CN104585880A - Mint essence solvent for cigarette dropping pill - Google Patents
Mint essence solvent for cigarette dropping pill Download PDFInfo
- Publication number
- CN104585880A CN104585880A CN201510027473.5A CN201510027473A CN104585880A CN 104585880 A CN104585880 A CN 104585880A CN 201510027473 A CN201510027473 A CN 201510027473A CN 104585880 A CN104585880 A CN 104585880A
- Authority
- CN
- China
- Prior art keywords
- dripping pill
- mint essence
- cigarette
- solvent
- surfactant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000006187 pill Substances 0.000 title claims abstract description 114
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 77
- 239000002904 solvent Substances 0.000 title claims abstract description 59
- 235000006679 Mentha X verticillata Nutrition 0.000 title claims abstract description 32
- 235000002899 Mentha suaveolens Nutrition 0.000 title claims abstract description 32
- 235000001636 Mentha x rotundifolia Nutrition 0.000 title claims abstract description 32
- 239000004094 surface-active agent Substances 0.000 claims abstract description 45
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 27
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 27
- 229940041616 menthol Drugs 0.000 claims abstract description 27
- 235000008390 olive oil Nutrition 0.000 claims abstract description 16
- 239000004006 olive oil Substances 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 235000010469 Glycine max Nutrition 0.000 claims description 17
- 244000068988 Glycine max Species 0.000 claims description 17
- 241000196324 Embryophyta Species 0.000 claims description 15
- 239000002253 acid Substances 0.000 claims description 15
- 125000005456 glyceride group Chemical group 0.000 claims description 15
- 239000000839 emulsion Substances 0.000 claims description 14
- 229920001296 polysiloxane Polymers 0.000 claims description 14
- 239000002131 composite material Substances 0.000 claims description 13
- 229920002472 Starch Polymers 0.000 claims description 11
- 235000019698 starch Nutrition 0.000 claims description 11
- 239000008107 starch Substances 0.000 claims description 11
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 2
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 2
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 2
- 229920001817 Agar Polymers 0.000 claims description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 2
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 claims description 2
- 239000005642 Oleic acid Substances 0.000 claims description 2
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 2
- 239000008272 agar Substances 0.000 claims description 2
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 2
- 150000002617 leukotrienes Chemical class 0.000 claims description 2
- 235000020778 linoleic acid Nutrition 0.000 claims description 2
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 claims description 2
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 2
- 229920000136 polysorbate Polymers 0.000 claims description 2
- 125000005471 saturated fatty acid group Chemical group 0.000 claims description 2
- 239000000600 sorbitol Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 30
- 239000000203 mixture Substances 0.000 abstract description 13
- 239000000463 material Substances 0.000 abstract description 12
- 229920001971 elastomer Polymers 0.000 abstract description 5
- 239000006260 foam Substances 0.000 abstract 1
- 238000009413 insulation Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 abstract 1
- 244000246386 Mentha pulegium Species 0.000 description 42
- 235000016257 Mentha pulegium Nutrition 0.000 description 42
- 235000004357 Mentha x piperita Nutrition 0.000 description 42
- 235000001050 hortel pimenta Nutrition 0.000 description 42
- 230000008569 process Effects 0.000 description 25
- 230000000694 effects Effects 0.000 description 15
- 239000003507 refrigerant Substances 0.000 description 13
- 230000000391 smoking effect Effects 0.000 description 13
- 230000035807 sensation Effects 0.000 description 12
- 235000019615 sensations Nutrition 0.000 description 12
- 238000003756 stirring Methods 0.000 description 11
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 7
- 239000003546 flue gas Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- NEHNMFOYXAPHSD-UHFFFAOYSA-N citronellal Chemical compound O=CCC(C)CCC=C(C)C NEHNMFOYXAPHSD-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000006340 racemization Effects 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 description 2
- 206010002091 Anaesthesia Diseases 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 239000005844 Thymol Substances 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 230000037005 anaesthesia Effects 0.000 description 1
- 238000001949 anaesthesia Methods 0.000 description 1
- 230000001139 anti-pruritic effect Effects 0.000 description 1
- 239000003908 antipruritic agent Substances 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 229940112822 chewing gum Drugs 0.000 description 1
- 235000015218 chewing gum Nutrition 0.000 description 1
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 1
- 235000000983 citronellal Nutrition 0.000 description 1
- 229930003633 citronellal Natural products 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006356 dehydrogenation reaction Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000001525 mentha piperita l. herb oil Substances 0.000 description 1
- 150000002729 menthone derivatives Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000036407 pain Effects 0.000 description 1
- 235000019477 peppermint oil Nutrition 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 235000021147 sweet food Nutrition 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 229960000790 thymol Drugs 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
- Confectionery (AREA)
Abstract
The invention discloses mint essence solvent for a cigarette dropping pill. The mint essence solvent is proportionally mixed by the following raw materials in parts by weight: 1-40 parts of menthol, 20-80 parts of olive oil, 85-15 parts of medium chain triglyceride, and 0.1-1.5 parts of surfactant. The mint essence solvent is prepared by the following method: the above materials are uniformly mixed according to the proportion and placed in a reactor, and then stirred at the room temperature; the mixture is enabled to melt and subjected to heat insulation for 1-2 hours; the mixture is then placed in stationary manner until the foam disappears, and finally the obtained solution is the mint essence solvent encapsulated in the cigarette dropping pill. The mint essence solvent is matched with the physical and chemical properties of the dropping pill cover and can be completely encapsulated by the dropping pill rubber, so that the mint essence can be well encapsulated in the dropping pill rubber, the eccentric rate of dropping pill in which mint essence is encapsulated is low, the damage rate of products is low, and the consumption of raw materials is low.
Description
Technical field
The present invention relates to technical field of cigarettes, refer to a kind of Mint Essence solvent for cigarette dripping pill particularly.
Background technology
Menthol, a kind of terpene, also known as menthol, molecular formula C
10h
20O.Levorotatory menthol is water white transparency acicular crystal, fusing point 4 DEG C, boiling point 216.4 DEG C, and specific rotatory power-48 °, is slightly soluble in water, is dissolved in ethanol, ether, acetone, chloroform; Racemization menthol is water white transparency acicular crystal, fusing point 38 DEG C, and boiling point 216 DEG C, is dissolved in ethanol, ether, acetone, benzene.Menthol hydrogenation generates alkane; Menthones is obtained with chromic acid oxidation or catalytic dehydrogenation; Racemization menthol splits by benzoic acid esterification process.Menthol can be separated from peppermint oil and obtain, also can by citronellal or thymol manufacture.Menthol is a kind of important spices.Levorotatory menthol is due to its cooling effect, in a large number in cigarette, cosmetics, toothpaste, chewing gum, sweet food and medicine, inuncts, play the effects such as antipruritic, the pain relieving in local, refrigerant (mechanism: the cold receptor on chafe but do not cause actual temperature change) and slight local anaesthesia, also play permeation enhancers effect.
Containing menthol in peppermint, peppermint is that people compare a kind of spices being happy to benefit from, and the scope of application is very wide.In cigarette industry, utilize peppermint to make a kind of tobacco product-peppermint cigarette of specific type, suck and can give a kind of peppermint of people fragrance and refrigerant jealous sensation.This jealous effect and strong smoke harmony combine, and get consumer reception very much.
But because menthol has strong volatility and permeability, thus the loss of peppermint is very large in the fabrication process, and strong peppermint gas pollutes to surrounding environment simultaneously; Peppermint gas has strong impulse to the larynx of people, nose, eye and skin, makes staff be difficult to stand; In addition, the peppermint in manufactured goods easily scatters and disappears, thus unstable product quality; Etc. factor cause peppermint cigarette to be produced being restricted, and limits throughput.
Summary of the invention
For the above-mentioned deficiency of prior art, the invention provides the Mint Essence solvent of a kind of cigarette dripping pill parcel, the physicochemical property of this essence solvent and dripping pill rubber matches, and enables peppermint be wrapped in dripping pill, is placed in cigarette filter rod.This essence solvent can be rolled in dripping pill by complete packet, when not aspirating, does not have volatilization and loss.
For achieving the above object, the present invention is achieved by the following technical solutions:
For a Mint Essence solvent for cigarette dripping pill, it is characterized in that: it is mixed according to parts by weight proportioning by following component raw material, and the parts by weight of each component raw material are as follows:
Menthol 1 ~ 40 part, 20 ~ 80 parts, olive oil, pungent certain herbaceous plants with big flowers acid glyceride 85 ~ 15 parts, 0.1 ~ 1.5 part, surfactant.
In technique scheme, in described olive oil, the weight percentage of each component is saturated fatty acid 10% ~ 18%, oleic acid 55% ~ 83%, linoleic acid 3.5% ~ 21%, leukotrienes 0.3% ~ 1.5%.
In technique scheme, the weight percentage of described menthol is 60% ~ 98%.
In technique scheme, the weight percentage of described pungent certain herbaceous plants with big flowers acid glyceride is 80% ~ 99.9%.
In technique scheme, described surfactant is one or more in sorbitol, tween, modified soy bean lipoid, agar, hydroxypropul starch, silicone emulsion, glycerin monostearate etc.
As preferably, described surfactant is modified soy bean lipoid.
As preferably, described surfactant is modified soy bean lipoid and silicone emulsion according to weight part ratio is the composite surfactant of 1:1.
As more preferably, described surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
The invention has the advantages that:
First: the physicochemical property of this essence solvent and dripping pill rubber matches, by the complete parcel of dripping pill rubber, can realize the good parcel of Mint Essence in dripping pill, the dripping pill eccentricity being enclosed with Mint Essence is low, product breakage rate is low, and consumption of raw materials is little.
Second: peppermint is wrapped in dripping pill, ensureing that cigarette does not have volatilization and loss when not aspirating, having reduced the loss of peppermint simultaneously in the fabrication process.
3rd: the peppermint in manufactured goods is not easy volatilization, scatters and disappears, the stability of product quality improves, and when smoking cigarette, dripping pill can be pinched brokenly, discharge the Mint Essence of parcel, and flue gas, by peppermint, takes cooling taste out of, improves the sensory effects of cigarette smoking.
4th: adopt composite surfactant, the consumption of surfactant can not only be reduced, reduce costs, and can result of use be improved, make parcel effective, can be easy to as required crumb during suction, pure and fresh for peppermint breath is discharged fast.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.Following examples are experimental data.
Embodiment 1:
By proportioning listed in table 1, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1 hour, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
Table 1 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 35 |
| Olive oil | Food-grade | 20 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 43.8 |
| Surfactant | Food-grade | 1.2 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and production stability is better, and dripping pill breakage rate is low, and yield rate is 86%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled the refrigerant sense of peppermint in taste and is obviously strengthened, and flue gas pleasant impression is comfortable, returns sense by force.
Embodiment 2:
By proportioning listed in table 2, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
Table 2 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 35 |
| Olive oil | Food-grade | 20 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 43.8 |
| Surfactant | Food-grade | 1.2 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and production stability is better, and dripping pill breakage rate is low, and yield rate is 90%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled the refrigerant sense of peppermint in taste and is obviously strengthened, and flue gas pleasant impression is comfortable, returns sense by force.
Embodiment 3:
By proportioning listed in table 3, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 2 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
Table 3 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 35 |
| Olive oil | Food-grade | 20 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 43.8 |
| Surfactant | Food-grade | 1.2 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and production stability is better, and dripping pill breakage rate is low, and yield rate is 90%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled the refrigerant sense of peppermint in taste and is obviously strengthened, and flue gas pleasant impression is comfortable, returns sense by force.
Embodiment 4:
By proportioning listed in table 4, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
Table 4 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 2 |
| Olive oil | Food-grade | 80 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 17.5 |
| Surfactant | Food-grade | 0.5 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and easily occur the situation that content (the essence solvent namely wrapped up) is eccentric, dripping pill breakage rate is higher, and yield rate is 50%.During cigarette smoking, pinch brokenly peppermint dripping pill, it is not obvious that sensation inhales refrigerant sense in taste.
Embodiment 5:
By proportioning listed in table 5, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
Table 4 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 5 |
| Olive oil | Food-grade | 60 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 34.2 |
| Surfactant | Food-grade | 0.8 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and to a certain degree can occur the situation that content (the essence solvent namely wrapped up) is eccentric, dripping pill breakage rate is general, and yield rate is 65%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled in taste more weak refrigerant sense.
Embodiment 6:
By proportioning listed in table 6, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
Table 6 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 15 |
| Olive oil | Food-grade | 40 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 44 |
| Surfactant | Food-grade | 1 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and not easily occur the situation that content (the essence solvent namely wrapped up) is eccentric, dripping pill breakage rate is lower, and yield rate is 78%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled in taste certain refrigerant sense.
Embodiment 7:
By proportioning listed in table 7, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
Table 7 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 35 |
| Olive oil | Food-grade | 20 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 43.8 |
| Surfactant | Food-grade | 1.2 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and production stability is better, and dripping pill breakage rate is low, and yield rate is 90%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled the refrigerant sense of peppermint in taste and is obviously strengthened, and flue gas pleasant impression is comfortable, returns sense by force.
Embodiment 8:
By proportioning listed in table 8, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid.
Table 8 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 35 |
| Olive oil | Food-grade | 20 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 43.8 |
| Surfactant | Food-grade | 1.2 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and be not easy the situation occurring that content (the essence solvent namely wrapped up) is eccentric, dripping pill there will be certain breakage, and yield rate is 80%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled the refrigerant sense of peppermint in taste and is obviously strengthened, and flue gas pleasant impression is comfortable, returns sense by force.
Embodiment 9:
By proportioning listed in table 9, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid.
Table 9 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 15 |
| Olive oil | Food-grade | 40 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 44 |
| Surfactant | Food-grade | 1 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and be not easy the situation occurring that content (the essence solvent namely wrapped up) is eccentric, dripping pill breakage rate is lower, and yield rate is 72%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled in taste certain refrigerant sense.
Embodiment 10:
By proportioning listed in table 10, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid and silicone emulsion according to weight part ratio is the composite surfactant of 1:1.
Table 10 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 35 |
| Olive oil | Food-grade | 20 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 43.8 |
| Surfactant | Food-grade | 1.2 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and be not easy the situation occurring that content (the essence solvent namely wrapped up) is eccentric, dripping pill breakage rate is lower, and yield rate is 85%.During cigarette smoking, pinch brokenly peppermint dripping pill, it is obvious that sensation inhales refrigerant sense in taste, and flue gas pleasant impression is comfortable.
Embodiment 11:
By proportioning listed in table 11, by mixing of materials evenly and be placed in retort stirring at normal temperature, mixture is dissolved, be incubated 1.5 hours, leave standstill, treat lather collapse, gained solution is the Mint Essence solvent that cigarette dripping pill wraps up.Wherein surfactant is modified soy bean lipoid and silicone emulsion according to weight part ratio is the composite surfactant of 1:1.
Table 11 solvent burden ratio
| Solvent kind | Specification | Ratio |
| Menthol | Food-grade | 15 |
| Olive oil | Food-grade | 40 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Food-grade | 44 |
| Surfactant | Food-grade | 1 |
Use dropping-pill machine to make cigarette dripping pill, in cigarette filter rod wire-beam forming process, location applies dripping pill, makes cigarette, evaluates the effect of peppermint dripping pill.Dripping pill is in dripping process, and be not easy the situation occurring that content (the essence solvent namely wrapped up) is eccentric, dripping pill breakage rate is lower, and yield rate is 76%.During cigarette smoking, pinch brokenly peppermint dripping pill, sensation is inhaled in taste certain refrigerant sense.
Claims (6)
1. for a Mint Essence solvent for cigarette dripping pill, it is characterized in that: it is mixed according to parts by weight proportioning by following component raw material, and the parts by weight of each component raw material are as follows:
Menthol 1 ~ 40 part, 20 ~ 80 parts, olive oil, pungent certain herbaceous plants with big flowers acid glyceride 85 ~ 15 parts, 0.1 ~ 1.5 part, surfactant.
2. a kind of Mint Essence solvent for cigarette dripping pill according to claim 1, is characterized in that: in described olive oil, the weight percentage of each component is saturated fatty acid 10% ~ 18%, oleic acid 55% ~ 83%, linoleic acid 3.5% ~ 21%, leukotrienes 0.3% ~ 1.5%.
3. a kind of Mint Essence solvent for cigarette dripping pill according to claim 1 and 2, is characterized in that: the weight percentage of described menthol is 60% ~ 98%.
4. a kind of Mint Essence solvent for cigarette dripping pill according to claim 1 and 2, is characterized in that: the weight percentage of described pungent certain herbaceous plants with big flowers acid glyceride is 80% ~ 99.9%.
5. a kind of Mint Essence solvent for cigarette dripping pill according to claim 1 and 2, is characterized in that: described surfactant is one or more in sorbitol, tween, modified soy bean lipoid, agar, hydroxypropul starch, silicone emulsion, glycerin monostearate etc.
6. a kind of Mint Essence solvent for cigarette dripping pill according to claim 5, is characterized in that: described surfactant is modified soy bean lipoid, hydroxypropul starch and silicone emulsion according to weight part ratio is the composite surfactant of 1:1:2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510027473.5A CN104585880B (en) | 2015-01-20 | 2015-01-20 | A kind of Mint Essence solvent for cigarette dripping pill |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510027473.5A CN104585880B (en) | 2015-01-20 | 2015-01-20 | A kind of Mint Essence solvent for cigarette dripping pill |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104585880A true CN104585880A (en) | 2015-05-06 |
| CN104585880B CN104585880B (en) | 2018-06-08 |
Family
ID=53112211
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510027473.5A Active CN104585880B (en) | 2015-01-20 | 2015-01-20 | A kind of Mint Essence solvent for cigarette dripping pill |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104585880B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106281680A (en) * | 2016-08-27 | 2017-01-04 | 山东中烟工业有限责任公司 | A kind of quick-fried pearl of Herba Menthae cigarette cool taste Mint Essence and preparation method and application |
| CN106387996A (en) * | 2016-09-08 | 2017-02-15 | 合肥智慧殿投资管理有限公司 | Adsorbent capable of decreasing ammonia and crotonaldehyde in smoke of cigarette, and preparation method and use thereof |
| CN106509982A (en) * | 2016-11-18 | 2017-03-22 | 湖北中烟工业有限责任公司 | High-cold-degree essence solution for cigarette dropping pill and preparation method thereof |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
| CN109171014A (en) * | 2018-10-11 | 2019-01-11 | 湖北中烟工业有限责任公司 | A kind of menthol eutectic solvent and cigarette capsule |
| JP2020188805A (en) * | 2016-05-20 | 2020-11-26 | ブリティッシュ アメリカン タバコ （インヴェストメンツ） リミテッドＢｒｉｔｉｓｈ Ａｍｅｒｉｃａｎ Ｔｏｂａｃｃｏ （Ｉｎｖｅｓｔｍｅｎｔｓ） Ｌｉｍｉｔｅｄ | Tobacco industrial product capsule |
| CN113163846A (en) * | 2018-12-31 | 2021-07-23 | 菲利普莫里斯生产公司 | Liquid nicotine formulation |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6852309B2 (en) * | 2002-07-18 | 2005-02-08 | Suheung Capsule Co., Ltd | Gelatin soft capsule having the properties of removal of oral smell and cleaning of oral cavity |
| CN1795900A (en) * | 2004-12-27 | 2006-07-05 | 孙梅君 | Soft capsule of acetic acid of hawkthorn, and preparation method |
| CN1803153A (en) * | 2005-09-01 | 2006-07-19 | 安徽威尔曼振星药业有限公司 | Toad essence capsule and its preparation method |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN101766332A (en) * | 2009-12-31 | 2010-07-07 | 云南烟草科学研究院 | Pills capable of adding fragrance to cigarettes |
| US20120064136A1 (en) * | 2010-09-10 | 2012-03-15 | Nanobio Corporation | Anti-aging and wrinkle treatment methods using nanoemulsion compositions |
| EP2755623A1 (en) * | 2011-09-14 | 2014-07-23 | University of Florida | Smarttm solid oral dosage forms |
-
2015
- 2015-01-20 CN CN201510027473.5A patent/CN104585880B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6852309B2 (en) * | 2002-07-18 | 2005-02-08 | Suheung Capsule Co., Ltd | Gelatin soft capsule having the properties of removal of oral smell and cleaning of oral cavity |
| CN1795900A (en) * | 2004-12-27 | 2006-07-05 | 孙梅君 | Soft capsule of acetic acid of hawkthorn, and preparation method |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN1803153A (en) * | 2005-09-01 | 2006-07-19 | 安徽威尔曼振星药业有限公司 | Toad essence capsule and its preparation method |
| CN101766332A (en) * | 2009-12-31 | 2010-07-07 | 云南烟草科学研究院 | Pills capable of adding fragrance to cigarettes |
| US20120064136A1 (en) * | 2010-09-10 | 2012-03-15 | Nanobio Corporation | Anti-aging and wrinkle treatment methods using nanoemulsion compositions |
| EP2755623A1 (en) * | 2011-09-14 | 2014-07-23 | University of Florida | Smarttm solid oral dosage forms |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2020188805A (en) * | 2016-05-20 | 2020-11-26 | ブリティッシュ アメリカン タバコ （インヴェストメンツ） リミテッドＢｒｉｔｉｓｈ Ａｍｅｒｉｃａｎ Ｔｏｂａｃｃｏ （Ｉｎｖｅｓｔｍｅｎｔｓ） Ｌｉｍｉｔｅｄ | Tobacco industrial product capsule |
| CN106281680A (en) * | 2016-08-27 | 2017-01-04 | 山东中烟工业有限责任公司 | A kind of quick-fried pearl of Herba Menthae cigarette cool taste Mint Essence and preparation method and application |
| CN106281680B (en) * | 2016-08-27 | 2019-11-26 | 山东中烟工业有限责任公司 | A kind of quick-fried pearl of peppermint cigarette cool taste Mint Essence and the preparation method and application thereof |
| CN106387996A (en) * | 2016-09-08 | 2017-02-15 | 合肥智慧殿投资管理有限公司 | Adsorbent capable of decreasing ammonia and crotonaldehyde in smoke of cigarette, and preparation method and use thereof |
| CN106509982A (en) * | 2016-11-18 | 2017-03-22 | 湖北中烟工业有限责任公司 | High-cold-degree essence solution for cigarette dropping pill and preparation method thereof |
| CN106509982B (en) * | 2016-11-18 | 2018-05-25 | 湖北中烟工业有限责任公司 | Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
| CN109171014A (en) * | 2018-10-11 | 2019-01-11 | 湖北中烟工业有限责任公司 | A kind of menthol eutectic solvent and cigarette capsule |
| CN113163846A (en) * | 2018-12-31 | 2021-07-23 | 菲利普莫里斯生产公司 | Liquid nicotine formulation |
| CN113163846B (en) * | 2018-12-31 | 2023-04-28 | 菲利普莫里斯生产公司 | Liquid nicotine formulation |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104585880B (en) | 2018-06-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104585880A (en) | Mint essence solvent for cigarette dropping pill | |
| CN106281680B (en) | A kind of quick-fried pearl of peppermint cigarette cool taste Mint Essence and the preparation method and application thereof | |
| RU2403831C1 (en) | Smokeless tobacco product (snus) production method (versions) | |
| CN106753787B (en) | Bead-blasting lemon mint essential oil for cigarettes as well as preparation method and application thereof | |
| CN101130715B (en) | Peony essential oil abstracted from supercritical CO* fluid and application of the same in perfuming cigarette | |
| CN108179066B (en) | Honeysuckle mint essential oil for cigarette bead blasting and preparation method and application thereof | |
| CN103704659B (en) | A kind of maple flavor formula | |
| CN105542958A (en) | Additive and method for supplementing sweetness and fragrance of cigarette | |
| CN104531356A (en) | Honeyed-sweet additive and electronic cigarette liquid with same | |
| KR20220129029A (en) | Capsules for flavored tobacco and manufacturing method thereof | |
| CN102994228A (en) | Preparation method of tobacco absolute | |
| CN102038625B (en) | Fruit powder type oral flavor correction refreshing agent and preparation method thereof | |
| CN103555424B (en) | Tomato essence | |
| CN105670790A (en) | Tobacco flavor with natural sweet fruity aroma characteristics and preparation method thereof | |
| MX2014008366A (en) | 1-vinylcyclohex-3-ene carbaldehyde and 4-vinylcyclohex-1-ene carbaldehyde for use in flavour and oral care compositions. | |
| CN106509982B (en) | Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof | |
| KR20220162136A (en) | Compositions containing menthol | |
| CN1986759A (en) | Petroleum extracted sophora flower extractum and its application in perfuming cigarette | |
| CN105925375B (en) | Composite tobacco essence, preparation method and application thereof | |
| CN107080168A (en) | A kind of vanilla method for making noodles | |
| CN104830534B (en) | A kind of preparation method of tomato extract and its application in production of cigarettes | |
| CN103666764A (en) | Cooling peppermint tobacco flavor composition | |
| JP6001031B2 (en) | Flavor modulator | |
| CN105062688A (en) | Manufacturing method of lemon hydrolat and application thereof | |
| CN110680947A (en) | Lavender slow-release fragrance source body and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |