CN111084409A - Dried orange peel type composite extract for cigarette bead blasting and preparation method thereof - Google Patents
Dried orange peel type composite extract for cigarette bead blasting and preparation method thereof Download PDFInfo
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- CN111084409A CN111084409A CN201911185117.0A CN201911185117A CN111084409A CN 111084409 A CN111084409 A CN 111084409A CN 201911185117 A CN201911185117 A CN 201911185117A CN 111084409 A CN111084409 A CN 111084409A
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- dried orange
- orange peel
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- type composite
- composite extract
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to the technical field of cigarettes, in particular to a dried orange peel type composite extract for cigarette bead blasting and a preparation method thereof. The dried orange peel type composite extract for popping the beads in cigarettes is formed by combining dried orange peel, trichosanthes peel, chrysanthemum, liquorice, momordica grosvenori and bamboo juice, can be mutually dissolved with a solvent wrapped by the popping beads, can completely cover bad smell brought by a popping bead wall material and the solvent, is added into a cigarette filter stick, and is pinched broken in the smoking process, so that the Chinese herbal medicine has comfortable and natural fragrance, soft and fine smoke, improved fragrance texture, sweet taste, comfortable throat, lung moistening, cough relieving and throat discomfort relieving, and the composite extract has the advantages of easily obtained raw materials, simple preparation method, suitability for large-scale industrial production and strong practical significance.
Description
Technical Field
The invention relates to the technical field of cigarettes, in particular to a dried orange peel type composite extract for cigarette bead blasting and a preparation method thereof.
Background
Tobacco belongs to leaves of tobacco of Solanaceae, and has effects of refreshing and tranquilizing central nervous system when made into cigarette for smoking, but can also bring respiratory tract diseases such as throat irritation, cough, excessive phlegm, etc.
According to the estimation of the primary statistical data, the patients with pharyngolaryngitis and tracheitis caused by smoking in China are the first to be pathogenic to smoke. Therefore, the Chinese herbal medicine with the functions of reducing phlegm and relieving cough, and relieving the respiratory diseases such as pharyngolaryngitis, bronchitis and the like is added, so that the Chinese herbal medicine has important significance and good market prospect. The Chinese herbal medicine extract is added into the tobacco, so that the property of the tobacco can be harmonized, meanwhile, the effective ingredients of the Chinese herbal medicine can enter main stream smoke and are absorbed by mucous membranes of a respiratory system, the effects of regulating qi, moistening lung and relieving cough are achieved, and the purposes of moistening and relieving cough are achieved.
In the tobacco industry, related Chinese herbal medicines have been used for perfuming cigarettes, but the main method is mainly to perfume cut tobacco directly or add perfume or microcapsule particles adhered with Chinese herbal medicines into a filter tip. The two methods have the defects of short retention time of the Chinese herbal medicines, short quality guarantee period of the cigarettes, difficult access of effective components to main stream smoke of the cigarettes and great loss of effect. The bead-blasting perfuming is a novel cigarette perfuming mode, and a filter tip of the bead-blasting cigarette is internally provided with a bead blasting made of a high polymer material, wherein essence or an extract is contained in the bead blasting cigarette. The consumer then burns and inhales the cigarette after breaking the exploded bead, and the smoke gas acts with the effective components in the exploded bead when passing through the filter tip, thus completing the perfuming process. The method effectively avoids the loss of the spice caused by the cigarette combustion, and meanwhile, the effective components are placed in the sealed blasting beads during the cigarette storage period, so that the loss caused by volatilization can be avoided.
Most of the bead blasting cigarettes in the market at present are essences with obvious characteristics, such as mint fragrance, agilawood, fruit fragrance and the like, and bead blasting with the effects of reducing phlegm, relieving cough and relieving respiratory tract discomfort is not frequent, so that the problem that the bead blasting with the effects of improving the aroma texture of the cigarettes, reducing phlegm, relieving cough and relieving respiratory tract discomfort is urgently needed to be solved at present is found.
Disclosure of Invention
In order to solve the technical problems in the prior art, the invention provides a dried orange peel type composite extract for cigarette bead blasting and a preparation method thereof, and the dried orange peel type composite extract is realized by the following technical scheme:
a dried orange peel type compound extract for bead blasting of cigarettes is prepared from dried orange peel, pericarpium trichosanthis, chrysanthemum, liquorice, momordica grosvenori and bamboo juice in a mass ratio of 10 (1-2) to 1-2 to 16-20.
Preferably, the dried orange peel, the snakegourd peel, the chrysanthemum, the liquorice, the momordica grosvenori and the bamboo juice are in the following mass ratio: 10:2:1:1:1:20. The proportion is moderate, and the obtained dried orange peel type composite extract for the cigarette bead blasting has better integrity.
The preparation method of the dried orange peel type composite extract for cigarette bead blasting comprises the following steps:
(1) weighing pericarpium Citri Tangerinae, pericarpium Trichosanthis, flos Chrysanthemi, Glycyrrhrizae radix, and fructus Siraitiae Grosvenorii in proportion, pulverizing, adding succus Bambusae, and performing microwave treatment under stirring;
(2) putting the mixture treated in the step (1) into an ultrasonic extraction pool, adding propylene glycol and an emulsifier, and carrying out ultrasonic extraction, wherein the ultrasonic power is 800-1000W, the ultrasonic frequency is 20KHz, and the time is 20-30 min;
(3) performing ultrasonic extraction, performing centrifugal separation to obtain supernatant, concentrating the supernatant under reduced pressure until no water exists, and performing centrifugation to obtain secondary supernatant;
(4) and (4) stirring and mixing the secondary supernatant obtained in the step (3) and the caprylic/capric glyceride, and stirring at normal temperature for 0.5-1.5h to obtain the tangerine peel type composite extract which can be used for preparing the popping beads.
Preferably, in the step (1), the microwave treatment is performed under the conditions of power of 600-. The microwave irradiation is helpful for the semi-volatile components to be quickly dissolved out of the cells, and the effect of the microwave irradiation is better under the condition.
Preferably, in the step (2), the addition amount of the propylene glycol is 20-30% of the weight of the mixture. The ultrasonic extraction effect is better.
Preferably, in the step (2), the emulsifier is 0.1-0.5% of the weight of the mixture. At the moment, the emulsifying system is stable and the effect is good.
Preferably, the emulsifier is tween 20. Tween 20 is a good class of oil/water emulsifiers.
The ultrasonic extraction can further dissolve out effective semi-volatile components in the raw materials, and the emulsifier is added to be helpful for forming an emulsifying system with propylene glycol and water, so as to effectively dissolve fat-soluble components.
Preferably, in the step (3), the centrifugation rate is 6000-. At the moment, the centrifugal separation effect is better, the hydrophilic macromolecular components can be removed, and the effective components can be fully separated.
Preferably, in the step (4), the mass of the supernatant is 1-3% of that of the caprylic/capric glyceride. The caprylic capric glyceride is colorless, odorless and transparent liquid, and has viscosity half of that of common vegetable oil. Low solidifying point and high oxidizing stability. Has good intersolubility with various solvents, grease, some oxidants and vitamins. The emulsifying property, the solubility, the extensibility and the lubricity of the grease are all better than those of common grease. The lipophilic liquid obtained by mixing the supernatant with caprylic capric glyceride can be used for assisting the formation of the bead blasting.
Compared with the prior art, the invention has the technical effects that:
1. the dried orange peel type composite extract for cigarette bead blasting can be mutually soluble with a solvent wrapped by bead blasting, and can completely cover the bad smell caused by the wall material and the solvent of the bead blasting.
2. The puffed bead prepared from the dried orange peel type composite extract for cigarette puffing is added into a cigarette filter stick, and is broken in a smoking process, so that the Chinese herbal medicine has comfortable and natural fragrance, fragrant and natural fragrance, soft and exquisite smoke and improved fragrance texture.
3. The puffed bead prepared from the dried orange peel type composite extract for the puffed bead of the cigarette is added into a cigarette filter stick, and the puffed bead is pinched and broken in the smoking process, so that the puffed bead has sweet taste, is comfortable in throat, moistens the lung and relieves cough, and relieves throat discomfort.
4. The dried orange peel type composite extract for cigarette bead blasting is easy to obtain raw materials, simple in preparation method, capable of improving fragrance and relieving throat discomfort, applicable to large-scale industrial production and very high in practical significance.
Detailed Description
The technical solution of the present invention is further limited by the following embodiments, but the scope of the claims is not limited to the description.
Example 1
(1) Weighing 10kg of dried orange peel, 1.5kg of snakegourd peel, 1.5kg of chrysanthemum, 1.5kg of liquorice and 1.5kg of fructus momordicae, crushing, adding 18kg of bamboo juice, and performing microwave treatment under the stirring state, wherein the microwave treatment condition is that the power is 800W, the irradiation time is 6.5min, and the temperature is 90 ℃;
(2) putting the mixture treated in the step (1) into an ultrasonic extraction pool, adding propylene glycol accounting for 25% of the weight of the mixture and an emulsifier accounting for 0.3%, and performing ultrasonic extraction, wherein the ultrasonic power is 900W, the ultrasonic frequency is 20KHz, the ultrasonic time is 25min, and the emulsifier is Tween 20;
(3) centrifuging after ultrasonic extraction to obtain supernatant, concentrating the supernatant under reduced pressure until no water exists, centrifuging at 7000rpm for 12.5min to obtain secondary supernatant;
(4) and (3) stirring and mixing the secondary supernatant obtained in the step (3) and the caprylic/capric glyceride, wherein the mass of the supernatant is 2% of that of the caprylic/capric glyceride, stirring at normal temperature for 1h to obtain the tangerine peel type composite extract which can be used for preparing the popping beads.
Example 2
(1) Weighing 10kg of dried orange peel, 1kg of snakegourd peel, 1kg of chrysanthemum, 2kg of liquorice and 2kg of momordica grosvenori, crushing, adding 16kg of bamboo juice, and performing microwave treatment under the stirring state, wherein the microwave treatment condition is that the power is 800W, the irradiation time is 6.5min, and the temperature is 90 ℃;
(2) putting the mixture treated in the step (1) into an ultrasonic extraction pool, adding propylene glycol accounting for 25% of the weight of the mixture and an emulsifier accounting for 0.3%, and performing ultrasonic extraction, wherein the ultrasonic power is 900W, the ultrasonic frequency is 20KHz, the ultrasonic time is 25min, and the emulsifier is Tween 20;
(3) centrifuging after ultrasonic extraction to obtain supernatant, concentrating the supernatant under reduced pressure until no water exists, centrifuging at 7000rpm for 12.5min to obtain secondary supernatant;
(4) and (3) stirring and mixing the secondary supernatant obtained in the step (3) and the caprylic/capric glyceride, wherein the mass of the supernatant is 2% of that of the caprylic/capric glyceride, stirring at normal temperature for 1h to obtain the tangerine peel type composite extract which can be used for preparing the popping beads.
Example 3
(1) Weighing 10kg of dried orange peel, 2kg of snakegourd peel, 2kg of chrysanthemum, 2kg of liquorice and 2kg of momordica grosvenori, crushing, adding 20kg of bamboo juice, and performing microwave treatment under the stirring state, wherein the microwave treatment condition is that the power is 800W, the irradiation time is 6.5min, and the temperature is 90 ℃;
(2) putting the mixture treated in the step (1) into an ultrasonic extraction pool, adding propylene glycol accounting for 25% of the weight of the mixture and an emulsifier accounting for 0.3%, and performing ultrasonic extraction, wherein the ultrasonic power is 900W, the ultrasonic frequency is 20KHz, the ultrasonic time is 25min, and the emulsifier is Tween 20;
(3) centrifuging after ultrasonic extraction to obtain supernatant, concentrating the supernatant under reduced pressure until no water exists, centrifuging at 7000rpm for 12.5min to obtain secondary supernatant;
(4) and (3) stirring and mixing the secondary supernatant obtained in the step (3) and the caprylic/capric glyceride, wherein the mass of the supernatant is 2% of that of the caprylic/capric glyceride, stirring at normal temperature for 1h to obtain the tangerine peel type composite extract which can be used for preparing the popping beads.
Example 4
(1) Weighing 10kg of dried orange peel, 2kg of snakegourd peel, 2kg of chrysanthemum, 1kg of liquorice and 1kg of momordica grosvenori, crushing, adding 16kg of bamboo juice, and performing microwave treatment under the stirring state, wherein the microwave treatment condition is that the power is 600W, the irradiation time is 8min, and the temperature is 80 ℃;
(2) putting the mixture treated in the step (1) into an ultrasonic extraction pool, adding propylene glycol accounting for 20% of the weight of the mixture and an emulsifier accounting for 0.1%, and performing ultrasonic extraction, wherein the ultrasonic power is 1000W, the ultrasonic frequency is 20KHz, the ultrasonic time is 20min, and the emulsifier is Tween 20;
(3) centrifuging after ultrasonic extraction to obtain supernatant, concentrating the supernatant under reduced pressure until no water exists, centrifuging at 6000rpm for 15min to obtain secondary supernatant;
(4) and (3) stirring and mixing the secondary supernatant obtained in the step (3) and the caprylic/capric glyceride, wherein the mass of the supernatant is 1% of that of the caprylic/capric glyceride, stirring at normal temperature for 0.5h to obtain the tangerine peel type composite extract which can be used for preparing the popping beads.
Example 5
(1) Weighing 10kg of dried orange peel, 2kg of snakegourd peel, 1kg of chrysanthemum, 1kg of liquorice and 1kg of momordica grosvenori, crushing, adding 20kg of bamboo juice, and performing microwave treatment under the stirring state, wherein the microwave treatment condition is that the power is 1000W, the irradiation time is 5min, and the temperature is 100 ℃;
(2) putting the mixture treated in the step (1) into an ultrasonic extraction pool, adding propylene glycol accounting for 30% of the weight of the mixture and an emulsifier accounting for 0.5%, and performing ultrasonic extraction, wherein the ultrasonic power is 800W, the ultrasonic frequency is 20KHz, the ultrasonic time is 30min, and the emulsifier is Tween 20;
(3) centrifuging after ultrasonic extraction to obtain supernatant, concentrating the supernatant under reduced pressure until no water exists, centrifuging at 8000rpm for 10min to obtain secondary supernatant;
(4) and (3) stirring and mixing the secondary supernatant obtained in the step (3) and the caprylic/capric glyceride, wherein the mass of the supernatant is 3% of that of the caprylic/capric glyceride, stirring at normal temperature for 1.5h to obtain the tangerine peel type composite extract which can be used for preparing the popping beads.
Comparative example 1
The procedure was as in example 1 of CN 107115485A.
Preparing a cigarette A sample, preparing the preparation obtained in the examples 1-5 and the comparative example 1 into exploded beads, respectively placing the exploded beads into the middle part of a filter tip of the cigarette A sample, and putting the extract into a cigarette filter tip after the exploded beads are crushed. And performing comparative smoking evaluation on the smoke characteristics of the cigarette A and blank cigarette A samples added with the exploded beads by 13 sensory evaluators according to YC/T497-2014 sensory evaluation method for Chinese style cigarettes in cigarettes to obtain evaluation values.
TABLE 1 flue gas characteristic index evaluation values
Preparing a cigarette A sample, preparing the dried orange peel type composite extract obtained in the examples 1-5 and the comparative example 1 into exploded beads, respectively placing the exploded beads into the middle part of the filter tip of the cigarette A sample, and putting the extract into the cigarette filter tip after the exploded beads are crushed. The 13 sensory evaluators compare and smoke the comfort characteristics of the cigarette A and the blank cigarette A samples added with the exploded beads according to YC/T497-2014 sensory evaluation method for Chinese style of cigarette type, and evaluation scores are obtained.
TABLE 2 evaluation values of comfort characteristic indices
And all evaluators can feel that the cigarette sample added with the cigarette popping bead is comfortable and natural in Chinese herbal medicine fragrance, natural in orange peel fragrance, soft and exquisite in smoke and improved in fragrance quality. The bead-blasting cigarette for cigarettes containing the Chinese herbal medicine compound extract has sweet taste and smooth throat by smoking. Compared with the comparative example 1, the cough-relieving and phlegm-resolving powder has more obvious cough-relieving and phlegm-resolving effects, is more coordinated with the original fragrance of tobacco, and is more acceptable.
Finally, it should be noted that the above embodiments are merely representative examples of the present invention. Obviously, the technical solution of the present invention is not limited to the above embodiments, and many variations are possible. All modifications which can be derived or suggested by a person skilled in the art from the disclosure of the present invention are to be considered within the scope of the invention.
Claims (10)
1. A dried orange peel type composite extract for cigarette blasting beads is characterized by being prepared from dried orange peel, pericarpium trichosanthis, chrysanthemum, liquorice, momordica grosvenori and bamboo juice in a combined mode, wherein the mass ratio of the dried orange peel, the pericarpium trichosanthis, the chrysanthemum, the liquorice, the momordica grosvenori and the bamboo juice is 10 (1-2) to (16-20).
2. The dried orange peel type composite extract for cigarette blasting beads according to claim 1, wherein the dried orange peel, the snakegourd peel, the chrysanthemum, the liquorice, the momordica grosvenori and the bamboo juice are in the following mass ratio: 10:2:1:1:1:20.
3. The method for preparing the dried orange peel type compound extract for the cigarette blasting bead as claimed in claim 1 and 2, is characterized by comprising the following steps:
(1) weighing pericarpium Citri Tangerinae, pericarpium Trichosanthis, flos Chrysanthemi, Glycyrrhrizae radix, and fructus Siraitiae Grosvenorii in proportion, pulverizing, adding succus Bambusae, and performing microwave treatment under stirring;
(2) putting the mixture treated in the step (1) into an ultrasonic extraction pool, adding propylene glycol and an emulsifier, and carrying out ultrasonic extraction, wherein the ultrasonic power is 800-1000W, the ultrasonic frequency is 20KHz, and the time is 20-30 min;
(3) performing ultrasonic extraction, performing centrifugal separation to obtain supernatant, concentrating the supernatant under reduced pressure until no water exists, and performing centrifugation to obtain secondary supernatant;
(4) and (4) stirring and mixing the secondary supernatant obtained in the step (3) and caprylic/capric glyceride, and stirring at normal temperature for 0.5-1.5h to obtain the tangerine peel type composite extract which can be used for preparing the popping beads.
4. The method for preparing the dried orange peel type composite extract for the cigarette bead blasting according to the claim 3, wherein the microwave treatment in the step (1) is performed under the power of 600-1000W, the irradiation time is 5-8min, and the temperature is 80-100 ℃.
5. The method for preparing the dried orange peel type composite extract for cigarette blasting beads according to claim 3, wherein in the step (2), the addition amount of the propylene glycol is 20-30% of the weight of the mixture.
6. The method for preparing the dried orange peel type composite extract for cigarette blasting beads according to claim 3, wherein in the step (2), the emulsifier accounts for 0.1-0.5% of the weight of the mixture.
7. The method for preparing the tangerine peel-type composite extract for cigarette blasting according to claim 3, wherein the emulsifier is Tween 20.
8. The method for preparing the tangerine peel-type composite extract for cigarette bead blasting according to claim 3, wherein in the step (3), the centrifugation speed is 6000-8000rpm, and the centrifugation time is 10-15 min.
9. The method for preparing the dried orange peel type composite extract for cigarette blasting beads according to claim 3, wherein in the step (4), the mass of the supernatant is 1-3% of the mass of the caprylic/capric glyceride.
10. The use of the dried orange peel type compound extract for cigarette blasting beads according to claims 1-2 in the preparation of cigarette blasting bead products.
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