CN101112254A - Composite Chinese herbal medicine preparations for making cigarette and method for preparing the same - Google Patents
Composite Chinese herbal medicine preparations for making cigarette and method for preparing the same Download PDFInfo
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- CN101112254A CN101112254A CNA2007100661485A CN200710066148A CN101112254A CN 101112254 A CN101112254 A CN 101112254A CN A2007100661485 A CNA2007100661485 A CN A2007100661485A CN 200710066148 A CN200710066148 A CN 200710066148A CN 101112254 A CN101112254 A CN 101112254A
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- negundo chastetree
- chinese herbal
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 69
- 241000411851 herbal medicine Species 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 238000000034 method Methods 0.000 title claims abstract description 13
- 239000002131 composite material Substances 0.000 title 1
- 244000248021 Vitex negundo Species 0.000 claims abstract description 56
- 235000013427 Vitex negundo var incisa Nutrition 0.000 claims abstract description 56
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- 235000014956 negundo chastetree Nutrition 0.000 claims abstract description 56
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 34
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- 239000007787 solid Substances 0.000 claims description 13
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- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 2
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- XMGQYMWWDOXHJM-JTQLQIEISA-N (+)-α-limonene Chemical compound CC(=C)[C@@H]1CCC(C)=CC1 XMGQYMWWDOXHJM-JTQLQIEISA-N 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a complex Chinese herbal medicine preparation used for cigarette and a method for preparation. After the negundo chastetree leaf being cleaned and disintegrated, the alcohol with the density of 65%-75% is added to wet the negundo chastetree leaf for 10-15 hours and mixed at the mixing speed of 50-60 rotation in one minute under the temperature of 70 DEG C to 80 DEG C, then the liquid is extracted by the microwave for 25-35 minutes. After the solid-liquid separation, the extract is concentrated under the temperature of 50 DEG C to 60 DEG C under the condition of vacuum, and the negundo chastetree leaf extract is obtained. Then the negundo chastetree leaf extract, the complex fruit extract and the methyl ethylene glycol are mixed evenly according to the weight ratio of 3-5.5:1-2.5:1-2.5. When in addition, the mixture is added in the cigarette elasticizer and mixed fully and evenly, which is used as the cigarette elasticizer after being statically arranged for 30 minutes.
Description
Technical field
The present invention relates to the additive of tobacco, more particularly, the present invention relates to a kind of tobacco aromatics using with flavouring and health care.Simultaneously, the invention still further relates to the preparation method of this tobacco aromatics using.
Background technology
For cigarette product, the fragrance of cigarette and jealous be vital, perfuming cigarette is reinforced to be one of core technology of tobacco industry.By perfuming, the reinforced deficiency that can remedy on the cigarette tobacco leaf formulation, reduce assorted gas, make the cigarette perfume (or spice) of product abundanter, sufficient, and the feature that can give the product distinctness.Along with the fall evil effect of Chinese herbal medicine class additive in cigarette accepted by consumers in general day by day, existing increasing tobacco researcher is sought essence spice for cigarette from Chinese herbal medicine.
Cigarette filter perfuming technology had once been done some trials as a kind of approach of perfuming cigarette.But how will organically gather after cigarette filter perfuming technology and the optimization of Chinese herbal medicine fragrance, this is a technical barrier that urgency is to be solved in the development.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, a kind of complex Chinese herbal medicine that is used for cigarette is provided.Said preparation can increase the fragrance of cigarette, has certain health care simultaneously again.Simultaneously, the present invention also provides the preparation method of described complex Chinese herbal medicine.
Purpose of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage that is adopted among the present invention is percetage by weight.
The invention provides a kind of complex Chinese herbal medicine that is used for cigarette, said preparation adopts following method to prepare: 1. choose 1000 gram leaves of negundo chastetree through cleaning, be crushed to 30 orders, 5000～7000 milliliters of the ethanol of adding 65%～75%, soaked into 10～15 hours, under 70 ℃～80 ℃,, carry out microwave abstracting with 50～60 rev/mins mixing speed, extracted 25～35 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 50 ℃～60 ℃ following vacuum, obtain the leaf of negundo chastetree extract; 2. with leaf of negundo chastetree extract, compound fruit extract and propane diols, by 3～5.5: 1～2.5: 1～2.5 weight ratio mixes, and promptly obtains required cigarette complex Chinese herbal medicine.
The invention provides a kind of preparation method who is used for the complex Chinese herbal medicine of cigarette, this method adopts following steps:
(1) choose 1000 gram leaves of negundo chastetree through cleaning, be crushed to 30 orders, 5000～7000 milliliters of the ethanol of adding 65%～75% soaked into 10～15 hours;
(2) under 70 ℃～80 ℃, with 50～60 rev/mins mixing speed, carry out microwave abstracting, extracted 25～35 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 50 ℃～60 ℃ following vacuum, obtain the leaf of negundo chastetree extract;
(3) (annotate: compound fruit extract GFT82271 can be purchased by Germany Flavour Technology Co.Ltd (being called for short GFT) company's production and sales in the marketization with leaf of negundo chastetree extract, compound fruit extract GFT82271.) and propane diols, by 3～5.5: 1～2.5: 1～2.5 weight ratio mixes, and promptly obtains being used for the complex Chinese herbal medicine of cigarette.
Technical scheme of the present invention is to propose on the basis of following further investigation.
A. to the research of leaf of negundo chastetree performance
1. leaf of negundo chastetree is Verenaceae plant (Viter negundo L, var cannabifolia[Sieb, et Zucc.] HAND.-Mazz) leaf, English name: Hempleaf Negundo Chastetree Leaf. another name: five-leaved chaste tree bavin, five-leaved chaste tree bar, the twigs of the chaste tree, the five fingers mandarin orange.Function cures mainly: eliminate the phlegm, cough-relieving is relievingd asthma.Be used for chronic bronchitis.Nature and flavor: property is flat, mildly bitter flavor, suffering.Chemical composition: contain volatile oil, main component is australene, nopinene, sabinene, citrene, cymol, 1,8-cineole, β-cloves alkene.Vitexilactone (vitexilac-tone).Vegetatively: be born in the roadside, hillside.Be distributed in various places on the south the Changjiang river.Phytomorph: machaka or dungarunga.Sprig is square, close living canescence fine hair.Leaf is to life, and palmate 5 goes out compound leaf, and there are most sawtooth at the vanelets edge, above green, below light green, do not have hair or hairiness slightly.Give birth on coniform inflorescence top; Calyx is bell, and there are 5 fissures on the top; Corolla lavender, top have 5 slivers.The fruit sphere, black.7～November of flowering fruit bearing stage.Gather and process: gathered when summer, autumn, branches and leaves were luxuriant, dry.
2. pharmacology: 1. phlegm-dispelling functions leaf of negundo chastetree volatile oil 1.04g/kg and 1.73g/kg irritate stomach, and the phenol red method experiment of mouse shows that significant phlegm-dispelling functions is arranged.This effect is main by vagus nerve, and phlegm-dispelling functions weakens behind the cut-out vagus nerve.After giving mouse gavaging or injection Vitex negundo var cannabifolia decoction or injection Vitex negundo var cannabifolia glycosides displayed, can be discharged by lung, its phlegm-dispelling functions may be correlated with therewith.Also the someone thinks the phlegm-dispelling functions of leaf of negundo chastetree, with its minimizing sputum inner acidic mucopolysaccharide fiber with promote that its cracking is relevant.2. antitussive effect cannabifolia leaf oil 1.04g/kg irritates stomach, and ammonia spraying is drawn the mouse that coughs significant antitussive effect.Injection Vitex negundo var cannabifolia glycosides displayed can suppress the cough due to the electro photoluminescence anesthetized cat superior laryngeal nerve, shows that its antitussive effect is relevant with the inhibition coughing centre.3. the test of antiasthmatic effect cavy constant voltage histamine spray-on process shows that cannabifolia leaf oil emulsion lg/kg gavages, and can obviously prolong the histamine IV order reaction time started, and reduces histamine IV order reaction outbreak mouse number, and showing has certain antiasthmatic effect.4. hypotensive activity cannabifolia leaf oil emulsion 0.1g/kg duodenal administration, the rabbit blood pressure on average descends 31% after one hour, continues two hours.5. the cannabifolia leaf oil 0.35mL/ (kg.d) that influences to body's immunity irritates stomach, and 6d has the peritoneal macrophage of enhancing to chicken red blood cell phagocytosis trend continuously.The chronic bronchitis patient that cannabifolia leaf oil is low to macrophage phagocytic function can make the phagocytic rate of macrophage, and phagocytic index and digestible degree significantly improve, and make it the level near the normal person.6. to the regulating action Herba Viticis Cannabifoliae volatile oil of haemocyanin albumin is gone up, to β-γ-and alpha-globulin dual regulation is arranged, can promote albuminised synthesizing and the adjusting immunoglobulin (Ig).7. antibacterial action Vitex negundo var cannabifolia water decoction has significant antibacterial action external to staphylococcus aureus and bacillus anthracis.To Escherichia coli, beta streptococcus, corynebacterium diphtheriae, typhoid bacillus, Pseudomonas aeruginosa and shigella dysenteriae etc. also has certain antibacterial action.8. the LD50 of toxicity acute toxicity test leaf of negundo chastetree volatile oil mouse stomach is 7.40g/kg or 8.68g/kg; The LD50 of leaf of negundo chastetree volatile oil emulsion mouse stomach is 5.20g/kg, and lumbar injection is 0.34g/kg.
B. to the research of extracting method
1. material and reagent
Leaf of negundo chastetree (medicinal material station, Guangxi), 95% ethanol (food-grade), distilled water
2. instrument and equipment
HWC10-B microwave Dynamic Extraction equipment (day wawter bloom circle pharmaceutical equipment Science and Technology Ltd.)
The new ACS series electronic of Heng claims (the new Electronics Co., Ltd. of the Heng of Zhongshan city)
FW80 high speed Universalpulverizer (Tianjin Tai Site Instr Ltd.)
RE-52AA rotary evaporator (Shanghai Yarong Biochemical Instrument Plant)
SHT-D (III) circulation ability of swimming vavuum pump (Ying Yu of Gongyi City gives magnificent instrument plant)
3. adopt the Microwave Extraction method
Microwave abstracting is that frequency electromagnetic waves penetrates the extraction medium, arrival is extracted the inside of material, microwave energy is converted into heat energy rapidly and makes cell interior temperature fast rise, when cell interior pressure surpasses the cell membrane ability to bear, cell rupture, active ingredient freely flows out in the cell, is dissolved in the extraction medium again by further filtering and separating under lower temperature, just obtains the extraction material.Under microwave irradiation effect, be extracted the material composition and quicken, thereby make extraction rate improve several times, also reduced extraction temperature simultaneously, guarantee the quality of extraction to greatest extent to the extractant interfacial diffusion.Microwave abstracting is to penetrate microwave moment the material inside and outside to heat simultaneously and extract.Traditional hot extraction phase ratio, the major advantage of microwave abstracting is: 1. quality height, can protect the functional component in food, medicine and other chemical materials effectively; 2. purity height, extraction yield height; 3. extract had high selectivity.4. solvent load is few, and heat time heating time is short.No matter be that rate of extraction, extraction efficiency or extraction quality microwave-assisted extraction technique have been compared remarkable advantages with the abstraction technique that has other now.Different extraction conditions and recovery rate comparing result are as follows:
| Concentration of alcohol | Extraction time (min) | |||
| 5 | 10 | 30 | 60 | |
| 60％ | 14.8％ | 15.7％ | 22.1％ | 23.5％ |
| 70％ | 16.3％ | 18.5％ | 2 3.6％ | 24.4％ |
| 80％ | 15.6％ | 17.9％ | 21.2％ | 22.5％ |
C. add test
Sample 1.
| Raw material | The place of production | Consumption (weight portion) | Remarks |
| The leaf of negundo chastetree extract | Self-control | 60 | |
| Compound fruit extract (GFT82271) | Germany | 20 | |
| Propane diols | Tao Shi | 20 |
Sample 2.
| Raw material | The place of production | Consumption | Remarks |
| The leaf of negundo chastetree extract | Self-control | 55 | |
| Compound fruit extract (GFT82271) | Germany | 25 | |
| Propane diols | Tao Shi | 20 |
Sample 3.
| Raw material | The place of production | Consumption | Remarks |
| The leaf of negundo chastetree extract | Self-control | 50 | |
| Compound fruit extract (GFT82271) | Germany | 25 | |
| Propane diols | Tao Shi | 25 |
Additive effect
| The pipe tobacco type | Sample | Gloss | Fragrance | Coordinate | Assorted gas | Stimulate | Pleasant impression | Add up to |
| 5 | 32 | 6 | 12 | 20 | 25 | 100 | ||
| Fire-cured tobacco type | To in the same old way | 5 | 29.5 | 5 | 10.5 | 17.5 | 22 | 89.5 |
| Sample 1 | 5 | 30.5 | 5.5 | 10.5 | 17.5 | 22.5 | 91.5 | |
| Sample 2 | 5 5 | 30.0 30.0 | 5.5 5 | 10.5 10.5 | 17.5 17.5 | 22 22 | 90.5 90.0 | |
| Sample 3 |
Result of the test shows, sample 1 is fine with tobacco harmony, and suitably consumption is very little to the interference of cigarette, keeping eliminating the phlegm of Vitex negundo var cannabifolia, cough-relieving, and the effect of grade of relievining asthma can improve jealous simultaneously, the sense of minimizing flue gas drying, and addition is 0.5%～5%, effect is ideal comparatively.
Compared with prior art, the present invention has following beneficial effect:
1. the present invention as the cigarette natural perfume material, not only has elegant special Chinese herbal medicine fragrance with the Vitex negundo var cannabifolia extract, can also make cigarette fragrance more coordinate, fragrant, pure and mild, fine and smooth, pleasant impression also is significantly improved.Clinical testing shows that the cigarette that has added Vitex negundo var cannabifolia has the effect that significantly slows down stimulation, has relaxed smoking and healthy contradiction preferably, plays the effect of protection health of smokers.Therefore, the Vitex negundo var cannabifolia essential oil is applied to the tobacco field and can plays the double action that strengthens cigarette quality and health care.
2. the preparation of the present invention's preparation both can be used in the middle of the cigarette shreds, also can put on cigarette filter tip rod simultaneously, had the comparatively broad scope of application.
3. leaf of negundo chastetree active ingredient is carried out Microwave Extraction, and add test on the mouth rod, effective ingredient is brought the oral cavity into by flue gas, owing to avoided the destruction of burning to drug ingedient, drug ingedient can be effectively, play a role fully.Effects such as mouth rod additive has the eliminating the phlegm of medicine, cough-relieving, relievings asthma, antibiotic improve jealous simultaneously in addition, reduce the effect of the dry grade of flue gas.
4. improve Chinese herbal medicine spices and be added on the defective that causes composition to destroy through burning in the pipe tobacco.When improving the smoking property of cigarette quality, the part active ingredient of Chinese herbal medicine can directly suck the harm that has to a certain degree alleviated smoking property of cigarette with main flume.
The specific embodiment
By preparation given below or interpolation embodiment, can further be well understood to the present invention.But they are not the qualification to protection domain of the present invention.
The embodiment that is used for cigarette filter:
Embodiment 1
Choose the 1000g leaf of negundo chastetree through cleaning and be crushed to 30 orders, 7000 milliliters of the ethanol of adding 65% soaked into 15 hours; Under 70 ℃, with 60 rev/mins mixing speed, carry out microwave abstracting, extracted 25 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 60 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; Leaf of negundo chastetree extract, compound fruit extract and the propane diols weight ratio by 3: 1: 1 is mixed, promptly obtain being used for the complex Chinese herbal medicine of cigarette filter.
Embodiment 2
Repeat embodiment 1, following difference is arranged: in the leaf of negundo chastetree of pulverizing, add 70%6000 milliliters, soaked into 12 hours; Under 75 ℃, with 55 rev/mins mixing speed, carry out microwave abstracting, extracted 30 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 55 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; With leaf of negundo chastetree extract, compound fruit extract and propane diols, mix by 5.5: 2.5: 2.0 weight ratios, promptly obtain being used for the complex Chinese herbal medicine of cigarette filter.
Embodiment 3
Repeat embodiment 1, following difference is arranged: 5000 milliliters of the ethanol of adding 75% in the leaf of negundo chastetree of pulverizing, soaked into 10 hours; Under 80 ℃, with 50 rev/mins mixing speed, carry out microwave abstracting, extracted 25～35 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 50 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; Leaf of negundo chastetree extract, compound fruit extract and PG are mixed by 5.5: 2.5: 2.5 weight ratio, promptly obtain being used for the complex Chinese herbal medicine of cigarette filter.
Embodiment 4
With the complex Chinese herbal medicine of sample 1, by 1: 200 weight ratio, add in the cigarette plasticizer, stir, leave standstill 30 minutes after, be re-used as the cigarette plasticizer and use, roll out cigarette filter tip rod.Use this filter rod to roll into cigarette.
Embodiment 5
With the complex Chinese herbal medicine of sample 1, by 1: 160 weight ratio, add in the cigarette plasticizer, stir, leave standstill 30 minutes after, be re-used as the cigarette plasticizer and use, roll out cigarette filter tip rod.Use this filter rod to roll into cigarette.
Embodiment 6
With the complex Chinese herbal medicine of sample, by 1: 120 weight ratio, add in the cigarette plasticizer, stir, leave standstill 30 minutes after, be re-used as the cigarette plasticizer and use, roll out cigarette filter tip rod.Use this filter rod to roll into cigarette.
Embodiment 7
With sample 1 described complex Chinese herbal medicine, by 1: 40 weight ratio, add in the cigarette plasticizer, stir, leave standstill 30 minutes after, be re-used as the cigarette plasticizer and use, roll out cigarette filter tip rod.Use this filter rod to roll into cigarette.
Embodiment 8
With the complex Chinese herbal medicine of sample 1, by 1: 20 weight ratio, add in the cigarette plasticizer, stir, leave standstill 30 minutes after, be re-used as the cigarette plasticizer and use, roll out cigarette filter tip rod.Use this filter rod to roll into cigarette.
Embodiment 9
With the complex Chinese herbal medicine of sample 1, by 1: 10 weight ratio, add in the cigarette plasticizer, stir, leave standstill 30 minutes after, be re-used as the cigarette plasticizer and use, roll out cigarette filter tip rod.Use this filter rod to roll into cigarette.
* complex Chinese herbal medicine provided by the invention also can add in the pipe tobacco of cigarette.
Embodiment 10
Choose the 1000g leaf of negundo chastetree through cleaning and be crushed to 30 orders, 7000 milliliters of the ethanol of adding 65% soaked into 15 hours; Under 70 ℃, with 60 rev/mins mixing speed, carry out microwave abstracting, extracted 25 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 60 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; Leaf of negundo chastetree extract, compound fruit extract and the propane diols weight ratio by 3: 1: 1 is mixed, get and mix back preparation 5g, the alcohol with 95% is diluted to 45 and restrains, with it spray into 50 kilograms tobacco shred in, roll into cigarette.
Embodiment 11
Choose the 1000g leaf of negundo chastetree through cleaning and be crushed to 30 orders, 7000 milliliters of the ethanol of adding 65% soaked into 15 hours; Under 70 ℃, with 60 rev/mins mixing speed, carry out microwave abstracting, extracted 25 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 60 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; Leaf of negundo chastetree extract, compound fruit extract and the propane diols weight ratio by 3: 1: 1 is mixed, get and mix back preparation 8g, the alcohol with 95% is diluted to 45 and restrains, with it spray into 50 kilograms tobacco shred in, roll into cigarette.
Embodiment 12
Choose the 1000g leaf of negundo chastetree through cleaning and be crushed to 30 orders, 7000 milliliters of the ethanol of adding 65% soaked into 15 hours; Under 70 ℃, with 60 rev/mins mixing speed, carry out microwave abstracting, extracted 25 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 60 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; Leaf of negundo chastetree extract, compound fruit extract and the propane diols weight ratio by 3: 1: 1 is mixed, get and mix back preparation 5g, the alcohol with 95% is diluted to 60 and restrains, with it spray into 50 kilograms tobacco shred in, roll into cigarette.
Embodiment 13
Choose the 1000g leaf of negundo chastetree through cleaning and be crushed to 30 orders, 7000 milliliters of the ethanol of adding 65% soaked into 15 hours; Under 70 ℃, with 60 rev/mins mixing speed, carry out microwave abstracting, extracted 25 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 60 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; Leaf of negundo chastetree extract, compound fruit extract and the propane diols weight ratio by 3: 1: 1 is mixed, get and mix back preparation 8g, the alcohol with 95% is diluted to 60 and restrains, with it spray into 50 kilograms tobacco shred in, roll into cigarette.
Embodiment 14
Choose the 1000g leaf of negundo chastetree through cleaning and be crushed to 30 orders, 7000 milliliters of the ethanol of adding 65% soaked into 15 hours; Under 70 ℃, with 60 rev/mins mixing speed, carry out microwave abstracting, extracted 25 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 60 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; Leaf of negundo chastetree extract, compound fruit extract and the propane diols weight ratio by 3: 1: 1 is mixed, get and mix back preparation 10g, the alcohol with 95% is diluted to 45 and restrains, with it spray into 50 kilograms tobacco shred in, roll into cigarette.
Embodiment 15
Choose the 1000g leaf of negundo chastetree through cleaning and be crushed to 30 orders, 7000 milliliters of the ethanol of adding 65% soaked into 15 hours; Under 70 ℃, with 60 rev/mins mixing speed, carry out microwave abstracting, extracted 25 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 60 ℃ of following vacuum, obtain the leaf of negundo chastetree extract; Leaf of negundo chastetree extract, compound fruit extract and the propane diols weight ratio by 3: 1: 1 is mixed, get and mix back preparation 10g, the alcohol with 95% is diluted to 60 and restrains, with it spray into 50 kilograms tobacco shred in, roll into cigarette.
Claims (3)
1. complex Chinese herbal medicine that is used for cigarette, it is characterized in that: this spices adopts following method to prepare: 1. choose 1000 gram leaves of negundo chastetree through cleaning and be crushed to 30 orders, 5000～7000 milliliters of the ethanol of adding 65%～75% soaked into 10～15 hours, under 70 ℃～80 ℃, mixing speed with 50～60 rev/mins, carry out microwave abstracting, extracted 25～35 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 50 ℃～60 ℃ following vacuum, obtain the leaf of negundo chastetree extract; 2. with leaf of negundo chastetree extract, compound fruit extract and propane diols, by 3～5.5: 1～2.5: 1～2.5 weight ratio mixes, and promptly obtains being used for the complex Chinese herbal medicine of cigarette.
2. complex Chinese herbal medicine according to claim 1 is characterized in that: leaf of negundo chastetree extract, compound fruit extract and the propane diols weight ratio by 3: 1: 1 is mixed.
3. preparation method who is used for the complex Chinese herbal medicine of cigarette, it is characterized in that: this method adopts following step:
(1) choose 1000 gram leaves of negundo chastetree through cleaning and be crushed to 30 orders, 5000～7000 milliliters of the ethanol of adding 65%～75% soaked into 10～15 hours;
(2) under 70 ℃～80 ℃, with 50～60 rev/mins mixing speed, carry out microwave abstracting, extracted 25～35 minutes, after the Separation of Solid and Liquid, again extract is concentrated in 50 ℃～60 ℃ following vacuum, obtain the leaf of negundo chastetree extract;
(3) with leaf of negundo chastetree extract, compound fruit extract and propane diols, by 3～5.5: 1～2.5: 1～2.5 weight ratio mixes, and promptly obtains being used for the complex Chinese herbal medicine of cigarette.
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| CNA2007100661485A CN101112254A (en) | 2007-08-30 | 2007-08-30 | Composite Chinese herbal medicine preparations for making cigarette and method for preparing the same |
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| CNA2007100661485A CN101112254A (en) | 2007-08-30 | 2007-08-30 | Composite Chinese herbal medicine preparations for making cigarette and method for preparing the same |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101928640A (en) * | 2010-09-16 | 2010-12-29 | 无锡华海香料有限公司 | Method for extracting natural perfume and application of extract |
| CN102058731A (en) * | 2010-12-31 | 2011-05-18 | 杨志勇 | Preparation of chaste tree twig leaf and fruit extract and anti-inflammatory medical application thereof |
| CN101514302B (en) * | 2008-02-20 | 2012-02-29 | 湖北中烟工业有限责任公司 | Method for comprehensively utilizing peanut shell |
| CN103087826A (en) * | 2011-11-08 | 2013-05-08 | 江西中烟工业有限责任公司 | Blueberry extract and preparation method thereof and application in cigarette |
| CN104207326A (en) * | 2013-05-29 | 2014-12-17 | 王天华 | Application of raspberry extract in cigarette |
| CN104207325A (en) * | 2013-05-29 | 2014-12-17 | 王天华 | Application of blackberry extractives in cigarettes |
| CN108041670A (en) * | 2017-12-15 | 2018-05-18 | 江西中烟工业有限责任公司 | A kind of smoke changes pastil |
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- 2007-08-30 CN CNA2007100661485A patent/CN101112254A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101514302B (en) * | 2008-02-20 | 2012-02-29 | 湖北中烟工业有限责任公司 | Method for comprehensively utilizing peanut shell |
| CN101928640A (en) * | 2010-09-16 | 2010-12-29 | 无锡华海香料有限公司 | Method for extracting natural perfume and application of extract |
| CN102058731A (en) * | 2010-12-31 | 2011-05-18 | 杨志勇 | Preparation of chaste tree twig leaf and fruit extract and anti-inflammatory medical application thereof |
| CN103087826A (en) * | 2011-11-08 | 2013-05-08 | 江西中烟工业有限责任公司 | Blueberry extract and preparation method thereof and application in cigarette |
| CN104207326A (en) * | 2013-05-29 | 2014-12-17 | 王天华 | Application of raspberry extract in cigarette |
| CN104207325A (en) * | 2013-05-29 | 2014-12-17 | 王天华 | Application of blackberry extractives in cigarettes |
| CN108041670A (en) * | 2017-12-15 | 2018-05-18 | 江西中烟工业有限责任公司 | A kind of smoke changes pastil |
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