CN108523221A - A kind of cigarette composite filter and preparation method thereof prepared by grosvenor momordica leaf - Google Patents

A kind of cigarette composite filter and preparation method thereof prepared by grosvenor momordica leaf Download PDF

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Publication number
CN108523221A
CN108523221A CN201810698566.4A CN201810698566A CN108523221A CN 108523221 A CN108523221 A CN 108523221A CN 201810698566 A CN201810698566 A CN 201810698566A CN 108523221 A CN108523221 A CN 108523221A
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China
Prior art keywords
grosvenor momordica
filter core
momordica leaf
wrapping layer
prepared
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Granted
Application number
CN201810698566.4A
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Chinese (zh)
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CN108523221B (en
Inventor
张峻松
董振山
刘春奎
何山
李庆祥
彭周舟
赵琪
杜赫
朱远洋
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Zhengzhou University of Light Industry
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Zhengzhou University of Light Industry
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Priority to CN201810698566.4A priority Critical patent/CN108523221B/en
Publication of CN108523221A publication Critical patent/CN108523221A/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02Manufacture of tobacco smoke filters
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/08Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
    • A24D3/10Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The present invention relates to cigarette preparation fields, particularly relate to a kind of cigarette composite filter and preparation method thereof prepared by grosvenor momordica leaf.Including the wrapping layer outside filter core and filter core, wrapping layer includes interior wrapping layer and outer casing, the filter core includes the filter core of three sections of different structures, every section of filter core is outer to be wrapped up by interior wrapping layer, first segment filter core is the fibre bundle added with grosvenor momordica leaf extract particles, second segment filter core is grosvenor momordica leaf particle, and third section filter core is the acetate fiber bonded through triacetyl glycerine.Three-element composite filter core prepared by the present invention, it is flavouring section that three sections of filter sticks, which have respective effect, first segment filter stick, and the natural faint scent of grosvenor momordica leaf and blueness can be brought fragrant, reduce dry sensation, and fragrance is lasting, improves the compatibility of flue gas.

Description

A kind of cigarette composite filter and preparation method thereof prepared by grosvenor momordica leaf
Technical field
The present invention relates to cigarette preparation field, a kind of cigarette composite filter prepared by grosvenor momordica leaf and its preparation are particularly related to Method.
Background technology
Smoking is always consumers in general with health problem and is engaged in tobacco business staff focus of interest.At present There is Three-element composite filter core, the sorbing materials such as activated carbon are added mainly in filter stick and are used for reducing the tar in flue gas, to reach Purpose of the cigarette to the harm of human body is reduced, but the type that compound filter tip is prepared currently with natural material is less, CN106617286 A disclose a kind of preparation method of lotus leaf type composite cigarette filter stick, and the filter stick being prepared can bring lotus The natural fragrant of leaf, and can persistently discharge, improve the suction quality of cigarette.Mainly natural perfume material discharges perfume in cigarette Taste endurance is insufficient.
Ingredient report is less in related grosvenor momordica leaf, extracts identification to the ingredient in grosvenor momordica leaf in relation to report, sends out Contain abundant Flavonoid substances in existing grosvenor momordica leaf, Flavonoid substances, some researches show that many studies have shown that antioxidant It is a kind of reproducibility compound for having phenolic hydroxyl group to have very strong scavenging effect, flavone compound to free radical, complicated anti- It answers in system, since its own has antioxidation by oxidation, there is anti-inflammatory, antiallergy, inhibit bacterium, prevention liver Disease, treatment of vascular disease, it is antitumor the effects that.
The application is mainly that natural perfume material discharges lasting fragrance power deficiency in cigarette, and this patent Three-element composite filter core is first It is secondary that grosvenor momordica leaf is added in filter stick, grosvenor momordica leaf extract is added in first segment filter core, is reached and is increased nature faint scent Purpose, and fragrance is more lasting.Second segment filter core is that the grosvenor momordica leaf of interior wrapping layer package is filter layer, is reaching reduction cigarette Tar achievees the purpose that harm reduction simultaneously in flue gas, moreover it is possible to reach and increase nature faint scent, reduce the purpose of dry sensation.
Invention content
The present invention proposes a kind of cigarette composite filter and preparation method thereof prepared by grosvenor momordica leaf, solves in the prior art The faint scent for increasing cigarette is prepared using grosvenor momordica leaf and blueness is fragrant, reduces the dry sensation that flue gas is brought, and the blueness for increasing flue gas is fragrant, mitigates Withered and burnt smell, the miscellaneous gas of soil, soft flue gas, the problem of suction quality of cigarette can be improved.
The technical proposal of the invention is realized in this way:
A kind of cigarette composite filter prepared by grosvenor momordica leaf, including the wrapping layer outside filter core and filter core, wrapping layer include interior package Layer and outer casing, the filter core include the filter core of three sections of different structures, and every section of filter core is outer to be wrapped up by interior wrapping layer, first segment Filter core is the fibre bundle added with grosvenor momordica leaf extract particles, and second segment filter core is grosvenor momordica leaf particle, third section filter core For the acetate fiber bonded through triacetyl glycerine.
The interior wrapping layer is three sections of forming papers, outer casing is tipping paper.
The mass percent that grosvenor momordica leaf extract particles are added in the first segment filter core is 0.01%-0.5%.
The length ratio of the first segment filter core, second segment filter core and third section filter core is:(35-63):(126-140): (126-140).
The preparation method of cigarette composite filter prepared by the grosvenor momordica leaf prepares arhat using grosvenor momordica leaf as raw material Fruit leaf particle and grosvenor momordica leaf extract particles, grosvenor momordica leaf extract particles are added in fibre bundle through interior wrapping layer I First segment filter core is made in package, second segment filter core is made in grosvenor momordica leaf particle package with interior wrapping layer II, by three triacetins The acetate fiber of ester bonding is wrapped up with interior wrapping layer III is made third section filter core, and three sections of filter cores are wrapped to form cigarette through outer casing and use Composite filter.
Grosvenor momordica leaf particle is that grosvenor momordica leaf is freeze-dried, is sieved in the second segment filter core, the arhat being prepared Fruit leaf granular size is 100-120 mesh.
The preparation method of the grosvenor momordica leaf extract particles is:
(1)After being crushed after freeze-dried 10 h -48 h of grosvenor momordica leaf, crossing 40-60 mesh sieve, refluxing extraction obtains grosvenor momordica leaf and carries Take liquid;
(2)For grosvenor momordica leaf extracting solution through grosvenor momordica leaf extract is concentrated under reduced pressure to obtain, grosvenor momordica leaf extract is freeze-dried, is sieved Form grosvenor momordica leaf extract particles.
The step(1)The organic solvent that middle refluxing extraction uses is that petroleum ether, dichloromethane, acetone, methanol, ethyl alcohol are molten The time of or mixtures thereof liquid, refluxing extraction is 0.5-5.0 h.
The step(1)The mass ratio of the organic solvent that middle refluxing extraction uses and the grosvenor momordica leaf after crushing, sieving is (5-20):1.
The beneficial effects of the present invention are:
Grosvenor momordica leaf is added in filter stick for cigarettes by the present invention for the first time, the Three-element composite filter core prepared by the present invention, three sections of filter sticks It is flavouring section to have respective effect, first segment filter stick, and the natural faint scent of grosvenor momordica leaf and blueness can be brought fragrant, reduce dry sensation, And fragrance is lasting, improves the compatibility of flue gas.Second segment filter stick is adsorption section, can adsorb the tar in flue gas, reduces volume Harm of the cigarette to human body.And for the filter stick of the invention using grosvenor momordica leaf as raw material, price is less expensive, simple production process.
Description of the drawings
Fig. 1 is the structural schematic diagram of composite filter of the present invention, wrapping layer I in wherein 1-, 2- outer casing, wrapping layer in 3- II, wrapping layer III, 5- first segments filter core, 6- second segments filter core, 7- third section filter cores in 4-.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme of the present invention is clearly and completely described, it is clear that institute The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, The every other embodiment that those of ordinary skill in the art are obtained under the premise of not making the creative labor, belongs to this hair The range of bright protection.
Embodiment 1
The preparation method of cigarette composite filter prepared by grosvenor momordica leaf, steps are as follows:
By grosvenor momordica leaf, 24 h are freeze-dried, are crushed, sieving forms 40-60 mesh grosvenor momordica leaf powder.Weigh grosvenor momordica leaf powder The ethyl alcohol of 500 mL a concentration of 70% is added in 1000 mL volumetric flasks in 50 g of end, and electric jacket is heated to slightly boiling, refluxing extraction 3 H is filtered, and is collected filtrate, is obtained grosvenor momordica leaf extracting solution, is 45 DEG C of reduced pressures in heating temperature, without the feelings dripped under solvent Under condition, heating temperature is raised to 65 DEG C and continues to concentrate, 15 min are kept in the case of drop under no solvent.Solvent is removed to obtain To grosvenor momordica leaf extract, grosvenor momordica leaf is freeze-dried 24 h, is crushed, sieving forms 40-60 mesh powder.By mangosteen powder End is added on fibre bundle, and after triacetyl glycerine bonds first segment filter core is made, filter core is through interior wrapping layer in fibre bundle Flavouring section is made in package, and grosvenor momordica leaf extract is 0.1% in the additive amount of first segment filter core(Mass ratio).
The grosvenor momordica leaf of freeze-drying is crushed, sieving forms 100-120 mesh particles, and grosvenor momordica leaf particle is through interior packet Covering layer is wrapped up, and adsorption section is made.Fibre bundle is made after triacetyl glycerine bonds through interior wrapping layer package third section filter core Suck section.Three sections of filter cores and interior package are prepared into Three-element composite filter core through outer casing package, and first segment filter core accounts for entire filter core 1/9, second segment filter core accounts for the 4/9 of entire filter core.
Embodiment 2
The preparation method of cigarette composite filter prepared by grosvenor momordica leaf, steps are as follows:
By grosvenor momordica leaf, 24 h are freeze-dried, are crushed, sieving forms 40-60 mesh grosvenor momordica leaf powder.Weigh grosvenor momordica leaf powder The ethyl alcohol of 500mL a concentration of 80% is added in 1000 mL volumetric flasks in 75 g of end, and electric jacket is heated to slightly boiling, refluxing extraction 4 H is filtered, and is collected filtrate, is obtained grosvenor momordica leaf extracting solution, is 45 DEG C of reduced pressures in heating temperature, without the feelings dripped under solvent Under condition, heating temperature is raised to 65 DEG C and continues to concentrate, 15 min are kept in the case of drop under no solvent.Solvent is removed to obtain To grosvenor momordica leaf extract, grosvenor momordica leaf is freeze-dried 24 h, is crushed, sieving forms 40-60 mesh powder.By mangosteen powder End is added on fibre bundle, and after triacetyl glycerine bonds first segment filter core is made, filter core is through interior wrapping layer in fibre bundle Flavouring section is made in package, and grosvenor momordica leaf extract is 0.3% in the additive amount of first segment filter core(Mass ratio).
The grosvenor momordica leaf of freeze-drying is crushed, sieving forms 100-120 mesh particles, and grosvenor momordica leaf particle is through interior packet Covering layer is wrapped up, and adsorption section is made.Fibre bundle is made after triacetyl glycerine bonds through interior wrapping layer package third section filter core Suck section.Three sections of filter cores and interior package are prepared into Three-element composite filter core through outer casing package, and first segment filter core accounts for entire filter core 1/7, second segment filter core accounts for the 3/7 of entire filter core.
Embodiment 3
The preparation method of cigarette composite filter prepared by grosvenor momordica leaf, steps are as follows:
By grosvenor momordica leaf, 24 h are freeze-dried, are crushed, sieving forms 40-60 mesh grosvenor momordica leaf powder.Weigh grosvenor momordica leaf powder The ethyl alcohol of 500mL a concentration of 90% is added in 1000 mL volumetric flasks in 100 g of end, and electric jacket is heated to slightly boiling, refluxing extraction 5 H is filtered, and is collected filtrate, is obtained grosvenor momordica leaf extracting solution, is 45 DEG C of reduced pressures in heating temperature, without the feelings dripped under solvent Under condition, heating temperature is raised to 65 DEG C and continues to concentrate, 15 min are kept in the case of drop under no solvent.Solvent is removed to obtain To grosvenor momordica leaf extract, grosvenor momordica leaf is freeze-dried 24 h, is crushed, sieving forms 40-60 mesh powder.By mangosteen powder End is added on fibre bundle, and after triacetyl glycerine bonds first segment filter core is made, filter core is through interior wrapping layer in fibre bundle Flavouring section is made in package, and grosvenor momordica leaf extract is 0.5% in the additive amount of first segment filter core(Mass ratio).
The grosvenor momordica leaf of freeze-drying is crushed, sieving forms 100-120 mesh particles, and grosvenor momordica leaf particle is through interior packet Covering layer is wrapped up, and adsorption section is made.Fibre bundle is made after triacetyl glycerine bonds through interior wrapping layer package third section filter core Suck section.Three sections of filter cores and interior package are prepared into Three-element composite filter core through outer casing package, and first segment filter core accounts for entire filter core 1/5, second segment filter core accounts for the 2/5 of entire filter core.
Application Example
By above-described embodiment prepare Three-element composite filter core, put into spicing machine and produced, smoke panel test personnel according to 《GB5606.4-2005 tobaccos and tobacco product sensory evaluation method》Sensory evaluating smoking is carried out, smoking result is as shown in table 1.
Influence of the 1 Siraitia grosvenorii essential oil Different adding amount of table to Sensory Quality of Cigarette
1#:Compare cigarette;2#:The one section of cigarette to connect of filter stick and cigarette prepared according to embodiment 1;3#:It is made according to embodiment 2 One section of cigarette to connect of standby filter stick and cigarette;One section of cigarette to connect of filter stick and cigarette that 4# is prepared according to embodiment 3.
From smoking result:2#, 3# cigarette integrally thought that irritation was declined, miscellaneous preferably compared with compareing cigarette Gas is mitigated, and pleasant impression is preferable, there is apparent sweet sense, has natural faint scent, flue gas elegant and delicate to assign the refrigerant gas of cigarette Taste.4# samples total score is declined slightly compared with compareing cigarette, is this perfume of cover tobacco because grosvenor momordica leaf additive amount is more, remaining Taste is poor.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.

Claims (9)

1. cigarette composite filter prepared by a kind of grosvenor momordica leaf, it is characterised in that:Including the wrapping layer outside filter core and filter core, package Layer includes interior wrapping layer and outer casing(2), interior wrapping layer includes interior wrapping layer I(1), interior wrapping layer II(3), interior wrapping layer III (4), the filter core includes the filter core of three sections of different structures, and every section of filter core is outer to be wrapped up by interior wrapping layer, first segment filter core(5)For Fibre bundle added with grosvenor momordica leaf extract particles, second segment filter core(6)For grosvenor momordica leaf particle, third section filter core(7) For the acetate fiber bonded through triacetyl glycerine.
2. cigarette composite filter prepared by grosvenor momordica leaf as described in claim 1, it is characterised in that:The interior wrapping layer is three Section forming paper, outer casing(2)For tipping paper.
3. cigarette composite filter prepared by grosvenor momordica leaf as described in claim 1, it is characterised in that:The first segment filter core (5)The mass percent of middle grosvenor momordica leaf extract particles addition is 0.01%-0.5%.
4. cigarette composite filter prepared by grosvenor momordica leaf as described in claim 1, it is characterised in that:The first segment filter core (5), second segment filter core(6)With third section filter core(7)Length ratio be:(35-63):(126-140):(126-140).
5. the preparation method of cigarette composite filter prepared by grosvenor momordica leaf according to any one of claims 1-4, feature exist In:Using grosvenor momordica leaf as raw material, grosvenor momordica leaf particle and grosvenor momordica leaf extract particles are prepared, by grosvenor momordica leaf extract particles It is added in fibre bundle through interior wrapping layer I(1)First segment filter core is made in package(5), with interior wrapping layer II(3)By grosvenor momordica leaf Second segment filter core is made in particle package(6), by the acetate fiber interior wrapping layer III of triacetyl glycerine bonding(4)Package is made Third section filter core(7), three sections of filter cores are through outer casing(2)It is wrapped to form cigarette composite filter.
6. the preparation method of cigarette composite filter prepared by grosvenor momordica leaf as claimed in claim 5, it is characterised in that:Described Two sections of filter cores(6)Middle grosvenor momordica leaf particle is that grosvenor momordica leaf is freeze-dried, is sieved, the grosvenor momordica leaf granular size being prepared For 100-120 mesh.
7. the preparation method of cigarette composite filter prepared by grosvenor momordica leaf as claimed in claim 5, which is characterized in that sieve The preparation method of Chinese fruit leaf extract particle is:
(1)After being crushed after freeze-dried 10 h -48 h of grosvenor momordica leaf, crossing 40-60 mesh sieve, refluxing extraction obtains grosvenor momordica leaf and carries Take liquid;
(2)For grosvenor momordica leaf extracting solution through grosvenor momordica leaf extract is concentrated under reduced pressure to obtain, grosvenor momordica leaf extract is freeze-dried, is sieved Form grosvenor momordica leaf extract particles.
8. cigarette composite filter prepared by grosvenor momordica leaf as claimed in claim 7, it is characterised in that:The step(1)In return The organic solvent that uses of stream extraction is or mixtures thereof petroleum ether, dichloromethane, acetone, methanol, ethanol solution, refluxing extraction Time is 0.5-5.0 h.
9. cigarette composite filter prepared by grosvenor momordica leaf as claimed in claim 7, it is characterised in that:The step(1)In return The mass ratio of organic solvent and the grosvenor momordica leaf after crushing, sieving that stream extraction uses is(5-20):1.
CN201810698566.4A 2018-06-29 2018-06-29 Composite cigarette filter rod prepared from momordica grosvenori leaves and preparation method thereof Active CN108523221B (en)

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CN109537365A (en) * 2018-11-05 2019-03-29 广西中烟工业有限责任公司 A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper
CN109527643A (en) * 2018-11-05 2019-03-29 广西中烟工业有限责任公司 A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor

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CN109537365A (en) * 2018-11-05 2019-03-29 广西中烟工业有限责任公司 A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper
CN109527643A (en) * 2018-11-05 2019-03-29 广西中烟工业有限责任公司 A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor

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