not be taken as limiting the scope of the invention. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The materials or equipment used are not indicated by manufacturers, and all are conventional products available by purchase.
Example 1
The Pu' er tea essence bead blasting for the cigarettes comprises the following components in percentage by mass:
10% of Pu' er green tea extract; 5% of Pu' er black tea extract; 1% of leaf alcohol; 0.5 percent of isophorone oxide; 1% of geranylacetone; solanesone 0.5%; and 82% of caprylic/capric glyceride.
The preparation method of the Pu' er tea essence bead for the cigarette comprises the following steps:
step (1), preparing an emulsion: according to the weight parts, 80 parts of deionized water, 3 parts of anhydrous calcium chloride, 0.5 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 1 part of poloxamer and 260 parts of Pu' er tea essence are stirred together and uniformly mixed to obtain emulsion;
step (2), preparing a forming liquid: according to the weight parts, 80 parts of deionized water, 1 part of sodium alginate, 0.5 part of sorbitol, 0.1 part of cyclodextrin and 800.1 parts of tween-800 are stirred together until the mixture is uniformly mixed to obtain a forming liquid;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning, drying, coating and dyeing to obtain the Pu' er tea puffed beads.
Example 2
The Pu' er tea essence bead blasting for the cigarettes comprises the following components in percentage by mass:
25% of Pu' er green tea extract; 10% of Pu' er black tea extract; 3% of leaf alcohol; 1.5 percent of isophorone oxide; geranylacetone 2.5%; 1.5 percent of solanesone; and 56.5% of caprylic capric glyceride.
The diameter specification of the Pu' er tea essence bead is 2.9mm-3.1mm, the content is 11.5 +/-1.0 mg/bead, the crushing pressure is 0.7kg-1.7kg, and the color is green.
The preparation method of the Pu' er tea essence bead for the cigarette comprises the following steps:
step (1), preparing an emulsion: according to the weight parts, 100 parts of deionized water, 5 parts of anhydrous calcium chloride, 1 part of sodium carboxymethylcellulose, 1 part of cyclodextrin, 5 parts of poloxamer and 300 parts of Pu' er tea essence are stirred together and uniformly mixed to obtain an emulsion;
step (2), preparing a forming liquid: according to the weight parts, 100 parts of deionized water, 3 parts of sodium alginate, 1 part of sorbitol, 0.3 part of cyclodextrin and 800.3 parts of tween are stirred together and uniformly mixed to obtain a forming solution;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning, drying, coating and dyeing to obtain the Pu' er tea puffed beads.
Example 3
The Pu' er tea essence bead blasting for the cigarettes comprises the following components in percentage by mass:
15% of Pu' er green tea extract; 7% of Pu' er black tea extract; 2% of leaf alcohol; 1% of isophorone oxide; 2% of geranylacetone; 1% of solanesone; the balance of caprylic capric glyceride, totaling 100%.
The diameter specification of the Pu' er tea essence bead is 2.9mm-3.1mm, the content is 11.5 +/-1.0 mg/bead, the crushing pressure is 0.7kg-1.7kg, and the color is green.
The preparation method of the Pu' er tea essence bead for the cigarette comprises the following steps:
step (1), preparing an emulsion: according to the weight parts, 90 parts of deionized water, 4 parts of anhydrous calcium chloride, 0.8 part of sodium carboxymethylcellulose, 0.1 part of cyclodextrin, 2 parts of poloxamer and 280 parts of Pu' er tea essence are stirred together and uniformly mixed to obtain emulsion;
step (2), preparing a forming liquid: according to the weight parts, 90 parts of deionized water, 2 parts of sodium alginate, 0.6 part of sorbitol, 0.2 part of cyclodextrin and 800.2 parts of tween are stirred together and uniformly mixed to obtain a forming solution;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning, drying, coating and dyeing to obtain the Pu' er tea puffed beads.
Wherein, the coating and dyeing are carried out by adopting an aqueous solution containing 0.24 percent of lemon yellow and 0.04 percent of brilliant blue by mass concentration. The drying mode is air drying.
Example 4
The Pu' er tea essence bead blasting for the cigarettes comprises the following components in percentage by mass:
18% of Pu' er green tea extract; 6% of Pu' er black tea extract; 1.5% of leaf alcohol; 0.7 percent of isophorone oxide; geranylacetone 1.2%; solanesone 0.6%; 72% of caprylic/capric glyceride.
The diameter specification of the Pu' er tea essence bead is 2.9mm-3.1mm, the content is 11.5 +/-1.0 mg/bead, the crushing pressure is 0.7kg-1.7kg, and the color is green.
The preparation method of the Pu' er tea essence bead for the cigarette comprises the following steps:
step (1), preparing an emulsion: according to the weight parts, 88 parts of deionized water, 4.3 parts of anhydrous calcium chloride, 0.7 part of sodium carboxymethylcellulose, 0.5 part of cyclodextrin, 4 parts of poloxamer and 275 parts of Pu' er tea essence are stirred together and uniformly mixed to obtain an emulsion;
step (2), preparing a forming liquid: according to the weight parts, 95 parts of deionized water, 2.2 parts of sodium alginate, 0.8 part of sorbitol, 0.18 part of cyclodextrin and 800.25 parts of tween-25 are stirred together until the mixture is uniformly mixed to obtain a forming solution;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning, drying, coating and dyeing to obtain the Pu' er tea puffed beads.
Wherein, the coating and dyeing are carried out by adopting an aqueous solution containing 0.24 percent of lemon yellow and 0.04 percent of brilliant blue by mass concentration. The drying mode is air drying.
Application example 1
According to the mass fraction, 5% of Pu ' er green tea extract, 4% of Pu ' er black tea extract, 0.5% of leaf alcohol, 0.3% of isophorone oxide, 0.5% of geranylacetone, 0.4% of solanesone and 89.3% of caprylic/capric glyceride are mixed and stirred uniformly to prepare the Pu ' er tea essence.
100 parts of deionized water, 3 parts of anhydrous calcium chloride, 0.75 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 3 parts of poloxamer and 260 parts of Pu' er tea essence are taken to prepare an emulsion.
100 parts of deionized water, 1.5 parts of sodium alginate, 0.5 part of sorbitol, 0.1 part of cyclodextrin and 800.1 parts of tween-1 are taken to prepare a forming solution.
Uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning and drying, and coating and dyeing by using an aqueous solution containing 0.24% of lemon yellow and 0.04% of brilliant blue in mass concentration to obtain the Pu' er tea popping beads.
Application example 1 results: the appearance and various indexes of the popping beads are in a standard range, the pinching hand feeling is moderate, the pinching sound is crisp, the tea aroma cannot be sensed in smoke during smoking, and the fresh and sweet feeling of the smoke aroma is not increased. After smoking evaluation, the sensory quality of the cigarettes is equivalent to the sensory quality of cigarettes without the exploded beads.
Application example 2
According to the mass fraction, 30% of Pu ' er green tea extract, 12% of Pu ' er black tea extract, 4% of leaf alcohol, 2% of isophorone oxide, 3% of geranylacetone, 2% of solanesone and 47% of caprylic/capric glyceride are mixed and stirred uniformly to prepare the Pu ' er tea essence.
100 parts of deionized water, 3 parts of anhydrous calcium chloride, 0.75 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 3 parts of poloxamer and 260 parts of Pu' er tea essence are taken to prepare an emulsion.
100 parts of deionized water, 1.5 parts of sodium alginate, 0.5 part of sorbitol, 0.1 part of cyclodextrin and 800.1 parts of tween-1 are taken to prepare a forming solution.
Uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning and drying, and coating and dyeing by using an aqueous solution containing 0.24% of lemon yellow and 0.04% of brilliant blue in mass concentration to obtain the Pu' er tea popping beads.
Application example 2 results: the appearance and various indexes of the puffed beads are in a standard range, the pinching hand feeling is moderate, the pinching sound is crisp, the smoke has thick tea fragrance during smoking, the harmony of the tobacco fragrance and the tea fragrance is poor, the smoke has high soft concentration and slight miscellaneous gas, the aftertaste is improved, and the fresh and sweet taste of the smoke fragrance is increased. After smoking evaluation, the sensory quality of the cigarettes is equivalent to the sensory quality of cigarettes without the exploded beads.
Application example 3
According to the mass fraction, 10% of Pu ' er green tea extract, 5% of Pu ' er black tea extract, 1% of leaf alcohol, 0.5% of isophorone oxide, 1% of geranylacetone, 0.5% of solanesone and 82% of caprylic/capric glyceride are mixed and stirred uniformly to prepare the Pu ' er tea essence.
100 parts of deionized water, 3 parts of anhydrous calcium chloride, 0.75 part of sodium carboxymethylcellulose, 0.05 part of cyclodextrin, 3 parts of poloxamer and 260 parts of Pu' er tea essence are taken to prepare an emulsion.
100 parts of deionized water, 1.5 parts of sodium alginate, 0.5 part of sorbitol, 0.1 part of cyclodextrin and 800.1 parts of tween-1 are taken to prepare a forming solution.
Uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning and drying, and coating and dyeing by using an aqueous solution containing 0.24% of lemon yellow and 0.04% of brilliant blue in mass concentration to obtain the Pu' er tea popping beads.
Application example 3 results: the appearance and various indexes of the Pu' er tea puffed bead are in a standard range, the pinching touch is moderate, the pinching sound is crisp, the smoke has light tea fragrance during smoking, the tobacco fragrance and the tea fragrance are good in harmony, the smoke is soft, the miscellaneous gas is less, the aftertaste is improved, and the fresh and sweet feeling of the smoke fragrance is increased. After smoking evaluation, the sensory quality score of the cigarette is improved by 1.5 points, the smoke permeability is good, the cigarette is rich and balanced, the tea aroma and the tobacco aroma are natural, the tea aroma and the tobacco aroma enter the throat softly, the tobacco aroma is full, the aftertaste is remained in the mouth, and the rich sense of relaxation, comfort and satisfaction are brought to consumers
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (6)
1. The Pu 'er tea essence bead for the cigarette is characterized in that the Pu' er tea essence in the bead comprises the following components in percentage by mass:
10-25% of Pu' er green tea extract; 5% -10% of Pu' er black tea extract; 1% -3% of leaf alcohol; 0.5 to 1.5 percent of isophorone oxide; geranylacetone 1% -2.5%; solanesone 0.5% -1.5%; 56.5 to 82 percent of caprylic capric glyceride.
2. The Pu 'er tea essence bead for cigarette according to claim 1, wherein the diameter of the Pu' er tea essence bead is 2.9mm-3.1mm, the content is 11.5 +/-1.0 mg/bead, the crushing pressure is 0.7kg-1.7kg, and the color is green.
3. The Pu 'er tea essence bead for the cigarette according to claim 1, wherein the Pu' er tea essence in the bead comprises the following components by mass percent:
18% of Pu' er green tea extract; 6% of Pu' er black tea extract; 1.5% of leaf alcohol; 0.7 percent of isophorone oxide; geranylacetone 1.2%; solanesone 0.6%; 72% of caprylic/capric glyceride.
4. The preparation method of the Pu' er tea essence bead for the cigarette according to any one of claims 1 to 3, which is characterized by comprising the following steps:
step (1), preparing an emulsion: according to the weight portion, 80-100 portions of deionized water, 3-5 portions of anhydrous calcium chloride, 0.5-1 portion of sodium carboxymethylcellulose, 0.05-1 portion of cyclodextrin, 1-5 portions of poloxamer and 300 portions of Pu' er tea essence are stirred together until the components are uniformly mixed to obtain emulsion;
step (2), preparing a forming liquid: according to the parts by weight, 80-100 parts of deionized water, 1-3 parts of sodium alginate, 0.5-1 part of sorbitol, 0.1-0.3 part of cyclodextrin and 800.1-0.3 part of tween-0.3 part are stirred together until the mixture is uniformly mixed to obtain a forming liquid;
step (3), the dripping pill is shaped: and uniformly dripping the emulsion into the forming liquid through dripping equipment, curing and forming, cleaning, drying, coating and dyeing to obtain the Pu' er tea puffed beads.
5. The preparation method of the Pu' er tea essence bead for the cigarette as claimed in claim 4, wherein the coating and dyeing are carried out by adopting an aqueous solution containing 0.24% of lemon yellow and 0.04% of brilliant blue in mass concentration.
6. The preparation method of the Pu' er tea essence bead for the cigarette according to claim 4, wherein the drying mode is air drying.
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| CN112869232A (en) * | 2021-01-13 | 2021-06-01 | 海南娜古芳沉香科技有限公司 | Agilawood blasting bead for cigarette and preparation method thereof |
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