CN108244689A - A kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic and its application in cigarette - Google Patents

A kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic and its application in cigarette Download PDF

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Publication number
CN108244689A
CN108244689A CN201711318124.4A CN201711318124A CN108244689A CN 108244689 A CN108244689 A CN 108244689A CN 201711318124 A CN201711318124 A CN 201711318124A CN 108244689 A CN108244689 A CN 108244689A
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CN
China
Prior art keywords
extract
leaf group
fragrance module
cigarette
odor characteristic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711318124.4A
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Chinese (zh)
Inventor
孙九喆
王鹏飞
段鹍
王宏伟
于建春
马宇平
申玉军
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China Tobacco Henan Industrial Co Ltd
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China Tobacco Henan Industrial Co Ltd
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Publication date
Application filed by China Tobacco Henan Industrial Co Ltd filed Critical China Tobacco Henan Industrial Co Ltd
Priority to CN201711318124.4A priority Critical patent/CN108244689A/en
Publication of CN108244689A publication Critical patent/CN108244689A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A24B15/26Use of organic solvents for extraction
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0003Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • C11B9/0015Aliphatic compounds containing oxygen as the only heteroatom

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Fats And Perfumes (AREA)

Abstract

The present invention relates to a kind of fragrance module formulas for improving burnt fragrant and sweet leaf group odor characteristic, are made of the component of following weight percentage:Fructus Jujubae extract 1-5%, malt extract 1.5-6%, apricot extract 0.3-4%, Prunus salicina Lindl. Extract 0.5-3.5%, Ergol 0-1.5%, limette oil 0.1-3%, isoamyl phenylacetate 0.2-4%, ethyl levulinate 0.1-2%, surplus are solvent.Addition fragrance module of the present invention match can make cigarette aroma characteristic be improved significantly, plumpness, solid sense increase, and miscellaneous gas also has larger reduction, are had a very important significance to improving the fragrant and sweet cigarette quality of coke.

Description

A kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic and its in cigarette Application
Technical field
The invention belongs to tobacco product meat flavor formulating technology fields, and in particular to a kind of to improve burnt fragrant and sweet leaf group odor characteristic(It is fragrant Makings, perfume quantity, thoroughly miscellaneous gas, the property sent out)Fragrance module formula and its application in cigarette.
Background technology
Odor characteristic mainly include rich fragrance texture, graceful degree, note, perfume quantity, plumpness, thick and solid degree, Hair degree, lucid and lively degree, the reduction of miscellaneous gas etc. thoroughly.It is burnt it is fragrant and sweet be a kind of high-quality note that sound tobacco shares, be Chinese style volume The important composition ingredient of cigarette flue gas aromatic style feature.It is found through investigation and experiment:The fragrant and sweet rhythm of coke in burnt fragrant and sweet leaf group and preceding Body object is affected in process by temperature and moisture, easily shows that aroma quality is poor, perfume quantity is insufficient, miscellaneous gas is brighter It is aobvious, the problems such as hair property is not good enough thoroughly.Therefore, in order to maintain the stability of product coke sweet tea style and features, according to the change of burnt fragrant and sweet leaf group It studies point, develops a fragrance module, after applying fragrance, reach the balance of formula chemical composition, improve the coke of flue gas Sweet tea odor characteristic, it appears particularly significant.
Fragrance module refers to allocating the approximate plurality of raw materials of odor characteristic into formed feature odor type unit in proportion.In State's patent of invention(104522875 B of Authorization Notice No. CN)Disclose a kind of burnt fragrant and sweet fragrance module formula of cigarette, invention profit The burnt fragrant and sweet ingredient present in cigarette smoke, the module formula provided can enhance the rich of electronic cigarette fragrance and with volume The similarity of cigarette fragrance characteristic, but the fragrance module can not achieve the purpose that improve burnt fragrant and sweet leaf group odor characteristic.It is based on This, the flavor component intrinsic from burnt fragrant and sweet leaf group, exploitation is a can be effectively improved burnt fragrant and sweet leaf group odor characteristic(Fragrance Matter, perfume quantity, thoroughly miscellaneous gas, the property sent out)Fragrance module, have highly important meaning to the stability for promoting burnt fragrant and sweet cigarette quality Justice.
Invention content
Present invention aims to overcome that prior art defect, provides a kind of improvement burnt fragrant and sweet leaf group odor characteristic(Aroma quality, Perfume quantity, thoroughly miscellaneous gas, the property sent out)Fragrance module formula.
The present invention also provides application of the above-mentioned fragrance module formula in cigarette.
To achieve the above object, the present invention adopts the following technical scheme that:
A kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic, is made of the component of following weight percentage:Greatly Jujube extract 1-5%, malt extract 1.5-6%, apricot extract 0.3-4%, Prunus salicina Lindl. Extract 0.5-3.5%, Benzyl Benzoate Ester 0-1.5%, limette oil 0.1-3%, isoamyl phenylacetate 0.2-4%, ethyl levulinate 0.1-2%, surplus are solvent. The sum of above-mentioned each component is 100%.
It is further preferred that the fragrance module formula of the burnt fragrant and sweet leaf group odor characteristic of above-mentioned improvement, the weight hundred of each component Point ratio is specially:Fructus Jujubae extract 2%, malt extract 2%, apricot extract 0.8%, Prunus salicina Lindl. Extract 0.8%, Ergol 0.8%, limette oil 0.2%, isoamyl phenylacetate 0.2%, ethyl levulinate 0.2%, solvent 93.0%.
Specifically, the solvent is preferably the mixing of one or more of water, ethyl alcohol and propylene glycol arbitrary proportion Object.
The present invention also provides application of the fragrance module formula in cigarette of the burnt fragrant and sweet leaf group odor characteristic of above-mentioned improvement.
In inventive formulation, Fructus Jujubae extract can promote burnt fragrant and sweet leaf group full aroma degree, reduce miscellaneous gas, improve flue gas Hair property thoroughly;Malt extract can promote burnt fragrant and sweet rhythm and more protrude, more graceful;Apricot extract can increase burnt fragrant and sweet leaf group Hair property thoroughly, makes the softer exquisiteness of flue gas;Prunus salicina Lindl. Extract can promote burnt fragrant and sweet leaf group concentration and aroma quality;Ergol Burnt fragrant and sweet leaf the group property sent out, smooth sense, conglobation property and soft sense thoroughly can be promoted;Limette oil can promote burnt fragrant and sweet leaf group and send out thoroughly Property and texture, make the softer exquisiteness of flue gas;Isoamyl phenylacetate can be promoted burnt fragrant and sweet leaf group sweet tea sense, smooth sense with it is agglomerating Property;Ethyl levulinate can promote burnt fragrant and sweet leaf group smoothness sense and sweet tea sense, and flue gas can be made more fine and smooth soft.Each component is assisted Same-action, so as to be effectively improved burnt fragrant and sweet leaf group odor characteristic.
The fragrance improved in the present invention in the fragrance module formula of burnt fragrant and sweet leaf group odor characteristic can directly be bought commonly Commercial product.Raw material in the present invention, if Fructus Jujubae extract, malt extract, apricot extract, Prunus salicina Lindl. Extract are by Henan gold Auspicious essence and flavoring agent Co., Ltd provides;The main alcohol extract that ethyl alcohol is used to extract acquisition as solvent.
Compared to the prior art, the invention has the advantages that:
1)The fragrance module of the burnt fragrant and sweet leaf group odor characteristic of present invention improvement can dramatically increase the fragrant and sweet impression of coke in flue gas, change Kind cigarette flavor amount deficiency and miscellaneous gas is overweight and suction after oral cavity residual it is overweight the problem of, burnt fragrant and sweet leaf group can be obviously improved Quality;
2)The fragrance module that the present invention improves burnt fragrant and sweet leaf group odor characteristic has stronger specific aim, and blending process is also relatively more square Just;
3)The raw material that the present invention improves used in the fragrance module formula of burnt fragrant and sweet leaf group odor characteristic is cheap and easy to get, production technology letter It is single.
Specific embodiment
Technical scheme of the present invention is further discussed in detail with reference to embodiments, but protection scope of the present invention It is not limited thereto.
Embodiment 1
A kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic, the weight percent of each component are specially:Jujube Extract 2%, malt extract 2%, apricot extract 0.8%, Prunus salicina Lindl. Extract 0.8%, Ergol 0.8%, limette oil 0.2%, isoamyl phenylacetate 0.2%, ethyl levulinate 0.2%, solvent(Absolute ethyl alcohol)93.0%.
The preparation method of the fragrance module formula of the burnt fragrant and sweet leaf group odor characteristic of above-mentioned improvement, specially:It takes in proportion each Component, then mixing to obtain the final product.
Take Bright Yellow(It is fragrant)Leaf group be subjects, by the fragrance module of above-mentioned composition according to tobacco quality 0.5% into Row addition, addition are placed on temperature(22±1)DEG C and relative humidity(60±2)It balances 48 hours in the environment of %, is had by 10 The method of the personnel establishing criteria GB 5606.4-2005 that smoke panel test of sensory evaluating smoking's qualification evaluates sample cigarette odor characteristic.It comments Result is inhaled to show:Compared with not injecting the leaf group of fragrance module of the present invention, the cigarette flavor that is added to after fragrance module of the present invention Amount significantly increased, and aroma quality is more graceful, and hair property improves thoroughly, and cigarette perfume is more coordinated, without apparent miscellaneous gas.
Different proportion is pressed into pipe tobacco to add, add using functional perfumery module formula made from embodiment 1 after silk is dried Dosage is respectively 0.1%, 0.3%, the 0.5% of tobacco quality, and 0.7%;Using no added cigarette as blank control cigarette.It is commented through sense organ It inhales, it is as a result as shown in table 1 below.
1 cigarette integrated sensory's mass smoking result of table
Marking of smokeing panel test is carried out by 9 points of point-scores processed to cigarette flavor characteristic, it is as a result as shown in table 2 below.
Aroma characteristic smoking result before and after 2 perfuming cigarette of table
As seen from the above table, add fragrance module of the present invention with can make cigarette aroma characteristic be improved significantly, highest can carry It is 1.4 points high, it is in particular in that aroma quality is finer and smoother, perfume quantity increases significantly, and cigarette perfume is more coordinated, and hair property improves thoroughly, without apparent Miscellaneous gas.Therefore fragrance module of the present invention, which is matched, can effectively promote burnt fragrant and sweet leaf group aroma characteristic(Aroma quality, perfume quantity, miscellaneous gas, thoroughly Hair property), had a very important significance to improving burnt fragrant and sweet cigarette quality.
Embodiment 2
A kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic, the weight percent of each component are specially:Jujube Extract 1%, malt extract 6%, apricot extract 0.3%, Prunus salicina Lindl. Extract 2%, Ergol 0%, limette oil 3%, benzene second Isoamyl valerate 2%, ethyl levulinate 1%, solvent(Water)84.7%.
The preparation method of the fragrance module formula of the burnt fragrant and sweet leaf group odor characteristic of above-mentioned improvement, specially:It takes in proportion each Component, then mixing to obtain the final product.
Take Bright Yellow(It is fragrant)Leaf group is subjects, by the fragrance module fragrance module of above-mentioned composition according to tobacco quality 0.5% be added, addition is placed on temperature(22±1)DEG C and relative humidity(60±2)It is balanced 48 hours in the environment of %, by 10 have sensory evaluating smoking's qualification the personnel establishing criteria GB 5606.4-2005 that smoke panel test method to sample cigarette odor characteristic into Row evaluation.Smoking result is shown:Compared with not injecting the leaf group of fragrance module of the present invention, after being added to fragrance module of the present invention Cigarette flavor amount has increased slightly, aroma quality variation unobvious, and hair property improves thoroughly, and cigarette perfume harmony improves, slightly miscellaneous gas..
Embodiment 3
A kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic, the weight percent of each component are specially:Jujube Extract 5%, malt extract 4%, apricot extract 4%, Prunus salicina Lindl. Extract 3.5%, Ergol 1.5%, limette oil 1%, benzene Isoamyl acetate 3.8%, ethyl levulinate 2%, solvent(Propylene glycol and water volume 1:1 mixing)75.2%.
The preparation method of the fragrance module formula of the burnt fragrant and sweet leaf group odor characteristic of above-mentioned improvement, specially:It takes in proportion each Component, then mixing to obtain the final product.
Take Bright Yellow(It is fragrant)Leaf group is subjects, by the fragrance module fragrance module of above-mentioned composition according to tobacco quality 0.5% be added, addition is placed on temperature(22±1)DEG C and relative humidity(60±2)It is balanced 48 hours in the environment of %, by 10 have sensory evaluating smoking's qualification the personnel establishing criteria GB 5606.4-2005 that smoke panel test method to sample cigarette odor characteristic into Row evaluation.Smoking result is shown:Compared with not injecting the leaf group of fragrance module of the present invention, after being added to fragrance module of the present invention Cigarette flavor qualitative change is good, and perfume quantity increases significantly, and hair property is slightly good thoroughly, harmony variation unobvious, without significantly miscellaneous gas.

Claims (4)

1. a kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic, which is characterized in that by following weight percentage Component forms:Fructus Jujubae extract 1-5%, malt extract 1.5-6%, apricot extract 0.3-4%, Prunus salicina Lindl. Extract 0.5- 3.5%, Ergol 0-1.5%, limette oil 0.1-3%, isoamyl phenylacetate 0.2-4%, ethyl levulinate 0.1- 2%, surplus is solvent.
2. improve the fragrance module formula of burnt fragrant and sweet leaf group odor characteristic as described in claim 1, which is characterized in that each component Weight percent is specially:Fructus Jujubae extract 2%, malt extract 2%, apricot extract 0.8%, Prunus salicina Lindl. Extract 0.8%, benzoic acid Benzyl ester 0.8%, limette oil 0.2%, isoamyl phenylacetate 0.2%, ethyl levulinate 0.2%, solvent 93.0%.
3. improve the fragrance module formula of burnt fragrant and sweet leaf group odor characteristic as described in claim 1, which is characterized in that the solvent Mixture for one or more of water, ethyl alcohol and propylene glycol arbitrary proportion.
4. application of any fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic of claims 1 to 3 in cigarette.
CN201711318124.4A 2017-12-12 2017-12-12 A kind of fragrance module formula for improving burnt fragrant and sweet leaf group odor characteristic and its application in cigarette Pending CN108244689A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111406970A (en) * 2020-03-27 2020-07-14 四川中烟工业有限责任公司 Sweet-burning base for cigarettes
WO2023179870A1 (en) * 2022-03-25 2023-09-28 Symrise Ag Ethyl 4-oxopentanoate for reducing odors

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000060520A (en) * 1998-08-17 2000-02-29 ▲吉▼田 及也 Perfume for tobacco
CN101406318A (en) * 2008-11-21 2009-04-15 深圳烟草工业有限责任公司 Sweet functional clustering formulation approaching to tobacco sweet and capable of markedly increasing cigarette sweet rhyme
CN104219963A (en) * 2012-03-30 2014-12-17 奇华顿股份有限公司 N-acylated amino acid derivative as food flavouring compounds and powder flavour composition comprising same
CN104830533A (en) * 2015-05-14 2015-08-12 湖北中烟工业有限责任公司 Perfuming essence for enhancing cigarette fruit sweetness

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000060520A (en) * 1998-08-17 2000-02-29 ▲吉▼田 及也 Perfume for tobacco
CN101406318A (en) * 2008-11-21 2009-04-15 深圳烟草工业有限责任公司 Sweet functional clustering formulation approaching to tobacco sweet and capable of markedly increasing cigarette sweet rhyme
CN104219963A (en) * 2012-03-30 2014-12-17 奇华顿股份有限公司 N-acylated amino acid derivative as food flavouring compounds and powder flavour composition comprising same
CN104830533A (en) * 2015-05-14 2015-08-12 湖北中烟工业有限责任公司 Perfuming essence for enhancing cigarette fruit sweetness

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111406970A (en) * 2020-03-27 2020-07-14 四川中烟工业有限责任公司 Sweet-burning base for cigarettes
CN111406970B (en) * 2020-03-27 2022-03-01 四川中烟工业有限责任公司 Sweet-burning base for cigarettes
WO2023179870A1 (en) * 2022-03-25 2023-09-28 Symrise Ag Ethyl 4-oxopentanoate for reducing odors

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Application publication date: 20180706

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