CN105038983A - Glycerol triacetate extract of Zimbabwe tobacco and application thereof to cigarettes - Google Patents
Glycerol triacetate extract of Zimbabwe tobacco and application thereof to cigarettes Download PDFInfo
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- CN105038983A CN105038983A CN201510339085.0A CN201510339085A CN105038983A CN 105038983 A CN105038983 A CN 105038983A CN 201510339085 A CN201510339085 A CN 201510339085A CN 105038983 A CN105038983 A CN 105038983A
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- zimbabwe
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Abstract
The invention discloses a glycerol triacetate extract of Zimbabwe tobacco and application thereof to cigarettes. The glycerol triacetate extract of Zimbabwe tobacco is prepared through the following steps: with 20-40 mesh dried and smashed Zimbabwe tobacco as a raw material and glycerol triacetate as an extraction agent, using a heating reflux method to carry out extraction and then performing ultrasonic extraction to obtain the glycerol triacetate extract of Zimbabwe tobacco. The glycerol triacetate extract of Zimbabwe tobacco is prepared into a solution with the concentration of 0.5-2% by using glycerol triacetate as a solvent; the solution is uniformly sprayed to filter stick bundles according the ratio that the solution accounts for 7-8 percent by weight of the cellulose acetate fiber bundles so as to obtain cigarette filter sticks and further cigarettes of which the filter sticks contain effective constituents of Zimbabwe tobacco are prepared. The extract provided by the invention can remarkably increase the fragrance of the cigarettes, enables the fragrance to be strong and full and the smoking flavor to be pure and mild, and greatly improves the smoking quality; the production technology is simple, and high in operability and standardability, raw materials are easy to obtain, the cost is low, industrial production is realized easily, and a good application prospect is realized.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of Zimbabwe tobacco leaf glycerine triacetate extract.Meanwhile, the invention still further relates to the described application of Zimbabwe's tobacco leaf glycerine triacetate extract in cigarette.
Background technology
Zimbabwe's tobacco leaf due to best in quality, there is unique odour characteristics and good compatibleness, entered the cigarette composition of countries in the world.Correlative study shows, its intrinsic chemical composition is coordinated, and tobacco incense tolerance foot, aroma quality is good, has typical cigarette fragrance, jealous alcohol and and aroma quality give prominence to, strength and pungency moderate.Compared with the tobacco leaf in other areas, Zimbabwe's tobacco leaf has more flavor matter content and stronger operability.It can be used as a kind of tobacco aromatics using of high-quality, possess characteristic perfume obviously, give off a strong fragrance, make cigarette flavor plentiful, sweet, fine and smooth simultaneously, improve cigarette pleasant impression, reduce irritating effect, can cigarette quality be significantly improved.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent need first by extract or allocate additive again in glycerine triacetate dissolve add in cigarette, or the additive some being insoluble in glycerine triacetate is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the dissolving power of glycerine triacetate to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in glycerine triacetate, limit the application of spices in cigarette filter rod perfuming.On the other hand, if be not that medium carries out filter stick perfuming by glycerine triacetate, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable Technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco industry in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of Zimbabwe's leaf tobacco extract prepared using glycerine triacetate as extraction agent is provided, this extract is applied to cigarette effectively can strengthen that cigarette feature cigarette is fragrant, fragrance is coordinated strong, inhales taste alcohol and full.
The present invention also aims to provide the described application of Zimbabwe's tobacco leaf glycerine triacetate extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage ratio adopted in the present invention is mass percent.
A kind of Zimbabwe tobacco leaf glycerine triacetate extract, is obtained by the method for following steps:
(1) cross 20 ~ 40 mesh sieves after Zimbabwe's drying tobacco being pulverized, obtain tobacco leaf powder, for subsequent use;
(2) take 100g Zimbabwe tobacco leaf powder and be placed in round-bottomed flask, be that 1:10 ~ 20 add glycerol triacetate for tobacco as extraction agent by solid-liquid ratio, soaking at room temperature is after 3 ~ 5 hours, refluxing extraction is carried out under 60 ~ 120 DEG C of conditions, 4 ~ 6 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 600W, 40kHZ condition, extract 20 ~ 50 minutes, obtain settled solution after excessively filtering filter residue and be required Zimbabwe's tobacco leaf glycerine triacetate extract.
The described application of Zimbabwe's tobacco leaf glycerine triacetate extract in cigarette, it is characterized in that: take glycerine triacetate as solvent, described Zimbabwe's tobacco leaf glycerine triacetate extract is mixed with the solution that concentration is 0.5 ~ 2%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the Zimbabwe's tobacco leaf glycerine triacetate extract prepared by the present invention, can dissolve each other in any proportion with glycerine triacetate, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that Zimbabwe's tobacco leaf exists by prior art when filter stick additive is mixed and is fitted in softening agent.
2. adopt glycerine triacetate to be that extraction agent extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in glycerine triacetate in Zimbabwe's tobacco leaf fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to glycerine triacetate time, the loss of effective efficiency composition.
3. gained Zimbabwe tobacco leaf glycerine triacetate extract effectively can be given prominence to cigarette feature cigarette perfume, be that fragrance is coordinated strong, has simultaneously and makes suction taste alcohol and fine and smooth, irritating effect of reduction flue gas.
4. material used herein is food grade, has higher safety in utilization.
5. production technique of the present invention is simple, operability and standardization strong, raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
With Zimbabwe's tobacco leaf for raw material, drying and crushing, cross 20-40 mesh sieve and obtain tobacco leaf powder, take 100g Zimbabwe tobacco leaf powder and be placed in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:10 is as extraction agent, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 4 hours, to be cooled to room temperature, Zimbabwe's tobacco leaf after described refluxing extraction and glycerine triacetate mixture are placed in ultrasonic extractor (400W, 40kHZ), extract 30 minutes, cross after filtering filter residue and obtain settled solution, be required Zimbabwe tobacco leaf glycerine triacetate extract.
Be that described Zimbabwe's tobacco leaf glycerine triacetate extract is mixed with the solution that concentration is 0.5% by solvent with glycerine triacetate, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains Zimbabwe's tobacco leaf effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette feature cigarette perfume adding above-mentioned Zimbabwe tobacco leaf glycerine triacetate extract is outstanding, and give off a strong fragrance exquisiteness, and inhale taste alcohol and full, pleasant impression obviously improves.
Embodiment 2
With Zimbabwe's tobacco leaf for raw material, drying and crushing, cross 20-40 mesh sieve and obtain tobacco leaf powder, take 100g Zimbabwe tobacco leaf and be placed in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:15 is as extraction agent, soaking at room temperature is after 3 hours, refluxing extraction is carried out under 60 DEG C of conditions, extraction time is 6 hours, to be cooled to room temperature, Zimbabwe's tobacco leaf after described refluxing extraction and glycerine triacetate are placed in ultrasonic extractor (600W, 40kHZ), extract 50 minutes, cross after filtering filter residue and obtain settled solution, required Zimbabwe tobacco leaf glycerine triacetate extract can be obtained.
Be that Zimbabwe's tobacco leaf glycerine triacetate extract is mixed with the solution that concentration is 1% by solvent with glycerine triacetate, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains Zimbabwe's tobacco leaf effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, add above-mentioned Zimbabwe tobacco leaf glycerine triacetate extract cigarette smoke alcohol and, give off a strong fragrance, full, flue gas pungency reduces, and pleasant impression obviously improves, and suction satisfaction has certain lifting.
Embodiment 3
With Zimbabwe's tobacco leaf for raw material, drying and crushing, cross 20-40 mesh sieve and obtain tobacco leaf powder, take 100g Zimbabwe tobacco leaf and be placed in round-bottomed flask, adding solid-liquid ratio is that the glycerol triacetate for tobacco of 1:20 is as extraction agent, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 100 DEG C of conditions, extraction time is 6 hours, to be cooled to room temperature, Zimbabwe's tobacco leaf after described refluxing extraction and glycerine triacetate are placed in ultrasonic extractor (400W, 40kHZ), extract 50 minutes, cross after filtering filter residue and obtain settled solution, namely required Zimbabwe tobacco leaf glycerine triacetate extract is obtained.
Be that Zimbabwe's tobacco leaf glycerine triacetate extract is mixed with the solution that concentration is 2% by solvent with glycerine triacetate, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains Zimbabwe's tobacco leaf glycerine triacetate extract.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette of adding above-mentioned Zimbabwe tobacco leaf glycerine triacetate extract obviously increases cigarette perfume (or spice), and fragrance is coordinated, plentiful, and flue gas pungency reduces, and jealous comfortable, pleasant impression improves.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. Zimbabwe's tobacco leaf glycerine triacetate extract, is obtained by the method for following steps:
(1) cross 20 ~ 40 mesh sieves after Zimbabwe's drying tobacco being pulverized, obtain tobacco leaf powder, for subsequent use;
(2) take 100g Zimbabwe tobacco leaf powder and be placed in round-bottomed flask, be that 1:10 ~ 20 add glycerol triacetate for tobacco as extraction agent by solid-liquid ratio, soaking at room temperature is after 3 ~ 5 hours, refluxing extraction is carried out under 60 ~ 120 DEG C of conditions, 4 ~ 6 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 600W, 40kHZ condition, extract 20 ~ 50 minutes, obtain settled solution after excessively filtering filter residue and be required Zimbabwe's tobacco leaf glycerine triacetate extract.
2. the application of Zimbabwe's tobacco leaf glycerine triacetate extract according to claim 1 in cigarette, it is characterized in that: take glycerine triacetate as solvent, described Zimbabwe's tobacco leaf glycerine triacetate extract is mixed with the solution that concentration is 0.5 ~ 2%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510339085.0A CN105038983A (en) | 2015-06-17 | 2015-06-17 | Glycerol triacetate extract of Zimbabwe tobacco and application thereof to cigarettes |
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| CN201510339085.0A CN105038983A (en) | 2015-06-17 | 2015-06-17 | Glycerol triacetate extract of Zimbabwe tobacco and application thereof to cigarettes |
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| CN105038983A true CN105038983A (en) | 2015-11-11 |
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| CN201510339085.0A Pending CN105038983A (en) | 2015-06-17 | 2015-06-17 | Glycerol triacetate extract of Zimbabwe tobacco and application thereof to cigarettes |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110279163A (en) * | 2019-08-06 | 2019-09-27 | 四川三联新材料有限公司 | Fragrance dose for heating cigarette smoke section of not burning and its preparation method and application and heating are not burnt cigarette |
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| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
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| CN104544553A (en) * | 2014-12-31 | 2015-04-29 | 贵州中烟工业有限责任公司 | Fen-flavor electronic tobacco liquid |
| CN104585858A (en) * | 2014-12-31 | 2015-05-06 | 贵州中烟工业有限责任公司 | Electronic cigarette tobacco juice with bowel relaxing function |
| CN104621709A (en) * | 2015-01-29 | 2015-05-20 | 湖南中烟工业有限责任公司 | Flue-cured tobacco extract and electronic cigarette liquid |
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2015
- 2015-06-17 CN CN201510339085.0A patent/CN105038983A/en active Pending
Patent Citations (5)
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| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN104544549A (en) * | 2014-12-31 | 2015-04-29 | 贵州中烟工业有限责任公司 | Electronic cigarette smoke solution prepared through green tea leaf extract |
| CN104544553A (en) * | 2014-12-31 | 2015-04-29 | 贵州中烟工业有限责任公司 | Fen-flavor electronic tobacco liquid |
| CN104585858A (en) * | 2014-12-31 | 2015-05-06 | 贵州中烟工业有限责任公司 | Electronic cigarette tobacco juice with bowel relaxing function |
| CN104621709A (en) * | 2015-01-29 | 2015-05-20 | 湖南中烟工业有限责任公司 | Flue-cured tobacco extract and electronic cigarette liquid |
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| 周民杰等: "废次烟叶超声提取烟碱的研究", 《化学工程师》 * |
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| CN110279163A (en) * | 2019-08-06 | 2019-09-27 | 四川三联新材料有限公司 | Fragrance dose for heating cigarette smoke section of not burning and its preparation method and application and heating are not burnt cigarette |
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