CN106281680B - A kind of quick-fried pearl of peppermint cigarette cool taste Mint Essence and the preparation method and application thereof - Google Patents
A kind of quick-fried pearl of peppermint cigarette cool taste Mint Essence and the preparation method and application thereof Download PDFInfo
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- CN106281680B CN106281680B CN201610736752.3A CN201610736752A CN106281680B CN 106281680 B CN106281680 B CN 106281680B CN 201610736752 A CN201610736752 A CN 201610736752A CN 106281680 B CN106281680 B CN 106281680B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
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- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a kind of quick-fried pearl of peppermint cigarette cool taste Mint Essences and the preparation method and application thereof.Cool taste Mint Essence formula of the present invention is made of the component as follows according to mass percentage: menthol 1-8%, menthyl lactate 1-10%, menthyl acetate 1-5%, coolant agent 0.2-0.5%, surplus are fat solvent.The present invention can make to assign cigarette natural mint flavored and cool feeling when quick-fried pearl pinches brokenly, and without the medicinal herbs breath of menthol and irritation, it can be merged well with cigarette flavor, be effectively improved the comfort of cigarette smoking, promote cigarette smoking quality.
Description
Technical field
The present invention relates to a kind of quick-fried pearl of peppermint cigarette cool taste Mint Essences and the preparation method and application thereof, belong to flavouring essence for tobacco
Fragrance technical field.
Background technique
" new ", " surprise ", " spy " are pursued, is the mainstream psychological characteristics in cigarette consumption market forever.It will be answered after essence capsule
For Field of Tobacco, it not only can come " new ", " surprise ", the bright spot of " spy " to tobacco rolling belt, traditional essence application side can also be solved
The problems such as the essence residence time existing for formula is short, and essence release is uneven.
The quick-fried pearl cigarette of peppermint is as a market segmentation most important in quick-fried pearl cigarette market, always deeply by the heat of consumer
It holds in both hands, and occupation rate of market is continuing to increase.From pure this perfume of tobacco, to pinching brokenly cool peppermint taste after quick-fried pearl, the quick-fried pearl of peppermint
Cigarette provides for consumer two different sucks mode.But the quick-fried pearl cigarette of peppermint is sold on cigarette market at present, made
Essence main component is menthol, and consumer can feel that one refrigerant breath enters throat in suction, then bring
Be medicinal herbs specific to menthol bad breath and oral stimulation, and bad with tobacco this perfume degrees of fusion, peppermint cool feeling is held
The continuous time is short.
Therefore, for the quick-fried pearl cigarette of peppermint with quick-fried pearl, the research that development removes the bad breath of medicinal herbs has highly important
Meaning.
Summary of the invention
The object of the present invention is to provide a kind of quick-fried pearl of peppermint cigarette cool taste Mint Essences and preparation method thereof.Of the invention is thin
The quick-fried pearl of lotus cigarette can be made to assign cigarette natural mint flavored and cool feeling when quick-fried pearl pinches brokenly with cool taste Mint Essence, and without thin
The medicinal herbs breath of lotus brain and irritation can merge well with cigarette flavor, be effectively improved the comfort of cigarette smoking, promote volume
Cigarette suction quality.
It is a further object of the present invention to provide purposes of the above-mentioned cool taste Mint Essence in the preparation quick-fried pearl cigarette of peppermint.
To achieve the above object, the present invention adopts the following technical scheme:
A kind of cool taste Mint Essence of quick-fried pearl of peppermint cigarette, is made of the raw material of following mass percent:
Menthol 1-8%, menthyl lactate 1-10%, menthyl acetate 1-5%, coolant agent 0.2-0.5%, surplus are oil
Fatsolvent；
Preferably, the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette, is made of the raw material of following mass percent:
Menthol 2-4%, menthyl lactate 1-2%, menthyl acetate 1-2%, coolant agent 0.2-0.4%, surplus are oil
Fatsolvent.
The fat solvent is selected from one of corn oil, olive oil or neodecanoic acid glyceride or a variety of.
The coolant agent is selected from carbonic acid l-menthol glycol ester (FEMA:3805), L- menthones glycerol ketal
(FEMA:3807), N- ethyl-menthyl formamide (FEMA:3455), L- menthoxy propylene glycol (FEMA:3784) or cool taste
One of agent WS-3 or a variety of.
The preparation method of the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette, comprising the following steps:
(1) coolant agent is dissolved in propylene glycol, the solution that mass fraction is 8-12% is made；
(2) menthol, menthyl lactate and menthyl acetate are added into the solution of step (1), adds fat solvent,
Be uniformly mixed to get.
Preferably, in step (1), coolant agent is dissolved in propylene glycol, the solution that mass fraction is 10% is made.
Purposes of the above-mentioned quick-fried pearl of peppermint cigarette with cool taste Mint Essence in the quick-fried pearl of preparation peppermint cigarette or the quick-fried pearl cigarette of peppermint
It is protection scope of the present invention.
The present invention also provides a kind of quick-fried pearls of peppermint cigarette, contain a effective amount of above-mentioned cool taste Mint Essence.
The preparation method of the quick-fried pearl of peppermint cigarette, steps are as follows:
By olive oil and Glycerin, mixed triester with caprylic acid capric acid, 1:2 is mixed by volume, then presses olive oil and Glycerin, mixed triester with caprylic acid capric acid total weight
0.2-0.5% be added emulsifier, then stir evenly, the cool taste minty note of the above-mentioned quick-fried pearl of peppermint cigarette be added in whipping process
Essence, additive amount are the 1-2% of olive oil and Glycerin, mixed triester with caprylic acid capric acid total weight, are further continued for stirring 0.5h, complete process for preparation, finally
The quick-fried pearl of peppermint cigarette is made.
Preferably, the emulsifier is sorbester p17.
The present invention also provides a kind of quick-fried pearl cigarette of peppermint, contain the above-mentioned quick-fried pearl of peppermint cigarette.
The beneficial effects of the present invention are:
It (1) is the medicinal herbs breath of removal menthol, the quick-fried pearl of peppermint cigarette of the invention reduces peppermint with cool taste Mint Essence
The dosage of brain, while menthyl lactate and menthyl acetate is added, wherein menthyl lactate has slight peppermint fragrance, but companion
There is lasting, pleasant cooling effect；Menthyl acetate has soft peppermint and rose fragrance, passes through menthyl lactate
With the addition of menthyl acetate, the medicinal herbs breath of menthol is further masked, and overcomes single use menthol it is clear
The strong and very brief disadvantage of cool effect.In addition, to prevent the reduction for leading to cooling effect because of the reduction of menthol additional amount, this
In the quick-fried pearl of peppermint cigarette, with coolant agent is also added in cool taste Mint Essence, and investigation is optimized to coolant agent, through feeling in invention
Official's evaluation comparison, coolant agent added by the present invention can increase the harmonious feeling of cool taste, stay taste very long, cool taste is pure and fresh, long-acting, no hardship
Taste.
(2) with cool taste Mint Essence, the solvent which is wrapped up with quick-fried pearl can dissolve each other the quick-fried pearl of peppermint cigarette of the invention,
Quick-fried pearl wall material and the bad breath of solvent bring can be covered completely.
(3) pass through quick-fried pearl pilot production, quick-fried pearl stability is preferable, and notch is small, produces no any influence to quick-fried pearl.
(4) by adding the above-mentioned quick-fried pearl containing cool taste Mint Essence in mouth stick, quick-fried pearl is pinched brokenly in aspiration procedure, energy
It is merged well with cigarette flavor, is effectively improved the comfort of cigarette smoking, natural mint flavored and cool feeling is lasting.
(5) the quick-fried pearl of peppermint cigarette of the invention is easy, low in cost with cool taste Mint Essence preparation method, it is extensive to can be used for
Industrialized production has very strong practicability.
(6) for the quick-fried pearl of peppermint cigarette of the invention in cool taste Mint Essence, each raw material component is an organic whole, lacks one
It can not.Inventor has found in R&D process, reduces any one of above-mentioned cool taste Mint Essence raw material components, or to have
The raw material of similar performance is replaced the raw material components of the cool taste Mint Essence of the present invention and (such as replaces this hair with isovaleric acid menthyl ester
Menthyl acetate in bright), then the function and effect of cool taste Mint Essence entirety significantly reduce；In cool taste Mint Essence of the invention
On the basis of be further added by other raw material components, the overall effect of cool taste Mint Essence does not improve significantly, or even has cool
The case where overall effect of taste Mint Essence reduces occurs.
Specific embodiment
The present invention is further illustrated in conjunction with the embodiments, it should which explanation, following embodiments are merely to explain
The present invention is not defined its content.
Embodiment 1: the preparation of the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette
Raw material composition:
By mass percentage, it is prepared from the following materials:
Menthol 2%, menthyl lactate 1%, menthyl acetate 1%, coolant agent 0.2%, surplus are olive oil.
Used menthol, menthyl acetate and menthyl lactate are purchased from Jinan, Shandong Province nine divisions of China in remote antiquity Fu get Xiang in the present embodiment
Expect Co., Ltd；Coolant agent used is purchased from Jiangxi Jishui Lian Xing spice oil Co., Ltd, product name WS-3.
The physicochemical property and odor characteristic of each raw material such as table 1:
Table 1:
The cool taste Mint Essence the preparation method comprises the following steps:
(1) coolant agent is dissolved in propylene glycol, the solution that mass fraction is 10% is made；
(2) menthol, menthyl lactate and menthyl acetate are added into the solution of step (1), adds fat solvent
(olive oil), be uniformly mixed to get.
Embodiment 2: the preparation of the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette
Raw material composition:
By mass percentage, it is prepared from the following materials:
Menthol 4%, menthyl lactate 1%, menthyl acetate 2%, coolant agent 0.4%, surplus are neodecanoic acid glyceride.
Menthol, menthyl lactate, menthyl acetate and coolant agent source with embodiment 1.
The preparation method is the same as that of Example 1 for the cool taste Mint Essence.
Embodiment 3: the preparation of the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette
Raw material composition:
By mass percentage, it is prepared from the following materials:
Menthol 1%, menthyl lactate 10%, menthyl acetate 1%, coolant agent 0.5%, surplus are olive oil.
Menthol, menthyl lactate, menthyl acetate source with embodiment 1.
Coolant agent is L- menthones glycerol ketal (FEMA:3807).
The preparation method is the same as that of Example 1 for the cool taste Mint Essence.
Embodiment 4: the preparation of the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette
Raw material composition:
By mass percentage, it is prepared from the following materials:
Menthol 8%, menthyl lactate 1%, menthyl acetate 5%, coolant agent 0.2%, surplus are olive oil.
Menthol, menthyl lactate, menthyl acetate source with embodiment 1.
Coolant agent is N- ethyl-menthyl formamide (FEMA:3455).
The preparation method is the same as that of Example 1 for the cool taste Mint Essence.
Application examples 1: the preparation of the quick-fried pearl of peppermint cigarette
The preparation method is as follows:
By olive oil and Glycerin, mixed triester with caprylic acid capric acid, 1:2 is mixed by volume, then presses olive oil and Glycerin, mixed triester with caprylic acid capric acid total weight
0.3% be added emulsifier (sorbester p17), then stir evenly, in whipping process be added above-described embodiment 1 prepare peppermint
The cool taste Mint Essence of the quick-fried pearl of cigarette, additive amount are the 1.5% of olive oil and Glycerin, mixed triester with caprylic acid capric acid total weight, are further continued for stirring
0.5h completes process for preparation, is eventually fabricated the quick-fried pearl of peppermint cigarette.
Application examples 2: the preparation of the quick-fried pearl of peppermint cigarette
The preparation method is as follows:
By olive oil and Glycerin, mixed triester with caprylic acid capric acid, 1:2 is mixed by volume, then presses olive oil and Glycerin, mixed triester with caprylic acid capric acid total weight
0.3% be added emulsifier (sorbester p17), then stir evenly, in whipping process be added above-described embodiment 2 prepare peppermint
The cool taste Mint Essence of the quick-fried pearl of cigarette, additive amount are the 2% of olive oil and Glycerin, mixed triester with caprylic acid capric acid total weight, are further continued for stirring 0.5h,
Process for preparation is completed, the quick-fried pearl of peppermint cigarette is eventually fabricated.
Sensory quality assessment experiment:
The cool quick-fried pearl of taste peppermint in application examples 1-2 is added in cigarette filter rod, is carried out referring to national standard sensory evaluation method
Evaluation, pinches brokenly quick-fried pearl in aspiration procedure.Group of smokeing panel test is made of 9 cigarette sensory evaluation experts, using secretly commenting mode to carry out
Sensory quality assessment, sensory quality assessment table are as shown in table 2:
Table 2:
From table 2 it can be seen that the present invention can make to assign cigarette natural mint flavored and cool feeling when quick-fried pearl pinches brokenly, and
Without the medicinal herbs breath of menthol and irritation, it can be merged well with cigarette flavor, be effectively improved the comfort of cigarette smoking,
Promote cigarette smoking quality.
Comparative example 1: the preparation of the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette
The present inventor is investigated and has been studied to the plurality of raw materials with similar performance in R&D process, is as a result sent out
It is existing, even if the performance between certain several raw material is similar, but after the material combination use different from other, the whole effect realized
Fruit significant difference.For example, the investigation for the menthyl ester with menthol compatible use, the present invention is by the raw material prescription of embodiment 1
In menthyl lactate replace with menthyl carbonates, menthyl acetate is replaced with into isovaleric acid menthyl ester, the dosage of each raw material and
The preparation method is the same as that of Example 1, and cool taste Mint Essence is prepared.
The quick-fried pearl of peppermint cigarette is made by the method for application examples 1 in the cool taste Mint Essence of preparation, and the cool quick-fried pearl of taste peppermint is added
It is added in cigarette filter rod, is evaluated referring to national standard sensory evaluation method, quick-fried pearl is pinched brokenly in aspiration procedure, carry out aesthetic quality
Evaluation, as a result, it has been found that, the medicinal herbs breath of menthol, peppermint are still had by quick-fried pearl cigarette prepared by the cool taste Mint Essence of comparative example 1
The cool feeling duration is shorter, to the irritating effect of nose larynx.
Comparative example 2: the preparation of the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette
The dosage of each raw material can generate crucial effect, this hair to the overall performance of cool taste Mint Essence in cool taste Mint Essence
Bright people has carried out investigation and the research of function and effect to the content of each raw material in cool taste Mint Essence in R&D process, knot
Fruit discovery, inappropriate raw material proportioning relationship, function and effect significant difference.Such as: by the use of menthyl lactate in embodiment 1
Amount is adjusted to 15%, and the dosage of menthyl acetate is adjusted to 0.5%, and the dosage of coolant agent is adjusted to 1.0%, the use of other raw materials
Amount is prepared with embodiment 1, and as described in Example 1.
The quick-fried pearl of peppermint cigarette is made by the method for application examples 1 in the cool taste Mint Essence of preparation, and the cool quick-fried pearl of taste peppermint is added
It is added in cigarette filter rod, is evaluated referring to national standard sensory evaluation method, quick-fried pearl is pinched brokenly in aspiration procedure, carry out aesthetic quality
Evaluation, as a result, it has been found that, the medicinal herbs breath of menthol, flue gas are still had by quick-fried pearl cigarette prepared by the cool taste Mint Essence of comparative example 2
Thin, the peppermint cool feeling duration is shorter, to the irritating effect of nose larynx.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, those skilled in the art should understand that, based on the technical solutions of the present invention, those skilled in the art do not need
Make the creative labor the various modifications or changes that can be made still within protection scope of the present invention.
Claims (6)
1. a kind of cool taste Mint Essence of quick-fried pearl of peppermint cigarette, which is characterized in that be made of the raw material of following mass percent: thin
Lotus brain 1-8%, menthyl lactate 1-10%, menthyl acetate 1-5%, coolant agent 0.2-0.5%, surplus are fat solvent；It is described cool
Taste agent is selected from carbonic acid l-menthol glycol ester, L- menthones glycerol ketal, N- ethyl-menthyl formamide, L- peppermint oxygen
One of base propylene glycol or coolant agent WS-3 are a variety of；The fat solvent is selected from corn oil, olive oil or pungent capric acid glycerol
One of ester is a variety of.
2. the cool taste Mint Essence of the quick-fried pearl of peppermint cigarette as described in claim 1, which is characterized in that by following mass percent
Raw material is made: menthol 2-4%, menthyl lactate 1-2%, menthyl acetate 1-2%, coolant agent 0.2-0.4%, surplus are grease
Solvent.
3. the quick-fried pearl of peppermint cigarette of any of claims 1 or 2 is rolled up with cool taste Mint Essence in the quick-fried pearl of preparation peppermint cigarette or the quick-fried pearl of peppermint
Purposes in cigarette.
4. a kind of quick-fried pearl of peppermint cigarette, which is characterized in that contain a effective amount of cool taste Mint Essence of any of claims 1 or 2.
5. the preparation method of the quick-fried pearl of peppermint cigarette as claimed in claim 4, which is characterized in that steps are as follows: by olive oil and the pungent last of the ten Heavenly stems
1:2 is mixed acid glyceride by volume, then emulsifier is added by olive oil and the 0.2-0.5% of Glycerin, mixed triester with caprylic acid capric acid total weight, and
After stir evenly, the quick-fried pearl of peppermint cigarette cool taste Mint Essence, additive amount of any of claims 1 or 2 are added in whipping process
For the 1-2% of olive oil and Glycerin, mixed triester with caprylic acid capric acid total weight, it is further continued for stirring 0.5h, process for preparation is completed, is eventually fabricated peppermint cigarette
Quick-fried pearl.
6. a kind of quick-fried pearl cigarette of peppermint, which is characterized in that contain the quick-fried pearl of peppermint cigarette as claimed in claim 4.
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| CN112438427B (en) * | 2020-11-13 | 2022-09-09 | 山东中烟工业有限责任公司 | Cigarette blasting bead containing fruity mint essence, implantation device and method |
| CN113403141B (en) * | 2021-06-07 | 2023-03-21 | 上海应用技术大学 | Cool base with flower and fruit fragrance and preparation method thereof |
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| CN115226926A (en) * | 2022-08-16 | 2022-10-25 | 湖北中烟工业有限责任公司 | Mint essence, mint essence oil for cigarettes and cigarettes |
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| CN106281680A (en) | 2017-01-04 |
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