CN108219958A - A kind of quick-fried pearl fragrance and preparation method thereof, quick-fried pearl and the application of quick-fried pearl - Google Patents
A kind of quick-fried pearl fragrance and preparation method thereof, quick-fried pearl and the application of quick-fried pearl Download PDFInfo
- Publication number
- CN108219958A CN108219958A CN201810181790.6A CN201810181790A CN108219958A CN 108219958 A CN108219958 A CN 108219958A CN 201810181790 A CN201810181790 A CN 201810181790A CN 108219958 A CN108219958 A CN 108219958A
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- China
- Prior art keywords
- quick
- fried pearl
- fragrance
- snuff
- preparation
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to tobacco curing technical fields, provide a kind of quick-fried pearl fragrance and preparation method thereof, preparation method includes：The volatile oil that water and snuff powder are placed in extractor in distillation snuff powder is obtained into oil water mixture, the first extractant is placed in the oil water mixture for extracting in oil water separator and being distilled in extractor and obtains volatile oil.The snuff powder residue in extractor is taken out, using solvent extraction, extracts 0.5~2h under conditions of being 70~80 DEG C in ultrasound, temperature, filtering, liquid separation obtain the active constituent in snuff powder residue.Volatile oil and active constituent are mixed to get quick-fried pearl fragrance.This method is easy to operate, and quick-fried pearl fragrance obtained has the peat-reek of snuff.The present invention also provides a kind of quick-fried pearls, and above-mentioned quick-fried pearl fragrance is used to be made, which pinches the quick-fried rear fragrance with snuff.The quick-fried pearl is applied to when smelling cigarette and cigarette, can to smell cigarette and cigarette have effects that the special aroma of snuff and.
Description
Technical field
The present invention relates to tobacco curing technical field, in particular to a kind of quick-fried pearl fragrance and preparation method thereof, quick-fried pearl and quick-fried
The application of pearl.
Background technology
Snuff belongs to a kind of smoke-free tobacco product, and user is played mainly by way of hearing suction, smelling suction using snuff
Solution smoking addiction refreshes the mind, functional health, the functions such as aromatotherapy.Snuff is modulated by fermenting tobacco leaf powder, contemporary world nose
Cigarette has more than 1000 kinds, main flavor have tobacco, peppermint, dry fruit, berry, flower, herbal medicine, coffee, aroma, Radix Aucklandiae, soil, leather,
Moschus, ambergris etc..The fragrance and taste of snuff are more unique and abundant.
" quick-fried pearl " refers to a small glue bead of liquid in tobacco filter, it has wrapped up the liquid of different type fragrance
Body, smoker can pinch quick-fried in smoking process, flow out in pearl liquid, the mouthfeel for making cigarette is more rich, and more fragrant profit makes smoking
Person obtains more comfortably experiencing.Certainly, that glue bead must be pinched voluntarily quick-fried manually, then can root for pinching quick-fried time point
It arranges by oneself according to hobby.
Invention content
It is easy to operate the present invention provides a kind of preparation method of quick-fried pearl fragrance, it can be made quick-fried with snuff fragrance
Pearl fragrance.
The present invention also provides a kind of quick-fried pearl fragrance, with special snuff fragrance.
The present invention also provides a kind of quick-fried pearl, with special snuff fragrance.
The present invention also provides application of the above-mentioned quick-fried pearl with snuff fragrance in cigarette is smelt, and making to apply has smelling for this quick-fried pearl
Smoking set has special snuff fragrance and effect.
The present invention also provides application of the above-mentioned quick-fried pearl with snuff fragrance in cigarette, make using the volume for having this quick-fried pearl
Smoking set has special snuff fragrance and effect.
The invention is realized in this way：
A kind of preparation method of quick-fried pearl fragrance, includes the following steps：
The volatile oil that water and snuff powder are placed in extractor in distillation snuff powder is obtained into oil water mixture, distillation time 11
First extractant is placed in the oil water mixture for extracting in oil water separator and being distilled in extractor and obtains volatile oil by~20h；
The snuff powder residue in extractor is taken out, using solvent extraction, under conditions of ultrasound, temperature are 70~80 DEG C
0.5~2h is extracted, filtering, liquid separation obtain the active constituent in snuff powder residue；
Volatile oil and active constituent are mixed to get quick-fried pearl fragrance.
Further, in preferred embodiments of the present invention, the first extractant is pungent capric acid glyceride, is taken after extraction
Supernatant liquor is up to volatile oil.
Further, in preferred embodiments of the present invention, the mass ratio of the first extractant and snuff powder is 9~11:1.
Further, in preferred embodiments of the present invention, the extractant that solvent extraction is selected is the second extractant, the
Two extractants are pungent capric acid glyceride.
Further, in preferred embodiments of the present invention, the mass ratio of the second extractant and snuff powder residue is 1:4~
6。
Further, in preferred embodiments of the present invention, in oil water separator, snuff powder is located on liquid level.
A kind of quick-fried pearl fragrance, it is made using the preparation method of above-mentioned quick-fried pearl fragrance.
A kind of quick-fried pearl is made using above-mentioned quick-fried pearl fragrance.
Application of the above-mentioned quick-fried pearl in cigarette is smelt.
Application of the above-mentioned quick-fried pearl in cigarette.
The beneficial effects of the invention are as follows：The preparation method of quick-fried pearl fragrance that the present invention is obtained by above-mentioned design, due to only
Active constituent and volatile oil and active constituent mixing step is obtained by extraction including distilling, extracting extraction volatile oil and solution, therefore
Its operating method is simple.Since the quick-fried pearl fragrance uses snuff powder as raw material so that last quick-fried pearl fragrance obtained has snuff
Special aroma, and the preparation method, the volatile oil being extracted respectively in snuff and the active constituent with fragrance and activity will
Quick-fried pearl fragrance aroma obtained is strong after volatile oil and active constituent mixing and has been rich in the active flavor components in snuff powder.
The quick-fried pearl fragrance that the present invention is obtained by above-mentioned design, due to the preparation side using quick-fried pearl fragrance provided by the invention
Method is made, thus its have effects that the peat-reek of snuff and.
The quick-fried pearl that the present invention is obtained by above-mentioned design, since it uses quick-fried pearl fragrance provided by the invention to be made, therefore its
Pinch it is quick-fried after have effects that the peat-reek of snuff and.
When quick-fried pearl provided by the invention in cigarette is smelt in application, pinch quick-fried pearl, can be so that smelling smoking set has the special perfume (or spice) of snuff
Taste and effect.
When quick-fried pearl provided by the invention in cigarette in application, pinch quick-fried pearl, can be so that cigarette has the special perfume (or spice) of snuff
Taste and effect.
Specific embodiment
Purpose, technical scheme and advantage to make the embodiment of the present invention are clearer, below will be in the embodiment of the present invention
Technical solution be clearly and completely described.The person that is not specified actual conditions in embodiment, builds according to normal condition or manufacturer
The condition of view carries out.Reagents or instruments used without specified manufacturer is the conventional production that can be obtained by commercially available purchase
Product.
A kind of quick-fried pearl fragrance and preparation method thereof, quick-fried pearl and application is provided the embodiment of the present invention below to carry out specifically
It is bright.
A kind of preparation method of quick-fried pearl fragrance, includes the following steps：
S1, the volatile oil that water and snuff powder are placed in extractor in distillation snuff powder is obtained into oil water mixture, distillation time
For 11~20h, the first extractant is placed in the oil water mixture for extracting in oil water separator and being distilled in extractor to volatilize
Oil.
Specifically, high-quality traditional zymotic snuff powder is chosen as raw material, adds in water into extractor and snuff powder is distilled
Operation, it is preferable that in distillation process, snuff powder is placed in the upper area of extractor, is not connect positioned at the top of liquid level with liquid level
It touches, this mode is distilled so that distilling obtained volatile oil all in distillate, conducive to the separation of later stage volatile oil.Distillation 11
Terminating distillation after~20h, the distillate distilled is oil water mixture, this oil water mixture is placed in oil water separator,
And the first extractant is added in into oil water separator, supernatant liquor is taken after extraction up to volatile oil.
Preferably, the first extractant be pungent capric acid glyceride, colourless, the tasteless and nontoxic transparent liquid of pungent capric acid glyceride
Body, viscosity is low, is the half of general vegetable oil.Solidification point is low, and oxidation stability is good.With various solvents, grease, some oxidations
Agent, vitamin have good intersolubility, and emulsibility, dissolubility, extensibility and lubricity are better than common grease.Using pungent
Capric acid glyceride is as extractant, and effect of extracting is good, liquid separation process is convenient.
Further, to ensure that extraction is more abundant, the mass ratio of the first extractant and snuff powder is 9~11:1.
Snuff powder residue in S2, taking-up extractor, using solvent extraction, in ultrasound, the item that temperature is 70~80 DEG C
0.5~2h is extracted under part, filtering, liquid separation obtain the active constituent in snuff powder residue.
Specifically, the snuff powder residue after being distilled in extractor is taken out, be placed in container, using solvent extraction, to
The second extractant is wherein added in, 0.5~2h is extracted under conditions of being 70~80 DEG C in ultrasound, temperature, after extraction, filters
To mixing filtrate, then carry out liquid separation and subnatant is taken to obtain active constituent.
Preferably, the second extractant is also pungent capric acid glyceride.More preferable to guarantee active constituent purity, then adding in
The amount of two extractants then needs control in appropriate range, it is preferable that the mass ratio of the second extractant and snuff powder residue is 1:4~
6。
S3, volatile oil and active constituent are mixed to get quick-fried pearl fragrance.
Active constituent made from volatile oil made from S1 steps and S2 steps is mixed to get quick-fried pearl fragrance.
The preparation method of above-mentioned quick-fried pearl fragrance, operating procedure is simple, easily operated, and quick-fried pearl fragrance obtained has snuff
The special aroma of powder.
A kind of quick-fried pearl fragrance is made using the preparation method of above-mentioned quick-fried pearl fragrance.
A kind of quick-fried pearl is made using above-mentioned quick-fried pearl fragrance.
Application of the above-mentioned quick-fried pearl in cigarette is smelt smells the unique snuff powder fragrance of cigarette to assign.
Application of the above-mentioned quick-fried pearl in cigarette, to assign cigarette unique snuff powder fragrance.
A kind of preparation method of quick-fried pearl fragrance provided by the invention is specifically described below in conjunction with specific embodiment.
Embodiment 1
The present invention provides a kind of quick-fried pearl fragrance and its preparation method, preparation method is as follows：
Water is added in into extractor, using traditional snuff powder as raw material, snuff powder is positioned over extractor top, positioned at liquid level
Top, distilled, after distilling 11h, will distill obtained oil water mixture collect it is spare.
Oil water mixture is added in oil water separator, and pungent capric acid glyceride, pungent capric acid are added in into oil water separator
The addition of glyceride is 9 with the mass ratio of snuff powder:1.Liquid separation is carried out after extraction, takes supernatant liquor up to volatile oil.
Snuff powder residue after distillation is subjected to solvent extraction, using pungent capric acid glyceride as extractant, in ultrasound, temperature
It extracts 0.5h under conditions of being 70 DEG C, after the completion of extraction process, filters to get filtrate, filtrate is then subjected to liquid separation, it is clear to remove layer
Liquid obtains active constituent.
Volatile oil is mixed with active constituent to get quick-fried pearl fragrance.
Embodiment 2
The present invention provides a kind of quick-fried pearl fragrance and its preparation method, preparation method is as follows：
Water is added in into extractor, using traditional snuff powder as raw material, snuff powder is positioned over extractor top, positioned at liquid level
Top, distilled, after distilling 20h, will distill obtained oil water mixture collect it is spare.
Oil water mixture is added in oil water separator, and pungent capric acid glyceride, pungent capric acid are added in into oil water separator
The addition of glyceride is 11 with the mass ratio of snuff powder:1.Liquid separation is carried out after extraction, takes supernatant liquor up to volatile oil.
Snuff powder residue after distillation is subjected to solvent extraction, using pungent capric acid glyceride as extractant, in ultrasound, temperature
It extracts 2h under conditions of being 80 DEG C, after the completion of extraction process, filters to get filtrate, filtrate is then subjected to liquid separation, takes subnatant
Obtain active constituent.
Volatile oil is mixed with active constituent to get quick-fried pearl fragrance.
Embodiment 3
The present invention provides a kind of quick-fried pearl fragrance and its preparation method, preparation method is as follows：
Water is added in into extractor, using traditional snuff powder as raw material, snuff powder is positioned over extractor top, positioned at liquid level
Top, distilled, after distilling 15h, will distill obtained oil water mixture collect it is spare.
Oil water mixture is added in oil water separator, and pungent capric acid glyceride, pungent capric acid are added in into oil water separator
The addition of glyceride is 10 with the mass ratio of snuff powder:1.Liquid separation is carried out after extraction, takes supernatant liquor up to volatile oil.
Snuff powder residue after distillation is subjected to solvent extraction, using pungent capric acid glyceride as extractant, in ultrasound, temperature
It extracts 0.8h under conditions of being 72 DEG C, after the completion of extraction process, filters to get filtrate, filtrate is then subjected to liquid separation, it is clear to remove layer
Liquid obtains active constituent.
Volatile oil is mixed with active constituent to get quick-fried pearl fragrance.
Embodiment 4
The present invention provides a kind of quick-fried pearl fragrance and its preparation method, preparation method is as follows：
Water is added in into extractor, using traditional snuff powder as raw material, snuff powder is positioned over extractor top, positioned at liquid level
Top, distilled, after distilling 13h, will distill obtained oil water mixture collect it is spare.
Oil water mixture is added in oil water separator, and pungent capric acid glyceride, pungent capric acid are added in into oil water separator
The addition of glyceride is 9.5 with the mass ratio of snuff powder:1.Liquid separation is carried out after extraction, takes supernatant liquor up to volatile oil.
Snuff powder residue after distillation is subjected to solvent extraction, using pungent capric acid glyceride as extractant, in ultrasound, temperature
It extracts 1h under conditions of being 75 DEG C, after the completion of extraction process, filters to get filtrate, filtrate is then subjected to liquid separation, takes subnatant
Obtain active constituent.
Volatile oil is mixed with active constituent to get quick-fried pearl fragrance.
Embodiment 5
The present invention provides a kind of quick-fried pearl fragrance and its preparation method, preparation method is as follows：
Water is added in into extractor, using traditional snuff powder as raw material, snuff powder is positioned over extractor top, positioned at liquid level
Top, distilled, after distilling 18h, will distill obtained oil water mixture collect it is spare.
Oil water mixture is added in oil water separator, and pungent capric acid glyceride, pungent capric acid are added in into oil water separator
The addition of glyceride is 10.5 with the mass ratio of snuff powder:1.Liquid separation is carried out after extraction, takes supernatant liquor up to volatile oil.
Snuff powder residue after distillation is subjected to solvent extraction, using pungent capric acid glyceride as extractant, in ultrasound, temperature
It extracts 1.8h under conditions of being 78 DEG C, after the completion of extraction process, filters to get filtrate, filtrate is then subjected to liquid separation, it is clear to remove layer
Liquid obtains active constituent.
Volatile oil is mixed with active constituent to get quick-fried pearl fragrance.
Embodiment 6
The present invention provides a kind of quick-fried pearl fragrance and its preparation method, preparation method is as follows：
Water is added in into extractor, using traditional snuff powder as raw material, snuff powder is positioned over extractor top, positioned at liquid level
Top, distilled, after distilling 19h, will distill obtained oil water mixture collect it is spare.
Oil water mixture is added in oil water separator, and pungent capric acid glyceride, pungent capric acid are added in into oil water separator
The addition of glyceride is 10.8 with the mass ratio of snuff powder:1.Liquid separation is carried out after extraction, takes supernatant liquor up to volatile oil.
Snuff powder residue after distillation is subjected to solvent extraction, using pungent capric acid glyceride as extractant, in ultrasound, temperature
It extracts 1.5h under conditions of being 74 DEG C, after the completion of extraction process, filters to get filtrate, filtrate is then subjected to liquid separation, it is clear to remove layer
Liquid obtains active constituent.
Volatile oil is mixed with active constituent to get quick-fried pearl fragrance.
In conclusion the preparation method of quick-fried pearl fragrance provided by the invention, due to only including distillation, extraction extraction volatile oil
Active constituent and volatile oil and active constituent mixing step is obtained by extraction with solution, therefore its operating method is simple.Since this is quick-fried
Pearl fragrance uses snuff powder as raw material so that and last quick-fried pearl fragrance obtained has the special aroma of snuff, and the preparation method,
The volatile oil being extracted respectively in snuff and the active constituent with fragrance and activity, make after volatile oil and active constituent are mixed
The quick-fried pearl fragrance aroma obtained is strong and has been rich in the active flavor components in snuff powder.
The quick-fried pearl fragrance that the present invention is obtained by above-mentioned design, due to the preparation side using quick-fried pearl fragrance provided by the invention
Method is made, therefore its peat-reek with snuff.
The quick-fried pearl that the present invention is obtained by above-mentioned design, since it uses quick-fried pearl fragrance provided by the invention to be made, therefore its
Pinch the quick-fried rear peat-reek with snuff.When the quick-fried pearl is applied to smell cigarette and cigarette, it can to smell cigarette and cigarette is respectively provided with nose
The peat-reek of cigarette.
The foregoing is merely the preferred embodiment of the present invention, are not intended to restrict the invention, for this field
For technical staff, the invention may be variously modified and varied.All within the spirits and principles of the present invention, that is made is any
Modification, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of preparation method of quick-fried pearl fragrance, which is characterized in that include the following steps：
Water and snuff powder are placed in extractor and distills the volatile oil in snuff powder and obtains oil water mixture, distillation time for 11~
First extractant is placed in the oil water mixture for extracting in oil water separator and being distilled in extractor and obtains volatile oil by 20h；
The snuff powder residue in the extractor is taken out, using solvent extraction, under conditions of ultrasound, temperature are 70~80 DEG C
0.5~2h is extracted, filtering, liquid separation obtain the active constituent in the snuff powder residue；
The volatile oil and the active constituent are mixed to get quick-fried pearl fragrance.
2. the preparation method of quick-fried pearl fragrance according to claim 1, which is characterized in that first extractant is pungent capric acid
Glyceride takes supernatant liquor up to the volatile oil after extraction.
3. the preparation method of quick-fried pearl fragrance according to claim 2, which is characterized in that first extractant and the nose
The mass ratio of tobacco powder is 9~11:1.
4. the preparation method of quick-fried pearl fragrance according to claim 1, which is characterized in that the extraction that the solvent extraction is selected
Agent is taken as the second extractant, second extractant is pungent capric acid glyceride.
5. the preparation method of quick-fried pearl fragrance according to claim 4, which is characterized in that second extractant and the nose
The mass ratio of tobacco powder residue is 1:4~6.
6. the preparation method of quick-fried pearl fragrance according to claim 1, which is characterized in that in the oil water separator, institute
Snuff powder is stated to be located on liquid level.
7. a kind of quick-fried pearl fragrance, which is characterized in that using the preparation method such as the quick-fried pearl fragrance of claim 1-6 any one of them
It is made.
8. a kind of quick-fried pearl, which is characterized in that be made using quick-fried pearl fragrance as claimed in claim 7.
9. application of the quick-fried pearl according to claim 8 in cigarette is smelt.
10. application of the quick-fried pearl according to claim 8 in cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810181790.6A CN108219958A (en) | 2018-03-06 | 2018-03-06 | A kind of quick-fried pearl fragrance and preparation method thereof, quick-fried pearl and the application of quick-fried pearl |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810181790.6A CN108219958A (en) | 2018-03-06 | 2018-03-06 | A kind of quick-fried pearl fragrance and preparation method thereof, quick-fried pearl and the application of quick-fried pearl |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108219958A true CN108219958A (en) | 2018-06-29 |
Family
ID=62666800
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810181790.6A Pending CN108219958A (en) | 2018-03-06 | 2018-03-06 | A kind of quick-fried pearl fragrance and preparation method thereof, quick-fried pearl and the application of quick-fried pearl |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111838746A (en) * | 2019-04-30 | 2020-10-30 | 云南汉盟制药有限公司 | A bead, its preparation method and application in cigarette |
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| CN106010796A (en) * | 2016-07-22 | 2016-10-12 | 福建中烟工业有限责任公司 | Flavor preparation method, flavor prepared by preparation method and application of flavor |
| CN107034019A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl red-jujube flavor essence and its application in cigarette |
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2018
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101544927A (en) * | 2008-03-28 | 2009-09-30 | 湖北中烟工业有限责任公司 | Patchouli compound extract and application thereof in cigarette |
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| CN111838746A (en) * | 2019-04-30 | 2020-10-30 | 云南汉盟制药有限公司 | A bead, its preparation method and application in cigarette |
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