CN110760387A - Magnolia officinalis and pearl burst essential oil and preparation method thereof - Google Patents
Magnolia officinalis and pearl burst essential oil and preparation method thereof Download PDFInfo
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- CN110760387A CN110760387A CN201911052320.0A CN201911052320A CN110760387A CN 110760387 A CN110760387 A CN 110760387A CN 201911052320 A CN201911052320 A CN 201911052320A CN 110760387 A CN110760387 A CN 110760387A
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- 241001673966 Magnolia officinalis Species 0.000 title claims abstract description 63
- 239000000341 volatile oil Substances 0.000 title claims abstract description 57
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 239000003921 oil Substances 0.000 claims abstract description 21
- 239000008601 oleoresin Substances 0.000 claims abstract description 17
- 239000000706 filtrate Substances 0.000 claims abstract description 12
- 238000002386 leaching Methods 0.000 claims abstract description 11
- 229940093609 tricaprylin Drugs 0.000 claims abstract description 11
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229930003231 vitamin Natural products 0.000 claims abstract description 11
- 239000011782 vitamin Substances 0.000 claims abstract description 11
- 229940088594 vitamin Drugs 0.000 claims abstract description 11
- 235000013343 vitamin Nutrition 0.000 claims abstract description 11
- 244000269722 Thea sinensis Species 0.000 claims abstract description 10
- 235000009569 green tea Nutrition 0.000 claims abstract description 10
- 150000003722 vitamin derivatives Chemical class 0.000 claims abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 239000002245 particle Substances 0.000 claims abstract description 9
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 9
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 9
- ACTIUHUUMQJHFO-UHFFFAOYSA-N Coenzym Q10 Natural products COC1=C(OC)C(=O)C(CC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C)=C(C)C1=O ACTIUHUUMQJHFO-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000017471 coenzyme Q10 Nutrition 0.000 claims abstract description 8
- ACTIUHUUMQJHFO-UPTCCGCDSA-N coenzyme Q10 Chemical compound COC1=C(OC)C(=O)C(C\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CCC=C(C)C)=C(C)C1=O ACTIUHUUMQJHFO-UPTCCGCDSA-N 0.000 claims abstract description 8
- 229940110767 coenzyme Q10 Drugs 0.000 claims abstract description 8
- 108010059892 Cellulase Proteins 0.000 claims abstract description 6
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 6
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 6
- 235000006708 antioxidants Nutrition 0.000 claims abstract description 6
- 229940106157 cellulase Drugs 0.000 claims abstract description 6
- 238000007872 degassing Methods 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims abstract description 6
- 238000000227 grinding Methods 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000002904 solvent Substances 0.000 claims abstract description 5
- 238000005422 blasting Methods 0.000 claims description 12
- 239000002202 Polyethylene glycol Substances 0.000 claims description 10
- 229920001223 polyethylene glycol Polymers 0.000 claims description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 9
- 239000006187 pill Substances 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 6
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 4
- 229930003448 Vitamin K Natural products 0.000 claims description 3
- 238000007605 air drying Methods 0.000 claims description 3
- 238000009833 condensation Methods 0.000 claims description 3
- 230000005494 condensation Effects 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- SHUZOJHMOBOZST-UHFFFAOYSA-N phylloquinone Natural products CC(C)CCCCC(C)CCC(C)CCCC(=CCC1=C(C)C(=O)c2ccccc2C1=O)C SHUZOJHMOBOZST-UHFFFAOYSA-N 0.000 claims description 3
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 claims description 3
- 235000019168 vitamin K Nutrition 0.000 claims description 3
- 239000011712 vitamin K Substances 0.000 claims description 3
- 150000003721 vitamin K derivatives Chemical class 0.000 claims description 3
- 229940046010 vitamin k Drugs 0.000 claims description 3
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims description 2
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 claims description 2
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims description 2
- 230000036541 health Effects 0.000 claims description 2
- 235000019155 vitamin A Nutrition 0.000 claims description 2
- 239000011719 vitamin A Substances 0.000 claims description 2
- 229940045997 vitamin a Drugs 0.000 claims description 2
- 239000002671 adjuvant Substances 0.000 claims 2
- 240000003460 Polygala paniculata Species 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 18
- 239000011324 bead Substances 0.000 abstract description 13
- 239000000284 extract Substances 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 5
- 238000003860 storage Methods 0.000 abstract description 3
- 230000002045 lasting effect Effects 0.000 abstract description 2
- 238000000465 moulding Methods 0.000 abstract 1
- 229930013686 lignan Natural products 0.000 description 9
- 235000009408 lignans Nutrition 0.000 description 9
- 150000005692 lignans Chemical class 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 235000019504 cigarettes Nutrition 0.000 description 7
- 241000208125 Nicotiana Species 0.000 description 6
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 6
- VVOAZFWZEDHOOU-UHFFFAOYSA-N magnolol Chemical compound OC1=CC=C(CC=C)C=C1C1=CC(CC=C)=CC=C1O VVOAZFWZEDHOOU-UHFFFAOYSA-N 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 241000218378 Magnolia Species 0.000 description 4
- 239000011049 pearl Substances 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000007873 sieving Methods 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 1
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 206010043521 Throat irritation Diseases 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 239000002199 base oil Substances 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 229940116229 borneol Drugs 0.000 description 1
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000011162 core material Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940088598 enzyme Drugs 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 201000009240 nasopharyngitis Diseases 0.000 description 1
- 229960003512 nicotinic acid Drugs 0.000 description 1
- 235000001968 nicotinic acid Nutrition 0.000 description 1
- 239000011664 nicotinic acid Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 206010039083 rhinitis Diseases 0.000 description 1
- 238000002390 rotary evaporation Methods 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
- C11B9/0046—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
- C11B9/0049—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms
- C11B9/0053—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms both rings being six-membered
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The invention discloses a magnolia officinalis and exploded bead essential oil and a preparation method thereof, comprising 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 100-500 parts of tricaprylin, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble antioxidant; the preparation method comprises grinding cortex Magnolia officinalis to particle size of 2-10 mm; adding solvent and cellulase, ultrasonic heating and leaching for 5-10 hr, centrifuging at 1000r/min for 3-5min until water and oil are separated, and collecting oil phase to obtain Magnolia officinalis oleoresin; dissolving 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble coenzyme Q10 in 500 parts of tricaprylin 100, filtering and collecting filtrate; degassing the filtrate at 20-60 deg.C under negative pressure for 0.5-2 hr, standing for 2-24 hr to obtain cortex Magnolia officinalis and explode pearl essential oil, which has high content of cortex Magnolia officinalis extract, long storage time, no reaction of explode pearl essential oil with wall material, stable molding, comfortable, pure and natural fragrance, lasting and stable fragrance, and controllable fragrance intensity.
Description
Technical Field
The invention relates to the field of tobacco essence and flavor, and particularly relates to magnolia officinalis and pearl burst essential oil and a preparation method thereof.
Background
The bead blasting is a special process for perfuming auxiliary materials for cigarettes, is a great innovation in the tobacco industry, improves the safety of cigarette products in a bead blasting and perfuming mode, and greatly enriches the types of fragrant raw materials. In recent years, the investment of bead blasting of various large tobacco enterprises is increased, a large number of bead blasting cigarette products rich in self characteristics are provided, and the bead blasting of cigarettes is a brand new perfuming mode and is becoming an important direction of cigarette innovation in recent years. The essence for the bead blasting essential oil is basically a synthetic essence, plays an important role in the aspects of improving the aroma quality of bead blasting, enriching the tobacco aroma and the like, has thinner aroma and active chemical properties in the prior art, is very easy to react with base oil, wall materials and the like, and leads to an unstable state in the online bead blasting forming process, so that bead blasting forming is influenced, and the natural perfume is limited by the permission list of tobacco additives, so that the selectable aroma type is limited.
The magnolia bark-magnolia bark extract is a common traditional Chinese medicine and clinically has the effects of relieving cough and eliminating phlegm, helping digestion and guiding qi downward, and resolving dampness and harmonizing stomach, and the pharmacological test proves that the magnolia bark-magnolia bark extract has the obvious effects of reducing blood pressure and inhibiting pathogenic microorganisms, the smell of the magnolia bark is spicy, the chemical components are volatile oil, alkaloid, saponin, tannin, trace nicotinic acid and the like, and the magnolia bark-magnolia bark extract mainly contains magnolol and magnolol, eugenol-4' -O- β -D-glucopyranoside, magnolia bark lignan A, magnolia bark lignan B, magnolia bark lignan C, magnolia bark lignan D, magnolia bark lignan E, magnolia bark lignan F, magnolia bark lignan G, magnolia bark lignan H, magnolia bark lignan I, borneol magnolol and the like, and various magnolia bark extracts have a fresh and sweet taste in tobacco, are coordinated with smoke, and can obviously reduce the throat irritation in smoking, and are good natural tobacco flavors, and related magnolia bark-magnolia bark extracts are not reported at present.
Disclosure of Invention
In order to solve the problems, the invention provides the magnolia officinalis exploder essential oil and the preparation method thereof, the prepared magnolia officinalis exploder essential oil has high magnolia officinalis extract content and long storage time, the exploder essential oil does not react with wall materials, the forming is stable, the fragrance is comfortable, pure and natural, the fragrance is lasting and stable, and the fragrance intensity is controllable.
The technical scheme of the invention is that the magnolia officinalis and bulbus fritilariae essential oil is provided, and comprises the following components: 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 100-500 parts of tricaprylin, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of antioxidant.
Preferably, the fat-soluble sanitary vitamin comprises vitamin K and vitamin A.
Preferably, the antioxidant is fat-soluble coenzyme Q10.
Further, a preparation method of the magnolia officinalis and bulbus fritilariae essential oil is also provided, and comprises the following steps:
s1, grinding the particle size of the magnolia officinalis to 2-10 mm;
s2, adding a solvent and cellulase, ultrasonically heating and leaching for 5-10h, removing the organic solvent by rotary evaporation, centrifuging at 1000r/min for 3-5min until water and oil are separated, and taking an oil phase to obtain magnolia officinalis oleoresin;
s3, dissolving 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble coenzyme Q10 in 500 parts of tricaprylin 100, filtering to remove insoluble substances, and collecting filtrate;
s4, degassing the filtrate at 20-60 ℃ under negative pressure for 0.5-2h, and standing for 2-24h to obtain the magnolia officinalis and bulbus fritilariae essential oil.
Preferably, the solvent of S2 includes 20% to 40% aqueous ethanol.
Preferably, the heating temperature of S2 is 30-45 ℃, and the ultrasonic leaching power is 10-20 kHz.
Further, a use method of the magnolia officinalis and bulbus fritilariae essential oil is also provided, and the use method comprises the following steps: K1. 0.5-5 parts of the essential oil of the magnolia officinalis blasting pearls is scattered in polyethylene glycol, and an auxiliary agent is added; K2. placing the mixture obtained by K1 in a tank of a natural condensation pill dripping machine, heating at 60-80 deg.C, mixing liquid flow rate of 40-50 particles/s, dripper size of 2.5mm, dripping distance of 3-5cm, and dripping pill cooling oil temperature of 10-15 deg.C; K3. removing oil stain on the surface of the dripping pill obtained by K2 with oil absorbing paper, and air drying.
Further, the molecular weight of the polyethylene glycol is 1000-.
Further, the auxiliary agent comprises propylene glycol and sodium stearate.
The invention has the beneficial effects that:
1. when the magnolia officinalis is applied to cigarette flavoring, a remarkable fresh, spicy and sweet flavor can be brought by a small using amount, the fragrance is strong, the fragrance is comfortable and natural, and the stimulation during smoking can be obviously reduced;
2. the tricaprylin has better anti-corrosion effect and stable property, and cannot react with wall materials;
3. adding fat-soluble antioxidant into essential oil to prevent the rancidity of tricaprylin or essential oil, and prolong the storage time of essential oil;
4. the mangnolia officinalis oleoresin is released more thoroughly by using enzymolysis, the extraction rate is higher, on one hand, the use activity of enzyme is ensured by extracting with 20-40% ethanol water, on the other hand, the extraction efficiency is improved, nonpolar substances are removed as much as possible, and the essential oil is purer;
5.1000-2000 molecular weight polyethylene glycol is in gel state at normal temperature, and melts into liquid when heated, and can well lock fragrance when in gel state, the porosity is uniform and fine, the external fragrance is not penetrated, the fragrance is kept for a long time, and no obvious negative effect is caused, if the fragrance intensity is required to be enhanced, the polyethylene glycol can be broken by pinching or the part of a filter tip wrapping the polyethylene glycol is contacted with a mouth for continuous low-temperature heating, so that the polyethylene glycol melts, the magnolia officinalis essential oil is released, and the fragrance intensity is enhanced;
6. the green tea essential oil has effects of refreshing brain, treating common cold, cough, rhinitis and asthma, recovering activity, and resisting depression, and can be absorbed by steam; the fig essential oil can effectively cover up the miscellaneous gas of cigarettes, enables the smoke to be soft, has fine fragrance, has the effect of obviously improving the smoke quality and neutralizes the fragrance of the magnolia officinalis oleoresin, and the combination of the three components enables the fragrance to be more layered, and meanwhile, the fat-soluble vitamins are added to be beneficial to health.
Detailed Description
In order to make the present invention more comprehensible, the technical solutions of the present invention are further described below with reference to specific embodiments, but the present invention is not limited thereto.
Example 1
Grinding and sieving 100g of cortex Magnolia officinalis to obtain powder with particle size of 2-10 mm; adding 200ml of 20-40% ethanol water solution and 5U cellulase, leaching for 5-10h at 30-45 deg.C with ultrasonic leaching power of 10-20kHz, centrifuging for 3-5min with a 1000r/min centrifuge until water and oil are separated, and collecting oil phase to obtain Magnolia officinalis oleoresin;
mixing commercially available green tea essential oil 5g, fig essential oil 5g, 10g of cortex Magnolia officinalis oleoresin prepared above, vitamin K0.5 g commercially available, and fat-soluble coenzyme Q10 0.3g into Tween 80 1g, stirring, dissolving in tricaprylin 500g, stirring for 3-5 hr, filtering to remove insoluble substances, and collecting filtrate; degassing the filtrate at 20-60 deg.C under negative pressure for 0.5-2 hr, and standing for 2-24 hr to obtain the essential oil.
Example 2
Grinding and sieving 100g of cortex Magnolia officinalis to obtain powder with particle size of 2-10 mm; adding 200ml of 20-40% ethanol water solution and 5U cellulase, leaching for 5-10h at 30-45 deg.C with ultrasonic leaching power of 10-20kHz, centrifuging for 3-5min with a 1000r/min centrifuge until water and oil are separated, and collecting oil phase to obtain Magnolia officinalis oleoresin;
mixing commercially available 1g of green tea essential oil, 1g of fig essential oil, 5g of prepared Magnolia officinalis oleoresin, 0.1g of commercially available vitamin K, 0.1g of fat-soluble coenzyme Q10, and 0.1g of Tween 80, stirring, dissolving in 100g of tricaprylin, stirring for 3-5h, filtering to remove insoluble substances, and collecting filtrate; degassing the filtrate at 20-60 deg.C under negative pressure for 0.5-2 hr, and standing for 2-24 hr to obtain the essential oil.
Example 3
Grinding and sieving 100g of cortex Magnolia officinalis to obtain powder with particle size of 2-10 mm; adding 200ml of 20-40% ethanol water solution and 5U cellulase, leaching for 5-10h at 30-45 deg.C with ultrasonic leaching power of 10-20kHz, centrifuging for 3-5min with a 1000r/min centrifuge until water and oil are separated, and collecting oil phase to obtain Magnolia officinalis oleoresin;
mixing commercially available green tea essential oil 3g, fructus fici essential oil 3g, and cortex Magnolia officinalis oleoresin 8g, commercially available vitamin K0.3 g, and fat-soluble coenzyme Q10 0.2g into Tween 80 0.5g, stirring, dissolving in tricaprylin 300g, stirring for 3-5 hr, filtering to remove insoluble substances, and collecting filtrate; degassing the filtrate at 20-60 deg.C under negative pressure for 0.5-2 hr, and standing for 2-24 hr to obtain the essential oil.
Example 4
0.5-5 parts of the essential oil of the magnolia officinalis pearls are scattered into polyethylene glycol, and 1g of propylene glycol and 1g of sodium stearate are added; placing the above mixture in a tank of a natural condensation dripping pill machine, heating at 60-80 deg.C, mixing liquid flow rate of 40-50 particles/s, dripping head size of 2.5mm, dripping distance of 3-5cm, and dripping pill cooling oil temperature of 10-15 deg.C; removing oil stain on the surface of the dripping pill with oil absorbing paper, spreading and air drying to obtain cortex Magnolia officinalis puffed bead.
The Magnolia officinalis gel beads are placed in a filter tip, a sample is drawn for sucking, the fragrance lasts for 7h, and when the beads are pinched and exploded or heated, the polyethylene glycol releases core materials such as Magnolia officinalis essential oil, and the fragrance is strong and is released immediately.
The above description is only a preferred embodiment of the present invention, and all equivalent changes and modifications made in accordance with the claims of the present invention should be covered by the present invention.
Claims (9)
1. The magnolia officinalis and bulbus fritilariae essential oil is characterized by comprising the following components: 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 100-500 parts of tricaprylin, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble antioxidant.
2. The essential oil of Magnolia officinalis what is claimed in claim 1, wherein the fat-soluble health vitamin comprises vitamin K and vitamin A.
3. The essential oil of Magnolia officinalis what is claimed in claim 1, wherein the fat-soluble antioxidant is fat-soluble coenzyme Q10.
4. The preparation method of the magnolia officinalis and bulbus fritilariae essential oil is characterized by comprising the following steps:
s1, grinding the particle size of the magnolia officinalis to 2-10 mm;
s2, adding a solvent and cellulase, ultrasonically heating and leaching for 5-10h, centrifuging at 1000r/min for 3-5min until water and oil are separated, and taking an oil phase to obtain magnolia officinalis oleoresin;
s3, dissolving 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble coenzyme Q10 in 500 parts of tricaprylin 100, filtering to remove insoluble substances, and collecting filtrate;
s4, degassing the filtrate at 20-60 ℃ under negative pressure for 0.5-2h, and standing for 2-24h to obtain the magnolia officinalis and bulbus fritilariae essential oil.
5. The method for preparing magnolia officinalis and bulbus fritilariae essential oil as claimed in claim 4, wherein the solvent S2 comprises 20% -40% ethanol water solution.
6. The method for preparing magnolia officinalis and bulbus fritilariae essential oil as claimed in claim 4, wherein the heating temperature of S2 is 30-45 ℃, and the ultrasonic leaching power is 10-20 kHz.
7. The application method of the magnolia officinalis and bulbus fritilariae essential oil is characterized by comprising the following steps: K1. dispersing 0.5-5 parts of Magnolia officinalis blasting pearl essential oil in polyethylene glycol, and adding adjuvant; K2. placing the mixture obtained by K1 in a tank of a natural condensation pill dripping machine, heating at 60-80 deg.C, mixing liquid flow rate of 40-50 particles/s, dripper size of 2.5mm, dripping distance of 3-5cm, and dripping pill cooling oil temperature of 10-15 deg.C; K3. removing oil stain on the surface of the dripping pill obtained by K2 with oil absorbing paper, and air drying.
8. The application method of essential oil of cortex magnoliae officinalis and blasting pearl as claimed in claim 7, wherein the molecular weight of the polyethylene glycol is 1000-2000.
9. The use method of essential oil of Magnolia bark and Polygala paniculata as claimed in claim 7, wherein the adjuvant comprises propylene glycol and sodium stearate.
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| CN1092960A (en) * | 1993-03-21 | 1994-10-05 | 张铁林 | Additive in cigarette |
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| CN107802031A (en) * | 2017-10-18 | 2018-03-16 | 汉寿亿达新材料科技有限公司 | A kind of quick-fried pearl of cigarette |
| CN108285830A (en) * | 2018-01-24 | 2018-07-17 | 云南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1092960A (en) * | 1993-03-21 | 1994-10-05 | 张铁林 | Additive in cigarette |
| CN105112162A (en) * | 2015-08-25 | 2015-12-02 | 东莞波顿香料有限公司 | Multifunctional essence slow-release carrier and preparation method thereof |
| CN106551424A (en) * | 2016-11-29 | 2017-04-05 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of the Green tea essence for cigarette drop pill |
| CN107802031A (en) * | 2017-10-18 | 2018-03-16 | 汉寿亿达新材料科技有限公司 | A kind of quick-fried pearl of cigarette |
| CN108285830A (en) * | 2018-01-24 | 2018-07-17 | 云南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl herbal essential oil and quick-fried pearl preparation method |
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