CN107746748A - A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette - Google Patents
A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette Download PDFInfo
- Publication number
- CN107746748A CN107746748A CN201711089877.2A CN201711089877A CN107746748A CN 107746748 A CN107746748 A CN 107746748A CN 201711089877 A CN201711089877 A CN 201711089877A CN 107746748 A CN107746748 A CN 107746748A
- Authority
- CN
- China
- Prior art keywords
- powder
- ultramicro
- cigarette
- parts
- cassia bark
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 71
- 235000009508 confectionery Nutrition 0.000 title claims abstract description 43
- 230000033764 rhythmic process Effects 0.000 title claims abstract description 43
- 239000000654 additive Substances 0.000 title claims abstract description 31
- 230000000996 additive effect Effects 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000843 powder Substances 0.000 claims abstract description 156
- 244000037364 Cinnamomum aromaticum Species 0.000 claims abstract description 52
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 claims abstract description 52
- 239000002245 particle Substances 0.000 claims abstract description 43
- 238000000227 grinding Methods 0.000 claims abstract description 38
- 239000002994 raw material Substances 0.000 claims abstract description 37
- 235000007129 Cuminum cyminum Nutrition 0.000 claims abstract description 30
- 241000628997 Flos Species 0.000 claims abstract description 30
- 244000290333 Vanilla fragrans Species 0.000 claims abstract description 30
- 235000009499 Vanilla fragrans Nutrition 0.000 claims abstract description 30
- 235000012036 Vanilla tahitensis Nutrition 0.000 claims abstract description 30
- 244000046052 Phaseolus vulgaris Species 0.000 claims abstract description 29
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims abstract description 29
- 239000007788 liquid Substances 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 16
- 239000003292 glue Substances 0.000 claims abstract description 12
- 238000009777 vacuum freeze-drying Methods 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims abstract description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 50
- 241000510672 Cuminum Species 0.000 claims description 27
- 229910052757 nitrogen Inorganic materials 0.000 claims description 25
- 239000000463 material Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 235000012054 meals Nutrition 0.000 claims description 6
- 238000007873 sieving Methods 0.000 claims description 2
- 230000001681 protective effect Effects 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 9
- 230000035943 smell Effects 0.000 abstract description 8
- 230000008569 process Effects 0.000 abstract description 7
- 230000008901 benefit Effects 0.000 abstract description 4
- 244000304337 Cuminum cyminum Species 0.000 abstract description 3
- 238000013329 compounding Methods 0.000 abstract 1
- 235000013599 spices Nutrition 0.000 description 20
- 238000000605 extraction Methods 0.000 description 15
- 238000005516 engineering process Methods 0.000 description 14
- 235000013312 flour Nutrition 0.000 description 13
- 238000002474 experimental method Methods 0.000 description 9
- 239000002304 perfume Substances 0.000 description 9
- 235000013339 cereals Nutrition 0.000 description 8
- 238000011156 evaluation Methods 0.000 description 7
- 244000223014 Syzygium aromaticum Species 0.000 description 6
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000000796 flavoring agent Substances 0.000 description 6
- 235000019634 flavors Nutrition 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 235000019082 Osmanthus Nutrition 0.000 description 5
- 241000333181 Osmanthus Species 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 230000008859 change Effects 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 4
- 230000009467 reduction Effects 0.000 description 4
- 230000001953 sensory effect Effects 0.000 description 4
- 244000061176 Nicotiana tabacum Species 0.000 description 3
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 3
- 238000004891 communication Methods 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 230000000391 smoking effect Effects 0.000 description 3
- 241000522254 Cassia Species 0.000 description 2
- 241001062472 Stokellia anisodon Species 0.000 description 2
- 239000012496 blank sample Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 235000011194 food seasoning agent Nutrition 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 239000003595 mist Substances 0.000 description 2
- 210000000214 mouth Anatomy 0.000 description 2
- 238000010951 particle size reduction Methods 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 238000001303 quality assessment method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000723347 Cinnamomum Species 0.000 description 1
- 244000167125 Cinnamomum japonicum Species 0.000 description 1
- 235000002428 Cinnamomum japonicum Nutrition 0.000 description 1
- 241001503987 Clematis vitalba Species 0.000 description 1
- 241000006479 Cyme Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241000266331 Eugenia Species 0.000 description 1
- 240000006927 Foeniculum vulgare Species 0.000 description 1
- 235000004204 Foeniculum vulgare Nutrition 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- 241000218195 Lauraceae Species 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- 235000017803 cinnamon Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- HDERJYVLTPVNRI-UHFFFAOYSA-N ethene;ethenyl acetate Chemical group C=C.CC(=O)OC=C HDERJYVLTPVNRI-UHFFFAOYSA-N 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 235000015243 ice cream Nutrition 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid group Chemical group C(CCCCCCC\C=C/CCCCCCCC)(=O)O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000000284 resting effect Effects 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 235000019590 thick flavour Nutrition 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Toxicology (AREA)
- General Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette.The pungent fragrant and sweet rhythm cigarette additive is made up of flos caryophylli, cassia bark, vanilla beans, cumin, four kinds of raw materials are entered into coarse crushing of passing through, vacuum freeze drying, air-flow ultramicro grinding respectively, then the Ultramicro-powder of obtain four kinds of raw materials is subjected to compounding realization according to weight than 15 parts of 3 10 parts of flos caryophylli Ultramicro-powder, 27 parts of cassia bark Ultramicro-powder, 15 parts of vanilla beans Ultramicro-powder, cumin Ultramicro-powder compositions, its application process in cigarette is put in Cigarette to be well mixed with cigarette overlapping glue.The invention has the advantages that have the pungent fragrant and sweet rhythm of pleasant compared with the cigarette product using traditional liquid essence using cigarette product produced by the invention, and the characteristics of fragrance is natural, strong, particle is uniformly dispersed, and cigarette smells fragrant uniformity.
Description
Technical field
The present invention relates to tobacco additive agent field, particularly a kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and
Application in cigarette.
Background technology
Cloves is also known as clove tree, Myrtaceae Eugenia, is aiphyllium.Cloves is machaka or dungarunga.It is small
The nearly cylinder of branch or the prismatic of band four, have hole skin.Flower both sexes, cyme are arranged in panicle, basidixed or side life, with leaf simultaneously
Pumping after pumping or leaf；Has bennet or without bennet.Cloves described in this patent is flos caryophylli.
Cassia bark, scientific name bavin osmanthus, also known as Chinese cassia tree, official osmanthus or fragrant osmanthus, it is Lauraceae, cinnamon cinnamomum japonicum, burmannii, spire perfume
The common name of the barks such as osmanthus, Chinese cassia tree or river osmanthus, it is one of spices used earliest by the mankind.
Vanilla is climber liana, shallow rooted plant, and stem is plump, often saves raw a piece of leaf and an aerial root.Fruit is meat
Matter pod shape, often referred to as beanpod.Match somebody with somebody perfume material mainly for the manufacture of food such as ice cream, chocolate, ligueurs；Also it can use
In on cosmetic industry, tobacco, fermentation and ornament industry.
Cumin also known as fennel of resting in peace, the long 4.5-6 millimeters of cumin seed, wide 1-1.5 millimeters are High oleic, containing strong perfume (or spice)
Taste, crust is in dark green or yellow green.It is mainly used in seasoning, extracts spices etc., be burning, roasting product must first-class seasoning, mouth
Feel flavor it is extremely unique, rich in oiliness, fragrant odour and it is strong.
Superfine communication technique, refer to utilize various special disintegrating apparatus, by certain processing process, to material
Milled, impacted, sheared, so as to which more than 3mm material particles to be crushed to 5-15 μm of subparticle.As a kind of high
New technology processing method, although ultramicro grinding comes out soon, have been widely used for food, health products, medicine and other fields.By
Develop in particle to miniaturization direction, cause material table area and porosity to increase considerably, therefore ultrafine powder has uniqueness
Physicochemical property, such as good dissolubility, dispersiveness, adsorptivity.Can be by spice in low temperature using superfine communication technique
State lower moment is broken into uniform particle sizes, the ultramicro powder of good fluidity, and raw material flavor components lose less, product thick flavor
It is strongly fragrant, pure, and belong to pure physical technique processing, the pure natural attribute of product can be ensured.
Due to can not possibly extract the flavor component in raw material completely during extraction, and temperature-sensitive in purification process be present
Property fragrance matter loss etc. factor, compared with the liquid perfume after extraction, Ultramicro-powder spices is made up of raw material micro mist, flavor
In matter is integrally incorporated in, and protection of liquid nitrogen technology is used, raw material is in low-temperature condition all the time in crushing process, avoid heat
The loss of quick property fragrance matter, so Ultramicro-powder spices has obvious advantage at fragrance nature, strong pure aspect.
Domestic cigarette industry is more to be used using VAE emulsions (vinyl acetate-ethylene copolymerization emulsions) as overlapping glue.VAE is except tool
Standby good caking property, film forming, also with extensive intermiscibility.For example VAE emulsions can be with most of pigment and filler
It is used in mixed way, moreover it is possible to lower-molecular substance, macromolecular water-soluble polymer and other high scores such as many ketone, aldehyde, alcohol, organic acid
Sub- emulsion mixing.Ensure that overlapping glue good flowing properties, cementability are strong and rate of drying it is fast under conditions of, can suitably increase
The concentration of essence or spices in glue system, online application of the characteristic chicken flavor overlapping glue in cigarette high-speed production is realized, is assigned
The obvious feature of cigarette is given to smell fragrant breeze lattice.
In the case where smoking and health problem increasingly cause the situation of extensive concern, natural essence spices has turned into Chinese-style cigarette and increased
One important directions of fragrant humectation research.The application field of solid spice is concentrated mainly on food, daily use chemicals industry, and it is in cigarette system
Application study in product is less.
The content of the invention
To above-mentioned the deficiencies in the prior art, the present invention provide a kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and
Application in cigarette, it is obvious to solve the existing miscellaneous gas of traditional liquid essence, and the shortcomings of fragrance deficiency, the cigarette in the present invention adds
The characteristics of agent has the pungent fragrant and sweet rhythm of pleasant, and fragrance is natural, strong, particle is uniformly dispersed, and cigarette smells fragrant uniformity
Spices, improve its availability in cigarette tobacco leaf formulation.
Technical scheme provided by the invention：The pungent fragrant and sweet rhythm additive of a kind of cigarette, it is characterised in that be by following heavy
Measure the material composition of number：Flos caryophylli Ultramicro-powder 3-10 parts, cassia bark Ultramicro-powder 2-7 parts, vanilla beans Ultramicro-powder 1-5 parts, cumin
Ultramicro-powder 1-5 parts；
The flos caryophylli Ultramicro-powder, cassia bark Ultramicro-powder, vanilla beans Ultramicro-powder, cumin Ultramicro-powder are by above-mentioned raw materials respectively
After coarse powder carries out air-flow ultramicro grinding under the conditions of charging rate 0.1-1g/s, stream pressure 0.1-1Mpa and liquid nitrogen auxiliary protection
Obtain the ultra-micro powder of 1-20 μm of particle diameter.
The technical scheme of the present invention preferably：The pungent fragrant and sweet rhythm of a kind of cigarette is by the thing of following parts by weight with additive
Matter forms：8 parts of flos caryophylli Ultramicro-powder, 57 parts of cassia bark Ultramicro-powder, 2 parts of vanilla beans Ultramicro-powder, 1 part of cumin Ultramicro-powder.
The technical scheme of the present invention preferably：The particle diameter of the flos caryophylli Ultramicro-powder is 9 μm, and the particle diameter of cassia bark Ultramicro-powder is
8 μm, the particle diameter of vanilla beans Ultramicro-powder is 10 μm, and the particle diameter of cumin Ultramicro-powder is 10 μm.
The preparation method of a kind of pungent fragrant and sweet rhythm additive provided by the invention, it is characterised in that comprise the following steps that：
(1) using flos caryophylli, cassia bark, vanilla beans, cumin as raw material, raw material is first distinguished into attrition grinding, obtained raw material
Coarse grain sieves；
(2) by the raw material coarse grain after sieving in step (1) again respectively through -40 DEG C~-80 DEG C vacuum freeze dryings to aqueous
Amount is less than 5%, obtains raw material meal, i.e. flos caryophylli coarse powder, cassia bark coarse powder, vanilla beans coarse powder and cumin coarse powder；
(3) by step (2) dried raw material meal again respectively in charging rate 0.1-1g/s, stream pressure 0.1-1Mpa
With air-flow ultramicro grinding is carried out under the conditions of liquid nitrogen auxiliary protection 1-2 times to 1-20 μm of particle diameter, obtain flos caryophylli Ultramicro-powder, cassia bark surpasses
Micro mist, vanilla beans Ultramicro-powder and cumin Ultramicro-powder；
(4) the raw material Ultramicro-powder obtained by step (3) is mixed according to following ratio of weight and number：Flos caryophylli Ultramicro-powder
3-10 parts, cassia bark Ultramicro-powder 2-7 parts, vanilla beans Ultramicro-powder 1-5 parts, cumin Ultramicro-powder 1-5 parts are well mixed, that is, obtain pungent
Fragrant and sweet rhythm Ultramicro-powder；
The technical scheme of the present invention preferably：Flos caryophylli coarse powder carries out the condition of air-flow ultramicro grinding in the step (3)
For：Air-flow crushing is carried out under the conditions of charging rate 0.3g/s, stream pressure 0.4Mpa and liquid nitrogen auxiliary protection, crushes number 1
It is secondary；
The technical scheme of the present invention preferably：The condition of cassia bark coarse powder progress air-flow ultramicro grinding is in the step (3)：
Air-flow crushing is carried out under the conditions of charging rate 0.5g/s, stream pressure 0.4Mpa and liquid nitrogen auxiliary protection, crushes number 1 time；
The condition of vanilla beans coarse powder progress air-flow ultramicro grinding is in the step (3)：In charging rate 0.4g/s, gas
Air-flow crushing is carried out under the conditions of flowing pressure 0.6Mpa and liquid nitrogen auxiliary protection, crushes number 2 times；
The condition of cumin coarse powder progress air-flow ultramicro grinding is in the step (3)：In charging rate 0.5g/s, air-flow pressure
Air-flow crushing is carried out under the conditions of power 0.5Mpa and liquid nitrogen auxiliary protection, crushes number 1 time；
A kind of application of the pungent fragrant and sweet rhythm cigarette additive provided by the invention in cigarette, it is characterised in that：It will be prepared into
To the pungent fragrant and sweet super additive of rhythm compare 1-5 according to weight:100 ratio is added in cigarette overlapping glue, and mixes equal
Upper machine is put in Cigarette after even.
The technical scheme of the present invention preferably：The weight ratio of the pungent fragrant and sweet rhythm cigarette additive and cigarette overlapping glue is
1.5:100。
Flos caryophylli, cassia bark, vanilla beans in the present invention, cumin raw material are commercially available.
Beneficial effects of the present invention：
(1) the characteristic spices of the invention prepared using superfine communication technique has particle fine and even, dispersed preferable, suction
The characteristics of attached property is good, while the pure comfortable and natural true to nature of raw material flavor can be kept well；Natural perfume material Ultramicro-powder
Body can reach the particle degree of submicron order, have unrivaled advantage in terms of the fine degree of processing powder perfume, together
When can enrich perfume quantity, coordinate with cigarette perfume, the soft exquisiteness of flue gas, mitigate oral cavity residual, reducing stimulates, and covers miscellaneous gas, and fragrant
Taste lasting lasting stability；
(2) present invention first crushes, then be freeze-dried, last liquid nitrogen using flos caryophylli, cassia bark, vanilla beans, cumin as raw material
Secondary air ultra micro smashing prepares Ultramicro-powder, then compounds to obtain and have pungent fragrant and sweet rhythm Ultramicro-powder, is freeze-dried under low temperature, low pressure
Carry out, relative to other drying modes, save the color of raw material in itself to greatest extent；
(3) present invention is compounded by different natural perfume materials in 4, is formed the spices with unique pungent fragrant and sweet rhythm, is used this
The cigarette product of invention production has the pungent fragrant and sweet rhythm of pleasant compared with the cigarette product using traditional liquid essence, and fragrance is certainly
So, the characteristics of strong, particle are uniformly dispersed, and cigarette smells fragrant uniformity.
Brief description of the drawings
Fig. 1 is influence of the raw material granularity to cassia bark Ultramicro-powder particle diameter and flour extraction；
Fig. 2 is influence of the charging rate to cassia bark Ultramicro-powder particle diameter and flour extraction；
Fig. 3 is influence of the stream pressure to cassia bark Ultramicro-powder particle diameter and flour extraction；
Fig. 4 is influence of the different crushing numbers to cassia bark Ultramicro-powder particle diameter and flour extraction.
Embodiment
With reference to specific embodiment, the present invention is described further.
Stock preparation process in following examples is as follows：
The preparation of flos caryophylli Ultramicro-powder：By flos caryophylli attrition grinding, 150 μm of sieves are crossed, obtain cloves coarse grain, then through -40 DEG C
~-80 DEG C of vacuum freeze dryings to water content is less than 5%, flos caryophylli coarse powder is obtained, in charging rate 0.3g/s, stream pressure
Air-flow ultramicro grinding is carried out under the conditions of 0.4Mpa and liquid nitrogen auxiliary protection, crushes number 1 time, 9 μm of flos caryophylli ultra micros of collection cut size
Powder；
By cassia bark attrition grinding, cassia bark coarse grain crosses 180 μm of sieves, small to water content through -40 DEG C~-80 DEG C vacuum freeze dryings
In 5%, cassia bark coarse powder is obtained, is entered using under the conditions of charging rate 0.5g/s, stream pressure 0.4Mpa and liquid nitrogen auxiliary protection
Promoting the circulation of qi stream ultramicro grinding, crushes number 1 time, 8 μm of cassia bark Ultramicro-powders of collection cut size；
By vanilla bean powder breakdown mill, vanilla beans coarse grain crosses 180 μm of sieves, through -40 DEG C~-80 DEG C vacuum freeze dryings
It is less than 5% to water content, obtains vanilla beans coarse powder, aids in protecting in charging rate 0.4g/s, stream pressure 0.6Mpa and liquid nitrogen
Air-flow ultramicro grinding is carried out under the conditions of shield, crushes number 2 times, 10 μm of vanilla beans Ultramicro-powders of collection cut size；
By cumin attrition grinding, cloves coarse grain crosses 180 μm of sieves, small to water content through -40 DEG C~-80 DEG C vacuum freeze dryings
In 5%, cumin coarse powder is obtained, air-flow is carried out under the conditions of charging rate 0.5g/s, stream pressure 0.5Mpa and liquid nitrogen auxiliary protection
Ultramicro grinding, crushes number 1 time, 10 μm of cumin Ultramicro-powders of collection cut size.
Embodiment one, a kind of pungent fragrant and sweet rhythm cigarette additive are the raw material Ultramicro-powders that will be prepared by the above method, according to
Weight is more well mixed than 8 parts of flos caryophylli Ultramicro-powder, 5 parts of cassia bark Ultramicro-powder, 2 parts of vanilla beans Ultramicro-powder, 1 part of cumin Ultramicro-powder,
Produce pungent fragrant and sweet rhythm cigarette additive.
Again by the pungent fragrant and sweet rhythm cigarette additive compounded in embodiment 1 and existing cigarette overlapping glue by weight 1.5:
100 ratio is mixed and stirred evenly, and upper machine puts on Cigarette afterwards.
Embodiment two, the pungent fragrant and sweet rhythm cigarette additive of one kind, the raw material Ultramicro-powder that will be prepared by the above method, press
It is more equal than 2 parts of 5 parts of flos caryophylli Ultramicro-powder, 5 parts of cassia bark Ultramicro-powder, 3 parts of vanilla beans Ultramicro-powder, cumin Ultramicro-powder mixing according to weight
It is even, produce pungent fragrant and sweet rhythm cigarette additive.
By the pungent fragrant and sweet rhythm cigarette additive compounded in embodiment two and current cigarette overlapping glue by weight 2:100
Ratio is mixed and stirred evenly, and upper machine puts on Cigarette afterwards.
Embodiment three, the pungent fragrant and sweet rhythm cigarette additive of one kind, the raw material Ultramicro-powder that will be prepared by the above method, press
It is more equal than 1 part of 4 parts of flos caryophylli Ultramicro-powder, 6 parts of cassia bark Ultramicro-powder, 3 parts of vanilla beans Ultramicro-powder, cumin Ultramicro-powder mixing according to weight
It is even, produce pungent fragrant and sweet rhythm cigarette additive.
By the pungent fragrant and sweet rhythm Ultramicro-powder compounded in embodiment three and cigarette overlapping glue by weight 1:100 ratio is mixed
Merging stirs evenly, and upper machine puts on Cigarette afterwards.
Do not make using the pungent fragrant and sweet rhythm Ultramicro-powder of above-mentioned technology ultramicro grinding and the cigarette product that rolls as stated above and
Fragrant evaluation, which is smelt, with the cigarette of the pungent fragrant and sweet rhythm Ultramicro-powder is shown in Table 1-4.
The cigarette of the embodiment one of table 1 smells fragrant evaluation result
The cigarette of the embodiment two of table 2 smells fragrant evaluation result
The cigarette of the embodiment three of table 3 smells fragrant evaluation result
The cigarette of the blank sample of table 4 smells fragrant evaluation result
It can be seen that what is rolled using pungent fragrant and sweet rhythm Ultramicro-powder involved in the present invention by the contrast of table 1-3 and table 4
Cigarette, fragrant protrusion, and uniformity are smelt, the pungent fragrant and sweet rhythm with pleasant, and the characteristics of fragrance is natural, strong.
The cigarette of preparation in above three embodiment and blank cigarette are subjected to its sensory evaluating smoking, its sensory evaluating smoking's mass
It is shown in Table 5.
The sensory quality assessment of the cigarette product of table 5
As can be seen that using preparation and the application side of pungent fragrant and sweet rhythm Ultramicro-powder involved in the present invention from above-mentioned evaluation table
Its overall sensory quality assessment of the cigarette that method is rolled is above blank sample.
Example IV：Present inventor has carried out following for the selection of raw material meal progress Ultramicro-powder disintegrating process
Experiment, specifically using cassia bark as research object, weigh and crush dried cassia bark coarse powder 200g progress ultramicro grinding, and as base
Standard calculates flour extraction.Using flour extraction and granularity as evaluation index, respectively for raw material granularity, charging rate, stream pressure, powder
This 4 factors of broken number carry out experiment of single factor, draw the optimised process of ultramicro grinding.
Experiment 1, influence of the raw material granularity to cassia bark Ultramicro-powder particle diameter and flour extraction
Weigh 200g crush drying process after cassia bark coarse powder, stream pressure be 0.4MPa, charging rate 0.30g/
S, under conditions of crushing number is 1 time, influence of the different material granularity to crushing effect is compared.Concrete outcome is shown in Fig. 1, by Fig. 1
As can be seen that feed size is notable to cassia bark ultramicro grinding influential effect, with the reduction of feed size, diameter of particle reduces, and
Powder yield improves.
By considering, coarse grain of the feed size at 180 μm or so is selected, i.e., cassia bark coarse grain is through step (1) powder
180 μm of sieve was needed when pure, now the particle diameter of Ultramicro-powder is 8.3 μm, and powder yield can meet Ultramicro-powder substantially up to 90.4%
Broken requirement.
Experiment 2, influence of the charging rate to cassia bark Ultramicro-powder particle diameter and yield
Weigh 200g and crush the cassia bark coarse powder after drying process, stream pressure is 0.4MPa, raw material granularity is 180 μm,
Crush under conditions of number is 1 time, take different charging rate to carry out ultramicro grinding, respectively 0.20g/s, 0.30g/s,
0.40g/s, 0.50g/s, 0.60g/s, compare influence of the different feeds speed to crushing effect.Concrete outcome is shown in Fig. 2, by Fig. 2
As can be seen that with the raising of charging rate, material regurgitates reduction, after flour extraction improves, but charging rate improves, crushing material
Time is reduced, product granularity increase.Requirement of experiment must assure that flour extraction improves as far as possible while particle size reduction.Pass through survey
Fixed, for charging rate in 0.40g/s and 0.50g/s, raw meal particle size is relatively small and is more or less the same, but the product in 0.50g/s
Flour extraction but increases.Consider, it is 0.5g/s to select charging rate.
Experiment 3, influence of the stream pressure to cassia bark Ultramicro-powder particle diameter and yield
Weigh 200g crush drying process after cassia bark coarse powder, raw material granularity be 180 μm, charging rate 0.5g/s,
Crush under conditions of number is 1 time, take different stream pressure to carry out ultramicro grinding, respectively 0.20MPa, 0.30MPa,
0.40MPa, 0.50MPa, 0.60MPa, influence of the more different stream pressures to crushing effect, as seen from Figure 3, with gas
The increase of flowing pressure, the particle diameter of cassia bark ultrafine powder constantly reduce, but when stream pressure is more than 0.4MPa, just occur
Phenomenon is regurgitated, flour extraction will reduce, and the change of product granularity is not very big.So it is equal to 0.4MPa in stream pressure
When, numerical value that flour extraction and granularity can be more satisfied with.
Experiment 4, crush influence of the number to cassia bark Ultramicro-powder particle diameter and yield
Weigh 200g crush drying process after cassia bark coarse powder, raw material granularity be 180 μm, stream pressure 0.4MPa,
Under conditions of charging rate is 0.50g/s, 1 time, 2 times, 3 ultramicro grindings are carried out respectively.Compare different crushing numbers to crushing
The influence of effect, is as a result shown in Fig. 4.As seen from Figure 4, as the increase for crushing number, flour extraction are decreased obviously, particle size reduction
It is not too obvious, it is contemplated that economic benefit, i.e. selection crush once.
Experiment 5, influence of the liquid nitrogen auxiliary protection technology to cassia bark Ultramicro-powder particle diameter and yield
Airslide disintegrating mill, be it is a kind of using high pressure draught make the mutually fierce collision impact of pulverized material particle, friction,
The equipment that shearing reaches crushing effect.Due to comparative high temperature during comminution process be present, easily by low boiling and heat-sensitive substance
Take away, cause loss of aroma.Liquid nitrogen auxiliary protection technology can cause gas expands at nozzle can cool, and crushing process does not have
Association more heat transfer, therefore crushing temperature rise is low, can retain volatile aroma substance to greatest extent, so as to improve solid spice
Quality.Fixed charging rate is 0.50g/s, stream pressure 0.4MPa, crushes number once, to have studied liquid nitrogen auxiliary protection
Influence of the technology to cassia bark Ultramicro-powder product property.As shown in Table 6, after additional protection of liquid nitrogen, product cut size change is little, goes out powder
Rate increases to 91.5% by 89.3%, and the aroma strength increase of product, fragrance is stronger, pure, has obvious cassia bark gas
Breath.This explanation liquid nitrogen auxiliary protection technology can retain aroma substance to greatest extent, improve the quality of spices.
Influence of the liquid nitrogen auxiliary protection technology of table 6 to cassia bark Ultramicro-powder product
In summary, the optimal preparation technology of cassia bark ultramicro grinding is：Raw material granularity is 180 μm, charging rate is
0.50g/s, stream pressure 0.4MPa, it is 1 time to crush number, uses liquid nitrogen auxiliary protection technology.
Ultra-fine powder preparation technology research is carried out to remaining spices according to above method, obtains optimal preparation technology such as table 7 below.
The optimal preparation technology of the various spices Ultramicro-powders of table 7
Experiment 6：Studied for Ultramicro-powder powder characteristics, ultramicro grinding (including particle diameter, is stopped to its powder characteristics
Angle, heap density, specific surface area and water-soluble sex index) influence be shown in Table 8.
Influence of the ultramicro grinding of table 8 to spices powder characteristics
After ultramicro grinding is handled, obvious order of magnitude change occurs spices for particle diameter, is mainly distributed on 8.5~11.0 μm
Between.Angle of repose is an important parameter for evaluating powder fluidity, and angle of repose is smaller, illustrates that the frictional force between particle is got over
Small, mobility is better, and in general, then powder flowbility is good below 30 ° at angle of repose, 30~45 ° show powder flowbility compared with
Good, 45~60 ° show that mobility is general, and show poor fluidity higher than 60 °.With being obviously reduced for particle diameter, powder stops
The change that angle is also substantially reduced, mainly in the range of 30~45 °, this shows spices after ultramicro grinding, and its mobility becomes
Good, because after air-flow ultramicro grinding, powder surface is not easy to bond aggregation in smooth spherical, and this is with much studying
Conclusion is consistent.Heap density and the specific surface area of powder are closely related, and with the continuous reduction of particle diameter, the specific surface area of powder is not
Disconnected increase, heap density constantly increase, and this is probably that its homogeneity is better, and and neighboring particles because the particle diameter of powder is smaller
The contact area of environment is bigger, causes the space between particle to diminish, so that the heap density increase of powder.Water-soluble sex index
Refer to product soaked in water after material soluble in water quality, reflect product in solable matter quality.With powder
The reduction of particle diameter, its water-soluble sex index significantly increases, because spices, after ultramicro grinding, cell-wall breaking ratio is higher, its
In macromolecular substances be broken for less material, solable matter dissolution is more, so as to having larger water-soluble sex index.
By the studies above, air-flow ultramicro grinding condition and to obtain each Ultramicro-powder particle diameter after crushing be most in the present invention
Good state.
Claims (8)
1. a kind of pungent fragrant and sweet rhythm additive of cigarette, it is characterised in that be by the material composition of following parts by weight：Flos caryophylli ultra micro
Powder 3-10 parts, cassia bark Ultramicro-powder 2-7 parts, vanilla beans Ultramicro-powder 1-5 parts, cumin Ultramicro-powder 1-5 parts；
The flos caryophylli Ultramicro-powder, cassia bark Ultramicro-powder, vanilla beans Ultramicro-powder, cumin Ultramicro-powder are by above-mentioned raw materials coarse powder respectively
Obtained after carrying out air-flow ultramicro grinding under the conditions of charging rate 0.1-1g/s, stream pressure 0.1-1Mpa and liquid nitrogen auxiliary protection
The ultra-micro powder of 1-20 μm of particle diameter.
2. the pungent fragrant and sweet rhythm additive of one kind according to claim 1, it is characterised in that be by the thing of following parts by weight
Matter forms：8 parts of flos caryophylli Ultramicro-powder, 57 parts of cassia bark Ultramicro-powder, 2 parts of vanilla beans Ultramicro-powder, 1 part of cumin Ultramicro-powder.
3. the pungent fragrant and sweet rhythm additive of one kind according to claim 1, it is characterised in that：The grain of the flos caryophylli Ultramicro-powder
Footpath is 9 μm, and the particle diameter of cassia bark Ultramicro-powder is 8 μm, and the particle diameter of vanilla beans Ultramicro-powder is 10 μm, and the particle diameter of cumin Ultramicro-powder is 10
μm。
4. a kind of preparation method of pungent fragrant and sweet rhythm additive, it is characterised in that comprise the following steps that：
(1) using flos caryophylli, cassia bark, vanilla beans, cumin as raw material, raw material is first distinguished into attrition grinding, obtained raw material coarse grain
Sieving；
(2) it is the raw material coarse grain after being sieved in step (1) is small to water content through -40 DEG C~-80 DEG C vacuum freeze dryings respectively again
In 5%, raw material meal, i.e. flos caryophylli coarse powder, cassia bark coarse powder, vanilla beans coarse powder and cumin coarse powder are obtained；
(3) by step (2) dried raw material meal again respectively in charging rate 0.1-1g/s, stream pressure 0.1-1Mpa and liquid
Air-flow ultramicro grinding is carried out under the conditions of nitrogen auxiliary protection 1-2 times to 1-20 μm of particle diameter, obtain flos caryophylli Ultramicro-powder, cassia bark ultra micro
Powder, vanilla beans Ultramicro-powder and cumin Ultramicro-powder；
(4) the raw material Ultramicro-powder obtained by step (3) is mixed according to following ratio of weight and number：Flos caryophylli Ultramicro-powder 3-10
Part, cassia bark Ultramicro-powder 2-7 parts, vanilla beans Ultramicro-powder 1-5 parts, cumin Ultramicro-powder 1-5 parts are well mixed, that is, obtain pungent fragrant and sweet rhythm
Ultramicro-powder.
5. a kind of preparation method of pungent fragrant and sweet rhythm additive according to claim 4, it is characterised in that in the step (3)
Flos caryophylli coarse powder carry out air-flow ultramicro grinding condition be：Aided in charging rate 0.3g/s, stream pressure 0.4Mpa and liquid nitrogen
Air-flow crushing is carried out under protective condition, crushes number 1 time.
6. a kind of preparation method of pungent fragrant and sweet rhythm additive according to claim 4, it is characterised in that in the step (3)
Cassia bark coarse powder carry out air-flow ultramicro grinding condition be：Aid in protecting in charging rate 0.5g/s, stream pressure 0.4Mpa and liquid nitrogen
Air-flow crushing is carried out under the conditions of shield, crushes number 1 time；
The condition of vanilla beans coarse powder progress air-flow ultramicro grinding is in the step (3)：In charging rate 0.4g/s, air-flow pressure
Air-flow crushing is carried out under the conditions of power 0.6Mpa and liquid nitrogen auxiliary protection, crushes number 2 times；
The condition of cumin coarse powder progress air-flow ultramicro grinding is in the step (3)：In charging rate 0.5g/s, stream pressure
Air-flow crushing is carried out under the conditions of 0.5Mpa and liquid nitrogen auxiliary protection, crushes number 1 time.
7. a kind of application of pungent fragrant and sweet rhythm cigarette additive prepared by method according in claim 4 in cigarette, its feature
It is：The pungent fragrant and sweet super additive of rhythm being prepared is compared into 1-5 according to weight:100 ratio is added in cigarette overlapping glue,
And upper machine is put in Cigarette after being mixed evenly.
A kind of 8. application of the pungent fragrant and sweet rhythm cigarette additive according to claim 7 in cigarette, it is characterised in that：It is described
The weight ratio of pungent fragrant and sweet rhythm cigarette additive and cigarette overlapping glue is 1.5:100.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711089877.2A CN107746748A (en) | 2017-11-08 | 2017-11-08 | A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711089877.2A CN107746748A (en) | 2017-11-08 | 2017-11-08 | A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107746748A true CN107746748A (en) | 2018-03-02 |
Family
ID=61252007
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711089877.2A Pending CN107746748A (en) | 2017-11-08 | 2017-11-08 | A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107746748A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109875095A (en) * | 2019-02-01 | 2019-06-14 | 湖北中烟工业有限责任公司 | It can be used for the ultralow temperature preparation method of the cumin Ultramicro-powder of cigarette product flavoring and casing |
| CN111154548A (en) * | 2020-01-13 | 2020-05-15 | 合肥学院 | Extraction method of cinnamon essential oil |
| CN115232672A (en) * | 2022-08-16 | 2022-10-25 | 湖北中烟工业有限责任公司 | Preparation method of vanilla spice |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040123873A1 (en) * | 2002-12-31 | 2004-07-01 | Smokey Mountain Chew, Inc. | Nontobacco moist snuff composition |
| CN101215449A (en) * | 2008-01-07 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Function cigarette overlapping glue and preparation method thereof |
| CN103923579A (en) * | 2014-04-24 | 2014-07-16 | 川渝中烟工业有限责任公司 | Essence used in vanilla-scented holder adhesive for cigarettes |
| CN104687246A (en) * | 2015-01-05 | 2015-06-10 | 云南中烟工业有限责任公司 | Porous moringa oleifera particles, preparation method of porous moringa oleifera particles as well as cigarette filter stick containing porous particles |
| CN105192876A (en) * | 2015-10-20 | 2015-12-30 | 贵州中烟工业有限责任公司 | Oral smokeless tobacco composition added with plant composition and application of oral smokeless tobacco composition |
| CN106174684A (en) * | 2016-07-12 | 2016-12-07 | 湖北中烟工业有限责任公司 | The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof |
| CN106723306A (en) * | 2017-01-16 | 2017-05-31 | 云南中烟新材料科技有限公司 | A kind of method that American mint prepares cigarette filter rod additive |
-
2017
- 2017-11-08 CN CN201711089877.2A patent/CN107746748A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040123873A1 (en) * | 2002-12-31 | 2004-07-01 | Smokey Mountain Chew, Inc. | Nontobacco moist snuff composition |
| CN101215449A (en) * | 2008-01-07 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Function cigarette overlapping glue and preparation method thereof |
| CN103923579A (en) * | 2014-04-24 | 2014-07-16 | 川渝中烟工业有限责任公司 | Essence used in vanilla-scented holder adhesive for cigarettes |
| CN104687246A (en) * | 2015-01-05 | 2015-06-10 | 云南中烟工业有限责任公司 | Porous moringa oleifera particles, preparation method of porous moringa oleifera particles as well as cigarette filter stick containing porous particles |
| CN105192876A (en) * | 2015-10-20 | 2015-12-30 | 贵州中烟工业有限责任公司 | Oral smokeless tobacco composition added with plant composition and application of oral smokeless tobacco composition |
| CN106174684A (en) * | 2016-07-12 | 2016-12-07 | 湖北中烟工业有限责任公司 | The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof |
| CN106723306A (en) * | 2017-01-16 | 2017-05-31 | 云南中烟新材料科技有限公司 | A kind of method that American mint prepares cigarette filter rod additive |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109875095A (en) * | 2019-02-01 | 2019-06-14 | 湖北中烟工业有限责任公司 | It can be used for the ultralow temperature preparation method of the cumin Ultramicro-powder of cigarette product flavoring and casing |
| CN111154548A (en) * | 2020-01-13 | 2020-05-15 | 合肥学院 | Extraction method of cinnamon essential oil |
| CN115232672A (en) * | 2022-08-16 | 2022-10-25 | 湖北中烟工业有限责任公司 | Preparation method of vanilla spice |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105411944B (en) | Application and oil tea face mask cream of the oil tea in terms of beauty skin care product is prepared | |
| CN104323395B (en) | A kind of antioxidant of the peel extract containing Queensland nut and preparation method and application | |
| CN101143154B (en) | Method for preparing surface cladding super-micro traditional Chinese medicine material crude slice | |
| CN101444273A (en) | Health product oral fast-release preparation and production method thereof | |
| CN106174684A (en) | The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof | |
| KR20120098804A (en) | Method for manufacturing aloe powder | |
| CN107746748A (en) | A kind of pungent fragrant and sweet rhythm cigarette additive and preparation method thereof and the application in cigarette | |
| JP7525180B2 (en) | Powdered sesame processed product and its manufacturing method | |
| PT1401295E (en) | Hard bouillon tablet | |
| CN104687246A (en) | Porous moringa oleifera particles, preparation method of porous moringa oleifera particles as well as cigarette filter stick containing porous particles | |
| CN101715844A (en) | Method for preparing ultrafine tea powder | |
| CN101099558A (en) | Immediate cinder-free thirteen spices quelite product and preparing method | |
| CN105663176A (en) | Method for preparing traditional Chinese medicine granules from puffed traditional Chinese medicine decoction pieces | |
| CN106723303B (en) | A kind of method that wet pulverizing prepares tobacco flavor electronics tobacco tar | |
| CN109364210A (en) | A kind of fructus amomi superfine powder and preparation method thereof | |
| CN106617276B (en) | A kind of method that Chinese herbal medicine electronics tobacco tar and wet pulverizing prepare Chinese herbal medicine electronics tobacco tar | |
| EP4093212B1 (en) | Beverage composition | |
| CN109169965A (en) | A kind of preparation method of ginseng seed oil microcapsule powder | |
| CN112022764A (en) | Biomass anti-mosquito and anti-mite talcum powder and preparation method thereof | |
| CN108991128A (en) | The preparation method of instant soybeen milk powder | |
| KR101784992B1 (en) | Ginseng flower powder and the method for preparing thereof, and the cosmetic composition containing the same | |
| CN104187525B (en) | A kind of emblic cotyledon mixed food spices being rich in calcium iron ion and preparation method thereof | |
| CN104289294A (en) | Traditional Chinese medicine production method | |
| CN103478641A (en) | Whole lotus root powder and production method thereof | |
| JP7374495B2 (en) | Powdered beverage composition and method for producing the same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180302 |
|
| RJ01 | Rejection of invention patent application after publication |