CN107474958A - A kind of method of infiltration evaporation film preparation safflower extract - Google Patents
A kind of method of infiltration evaporation film preparation safflower extract Download PDFInfo
- Publication number
- CN107474958A CN107474958A CN201710700321.6A CN201710700321A CN107474958A CN 107474958 A CN107474958 A CN 107474958A CN 201710700321 A CN201710700321 A CN 201710700321A CN 107474958 A CN107474958 A CN 107474958A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- flower extract
- extract
- safranine flower
- safflower
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 27
- 238000001764 infiltration Methods 0.000 title claims abstract description 23
- 230000008595 infiltration Effects 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 238000001704 evaporation Methods 0.000 title claims abstract description 13
- 230000008020 evaporation Effects 0.000 title claims abstract description 13
- 229940119485 safflower extract Drugs 0.000 title claims abstract description 11
- 239000000284 extract Substances 0.000 claims abstract description 77
- OARRHUQTFTUEOS-UHFFFAOYSA-N safranin Chemical compound [Cl-].C=12C=C(N)C(C)=CC2=NC2=CC(C)=C(N)C=C2[N+]=1C1=CC=CC=C1 OARRHUQTFTUEOS-UHFFFAOYSA-N 0.000 claims abstract description 62
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 49
- 239000000126 substance Substances 0.000 claims abstract description 34
- 235000003255 Carthamus tinctorius Nutrition 0.000 claims abstract description 22
- 244000020518 Carthamus tinctorius Species 0.000 claims abstract description 22
- 239000012528 membrane Substances 0.000 claims abstract description 19
- 230000008016 vaporization Effects 0.000 claims abstract description 18
- 239000007788 liquid Substances 0.000 claims abstract description 16
- 239000002699 waste material Substances 0.000 claims abstract description 15
- 235000015655 Crocus sativus Nutrition 0.000 claims abstract description 14
- 244000124209 Crocus sativus Species 0.000 claims abstract description 14
- 238000000605 extraction Methods 0.000 claims abstract description 13
- 238000010992 reflux Methods 0.000 claims abstract description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
- 238000012545 processing Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- 239000002131 composite material Substances 0.000 claims description 5
- 230000000694 effects Effects 0.000 abstract description 10
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 8
- 239000003546 flue gas Substances 0.000 abstract description 8
- 235000009508 confectionery Nutrition 0.000 abstract description 6
- 239000000796 flavoring agent Substances 0.000 abstract description 6
- 235000019634 flavors Nutrition 0.000 abstract description 6
- 244000269722 Thea sinensis Species 0.000 abstract description 4
- 239000007789 gas Substances 0.000 abstract description 4
- 210000000214 mouth Anatomy 0.000 abstract description 4
- 239000012141 concentrate Substances 0.000 abstract description 3
- 239000002904 solvent Substances 0.000 description 9
- 239000003205 fragrance Substances 0.000 description 7
- 239000002304 perfume Substances 0.000 description 6
- 238000002474 experimental method Methods 0.000 description 5
- 238000009834 vaporization Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 4
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- QJJDNZGPQDGNDX-UHFFFAOYSA-N oxidized Latia luciferin Chemical compound CC(=O)CCC1=C(C)CCCC1(C)C QJJDNZGPQDGNDX-UHFFFAOYSA-N 0.000 description 4
- SGAWOGXMMPSZPB-UHFFFAOYSA-N safranal Chemical compound CC1=C(C=O)C(C)(C)CC=C1 SGAWOGXMMPSZPB-UHFFFAOYSA-N 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 150000001299 aldehydes Chemical class 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000004205 dimethyl polysiloxane Substances 0.000 description 3
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 3
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 description 3
- 239000005416 organic matter Substances 0.000 description 3
- 238000004987 plasma desorption mass spectroscopy Methods 0.000 description 3
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 244000061176 Nicotiana tabacum Species 0.000 description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 150000002576 ketones Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000008092 positive effect Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 235000017509 safranal Nutrition 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 230000035943 smell Effects 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 241000234270 Amaryllidaceae Species 0.000 description 1
- IMKHDCBNRDRUEB-UHFFFAOYSA-N Dihydroactinidiolide Natural products C1CCC(C)(C)C2=CC(=O)OC21C IMKHDCBNRDRUEB-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 244000014047 Polianthes tuberosa Species 0.000 description 1
- 235000016067 Polianthes tuberosa Nutrition 0.000 description 1
- 241001661920 Telosma Species 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- IMKHDCBNRDRUEB-LLVKDONJSA-N dihydroactinidiolide Chemical compound C1CCC(C)(C)C2=CC(=O)O[C@@]21C IMKHDCBNRDRUEB-LLVKDONJSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 238000005373 pervaporation Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
- B01D61/362—Pervaporation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Water Supply & Treatment (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Seasonings (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of method of infiltration evaporation film preparation safflower extract.The preparation method specifically comprises the following steps：(1) safflower dried flower is taken, refluxing extraction, obtains crocus sativus；(2) crocus sativus concentrates；(3) aroma substance in waste liquid after infiltrating and vaporizing membrane enrichment concentration is utilized；(4) aroma substance being enriched with out is instead mended into concentrate, cigarette safranine flower extract is made.Cigarette prepared by present invention safranine flower extract, remain the feature note of safflower, aroma of pure, it is added in cigarette, with increase cigarette flavor amount, flue gas mass is improved, assigns cigarette sweetness note, reducing stimulates, miscellaneous gas, soft fine and smooth flue gas are covered, oral cavity comfort level improves, increase cigarette and return the effect such as sweet tea sense, improve safranine flower extract adaptability in cigarette.
Description
Technical field
Aroma substance is mended simultaneously the present invention relates to the preparation method of essence spice for cigarette, in particular to a kind of infiltrating and vaporizing membrane are counter
Prepare method of the cigarette with safranine flower extract.
Background technology
In Modern cigarette industry production, flavoring and casing is considered as very important technology, and cigarette product is each due to having selected
The spices of formula various kinds and make product more rich in characteristic, and for consumer suction when bring uniqueness fragrance and satisfaction.Natural perfume
Material due to its fragrance is abundant, odor characteristic is unique, flavouring essence quality alcohol and the features such as widely use in cigarette, at present, cigarette day
Right spices is extracted using solvent more, is that concentration process is larger to fragrance loss the shortcomings that this technique maximum, therefore, is changed molten
Concentration causes the present situation that aroma substance loses in matchmaker's extraction process, turns into the focus of research.
Infiltration evaporation (Pervaporation) is a kind of emerging membrane separation technique, and it utilizes feed liquid film upstream and downstream group
Point difference in chemical potential is that driving force realizes mass transfer, and choosing is realized to the difference of different component compatibility and resistance to mass tranfer in feed liquid using film
Select.Infiltration evaporation process has compact high energy utilization efficiency, selectivity height, device, operation and controls easy, scaleable can
The advantages that change.Separation or indissociable nearly boiling, the separation of constant boiling point mixture thus are difficult to applied to conventional distillation, to organic
The removing of solvent and in the mixed solvent minor amount of water, the recovery to a small amount of organic matter in waste water, to organic matter/organic matter separation and instead
Should couple, constantly remove reaction product etc. have it is obvious economically with technical advantage.But carried in cigarette with safflower
Take and report is but had no in the preparation of thing.
Safflower (scientific name：Polianthes tuberosa), also known as cordate telosma, fragrant below the moon, Amaryllidaceae safflower category plant
Thing, it is distributed in the areas such as Mexico, South America.Contain safranal, furfural, dihydro-β-ionone, different Fo Er in safflower
The aroma substances such as ketone, dihydroactinidiolide, these aroma substances have the function that good to cigarette flavor.
Using infiltrating and vaporizing membrane technical finesse safflower concentrating spent liquor, aroma substance is collected, and instead mend to safflower and extract
In thing, the fragrant obvious and preferable safranine flower extract of application effect in cigarette of aroma of pure, feature can be obtained.
The content of the invention
Mend aroma substance and prepare cigarette safranine flower extract it is an object of the invention to provide a kind of infiltrating and vaporizing membrane is counter
Method, this method technique is simple, and cost is low, environmentally friendly, and safranine flower extract characteristic perfume content of material is high, cigarette effect
It is good.
The method of a kind of infiltration evaporation film preparation cigarette safranine flower extract provided by the invention, it is characterised in that including such as
Lower step：
(1) safflower dried flower is taken, the water of its 10~20 times of weight is added, refluxing extraction, extract solution is stood and cooled down, collect
Filtrate obtains crocus sativus；
(2) crocus sativus is concentrated under reduced pressure at 60-80 DEG C, it is 1.20-1.30 to be concentrated into relative density, is prepared into
Safflower extract A；And the waste collection after safranine flower extract is concentrated is got up；
(3) it is used as infiltration evaporation from POMS-PEI composite membranes (poly- caprylil methicone-PEI composite membrane)
Film, by step (2) safranine flower extract concentrate after waste liquid heating-up temperature be 50-80 DEG C, charging rate 10-100ml/
Min, liquid nitrogen cooling, under conditions of aroma substance collects pressure 20-100Pa, infiltration processing is vaporized, and collect fragrance thing
Matter；
(4) aroma substance after permeating will be vaporized instead to mend in the safflower extract A after concentrating into step (2), and stirred
Mix, be well mixed, obtain cigarette safranine flower extract.
Safflower dried flower in the step (1) carries out refluxing extraction 3-5h at 100 DEG C.
The present invention permeates that membrane technology is counter mends aroma substance to prepare safranine flower extract using vaporization, utilizes infiltrating and vaporizing membrane
Aromatic substance, anti-mend such as safranal, dihydro-β-ionone, isophorone in technology collection safflower concentrating spent liquor are arrived
In safranine flower extract, the cigarette safranine flower extract of characteristic is prepared, this method extracts yield height, selection to characteristic flavor compounds
Property is good, and fragrance-quality is good.The POMS-PEI films that the present invention uses, the film are existing composite membrane, are used in the present invention compound
The product that film is bought for the GKSS companies of Germany；Safflower aroma substance is enriched with using POMS-PEI films, its aroma substance returns
Receipts amount is apparently higher than EVA38, POMS, PDMS, PEI.
The safranine flower extract prepared using the method for the present invention, compared with traditional safranine flower extract, its furfural, different fluorine
The phase of 13 kinds of aroma substances such as your ketone, Zang Honghua aldehyde, 2,4,4- trimethyl -3- formaldehyde -5- hydroxyl -2,5- cyclohexadiene -1- ketone
There is increase to content.It is added in cigarette, there is increase cigarette flavor amount, improve flue gas mass, assign cigarette sweetness note,
Reducing is stimulated, and covers miscellaneous gas, soft fine and smooth flue gas, and oral cavity comfort level improves, and increase cigarette returns the effect such as sweet tea sense, and cigarette is integrally commented
Valency positive effect is better than traditional safranine flower extract.
Using the present invention method be prepared characteristic perfume content of material height, aroma of pure, cigarette application effect compared with
Good characteristic safranine flower extract, the extract have the floral notes of feature, aroma of pure.Safranine flower extract is added to
In cigarette, there is increase cigarette flavor amount, improve flue gas mass, assign cigarette sweetness note, reducing stimulates, and covers miscellaneous gas, soft
With fine and smooth flue gas, oral cavity comfort level improves, and increase cigarette returns the effect such as sweet tea sense, improves safranine flower extract and is adapted in cigarette
Property.The present invention, which realizes, to turn waste into wealth, while improves the quality of safranine flower extract, lifts safflower extract of knowing clearly and is rolling up
Adaptability in cigarette.
Embodiment
The relevant technical problem of the present invention is described in further detail with reference to embodiment.
Embodiment 1, a kind of method of infiltration evaporation film preparation cigarette safranine flower extract, it is characterised in that including following step
Suddenly：
(1) safflower dried flower is taken, adds the water of its 10 times of weight, refluxing extraction 3-5h, extract solution is stood at 100 DEG C
Cooling, collect filtrate and obtain crocus sativus；
(2) crocus sativus collected in step (1) is concentrated under reduced pressure at 60 DEG C, being concentrated into relative density is
1.20, safflower extract A is prepared into, and the waste collection after the concentration of safranine flower extract is got up；
(3) POMS-PEI infiltrating and vaporizing membranes are selected, the waste liquid after the safranine flower extract concentration collected in step (2) is existed
Heating-up temperature is 50 DEG C, charging rate 10ml/min, liquid nitrogen cooling, under conditions of aroma substance collects pressure 20Pa, is carried out
Infiltration processing is vaporized, and collects aroma substance.
(4) aroma substance after vaporization infiltration in step (3) is instead mended into the safranine flower extract after being concentrated into step (2)
In A, and stir, be well mixed, obtain cigarette safranine flower extract.
Embodiment 2, a kind of method of infiltration evaporation film preparation cigarette safranine flower extract, it is characterised in that including following step
Suddenly：
(1) safflower dried flower is taken, adds the water of its 15 times of weight, refluxing extraction 3-5h, extract solution is stood at 100 DEG C
Cooling, collect filtrate and obtain crocus sativus；
(2) crocus sativus collected in step (1) is concentrated under reduced pressure at 70 DEG C, being concentrated into relative density is
1.25, safflower extract A is prepared into, and the waste collection after the concentration of safranine flower extract is got up；
(3) POMS-PEI infiltrating and vaporizing membranes are selected, the waste liquid after the safranine flower extract concentration collected in step (2) is existed
Heating-up temperature is 65 DEG C, charging rate 50ml/min, liquid nitrogen cooling, under conditions of aroma substance collects pressure 60Pa, is carried out
Infiltration processing is vaporized, and collects aroma substance；
(4) aroma substance after the vaporization infiltration collected in step (3) is instead mended into the safflower after being concentrated into step (2)
In extract A, and stir, be well mixed, obtain cigarette safranine flower extract.
Embodiment 3, a kind of method of infiltration evaporation film preparation cigarette safranine flower extract, it is characterised in that including following step
Suddenly：
(1) safflower dried flower is taken, adds the water of its 20 times of weight, refluxing extraction 3-5h, extract solution is stood at 100 DEG C
Cooling, collect filtrate and obtain crocus sativus；
(2) crocus sativus collected in step (1) is concentrated under reduced pressure at 70 DEG C, being concentrated into relative density is
1.20, safflower extract A is prepared into, and the waste collection after the concentration of safranine flower extract is got up；
(3) POMS-PEI infiltrating and vaporizing membranes are selected, the waste liquid after the safranine flower extract concentration collected in step (2) is existed
Heating-up temperature is 70 DEG C, charging rate 50ml/min, liquid nitrogen cooling, under conditions of aroma substance collects pressure 100Pa, is carried out
Infiltration processing is vaporized, and collects aroma substance；
(4) safflower of the anti-benefit of the middle aroma substance collected after vaporizing infiltration of step (3) into step (2) after concentration is carried
Take in thing A, and stir, be well mixed, obtain cigarette safranine flower extract.
Embodiment 4, a kind of method of infiltration evaporation film preparation cigarette safranine flower extract, it is characterised in that including following step
Suddenly：
(1) safflower dried flower is taken, adds the water of its 20 times of weight, refluxing extraction 3-5h, extract solution is stood at 100 DEG C
Cooling, collect filtrate and obtain crocus sativus；
(2) crocus sativus collected in step (1) is concentrated under reduced pressure at 80 DEG C, being concentrated into relative density is
1.30, safflower extract A is prepared into, and the waste collection after the concentration of safranine flower extract is got up；
(3) POMS-PEI infiltrating and vaporizing membranes are selected, the waste liquid after the safranine flower extract concentration collected in step (2) is existed
Heating-up temperature is 80 DEG C, charging rate 100ml/min, liquid nitrogen cooling, under conditions of aroma substance collects pressure 100Pa, is entered
Row vaporization infiltration processing, and collect aroma substance.
(4) aroma substance after the vaporization infiltration collected in step (3) is instead mended into the safflower after being concentrated into step (2)
In extract A, and stir, be well mixed, obtain cigarette safranine flower extract.
Experiment one：Inventor is vaporized using different infiltrating and vaporizing membranes to the waste liquid after the concentration of safranine flower extract oozes
Processing thoroughly, analysis is using influence of the different infiltrating and vaporizing membranes to safranine flower extract aroma substance yield, specific experiment knot
Fruit is shown in Table 1：
Influence of the 1 different films of table to safranine flower extract aroma substance yield
| Film species | Yield (‰) |
| EVA38 | 0.26 |
| POMS | Do not isolate |
| PDMS | 0.45 |
| PEI | 0.32 |
| POMS-PEI | 0.85 |
Contrast EVA38, POMS, PDMS, PEI can be seen that by the correction data in table 1, used in the present invention
POMS-PEI composite membranes are to safranine flower extract aroma substance yield highest.
Experiment two：The preparation safranine flower extract that will be prepared using the method in the application, prepared with traditional solvent method
The fragrance component of safranine flower extract carry out analysis contrast, concrete outcome is shown in Table 2：
2 traditional solvent of table extracts and the safranine flower extract characteristic flavor compounds relative amount of the application method extraction compares
It can be seen from Table 2 that compared with traditional solvent extracts, chaff in the safranine flower extract prepared in the application
13 kinds of safflowers such as aldehyde, isophorone, Zang Honghua aldehyde, 2,4,4- trimethyl -3- formaldehyde -5- hydroxyl -2,5- cyclohexadiene -1- ketone
The relative amount of characteristic perfume material has increase.
Experiment three：Safranine prepared by the method extraction of safranine flower extract prepared by the application and conventional steam distillation
Flower extract carries out smelling fragrant contrast, its comparing result such as table 3：
The safranine flower extract that 3 traditional solvent of table extracts and prepared by the application smells fragrant contrast
| Processing mode | Steam distillation | The application |
| Smell perfume (or spice) | Fragrant and sweet, cream is fragrant | The feature fragrance of a flower, aroma of pure |
Experiment four：The method that the safranine flower extract prepared according to the method in the application distills with conventional steam is carried
Take the safranine flower extract of preparation to be added to respectively according to the 0.1% of pipe tobacco weight in blank pipe tobacco, roll into cigarette and lead to respectively
Cross the group of smokeing panel test to be smoked panel test, specific sensory evaluation Contrast on effect such as table 4：
The safranine flower extract that 4 traditional solvent of table extracts and prepared by the application is added to the sensory evaluation effect pair in cigarette
Than
The fragrant and sense organ of smelling that safranine flower extract and the safranine flower extract of the application preparation are extracted by traditional solvent is commented
Valency Contrast on effect (table 3 and table 4) is as can be seen that the safranine flower extract fragrance prepared using the method in the application is purer
Just, feature note is more obvious, is added in cigarette, has increase perfume quantity, improves flue gas mass, it is fresh and sweet to assign cigarette cigarette
Note, reducing stimulates, and covers miscellaneous gas, soft fine and smooth flue gas, and oral cavity comfort level improves, and has back the effect such as sweet tea sense, positive effect
The safranine flower extract prepared better than the extraction of traditional solvent.
The detailed description of specific embodiments of the present invention is the foregoing is only, the present invention is not limited with this, it is all at this
All any modification, equivalent and improvement made in the mentality of designing of invention etc., should be included in protection scope of the present invention it
It is interior.
Claims (2)
- A kind of 1. method of infiltration evaporation film preparation cigarette safranine flower extract, it is characterised in that comprise the following steps：(1) safflower dried flower is taken, the water of its 10~20 times of weight is added, refluxing extraction, extract solution is stood and cooled down, collect filtrate Obtain crocus sativus；(2) crocus sativus is concentrated under reduced pressure at 60-80 DEG C, it is 1.20-1.30 to be concentrated into relative density, is prepared into safranine Flower extract A；And the waste collection after safranine flower extract is concentrated is got up；(3) from POMS-PEI composite membranes as infiltrating and vaporizing membrane, the waste liquid after step (2) safranine flower extract is concentrated is adding Hot temperature is 50-80 DEG C, charging rate 10-100ml/min, and liquid nitrogen cooling, it is 20-100Pa's that aroma substance, which collects pressure, Under the conditions of, infiltration processing is vaporized, and collect aroma substance；(4) aroma substance after permeating will be vaporized instead to mend in the safflower extract A after concentrating into step (2), and stirred, mixed Close uniformly, obtain cigarette safranine flower extract.
- A kind of 2. method of infiltration evaporation film preparation cigarette safranine flower extract according to claim 1, it is characterised in that Safflower dried flower in the step (1) carries out refluxing extraction 3-5h at 100 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710700321.6A CN107474958B (en) | 2017-08-16 | 2017-08-16 | Method for preparing saffron crocus extract by using pervaporation membrane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710700321.6A CN107474958B (en) | 2017-08-16 | 2017-08-16 | Method for preparing saffron crocus extract by using pervaporation membrane |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107474958A true CN107474958A (en) | 2017-12-15 |
| CN107474958B CN107474958B (en) | 2021-01-01 |
Family
ID=60599623
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710700321.6A Active CN107474958B (en) | 2017-08-16 | 2017-08-16 | Method for preparing saffron crocus extract by using pervaporation membrane |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107474958B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110804497A (en) * | 2019-11-18 | 2020-02-18 | 湖北中烟工业有限责任公司 | Preparation method of saffron extract for tobacco bead blasting |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101301112A (en) * | 2008-04-30 | 2008-11-12 | 广西中烟工业公司 | Additive agent for flavoring natural tobacco and preparation method and use thereof |
| CN101619271A (en) * | 2009-07-02 | 2010-01-06 | 华顺香料(上海)有限公司 | Traditional Chinese medicine combination spice for cigarette as well as preparation method and application thereof |
| CN103385338A (en) * | 2013-06-09 | 2013-11-13 | 南京工业大学 | Method for recovering aroma components in production process of instant tea powder |
| CN106148013A (en) * | 2016-08-31 | 2016-11-23 | 陈爱梅 | A kind of plant perfume low-temperature extraction technology |
| CN106957880A (en) * | 2016-10-13 | 2017-07-18 | 湖北中烟工业有限责任公司 | A kind of immobilization beta glucuroide prepares method of the cigarette with safranine flower extract |
-
2017
- 2017-08-16 CN CN201710700321.6A patent/CN107474958B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101301112A (en) * | 2008-04-30 | 2008-11-12 | 广西中烟工业公司 | Additive agent for flavoring natural tobacco and preparation method and use thereof |
| CN101619271A (en) * | 2009-07-02 | 2010-01-06 | 华顺香料(上海)有限公司 | Traditional Chinese medicine combination spice for cigarette as well as preparation method and application thereof |
| CN103385338A (en) * | 2013-06-09 | 2013-11-13 | 南京工业大学 | Method for recovering aroma components in production process of instant tea powder |
| CN106148013A (en) * | 2016-08-31 | 2016-11-23 | 陈爱梅 | A kind of plant perfume low-temperature extraction technology |
| CN106957880A (en) * | 2016-10-13 | 2017-07-18 | 湖北中烟工业有限责任公司 | A kind of immobilization beta glucuroide prepares method of the cigarette with safranine flower extract |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110804497A (en) * | 2019-11-18 | 2020-02-18 | 湖北中烟工业有限责任公司 | Preparation method of saffron extract for tobacco bead blasting |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107474958B (en) | 2021-01-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102781264B (en) | The method of the composition of extraction and separation cellulosic material | |
| CN101708063B (en) | Method for concentrating extraction liquid in production of tobacco sheet by papermaking process | |
| CN106929153A (en) | A kind of preparation method and applications of rosemary hydrosol | |
| CN105950298A (en) | Preparation methods of tea hydrolat and tea essential oil | |
| CN102250689A (en) | Equipment and method for extracting perfume plant essential oil by reduced pressure steam distillation | |
| CN106318640A (en) | Preparation method of aromatic tobacco extract and application thereof in cigarettes | |
| CN106174683A (en) | A kind of compositions and the tobacco juice for electronic smoke containing said composition | |
| CN103616461A (en) | Method for separating neutral aroma component from mainstream cigarette smoke | |
| CN106520368A (en) | Formula of Amadori reactive flavor, preparation method of Amadori reactive flavor and use of Amadori reactive flavor | |
| CN107474958A (en) | A kind of method of infiltration evaporation film preparation safflower extract | |
| CN106167739B (en) | Microcapsule containing green tea extract, preparation method and application thereof | |
| CN111417317A (en) | Preparation of a flavour concentrate by osmosis | |
| CN106350225A (en) | Preparation method and application of solid tree moss extract for cigarettes | |
| CN104818117B (en) | Utilize the cigarette wooden fork essential oil of tobacco waste preparation and its application and preparation method | |
| CN111363626B (en) | Holographic rose essential oil and green preparation method thereof | |
| CN109198574A (en) | A kind of tea aroma material collection method and tea aroma substance obtained | |
| Fleisher | The poroplast extraction technique in the flavor and fragrance industry | |
| BRPI0701771B1 (en) | CLARIFICATION AND ENRICHMENT PROCESS OF CITRUS OIL | |
| CN106010796A (en) | Flavor preparation method, flavor prepared by preparation method and application of flavor | |
| CN114931234B (en) | Tobacco source aroma substance, extraction method thereof and cigarette | |
| DE2244065A1 (en) | METHOD OF EXTRACTION OF HOP | |
| CN108865437A (en) | A kind of cigarette preparation method of perilla seed fragrance and the application in cigarette | |
| CN105733815B (en) | Natural spice preparation method and equipment | |
| CN116675598B (en) | Method for preparing natural benzaldehyde from green calyx plums | |
| Babu et al. | Comparative chemical composition of direct, recovered and combined essential oils of Lavandula angustifolia Mill |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |