CN106263014A - A kind of process for purification containing Herba thymi vulgaris perfume material and application - Google Patents
A kind of process for purification containing Herba thymi vulgaris perfume material and application Download PDFInfo
- Publication number
- CN106263014A CN106263014A CN201610703177.7A CN201610703177A CN106263014A CN 106263014 A CN106263014 A CN 106263014A CN 201610703177 A CN201610703177 A CN 201610703177A CN 106263014 A CN106263014 A CN 106263014A
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- CN
- China
- Prior art keywords
- herba thymi
- thymi vulgaris
- perfume material
- purification
- extraction solvent
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses the process for purification of a kind of Herba thymi vulgaris perfume material, the method uses propylene glycol, glycerol to be solvent；Optimum solvent ratio is propylene glycol: the consumption of glycerol (30:40) is (35:1) with Herba thymi vulgaris stem, the more ratio of greater inequality example of leaf；The optimal time that Extraction solvent extracts the most naturally is 35 days；Filter, remove stem, leaf slag, obtain Herba thymi vulgaris perfume material.It is applied in blank tobacco shred by best proportion 0.0009%, after preserving 24 hours, smokes panel test.Fruit shows: the Herba thymi vulgaris perfume material that the process for purification of employing Herba thymi vulgaris perfume material the refines distinctive style to showing cigarette product, fragrant to abundant cigarette, make flue gas fine and smooth, soft, reduce flue gas to oral cavity and the stimulation of throat, promoting or transferring Medicated cigarette suck mouthfeel, the distinctive style such as lasting is lasting, pleasant impression is comfortable have good effect.
Description
Technical field
The present invention relates to the process for purification of the natural cigarette flavor of a kind of characteristic, be specially a kind of characteristic natural tobacco fragrant former
The process for purification of material and application.
Background technology
Herba thymi vulgaris (Thymus mongolicus Ronn.) have another name called Herba thymi vulgaris, Murraya paniculata (L.) Jack., Herba Thymi leaf, corner piece, be lip
Section Thymus plant, fruticuli.Many stems are raw, crawl or upper elongation；Sterile plate, for basal part of stem, is crawled or upper elongation, by short,
Fine and soft hair；Spray is high about 8.2 centimetres, about 4 pairs of leaves.Leaf ovalize, is about 8.2 millimeters, wide about 4.1 millimeters, the sharp point of tip, base
Portion's wedge shape, Quan Yuan, just, back of the body two sides smooth, the most about 3 offside faint pulse projections, gland point is slightly obvious, has petiole, and top is short, nearly bottom
Petiole is about blade length 1/2；Bract is close, the nearly 1/3 tool echinid of edge lower part.
Inflorescence is head, short stalk flower tool.The bell calyx of tubulose, is about 4.2 millimeters, and the nearly Glabrous in top, bottom is dilute
Dredging fine and soft hair, lower lip is slightly longer, upper lip is the shortest or upper and lower two lips are the most equal, triangle upper lip, tool echinid or without hair.Corolla is purple
Red, it is about 7.2 millimeters, by sparse short fine and soft hair, corolla tube is increased up, and is about 5.2 millimeters.The flat-shaped nut of oval, smooth.Flower
Nearly 7-8 month phase.It is mainly distributed on China Heilungkiang, Liaoning, the Inner Mongol, Jilin, Hebei, Shanxi, Shaanxi, Shandong, Gansu, new
Boundary, Jiangsu, Sichuan, Guizhou and Guangxi etc. save (autonomous region).
Generally with steam distillation, the Herba thymi vulgaris stem of band inflorescence is obtained lurid thyme oil through steam distillation,
Proportion (20 DEG C): 0.917～0.938, refraction index (20 DEG C): 1.496～1.507.Quintessence oil for soft drink, bakery product,
Flavoring agent, alcoholic beverage, confection, meat product etc..After being also used for toothpaste, dentifrice, talcum powder and shaving in the perfuming of goods.Few
Measure in for fancy soap, detergent, wash with water, spray water flavoring essence in, be that to make head with its pungent perfume (or spice) fragrant.Often and Herba Menthae, eucalyptus globulus
Leaf oil is with among cough drop or cough syrup.Thyme oil has strong sterilizing power, therefore for medical and health goods.Also can use
In isolated thymol.Quintessence oil has the factor causing variable color.
Herba thymi vulgaris perfume material is fragrant to abundant cigarette, makes flue gas fine and smooth, soft, and minimizing flue gas, to oral cavity and the stimulation of throat, carries
Asking for files for examination the mouthfeel of sucking of cigarette, the distinctive style such as lasting is lasting, pleasant impression is comfortable have good effect.
Summary of the invention
The purpose of the present invention for the distinctive style of Herba thymi vulgaris perfume (or spice) perfume material, develops a kind of Herba thymi vulgaris perfume material just
Process for purification.The Herba thymi vulgaris perfume material using the process for purification of patent of the present invention to refine has the characteristic wind showing cigarette product
Lattice, fragrant to abundant cigarette, make flue gas fine and smooth, soft, reduce flue gas to oral cavity and the stimulation of throat, promoting or transferring Medicated cigarette suck mouthfeel,
The distinctive style such as lasting is lasting, pleasant impression is comfortable have good effect.
The present invention is achieved through the following technical solutions:
The process for purification of a kind of Herba thymi vulgaris perfume material, including Extraction solvent propylene glycol, glycerol, it is characterised in that: by third
Glycol, glycerol dissolve each other according to a certain percentage, refine thyme leaf as refining solvent.
Described propylene glycol, glycerol are food grade solvent.Herba thymi vulgaris stem, leaf.
Described method uses propylene glycol, glycerol to be Extraction solvent；Extraction solvent is with mass ratio range as propylene glycol: glycerol
For 10-40:20-60；The consumption of Extraction solvent is 10-40:1 with Herba thymi vulgaris stem, the weight ratio of leaf；Extraction solvent is at normal temperature and pressure
Lower natural extraction time is 30-45 days.
Preferred version is, Extraction solvent is with mass ratio range as propylene glycol: glycerol is as 20-30:40-50.
Propylene glycol: the weight ratio of glycerol is most preferably 30:40.
Extraction solvent consumption and Herba thymi vulgaris stem, the consumption of leaf are preferably 20-40:1 with mass ratio range..
Extraction solvent consumption and Herba thymi vulgaris stem, the consumption of leaf are most preferably 35:1 with mass ratio range.
The time that Extraction solvent extracts the most naturally is preferably 30 days-40 days, most preferably 35 days.
The best-of-breed technology scheme of the application is that Extraction solvent is with mass ratio range as propylene glycol: the weight ratio of glycerol is 30:
40, the consumption of Extraction solvent and Herba thymi vulgaris stem, leaf weight more than for 35:1；When Extraction solvent extracts the most naturally
Between be 35 days.
Invention also provides the Herba thymi vulgaris perfume material that the process for purification of above-mentioned Herba thymi vulgaris perfume material prepares should
With, Herba thymi vulgaris perfume material addition in tobacco shred is the 0.0005%-0.002% of tobacco shred weight.
Herba thymi vulgaris perfume material addition in tobacco shred is preferably the most preferred ratio of tobacco shred weight: 0.0009%.
This practicality is that the Herba thymi vulgaris perfume material using the process for purification of Herba thymi vulgaris perfume material to refine is to showing cigarette product
Distinctive style, fragrant to abundant cigarette, make flue gas fine and smooth, soft, reduce flue gas to oral cavity and the stimulation of throat, sucking of promoting or transferring Medicated cigarette
Mouthfeel, the distinctive style such as lasting is lasting, pleasant impression is comfortable have good effect.
Detailed description of the invention
Embodiment 1:
Extraction solvent propylene glycol: the weight ratio of glycerol is 30:40.
The consumption of Extraction solvent is 35:1 with Herba thymi vulgaris stem, the ratio (weight ratio) of leaf, extraction 35 naturally under normal temperature and pressure
My god, filter, remove stem, leaf slag, obtain Herba thymi vulgaris perfume material.It is applied in blank tobacco shred by best proportion 0.0009%, preserves 24
After hour, smoke panel test.Fruit shows: use the Herba thymi vulgaris perfume material that the process for purification of Herba thymi vulgaris perfume material refines to showing volume
The distinctive style of smoke product, fragrant to abundant cigarette, make flue gas fine and smooth, soft, reduce flue gas and oral cavity and the stimulation of throat, promoting or transferring are rolled up
Cigarette suck mouthfeel, the distinctive style such as lasting is lasting, pleasant impression is comfortable have good effect.
Claims (10)
1. the process for purification of a Herba thymi vulgaris perfume material, it is characterised in that described method uses propylene glycol, glycerol molten for extracting
Agent；Extraction solvent is with mass ratio range as propylene glycol: glycerol is as 10-40:20-60；The consumption of Extraction solvent and Herba thymi vulgaris stem, leaf
Weight ratio be 10-40:1；The time that Extraction solvent extracts the most naturally is 30-45 days.
The process for purification of Herba thymi vulgaris perfume material the most according to claim 1, it is characterised in that Extraction solvent is with weight ratio third
Glycol: glycerol is calculated as 20-30:40-50.
The process for purification of Herba thymi vulgaris perfume material the most according to claim 1, it is characterised in that propylene glycol: the weight of glycerol
Amount ratio is 30:40.
The process for purification of Herba thymi vulgaris perfume material the most according to claim 1, it is characterised in that in Extraction solvent consumption and hundred
Fragrant stem, leaf consumption with mass ratio range as 20-40:1.
The process for purification of Herba thymi vulgaris perfume material the most according to claim 1, it is characterised in that in Extraction solvent consumption and hundred
Fragrant stem, leaf consumption with mass ratio range as 35:1.
The process for purification of Herba thymi vulgaris perfume material the most according to claim 1, it is characterised in that Extraction solvent is at normal temperature and pressure
The time of lower extraction naturally is 30 days-40 days.
The process for purification of Herba thymi vulgaris perfume material the most according to claim 1, it is characterised in that Extraction solvent is at normal temperature and pressure
The time of lower extraction naturally is 35 days.
The process for purification of Herba thymi vulgaris perfume material the most according to claim 1, it is characterised in that Extraction solvent is with mass ratio range
For propylene glycol: glycerol is 30:40, the consumption of Extraction solvent and Herba thymi vulgaris stem, leaf weight more than for 35:1；Extraction solvent exists
Under normal temperature and pressure, natural extraction time is 35 days.
9. the Herba thymi vulgaris perfume material prepared according to the process for purification of described Herba thymi vulgaris perfume material arbitrary in claim 1-8
Application, it is characterised in that Herba thymi vulgaris perfume material addition in tobacco shred is the 0.0005%-0.002% of tobacco shred weight.
The application of the Herba thymi vulgaris perfume material that the process for purification of Herba thymi vulgaris perfume material the most according to claim 9 prepares,
It is characterized in that, Herba thymi vulgaris perfume material addition in tobacco shred is the 0.0009% of tobacco shred weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610703177.7A CN106263014A (en) | 2016-08-22 | 2016-08-22 | A kind of process for purification containing Herba thymi vulgaris perfume material and application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610703177.7A CN106263014A (en) | 2016-08-22 | 2016-08-22 | A kind of process for purification containing Herba thymi vulgaris perfume material and application |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112251290A (en) * | 2020-10-19 | 2021-01-22 | 甘肃烟草工业有限责任公司 | Thyme and benzoin composite essence for cigarettes and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105695095A (en) * | 2016-01-29 | 2016-06-22 | 广西中烟工业有限责任公司 | Refinement method and application of rosemary-containing fragrance raw material |
-
2016
- 2016-08-22 CN CN201610703177.7A patent/CN106263014A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105695095A (en) * | 2016-01-29 | 2016-06-22 | 广西中烟工业有限责任公司 | Refinement method and application of rosemary-containing fragrance raw material |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112251290A (en) * | 2020-10-19 | 2021-01-22 | 甘肃烟草工业有限责任公司 | Thyme and benzoin composite essence for cigarettes and preparation method and application thereof |
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Application publication date: 20170104 |