CN106350225A - Preparation method and application of solid tree moss extract for cigarettes - Google Patents
Preparation method and application of solid tree moss extract for cigarettes Download PDFInfo
- Publication number
- CN106350225A CN106350225A CN201610808879.1A CN201610808879A CN106350225A CN 106350225 A CN106350225 A CN 106350225A CN 201610808879 A CN201610808879 A CN 201610808879A CN 106350225 A CN106350225 A CN 106350225A
- Authority
- CN
- China
- Prior art keywords
- tree moss
- extract
- solid
- cigarette
- redistillation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000284 extract Substances 0.000 title claims abstract description 55
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 50
- 239000007787 solid Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000000758 substrate Substances 0.000 claims abstract description 18
- 239000000706 filtrate Substances 0.000 claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 8
- 238000010992 reflux Methods 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 15
- 241000208125 Nicotiana Species 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 11
- 238000005374 membrane filtration Methods 0.000 claims description 10
- 235000013599 spices Nutrition 0.000 claims description 10
- 238000004321 preservation Methods 0.000 claims description 7
- 239000002304 perfume Substances 0.000 claims description 5
- 238000002390 rotary evaporation Methods 0.000 claims description 3
- 210000000214 mouth Anatomy 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 7
- 238000004821 distillation Methods 0.000 abstract description 6
- 238000000605 extraction Methods 0.000 abstract description 3
- 238000001914 filtration Methods 0.000 abstract 2
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 239000012528 membrane Substances 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 230000000717 retained effect Effects 0.000 abstract 1
- 239000003205 fragrance Substances 0.000 description 11
- 239000000047 product Substances 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 3
- 235000011613 Pinus brutia Nutrition 0.000 description 3
- 241000018646 Pinus brutia Species 0.000 description 3
- 239000012141 concentrate Substances 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 230000002045 lasting effect Effects 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 230000000638 stimulation Effects 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- UUQHKWMIDYRWHH-UHFFFAOYSA-N Methyl beta-orcinolcarboxylate Chemical compound COC(=O)C1=C(C)C=C(O)C(C)=C1O UUQHKWMIDYRWHH-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- 244000307697 Agrimonia eupatoria Species 0.000 description 1
- 235000016626 Agrimonia eupatoria Nutrition 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 241000566918 Ramalina fastigiata Species 0.000 description 1
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001944 continuous distillation Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 235000018219 lavender Nutrition 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- OVXRPXGVKBHGQO-UYWIDEMCSA-N methyl (1r,4ar,4br,10ar)-1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylate Chemical compound C1CC(C(C)C)=CC2=CC[C@H]3[C@@](C(=O)OC)(C)CCC[C@]3(C)[C@H]21 OVXRPXGVKBHGQO-UYWIDEMCSA-N 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- OIPPWFOQEKKFEE-UHFFFAOYSA-N orcinol Chemical compound CC1=CC(O)=CC(O)=C1 OIPPWFOQEKKFEE-UHFFFAOYSA-N 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- -1 reflux Substances 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 239000002680 soil gas Substances 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The invention provides a preparation method and application of solid tree moss extract for cigarettes. The preparation method includes: taking a tree moss raw material, adding an alcohol solution of 70% in concentration according to a material-liquid ratio of 1:8-1:10 for reflux extraction, and filtering and collecting filtrate; continuously distilling the filtrate for two times, taking substrates of distillation of two times for rotating, evaporating and concentrating in conditions of 32-40 DEG C and -0.8-1.0kPa; refrigerating and standing at 2-5 DEG C for precipitation for more than 12h, and filtering through a 0.8u membrane to obtain the solid tree moss extract. The tree moss extract prepared by the method is better in aroma, special aroma and good aroma enhancement effect of tree moss are retained, massive portions with offensive odor of conventional extract are reduced, and the aroma is more fresh and more comfortable; the solid tree moss extract has extremely small irritation to oral cavity and is free of residue when being applied in the cigarettes.
Description
Technical field
The present invention relates to medicated cigarette technical field is and in particular to a kind of cigarette preparation method of solid tree moss extract and should
With.
Background technology
Tree moss (treemoss), scientific name everniafurfuraceae, another name Ramalina fastigiata, tree Herba Astragali Sinici, epiphytic lichen class
Plant, is more common on pine, fir, oak, PiceameyeriRehd. Et Wils. or fir tree.For natural perfume material, the fragrance being grown on coniferous tree is poor, and grows
Preferably, especially more on the tree stem of robur one class, yield is higher for fragrance on the broad leaf trees such as fruit tree.Belong to pine with oak moss together
Luo Ke, its extractum or absolute oil product all have supply of commodities, and common odor characteristic is a kind of the natural blue or green of unique liverwort material
Fragrant and strong resin breath, but tree moss fragrance is slightly poorer than oak moss, with Masson Pine gas, as the succedaneum of oak moss, adjustable
The essence such as chypre fragrance is strange, Garden lavender, all sorts of flowers, tongue perfume (or spice), have preferable fixation effect.At present, Ge great tobacco company and its research
Mechanism is all increasingly using tree moss product and gives cigarette product unique aromatic style.
Research shows, the content of methyl β-orcinolcarboxylate and orcin monomethyl ether has direct contribution to its aroma strength.
In terms of fragrance with the security standpoint using, reduce A Lan phenol, rosin acid, isoabietic acid, Abalyn. and dihydro pine as far as possible
The content of the Resin Acid compositions such as fragrant acid methyl ester would be even more beneficial to the use of tree moss.Tree moss concrete have uniqueness Radix Glycyrrhizae delicate fragrance and
Strong resin is fragrant, and absolute oil has medical herbs taste, and lasting is lasting.For perfuming cigarette, delicate fragrance and natural flavor can be promoted, cover Nicotiana tabacum L.
Bad miscellaneous QI and soil gas, improve flue gas inhale taste.
Industrial at present typically directly obtain tree moss concrete with alcohol heating reflux legal system, using alcohol heating reflux and oil
Ether method for refining obtains tree moss absolute.For perfuming cigarette, fragrance is special, and flavouring is obvious, but oral cavity residual is heavier, leads to mouthfeel relatively
Difference.
Content of the invention
The present invention provides a kind of preparation method and application of cigarette solid tree moss extract, and the tree moss of the method preparation extracts
Thing active constituent content is high, remains the special aroma of tree moss and good flavouring effect, fragrance more fresh and comfortable, is applied
To in cigarette, its oral stimulation is few, noresidue.
The technical scheme that the present invention provides: a kind of cigarette is with the preparation method of tree moss solid extract it is characterised in that concrete
Step is as follows:
(1) take tree moss raw material, the ratio according to solid-liquid ratio 1:8～1:10 adds the ethanol solution that concentration is 70%, in temperature
Reflux, extract, 2～3h under 80～95 DEG C of degree, normal pressure, takes extracting solution to collect filtrate using the membrane filtration that aperture is 0.8 μm；
(2) filtrate collected in step (1) is carried out double continuous still, a redistillation temperature is 85～95 DEG C, double
Vapo(u)rizing temperature is 65～70 DEG C, and the flow velocity of distillating material is 1.5～2.5kg/h, and takes two redistillation substrates at 32～40 DEG C ,-
Under conditions of 0.8～-1.0kpa, rotary evaporation is concentrated into the 1/2 of two redistillation substrate quality；
(3) by two redistillation substrates after concentrating in step (2) under conditions of 2～5 DEG C cold preservation standing separate out 12h with
On, afterwards described cigarette tree moss solid extract is obtained by 0.8 μ membrane filtration.
The present invention preferably technical scheme: two redistillation in described step (2) are to carry out in triple spice distillators
Double continuous still, two redistillation are common distillation.Described triple spice distillator is the patent No. of application in 2015:
Number cn201520262268.2, the utility model patent product of publication number: cn204569880u.This distillator includes three horizontal types
Flask, arranges a condensing tube in the upper end of each horizontal type flask, is provided with condensate pipe, under each condensing tube in each condensing tube
Bring out material mouth to connect with the charging aperture on another horizontal type flask by threeway, the 3rd port of threeway is provided with distillate discharging
Mouthful.The outlet of each condensing tube of this triple distillation device is provided with two branch roads of distillation and condensation, does not interfere with each other, both can be continuous
Distillation is it is also possible to individually collect the substrate of each distillation.The present invention adopts this equipment to test continuous still twice, in the mistake of distillation
In journey, the distillate discharging opening of first condensing tube is closed, second condensing tube threeway connects the port of the 3rd horizontal type flask
Closing, just can realize double continuous still, then collect substrate from the distillate discharging opening of second condensing tube.
The present invention preferably technical scheme: in described step (3), the time of cold preservation standing is 12～24h.
The present invention provide a kind of cigarette tree moss solid extract application it is characterised in that: prepared by said method
Tree moss solid extract is directly appended in tobacco shred or reconstituted tobacoo as spice after being dissolved in the ethanol of concentration more than 95%,
Make cigarette；Or the tree moss solid extract preparing said method is added in flavouring essence for tobacco as spice as perfume material,
Then add in tobacco shred or reconstituted tobacoo and make Medicated cigarette；The addition of described tree moss solid extract is cigarette total tobacco shred amount
0.01%～0.1%.
Present invention utilizes part effective ingredient is solid at normal temperatures in tree moss extract, ethanol can be dissolved in and not dissolve in
The different principle of the material volatilization temperature of the characteristic of water and different molecular size.Spirit solvent first with 70% is by tree moss
Water can be dissolved in and the composition of ethanol all extracts, then utilize the redistillation in two redistillation will to affect the macromole of mouthfeel
Composition removes, and separation of ethanol, finally comprise in remaining two redistillation substrates is exactly water, is dissolved in little point of water two redistillation
Subconstiuent and target component, because target component is water insoluble, so separate out both can get target product.
Beneficial effects of the present invention:
(1) Extraction solvent of the present invention is 70% ethanol solution, can guarantee that the yield of tree moss solid cigarette extract relatively
High；
(2) present invention adopts double continuous still, and a Beijing South Maxpower Technology Co. Ltd ensures small molecule component separation and concentration, two redistillation can be protected
Separation of ethanol is gone out by card, thus separating out product, can remove the macromolecular components of impact mouthfeel, the extract mouthfeel obtaining is more
Well hence it is evident that improving oral cavity and the sensory issues of current tree moss extract；
(3) two redistillation substrate vacuum rotary steams are concentrated by the present invention, and control the condition of its revolving, are further separated out two
The ethanol remaining during redistillation, and guarantee that a separated goes out ethanol, the effective ingredient that further improve in product contains
Amount, improves quality and the yield of extract；
(4) concentrate is finally adopted stand at low temperature to separate out by the present invention, reduces temperature and can reduce dissolubility, improves yield,
And solid product can be obtained, its states of matter more preferably, is more easy to store compared to traditional extract of mostly liquid and transports；
The tree moss extract fragrance of present invention preparation more preferably, remains the special aroma of tree moss and good flavouring effect,
Decrease the more thick and heavy miscellaneous perfume part of traditional extract, fragrance more fresh and comfortable simultaneously, apply it to its oral cavity in cigarette
Stimulate few, noresidue.
Specific embodiment
Below in conjunction with embodiment, the technical scheme in the present invention is clearly and completely described.
Embodiment 1, a kind of preparation method of cigarette tree moss solid extract is it is characterised in that specifically comprise the following steps that
(1) 200 parts of tree moss raw materials are weighed, the ratio 1600 parts of concentration of addition according to solid-liquid ratio 1:8 are 70% ethanol,
Temperature is 95 DEG C, reflux, extract, 2h under normal pressure, takes extracting solution to collect filtrate using the membrane filtration that aperture is 0.8 μm；
(2) filtrate in step (1) is carried out in triple spice distillators two redistillation, wherein one redistillation temperature is
95 DEG C, double vapo(u)rizing temperature is 70 DEG C, and the flow velocity of distillating material is 2.5kg/h；Take two redistillation substrates in 40 DEG C, -0.8kpa
Under the conditions of rotary evaporation be concentrated into 1/2；Concentrate is placed in 4 DEG C of cold preservation standings and separates out 12h, then obtained final product using 0.8 μ membrane filtration
To cigarette of the present invention tree moss solid extract.
The cigarette of preparation in embodiment 1 is added according to the 0.01% of Dan Zhiyan tobacco shred silk gross weight with tree moss solid extract
In tobacco shred, make cigarette, then allow perfumer inhale according to GB product, its result shows that the cigarette that increased preparation in embodiment 1 is used
The cigarette of tree moss solid extract has the special aroma of tree moss and good flavouring effect, and oral stimulation is few, and noresidue is bright
Aobvious oral cavity and the sensory issues improving current tree moss extract.
Embodiment 2: a kind of preparation method of cigarette tree moss solid extract is it is characterised in that specifically comprise the following steps that
(1) 150 tree moss raw materials are taken, the ratio 1500 parts of concentration of addition according to solid-liquid ratio 1:10 are 70% ethanol solution,
Reflux, extract, 2.5h under 90 DEG C of temperature, normal pressure, takes extracting solution to collect filtrate using the membrane filtration that aperture is 0.8 μm；
(2) filtrate collected in step (1) is carried out double continuous still, a redistillation temperature is 60 DEG C, two redistillation
Temperature is 70 DEG C, and the flow velocity of distillating material is 1.5kg/h, and takes two redistillation substrates to rotate steaming under conditions of 35 DEG C, -1kpa
Send out and be concentrated into the 1/2 of two redistillation substrate quality；
(3) by two redistillation substrates after concentrating in step (2), under conditions of 5 DEG C, cold preservation standing separates out 14h, leads to afterwards
Cross 0.8 μ membrane filtration and obtain described cigarette tree moss solid extract.
The cigarette of preparation in embodiment 2 is added cigarette with tree moss solid extract according to the 0.05% of Dan Zhiyan tobacco shred gross weight
In silk, make cigarette, then allow perfumer inhale according to GB product, its result shows the cigarette tree that with the addition of preparation in embodiment 2
The cigarette of tongue solid extract has the special aroma of tree moss and good flavouring effect, and oral stimulation is few, noresidue hence it is evident that
Improve oral cavity and the sensory issues of current tree moss extract.
Embodiment 3: a kind of preparation method of cigarette tree moss solid extract is it is characterised in that specifically comprise the following steps that
(1) 100 parts of tree moss raw materials are taken, the ethanol that the ratio according to solid-liquid ratio 1:10 adds 1000 parts of concentration to be 70% is molten
Liquid, reflux, extract, 3h under 85 DEG C of temperature, normal pressure, take extracting solution to collect filtrate using the membrane filtration that aperture is 0.8 μm；
(2) filtrate collected in step (1) is carried out double continuous still, a redistillation temperature is 85 DEG C, two redistillation
Temperature is 65 DEG C, and the flow velocity of distillating material is 2kg/h, and takes two redistillation substrates at 32 DEG C, and rotation under conditions of -1.0kpa is steamed
Send out and be concentrated into the 1/2 of two redistillation substrate quality；
(3) by two redistillation substrates after concentrating in step (2), under conditions of 2 DEG C, cold preservation standing separates out 12h, leads to afterwards
Cross 0.8 μ membrane filtration and obtain described cigarette tree moss solid extract.
By in embodiment 3 preparation cigarette with tree moss solid extract according to Dan Zhiyan tobacco shred gross weight 0.1% addition
In tobacco shred, make cigarette, then allow perfumer inhale according to GB product, its result shows that the cigarette that increased preparation in embodiment 3 is used
The cigarette of tree moss solid extract has the special aroma of tree moss and good flavouring effect, and oral cavity is non-stimulated, noresidue hence it is evident that
Improve oral cavity and the sensory issues of current tree moss extract.
The present invention is directed to the feature of tree moss raw material, with 70% ethanol as solvent during extraction, so can fully extract tree
Effective ingredient in tongue；Triple spice distillators using autonomous Design transformation carry out two redistillation process to filtrate, effectively remove
Go to affect the macromolecular substances of mouthfeel；According to the physical characteristics of product and solvent, adopt middle temperature to concentrate and low temperature separates out to carry
High yield and purity.
Above-described embodiment gained cigarette and the cigarette adding 0.05% tree moss concrete are carried out lasting and suction contrast, specifically
Comparing result is as shown in table 1.
The comparing result of the cigarette that the cigarette that table 1 present invention adds is added with traditional extract
The above, the only specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, and any
Belong to those skilled in the art the invention discloses technical scope in, the change or replacement that can readily occur in, all answer
It is included within the scope of the present invention.Therefore, protection scope of the present invention should be defined by scope of the claims.
Claims (4)
1. a kind of preparation method of cigarette solid tree moss extract is it is characterised in that specifically comprise the following steps that
(1) take tree moss raw material, the ratio according to solid-liquid ratio 1:8～1:10 adds the ethanol solution that concentration is 70%, in temperature 80
～95 DEG C, reflux, extract, 2～3h under normal pressure, extracting solution is collected filtrate using the membrane filtration that aperture is 0.8 μm；
(2) filtrate collected in step (1) is carried out double continuous still, a redistillation temperature is 85～95 DEG C, two redistillation
Temperature is 65～70 DEG C, and the flow velocity of distillating material is 1.5～2.5kg/h, and takes two redistillation substrates at 32～40 DEG C, -0.8
Under conditions of～-1.0kpa, rotary evaporation is concentrated into the 1/2 of two redistillation substrate quality；
(3) by two redistillation substrates after concentrating in step (2), under conditions of 2～5 DEG C, cold preservation standing separates out more than 12h, it
Afterwards described cigarette solid tree moss extract is obtained by 0.8 μ membrane filtration.
2. a kind of cigarette according to claim 1 with the preparation method of solid tree moss extract it is characterised in that: described step
(2) two redistillation in are the double continuous stills carrying out in triple spice distillators.
3. a kind of cigarette according to claim 1 with the preparation method of solid tree moss extract it is characterised in that: described step
(3) in, the time of cold preservation standing is 12～24h.
4. a kind of cigarette described in a kind of claim 1 with the application of solid tree moss extract it is characterised in that: by said method system
Standby tree moss solid extract is directly appended to tobacco shred or reconstituted tobacoo as spice after being dissolved in the ethanol of concentration more than 95%
In, make cigarette；Or the tree moss solid extract preparing said method is added to flavouring essence for tobacco as spice as perfume material
In, add in tobacco shred or reconstituted tobacoo and make Medicated cigarette；The addition of described tree moss solid extract is cigarette total tobacco shred amount
0.01%～0.1%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610808879.1A CN106350225A (en) | 2016-09-08 | 2016-09-08 | Preparation method and application of solid tree moss extract for cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610808879.1A CN106350225A (en) | 2016-09-08 | 2016-09-08 | Preparation method and application of solid tree moss extract for cigarettes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106350225A true CN106350225A (en) | 2017-01-25 |
Family
ID=57859799
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610808879.1A Pending CN106350225A (en) | 2016-09-08 | 2016-09-08 | Preparation method and application of solid tree moss extract for cigarettes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106350225A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108192726A (en) * | 2018-03-29 | 2018-06-22 | 武汉黄鹤楼香精香料有限公司 | A kind of preparation method of cigarette tree moss absolute |
| CN111449280A (en) * | 2020-03-27 | 2020-07-28 | 河南中烟工业有限责任公司 | Replaceable filter stick with green and fresh fragrance and application |
| CN111827002A (en) * | 2020-07-13 | 2020-10-27 | 河南中烟工业有限责任公司 | Faint scent cigarette paper and preparation method thereof |
| CN113180286A (en) * | 2021-04-28 | 2021-07-30 | 江苏中烟工业有限责任公司 | Separation and purification method of macromolecular dephenolic acids in tree moss extract |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204569880U (en) * | 2015-04-27 | 2015-08-19 | 湖北中烟工业有限责任公司 | A kind of triple spices distillation plant |
-
2016
- 2016-09-08 CN CN201610808879.1A patent/CN106350225A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204569880U (en) * | 2015-04-27 | 2015-08-19 | 湖北中烟工业有限责任公司 | A kind of triple spices distillation plant |
Non-Patent Citations (1)
| Title |
|---|
| 杨伟平等: "不同工艺的树苔提取物中As的总量和形态", 《烟草科技》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108192726A (en) * | 2018-03-29 | 2018-06-22 | 武汉黄鹤楼香精香料有限公司 | A kind of preparation method of cigarette tree moss absolute |
| CN111449280A (en) * | 2020-03-27 | 2020-07-28 | 河南中烟工业有限责任公司 | Replaceable filter stick with green and fresh fragrance and application |
| CN111827002A (en) * | 2020-07-13 | 2020-10-27 | 河南中烟工业有限责任公司 | Faint scent cigarette paper and preparation method thereof |
| CN113180286A (en) * | 2021-04-28 | 2021-07-30 | 江苏中烟工业有限责任公司 | Separation and purification method of macromolecular dephenolic acids in tree moss extract |
| CN113180286B (en) * | 2021-04-28 | 2022-04-29 | 江苏中烟工业有限责任公司 | Separation and purification method of macromolecular dephenolic acids in tree moss extract |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101461433B (en) | Tea extract and preparation method thereof | |
| CN106350225A (en) | Preparation method and application of solid tree moss extract for cigarettes | |
| CN105950298A (en) | Preparation methods of tea hydrolat and tea essential oil | |
| CN104140889B (en) | A kind of preparation method of rose absolute | |
| CN102504957A (en) | Method for preparing essential oils | |
| CN105566402B (en) | A kind of method of comprehensive extraction tea perfume essence, tea polysaccharide and Tea Polyphenols | |
| CN102250689A (en) | Equipment and method for extracting perfume plant essential oil by reduced pressure steam distillation | |
| CN101775337A (en) | Method for simultaneously preparing osmanthus essential oil, dry osmanthus product and osmanthus essential lotion | |
| CN104327948B (en) | A kind of preparation method and application of cigarette yellow chamomile fragrance | |
| CN101928642B (en) | Method for extracting and separating spice and medicinal components from whole plants of Dendranthema indicum | |
| CN103300182A (en) | Method for extracting aromatic substances and tea polyphenols from tea leaves step by step | |
| CN106174683A (en) | A kind of compositions and the tobacco juice for electronic smoke containing said composition | |
| CN103525558A (en) | Tea flower essence with fruity flavor characteristic and application thereof to cigarettes | |
| CN102423116B (en) | Preparation method for pineapple spice for cigarette | |
| CN103525556A (en) | Ecological flower planting method before extracting jasmine flower aroma substances | |
| CN106037012A (en) | Electronic cigarette liquid | |
| CN104544543A (en) | Electronic cigarette smoke solution prepared through black tea leaf extract | |
| CN107637858A (en) | A kind of plant for improving water extraction and alcohol precipitation method extraction causes perfumery and extracting method and application | |
| CN106916628B (en) | Bitter citrus immature flower essential oil, preparation method and application | |
| CN106617275A (en) | Method for preparing electronic cigarette essence by mixing tobacco with tea | |
| CN101486949A (en) | Preparation of Schisandra chinensis clean oil | |
| CN106167739A (en) | A kind of containing doing the microcapsule of extract of Folium Camelliae sinensis, Preparation Method And The Use | |
| CN106635418A (en) | Preparation method of high-purity citrus aurantium flower essential oil and flavor addition essence used for cigarettes and blended with high-purity citrus aurantium flower essential oil | |
| CN106010796A (en) | Flavor preparation method, flavor prepared by preparation method and application of flavor | |
| CN109055009A (en) | A kind of tea flavor flavouring essence for tobacco and its application |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170125 |