CN108219943A - A kind of quick-fried pearl essential oil of cigarette and the method for preparing quick-fried pearl - Google Patents
A kind of quick-fried pearl essential oil of cigarette and the method for preparing quick-fried pearl Download PDFInfo
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- CN108219943A CN108219943A CN201810068607.1A CN201810068607A CN108219943A CN 108219943 A CN108219943 A CN 108219943A CN 201810068607 A CN201810068607 A CN 201810068607A CN 108219943 A CN108219943 A CN 108219943A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/281—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed
- A24B15/283—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances
- A24B15/284—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances the additive being bound to a host by chemical, electrical or like forces, e.g. use of precursors, inclusion complexes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/285—Treatment of tobacco products or tobacco substitutes by chemical substances characterised by structural features, e.g. particle shape or size
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/12—Use of materials for tobacco smoke filters of ion exchange materials
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0288—Applications, solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
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- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
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- Oil, Petroleum & Natural Gas (AREA)
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Abstract
The invention discloses a kind of quick-fried pearl essential oil of cigarette and the methods for preparing quick-fried pearl.Lavandulae flos essential oil, marjoram essential oil, ylang-ylang essential oil, chamomile essential oil, sandalwood essential oil, vanilla soya-bean oil, Chinese ilex essential oil, borneol extract, cloud angelica extract and fat solvent are mixed evenly to prepare quick-fried pearl essential oil.Routinely the quick-fried pearl of cigarette is made in technique again.The quick-fried pearl essential oil has pure and fresh herbal, enriches the quick-fried pearl odor type feature of style type, while the personalization and multiple demand for meeting consumer, also have refresh the mind, qi-tonifying health-care and other effects.The quick-fried pearl of the present invention is added in cigarette filter tip, the essential oil fragrance released is coordinated naturally in itself with cigarette perfume, and flue gas fragrance texture is obviously improved, rich and sophistication dramatically increases, alcohol is moistened in flue gas more Tianjin and irritation reduces, and can be obviously improved the suction comfort of cigarette.
Description
Technical field
The invention belongs to technical field of cigarette flavors, are specifically related to a kind of quick-fried pearl essential oil of cigarette.Meanwhile this hair
The bright method for further relating to prepare the quick-fried pearl of cigarette using the essential oil.
Background technology
Low coking has been the inexorable trend of tobacco business development, but the cigarette smoking mouthfeel that low coking is brought reduces, fragrance
The problems such as insufficient, is also increasingly prominent.How to capture influences tobacco aroma quality, the key technology of perfume quantity, just becomes and improves cigarette life
Where the core for producing competitiveness.Essence spice for cigarette is added in cigarette shreds, is a kind of conventional, required supplement fragrance
Technological means, but the space of its promotion cigarette quality is relatively limited, therefore from the non-burning section of cigarette, it finds relevant novel
Material improves, is promoted the fragrance of cigarette, and to reduce cigarette smoke irritation become new development trend.Wherein, it is filtered in cigarette
The quick-fried pearl of cigarette is added in stick, is a kind of effective and feasible mode by application attestation.Quick-fried pearl is one made an addition in filter tip
Or the more flavored capsules by pinching brokenly release content, to realize the artificial controllable characteristic fragrance during smoking property of cigarette
Release reduces external environment and the influence essence with caused by for inhaling taste is lost, plays abundant smoking property of cigarette taste, realization was sucked
The effects that flavouring humectation of journey.It is lost to make up smoke perfume caused by tar content reduces, more and more brands start
" quick-fried pearl addition " technology is used as auxiliary flavoring means.
But the quick-fried pearl of cigarette is usually to be made of some macromolecule organics, glue class, cellulose and some auxiliary materials, these groups
Bring bad breath in varying degrees into ingredient.During the quick-fried pearl of cigarette pinches brokenly, wall material is destroyed, solvent release,
Chemical breath significantly aggravates during this, influences the sensory experience of consumer.
Meanwhile common quick-fried pearl cigarette, essence and flavoring agents that mainly some and cigarette smoke differ greatly in quick-fried pearl, example
Such as minty note, aroma, fruit perfume (or spice), these quick-fried pearls change the odor characteristic of cigarette in itself larger.Also have in the prior art
Some are close to the quick-fried pearl of cigarette smoke aromatic style, although cigarette can be made to have certain fragrance in absorption, there is also quick-fried
Pearl fragrance is not merged with the fragrance of cigarette in itself, and effect is bad, it is impossible to fundamentally make up that cigarette perfume is insufficient and moisture feeling is insufficient asks
Topic.Moreover, as people are to diversification and personalized all the more pursuit, present quick-fried pearl type has been unable to meet public consumption
Demand.Therefore, carry out removal for the quick-fried pearl of cigarette or cover the technical research of adverse chemical breath, the novel quick-fried pearl of Persisting exploitation and
The quick-fried pearl essence of new style, it has also become the emphasis direction of the quick-fried pearl research and development of cigarette.
Invention content
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide one kind can enrich the quick-fried pearl odor type feature of cigarette,
Cover bad breath, the quick-fried pearl essential oil of cigarette coordinated with cigarette cigarette perfume.
The present invention also aims to provide a kind of method that the quick-fried pearl of cigarette is prepared using the essential oil.
The purpose of the present invention is achieved by following technical proposals.
Unless otherwise indicated, percentage of the present invention is mass percent.
A kind of quick-fried pearl essential oil of cigarette, which is characterized in that be mixed evenly to prepare by the raw material of following mass parts：Lavender anthosin
1.5~3 parts of oil, 0.5~1.5 part of marjoram essential oil, 1~2 part of ylang-ylang essential oil, 0.5~1.5 part of chamomile essential oil, santal
1~2 part of another name for oil, 0.5~1.5 part of vanilla soya-bean oil, 0.2~0.5 part of Chinese ilex essential oil, 1~3 part of borneol extract, cloud Radix Angelicae Sinensis carry
Take 75~89.8 parts of 4~10 parts of object and fat solvent.
Preferably, the cloud angelica extract, is prepared by following methods：
(1) by the drying of cloud Radix Angelicae Sinensis, crushing, the second of concentration 70%~95% is added in by 10~20 times of cloud Chinese Angelica Root quality
Alcohol solution, 60~80 DEG C of 1~3h of circumfluence distillation；
(2) extracting solution filters while hot, and being then concentrated into volume under the conditions of 45~60 DEG C, 60~90kPa no longer changes, i.e.,
Obtain cloud angelica extract.
The fat solvent is：By 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixing, then by mixing
0.5%~0.8% addition sorbester p17 of object gross mass, is mixed evenly to prepare.
The method for preparing the quick-fried pearl essential oil of the cigarette, includes the following steps：
(1) by the mass parts by lavandulae flos essential oil, marjoram essential oil, ylang-ylang essential oil, chamomile essential oil, santal
Another name for oil, vanilla soya-bean oil, Chinese ilex essential oil, borneol extract and cloud angelica extract are uniformly mixed, and obtain essence；
(2) by 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixing, then by mixture gross mass
0.5%~0.8% addition sorbester p17, stirring at normal temperature are slowly added to essence obtained by step (1) in whipping process, after essence adds
Continue 0.5~1.5h of stirring, standing treats lather collapse to get to the required quick-fried pearl essential oil of cigarette.
The quick-fried pearl of the cigarette is with the preferred raw material proportioning of essential oil：2 parts of lavandulae flos essential oil, 1.2 parts of marjoram essential oil,
1.6 parts of ylang-ylang essential oil, 0.8 part of chamomile essential oil, 1 part of sandalwood essential oil, 0.6 part of vanilla soya-bean oil, 0.3 part of Chinese ilex essential oil,
83 parts of 2 parts of borneol extract, 7.5 parts of cloud angelica extract and fat solvent.
The present invention also provides a kind of methods that the quick-fried pearl of cigarette is prepared with the essential oil, include the following steps：
(1) essential oil is added in the hopper of pill dripping machine；
(2) dripping pill lapping is added in the rubber cement tank of pill dripping machine, keeps 70 DEG C of temperature；
(3) it is put into calcium ion salts solution solidifying agent in dripping pill device is contained；
(4) pill dripping machine is opened, essential oil and dripping pill lapping ooze respectively from discharge port and gum outlet, and essential oil is wrapped in drop
In ball lapping, and cured dose of curing molding, obtain the quick-fried pearl of cigarette.
The dripping pill lapping is made of the raw material of following mass parts：6~20 parts of sodium alginate, Arabic gum 0.1
~3 parts, 77~95 parts of water；Wherein, the viscosity of sodium alginate is 5~40Pa.s；The viscosity of Arabic gum is 80~140cP；It will
Each raw material, which is placed in retort, to be stirred, 70 DEG C of reaction temperature, after material melting, is kept the temperature 1~2h, is stood, after foam floating,
It filters and obtains under the conditions of 70 DEG C of heat preservation.
During cigarette filter wire-beam forming, prepared quick-fried pearl positioning is applied in filter rod, you can roll into
Quick-fried pearl type cigarette.
Relative to the prior art, the invention has the advantages that：
1st, the main component of cigarette of the present invention quick-fried pearl essential oil is borneol extract and cloud angelica extract, is had pure and fresh
Herbal enriches the quick-fried pearl odor type feature of style type, can also meet personalization and the multiple demand of consumer, while also has
It refreshes the mind, qi-tonifying health-care and other effects.
2nd, the perfume ingredient in essential oil can dissolve each other with fat solvent, and aromatic flavour is naturally, quick-fried Zhu Bi can be hidden well
The bad breath that material and solvent bank come.
3rd, the quick-fried pearl of the present invention is added in cigarette filter tip, is pinched brokenly quick-fried pearl in aspiration procedure, the essential oil fragrance released
Coordinate naturally in itself with cigarette perfume, flue gas fragrance texture is obviously improved, and rich and sophistication dramatically increases, flue gas more Tianjin profit alcohol
It is reduced with, irritation, the suction comfort of cigarette can be obviously improved.
4th, preparation method of the present invention is simple, and raw material is easy to get, of low cost, is easy to implement industrialized production, there is good answer
With value.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is described in further detail.It should be appreciated that specific embodiment described herein is only to explain the present invention, it is not to this hair
The restriction of bright technical solution.
Embodiment 1
1. the preparation of the quick-fried pearl essential oil of manner
(1) preparation of cloud angelica extract
Dry cloud Radix Angelicae Sinensis 1kg by pulverizer is crushed, is sieved with 100 mesh sieve；Add in 15kg's into cloud Chinese Angelica Root
80% concentration ethanol, circumfluence distillation 2h at 60 DEG C；It filters while hot, 50 DEG C, carry out vacuum-concentrcted to body under the conditions of 80kPa
Product no longer changes to get cloud angelica extract.
(2) preparation of the quick-fried pearl essence of manner
By mass fraction weigh 2 parts of lavandulae flos essential oil, 1.2 parts of marjoram essential oil, 1.6 parts of ylang-ylang essential oil, ocean it is sweet
0.8 part of chrysanthemum essential oil, 1 part of sandalwood essential oil, 0.6 part of vanilla soya-bean oil, 0.3 part of Chinese ilex essential oil, 2 parts of borneol extract, cloud Radix Angelicae Sinensis carry
The various essence and flavoring agents of 7.5 parts of object is taken to be uniformly mixed and are configured to the quick-fried pearl essence of manner.
(3) preparation of the quick-fried pearl essential oil of manner
By 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixed preparing obtains fat solvent；Again by 24 degree of palm fibres
0.7% addition sorbester p17 of palmitic acid oil and neodecanoic acid glyceride gross mass, stirs evenly at normal temperatures；It is 83 parts to weigh mass fraction
The above-mentioned fat solvent containing sorbester p17, the quick-fried pearl essence of manner is slowly added in whipping process so that the manner finally obtained
Fat solvent in quick-fried pearl essential oil：The mass percent of the quick-fried pearl essence of manner is 83:17, quick-fried pearl essence continues to stir 1h after adding,
Standing treats lather collapse to get the quick-fried pearl essential oil of manner.
2. the preparation of the quick-fried pearl of cigarette manner, includes the following steps：
It prepares in glue 500ml addition Sandwich pots and stirs by proportioning listed in table 1, steam jacket is heated to 70 DEG C, makes it
Fusing keeps the temperature 2 hours, stands after foam floating, and heat preservation filtering obtains dripping pill lapping；Dripping pill lapping is added in
In the rubber cement tank of pill dripping machine, and keep 70 DEG C of temperature.The quick-fried pearl essential oil 600g of manner is weighed, is added in the hopper of pill dripping machine, is contained
10% calcium chloride water is put into dripping pill device as curing agent.Quality, which is made, using the small capsule and pill dropping-pill machine of DWJSYJ-I types is
15mg, crushing strength 2.5kPa, 250 μm of rubber thickness, the quick-fried pearl of cigarette manner of a diameter of 3.5mm.
1 dripping pill lapping glue of table is with tabulation
| Specification | Parts by weight | |
| Sodium alginate | Viscosity (Pa.s) 15 | 12 |
| Arabic gum | Viscosity (cP) 100 | 1 |
| Water | Pure water | 87 |
3. application and evaluation of the quick-fried pearl of cigarette manner in cigarette
During cigarette filter wire-beam forming, by the quick-fried pearl positioning of the cigarette of preparation manner be applied in filter rod to get
The cigarette of the quick-fried pearl containing cigarette manner.Sensory evaluating smoking, Analyses Methods for Sensory Evaluation Results table are carried out as control using the cigarette for not adding above-mentioned quick-fried pearl
It is bright：Compared with the control, the cigarette flue gas for being added to the quick-fried pearl of cigarette manner has pure and fresh herbal, and quick-fried pearl fragrance and cigarette perfume are in itself
Naturally coordinate, flue gas is rich to be dramatically increased, and fragrance texture and Tianjin moisture feeling are obviously improved, and pleasant impression is comfortable.
Embodiment 2
1. the preparation of the quick-fried pearl essential oil of manner
(1) preparation of cloud angelica extract
Dry cloud Radix Angelicae Sinensis 2kg by pulverizer is crushed, is sieved with 100 mesh sieve；Add in 20kg's into cloud Chinese Angelica Root
80% concentration ethanol, circumfluence distillation 2h at 65 DEG C；It filters while hot, 50 DEG C, carry out vacuum-concentrcted to body under the conditions of 70kPa
Product no longer changes to get cloud angelica extract.
(2) preparation of the quick-fried pearl essence of cigarette manner
By mass fraction weigh 1.5 parts of lavandulae flos essential oil, 1.5 parts of marjoram essential oil, 1 part of ylang-ylang essential oil, ocean it is sweet
0.5 part of chrysanthemum essential oil, 1.8 parts of sandalwood essential oil, 1 part of vanilla soya-bean oil, 0.5 part of Chinese ilex essential oil, 1.2 parts of borneol extract, cloud Radix Angelicae Sinensis
The various essence and flavoring agents of 5 parts of extract, which are uniformly mixed, is configured to the quick-fried pearl essence of manner；
(3) preparation of the quick-fried pearl essential oil of manner
By 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixed preparing obtains fat solvent；Again by 24 degree of palm fibres
0.6% addition sorbester p17 of palmitic acid oil and neodecanoic acid glyceride total weight, stirs evenly at normal temperatures.It is 86 parts to weigh mass fraction
The above-mentioned fat solvent containing sorbester p17, the quick-fried pearl essence of manner is slowly added in whipping process so that the manner finally obtained
Fat solvent in quick-fried pearl essential oil：The mass percent of the quick-fried pearl essence of manner is 86:14, quick-fried pearl essence continues to stir after adding
1.5h, standing treat lather collapse to get the quick-fried pearl essential oil of manner.
2. the preparation of the quick-fried pearl of cigarette manner, includes the following steps：
It prepares in glue 500ml addition Sandwich pots and stirs by proportioning listed in table 2, steam jacket is heated to 70 DEG C, makes it
Fusing keeps the temperature 2 hours, stands after foam floating, and heat preservation filtering obtains dripping pill lapping；Dripping pill lapping is added in
In the rubber cement tank of pill dripping machine, and kept for 70 DEG C.The quick-fried pearl essential oil 650g of manner is weighed, is added in the hopper of pill dripping machine, contains dripping pill
8% Dicalcium Phosphate aqueous solution is put into device as curing agent.Quality, which is made, using the small capsule and pill dropping-pill machine of DWJSYJ-I types is
16mg, crushing strength 2.0kPa, 200 μm of rubber thickness, the quick-fried pearl of cigarette manner of a diameter of 3.2mm.
2 dripping pill lapping glue of table is with tabulation
| Specification | Parts by weight | |
| Sodium alginate | Viscosity (Pa.s) 20 | 8 |
| Arabic gum | Viscosity (cP) 120 | 0.5 |
| Water | Pure water | 91.5 |
3. application and evaluation of the quick-fried pearl of cigarette manner in cigarette
During cigarette filter wire-beam forming, by the quick-fried pearl positioning of the cigarette of preparation manner be applied in filter rod to get
The cigarette of the quick-fried pearl containing cigarette manner.Sensory evaluating smoking, Analyses Methods for Sensory Evaluation Results table are carried out as control using the cigarette for not adding above-mentioned quick-fried pearl
It is bright：Compared with the control, the quick-fried pearl fragrance for being added to the quick-fried pearl cigarette of cigarette manner is coordinated naturally in itself with cigarette perfume, and flue gas is rich aobvious
Writing increases, and sophistication is promoted, and alcohol is moistened in flue gas more Tianjin and irritation reduces.
Claims (7)
1. a kind of quick-fried pearl essential oil of cigarette, which is characterized in that be mixed evenly to prepare by the raw material of following mass parts：Lavandulae flos essential oil
1.5~3 parts, 0.5~1.5 part of marjoram essential oil, 1~2 part of ylang-ylang essential oil, 0.5~1.5 part of chamomile essential oil, sandalwood
1~2 part of essential oil, 0.5~1.5 part of vanilla soya-bean oil, 0.2~0.5 part of Chinese ilex essential oil, 1~3 part of borneol extract, the extraction of cloud Radix Angelicae Sinensis
75~89.8 parts of 4~10 parts of object and fat solvent.
2. the quick-fried pearl essential oil of cigarette according to claim 1, which is characterized in that preferably raw material proportioning is：Lavandulae flos
2 parts of essential oil, 1.2 parts of marjoram essential oil, 1.6 parts of ylang-ylang essential oil, 0.8 part of chamomile essential oil, 1 part of sandalwood essential oil, vanilla
83 parts of 0.6 part of soya-bean oil, 0.3 part of Chinese ilex essential oil, 2 parts of borneol extract, 7.5 parts of cloud angelica extract and fat solvent.
3. the quick-fried pearl essential oil of cigarette according to claim 1, it is characterised in that：The cloud angelica extract, by following
Method is prepared：
(1) by the drying of cloud Radix Angelicae Sinensis, crushing, the ethanol water of concentration 70%~95% is added in by 10~20 times of cloud Chinese Angelica Root quality
Solution, 60~80 DEG C of 1~3h of circumfluence distillation；
(2) extracting solution filters while hot, and volume is then concentrated under the conditions of 45~60 DEG C, 60~90kPa and is no longer changed to get cloud
Angelica extract.
4. the quick-fried pearl essential oil of cigarette according to claim 1, it is characterised in that：The fat solvent is：By 24 degree of palm fibres
Palmitic acid oil and Glycerin, mixed triester with caprylic acid capric acid are according to mass ratio 5:1 mixing, then sorbester p17 is added by the 0.5%~0.8% of mixture gross mass,
It is mixed evenly to prepare.
5. preparing the method for the quick-fried pearl essential oil of cigarette described in claims 1 or 2, include the following steps：
(1) by the mass parts by lavandulae flos essential oil, marjoram essential oil, ylang-ylang essential oil, chamomile essential oil, santal another name for
Oil, vanilla soya-bean oil, Chinese ilex essential oil, borneol extract and cloud angelica extract are uniformly mixed, and obtain essence；
(2) by 24 degree of palm oils and Glycerin, mixed triester with caprylic acid capric acid according to mass ratio 5:1 mixing, then by mixture gross mass 0.5%~
0.8% addition sorbester p17, stirring at normal temperature are slowly added to essence obtained by step (1) in whipping process, and essence continues to stir after adding
0.5~1.5h, standing treat lather collapse to get to the required quick-fried pearl essential oil of cigarette.
6. the method for preparing the quick-fried pearl of cigarette using 2 or 3 or 4 essential oil of claims 1 or 2, includes the following steps：
(1) essential oil is added in the hopper of pill dripping machine；
(2) dripping pill lapping is added in the rubber cement tank of pill dripping machine, keeps 70 DEG C of temperature；
(3) it is put into calcium ion salts solution solidifying agent in dripping pill device is contained；
(4) pill dripping machine is opened, essential oil and dripping pill lapping ooze respectively from discharge port and gum outlet, and essential oil is wrapped in dripping pill packet
It wraps up in material, and cured dose of curing molding, obtains the quick-fried pearl of cigarette.
7. preparation method according to claim 6, it is characterised in that：The dripping pill lapping is by following mass parts
Raw material is made：6~20 parts of sodium alginate, 0.1~3 part of Arabic gum, 77~95 parts of water；Wherein, the viscosity of sodium alginate for 5~
40Pa.s；The viscosity of Arabic gum is 80~140cP；Each raw material is placed in retort and is stirred, 70 DEG C of reaction temperature treats material
After fusing, 1~2h is kept the temperature, is stood, after foam floating, filters and obtains under the conditions of 70 DEG C of heat preservation.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108913363A (en) * | 2018-09-11 | 2018-11-30 | 鹰潭华宝香精有限公司 | A kind of extraction and its molecular distillation refining methd of celery seed essential oil product |
| CN109536280A (en) * | 2018-11-27 | 2019-03-29 | 湖北中烟工业有限责任公司 | The quick-fried pearl preparation method of cigarette of internal essence further progress Maillard reaction after molding |
| CN110326814A (en) * | 2019-05-06 | 2019-10-15 | 广东云瑶生物医药科技有限公司 | The quick-fried pearl of borneol essential oil and its application |
| CN110540899A (en) * | 2019-09-18 | 2019-12-06 | 成都中医药大学 | Zanthoxylum bungeanum flavor essence for cigarette bead blasting and application of zanthoxylum bungeanum flavor essence in cigarettes |
| CN110584194A (en) * | 2019-09-25 | 2019-12-20 | 湖北中烟工业有限责任公司 | Preparation method of coffee-flavor blasting bead for cigarettes |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
| CN111084416A (en) * | 2019-11-22 | 2020-05-01 | 云南中烟工业有限责任公司 | Bitter inhibitor-containing blasting bead for Yunnan gentian-flavored cigarette and preparation method and application thereof |
| CN111955786A (en) * | 2020-06-28 | 2020-11-20 | 云南中烟工业有限责任公司 | Additive for highlighting fragrance style characteristics of chamomile, preparation method of additive and cigarette comprising additive |
| CN112048388A (en) * | 2020-09-03 | 2020-12-08 | 河北瑞龙生物科技有限公司 | Extraction method of melia azedarach essential oil and application of melia azedarach essential oil in tobacco and tobacco products |
| CN112795428A (en) * | 2021-02-02 | 2021-05-14 | 河北中烟工业有限责任公司 | Lotus-fragrance-style tobacco essence and preparation method and application thereof |
| CN113796575A (en) * | 2021-09-15 | 2021-12-17 | 成都生制堂生物科技有限公司 | Natural compound essential oil for cigarette bead blasting and preparation method thereof |
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| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108913363A (en) * | 2018-09-11 | 2018-11-30 | 鹰潭华宝香精有限公司 | A kind of extraction and its molecular distillation refining methd of celery seed essential oil product |
| CN109536280A (en) * | 2018-11-27 | 2019-03-29 | 湖北中烟工业有限责任公司 | The quick-fried pearl preparation method of cigarette of internal essence further progress Maillard reaction after molding |
| CN110326814A (en) * | 2019-05-06 | 2019-10-15 | 广东云瑶生物医药科技有限公司 | The quick-fried pearl of borneol essential oil and its application |
| CN110326814B (en) * | 2019-05-06 | 2024-04-26 | 乳源瑶族自治县精润生态农业有限公司 | Borneol essential oil explosion bead and application thereof |
| CN110540899A (en) * | 2019-09-18 | 2019-12-06 | 成都中医药大学 | Zanthoxylum bungeanum flavor essence for cigarette bead blasting and application of zanthoxylum bungeanum flavor essence in cigarettes |
| CN110584194A (en) * | 2019-09-25 | 2019-12-20 | 湖北中烟工业有限责任公司 | Preparation method of coffee-flavor blasting bead for cigarettes |
| CN111084416A (en) * | 2019-11-22 | 2020-05-01 | 云南中烟工业有限责任公司 | Bitter inhibitor-containing blasting bead for Yunnan gentian-flavored cigarette and preparation method and application thereof |
| CN111084416B (en) * | 2019-11-22 | 2022-07-01 | 云南中烟工业有限责任公司 | Bitter inhibitor-containing blasting bead for Yunnan gentian-flavored cigarette and preparation method and application thereof |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
| CN111955786A (en) * | 2020-06-28 | 2020-11-20 | 云南中烟工业有限责任公司 | Additive for highlighting fragrance style characteristics of chamomile, preparation method of additive and cigarette comprising additive |
| CN112048388A (en) * | 2020-09-03 | 2020-12-08 | 河北瑞龙生物科技有限公司 | Extraction method of melia azedarach essential oil and application of melia azedarach essential oil in tobacco and tobacco products |
| CN112048388B (en) * | 2020-09-03 | 2023-01-31 | 河北瑞龙生物科技有限公司 | Extraction method of melia azedarach essential oil and application of melia azedarach essential oil in tobacco and tobacco products |
| CN112795428A (en) * | 2021-02-02 | 2021-05-14 | 河北中烟工业有限责任公司 | Lotus-fragrance-style tobacco essence and preparation method and application thereof |
| CN113796575A (en) * | 2021-09-15 | 2021-12-17 | 成都生制堂生物科技有限公司 | Natural compound essential oil for cigarette bead blasting and preparation method thereof |
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