CN104939309A - Florists chrysanthemum glycerol triacetate extract and application thereof in cigarettes - Google Patents
Florists chrysanthemum glycerol triacetate extract and application thereof in cigarettes Download PDFInfo
- Publication number
- CN104939309A CN104939309A CN201510337083.8A CN201510337083A CN104939309A CN 104939309 A CN104939309 A CN 104939309A CN 201510337083 A CN201510337083 A CN 201510337083A CN 104939309 A CN104939309 A CN 104939309A
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- CN
- China
- Prior art keywords
- extract
- cigarette
- glycerol triacetate
- triacetyl glycerine
- chrysanthemum
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Seasonings (AREA)
Abstract
The invention discloses a florists chrysanthemum glycerol triacetate extract and application thereof in cigarettes. Florists chrysanthemum powder with the moisture content of 6-8% and the grain size of 20-40 meshes serves as a raw material, glycerol triacetate serves as an extraction agent, and the florists chrysanthemum glycerol triacetate extract is obtained first through extraction in a heating reflux mode and then through ultrasonic extraction. Glycerol triacetate serves as a solvent to prepare the florists chrysanthemum glycerol triacetate extract into a solution with the concentration of 1-5%, the solution is evenly sprayed to tows according to the proportion of 7-9% of the weight of cellulose acetate tows to prepare a cigarette filter stick, and a cigarette with the filter stick containing effective florists chrysanthemum components is prepared in the conventional cigarette winding process. The extract can remarkably enhance sweet taste of smoke and enables the sweet taste to remain in the oral cavity for a long time. The florists chrysanthemum glycerol triacetate extract is simple in production process and high in operability and normativity, raw materials can be obtained easily, the cost is low, industrial production is achieved conveniently, and the florists chrysanthemum glycerol triacetate extract has good application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to the triacetyl glycerine extract of a kind of tribute chrysanthemum.Meanwhile, the invention still further relates to the described application of tribute chrysanthemum triacetyl glycerine extract in cigarette.
Background technology
Tribute chrysanthemum taste is sweet, cold nature, is rich in the multiple bioactive ingredients such as chrysanthemum glucoside, flavone compound, volatile oil (chrysanthemum ketone, borneol, borneol acid esters), amino acid and vitamin.Through modern pharmacological research, it has wind-dispelling heat-dissipating, flat liver improving eyesight, refreshing and detoxicating and effects such as falling fire of getting rid of evils.Studies have reported that, tribute chrysanthemum tea has the effect of calmness and anti-inflammatory sterilization to nervous centralis, composite with other plant raw material, also can be made into relieve sore throat and supports larynx, inflammation-diminishing and cough-controlling, falls the drinks that fire moisturizes.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN 103271441A) thereof, a kind of filter stick fiber base material additive and application (CN 103126073 A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN 104161303 A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582 A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in triacetyl glycerine dissolve add in cigarette, or the additive some being insoluble in triacetyl glycerine is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the solvability of triacetyl glycerine to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in triacetyl glycerine, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by triacetyl glycerine, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of tribute chrysanthemum extract prepared using triacetyl glycerine as extractant is provided, this extract is applied to cigarette can strengthen the rich of cigarette and harmony, and it is soft, sweet that flue gas inhales taste, covers assorted gas, alleviates excitant.
The present invention also aims to provide the described embody rule of tribute chrysanthemum triacetyl glycerine extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of tribute chrysanthemum triacetyl glycerine extract, is obtained by the method for following steps:
(1) tribute chrysanthemum being dried under 60 DEG C of conditions moisture is 6% ~ 8%, directly pulverizes 20 ~ 40 mesh sieves, for subsequent use;
(2) take 4 ~ 8 parts of tribute inulin according to weight portion and be placed in round-bottomed flask, add 60 ~ 120 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature, after 3 ~ 5 hours, carries out refluxing extraction under 70 ~ 100 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 800W, 40kHZ condition, extract 20 ~ 60 minutes, obtain settled solution after excessively filtering filter residue and be required tribute chrysanthemum triacetyl glycerine extract.
The described application of tribute chrysanthemum triacetyl glycerine extract in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described tribute chrysanthemum triacetyl glycerine extract is mixed with the solution that concentration is 1 ~ 5%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 9%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the tribute chrysanthemum triacetyl glycerine extract prepared by the present invention, can dissolve each other in any proportion with triacetyl glycerine, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that tribute chrysanthemum exists by prior art when filter stick additive is mixed and is fitted in plasticizer.
2. adopt triacetyl glycerine to be that extractant extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in triacetyl glycerine in tribute chrysanthemum fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to triacetyl glycerine time, the loss of effective efficiency composition.
3. gained tribute chrysanthemum triacetyl glycerine extract effectively can improve smoking property of cigarette quality, upgrading flavouring, has the effect reducing flue gas excitant, improve pleasant impression simultaneously.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, operability and normative strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
Tribute chrysanthemum being dried under 60 DEG C of conditions moisture is 6%, directly pulverizes, crosses 20-40 mesh sieve, obtain tribute inulin.Take 8 parts of tribute inulin ends according to weight portion and be placed in round-bottomed flask, add 100 parts of glycerol triacetate for tobacco and make extractant, soaking at room temperature, after 5 hours, carries out refluxing extraction under 100 DEG C of conditions, and extraction time is 8 hours, after being cooled to room temperature, tribute chrysanthemum after refluxing extraction and triacetyl glycerine mixture are placed in ultrasonic extractor (600W, 40kHZ), extract 40 minutes, cross after filtering filter residue and obtain settled solution, required tribute chrysanthemum triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, tribute chrysanthemum triacetyl glycerine extract is mixed with the solution that concentration is 2%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains tribute chrysanthemum active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds the cigarette flue gas upgrading flavouring of above-mentioned tribute chrysanthemum triacetyl glycerine extract, covers the assorted gas of part, and flue gas exquisiteness is soft, have sweet sense, and excitant reduces, and pleasant impression improves.
Embodiment 2
Tribute chrysanthemum being dried under 60 DEG C of conditions moisture is 8%, directly pulverizes 20-40 mesh sieve, and obtains tribute inulin.Take 7 parts of tribute inulin ends according to weight portion and be placed in round-bottomed flask, the glycerol triacetate for tobacco adding 95 parts makes extractant, soaking at room temperature, after 4 hours, carries out refluxing extraction under 70 DEG C of conditions, and extraction time is 4 hours, to be cooled to room temperature, tribute chrysanthemum after refluxing extraction and triacetyl glycerine mixture are placed in ultrasonic extractor (400W, 40kHZ), extract 52 minutes, cross after filtering filter residue and obtain settled solution, required tribute chrysanthemum triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, tribute chrysanthemum triacetyl glycerine extract is mixed with the solution that concentration is 1%, by acetate silk 7.5% ratio uniform be sprayed onto on filter stick tow, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains tribute chrysanthemum active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned tribute chrysanthemum triacetyl glycerine extract is obvious, and cigarette perfume is abundant to be coordinated, and pleasant impression and flue gas excitant are improved, smoking property of cigarette quality-improving.
Embodiment 3
Tribute chrysanthemum being dried under 60 DEG C of conditions moisture is 7%, directly pulverizes 20-40 mesh sieve, and obtains tribute inulin.Take 5 parts of tribute inulin ends according to weight portion and be placed in round-bottomed flask, the glycerol triacetate for tobacco adding 120 parts makes extractant, soaking at room temperature is after 3 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 8 hours, to be cooled to room temperature, tribute chrysanthemum after refluxing extraction and triacetyl glycerine mixture are placed in ultrasonic extractor (600W, 40kHZ), extract 30 minutes, cross after filtering filter residue and obtain settled solution, required tribute chrysanthemum triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, tribute chrysanthemum triacetyl glycerine extract is mixed with the solution that concentration is 4%, by acetate silk 9% ratio uniform be sprayed onto on filter stick tow and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains tribute chrysanthemum active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, adds that the cigarette cigarette perfume of above-mentioned tribute chrysanthemum triacetyl glycerine extract is abundant to be coordinated, free from extraneous odour, and mix gas and excitant of flue gas alleviates, and pleasant impression improves, and has salubrious sweet sense.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a tribute chrysanthemum triacetyl glycerine extract, is obtained by the method for following steps:
(1) tribute chrysanthemum being dried under 60 DEG C of conditions moisture is 6% ~ 8%, directly pulverizes 20 ~ 40 mesh sieves, for subsequent use;
(2) take 4 ~ 8 parts of tribute inulin according to weight portion and be placed in round-bottomed flask, add 60 ~ 120 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature, after 3 ~ 5 hours, carries out refluxing extraction under 70 ~ 100 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 800W, 40kHZ condition, extract 20 ~ 60 minutes, obtain settled solution after excessively filtering filter residue and be required tribute chrysanthemum triacetyl glycerine extract.
2. the application of tribute chrysanthemum triacetyl glycerine extract according to claim 1 in cigarette, it is characterized in that: be that described tribute chrysanthemum triacetyl glycerine extract is mixed with the solution that concentration is 1 ~ 5% by solvent with triacetyl glycerine, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 9%, make cigarette filter rod, and this filter stick is applied to cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510337083.8A CN104939309A (en) | 2015-06-17 | 2015-06-17 | Florists chrysanthemum glycerol triacetate extract and application thereof in cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510337083.8A CN104939309A (en) | 2015-06-17 | 2015-06-17 | Florists chrysanthemum glycerol triacetate extract and application thereof in cigarettes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104939309A true CN104939309A (en) | 2015-09-30 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510337083.8A Pending CN104939309A (en) | 2015-06-17 | 2015-06-17 | Florists chrysanthemum glycerol triacetate extract and application thereof in cigarettes |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| KR20130095598A (en) * | 2012-02-20 | 2013-08-28 | 황영보 | Aromatic stuffed-filter, the method of producing the same, and the tobacco pipe including thereof |
| CN103479704A (en) * | 2013-09-27 | 2014-01-01 | 天津工业大学 | Method for extracting total flavones from chrysanthemum |
| CN104403794A (en) * | 2014-09-24 | 2015-03-11 | 云南中烟工业有限责任公司 | Preparation method and application of Pu'er tea extract to cigarettes |
| CN104498192A (en) * | 2014-12-15 | 2015-04-08 | 云南中烟工业有限责任公司 | Preparation method and application of florists chrysanthemum extract |
-
2015
- 2015-06-17 CN CN201510337083.8A patent/CN104939309A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| KR20130095598A (en) * | 2012-02-20 | 2013-08-28 | 황영보 | Aromatic stuffed-filter, the method of producing the same, and the tobacco pipe including thereof |
| CN103479704A (en) * | 2013-09-27 | 2014-01-01 | 天津工业大学 | Method for extracting total flavones from chrysanthemum |
| CN104403794A (en) * | 2014-09-24 | 2015-03-11 | 云南中烟工业有限责任公司 | Preparation method and application of Pu'er tea extract to cigarettes |
| CN104498192A (en) * | 2014-12-15 | 2015-04-08 | 云南中烟工业有限责任公司 | Preparation method and application of florists chrysanthemum extract |
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| PB01 | Publication | ||
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Application publication date: 20150930 |