CN108523221B - Composite cigarette filter rod prepared from momordica grosvenori leaves and preparation method thereof - Google Patents
Composite cigarette filter rod prepared from momordica grosvenori leaves and preparation method thereof Download PDFInfo
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- CN108523221B CN108523221B CN201810698566.4A CN201810698566A CN108523221B CN 108523221 B CN108523221 B CN 108523221B CN 201810698566 A CN201810698566 A CN 201810698566A CN 108523221 B CN108523221 B CN 108523221B
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- momordica grosvenori
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
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- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to the field of cigarette preparation, in particular to a composite filter rod for cigarettes prepared from momordica grosvenori leaves and a preparation method thereof. Including the outer parcel layer of filter core and filter core, the parcel layer includes interior parcel layer and outer parcel layer, the filter core includes the filter core of the different structures of three-section, every section filter core is wrapped up by interior parcel layer outward, and first section filter core is for adding the fibre silk bundle that has luohan fruit leaf extract granule, and second section filter core is luohan fruit leaf granule, and third section filter core is the acetate fiber through the bonding of triacetin. The three sections of the three-element composite filter stick prepared by the invention have respective effects, the first section of the filter stick is an aroma-increasing section, the natural faint scent and the green scent of the momordica grosvenori leaves can be brought, the dryness is reduced, the aroma is lasting, and the compatibility of smoke is improved.
Description
Technical Field
The invention relates to the field of cigarette preparation, in particular to a composite filter rod for cigarettes prepared from momordica grosvenori leaves and a preparation method thereof.
Background
Smoking and health concerns have been a focus of attention for both consumers and workers engaged in the tobacco industry. At present, a ternary composite filter stick is mainly formed by adding absorbent materials such as activated carbon and the like into the filter stick to reduce tar in smoke so as to achieve the purpose of reducing the harm of cigarettes to human bodies, but the types of composite filter tips prepared by utilizing natural raw materials are few at present, and CN 106617286A discloses a preparation method of a lotus leaf type cigarette composite filter stick, and the prepared filter stick can bring natural fresh scent of lotus leaves, can release the natural fresh scent of the lotus leaves for a long time and improves the smoking quality of the cigarettes. Mainly, the natural fragrant raw materials have insufficient lasting fragrance released in the cigarettes.
The reports on the components in the momordica grosvenori leaves are less, and the reports on the extraction and identification of the components in the momordica grosvenori leaves show that the momordica grosvenori leaves contain abundant flavonoids and flavonoids, and many researches show that the antioxidant has a strong scavenging effect on free radicals, and the flavonoids are reductive compounds with phenolic hydroxyl groups, have an antioxidation effect due to oxidation of the flavonoids, and have the effects of resisting inflammation, resisting allergy, inhibiting bacteria, preventing and treating liver diseases, preventing and treating vascular diseases, resisting tumors and the like in a complex reaction system.
The application mainly aims to solve the problem that the natural fragrant raw materials release fragrance in cigarettes, the fragrance lasting force is insufficient, the momordica grosvenori leaves are added into the filter stick by the ternary composite filter stick, and the momordica grosvenori leaf extract is added into the first section of filter element for the first time, so that the purpose of increasing natural fragrance is achieved, and the fragrance is lasting. The second section of filter element is a filter layer made of momordica grosvenori leaves wrapped by an inner wrapping layer, so that the purposes of reducing tar in cigarette smoke, reducing harm and increasing natural fragrance and reducing dry feeling can be achieved.
Disclosure of Invention
The invention provides a composite filter stick for cigarettes prepared from momordica grosvenori leaves and a preparation method thereof, and solves the problems that in the prior art, the faint scent and the green scent of the cigarettes are increased, the dryness brought by smoke is reduced, the green scent of the smoke is increased, the scorched smell, the soil impurity smell and the soft smoke are reduced, and the smoking quality of the cigarettes can be improved.
The technical scheme of the invention is realized as follows:
the utility model provides a cigarette composite filter rod of grosvenor momordica leaf preparation, includes the wrapping layer outside filter core and the filter core, and the wrapping layer includes interior wrapping layer and outer wrapping layer, the filter core includes the filter core of three-section different structure, and every section of filter core is wrapped up by interior wrapping layer outward, and first section filter core is for adding the fibre silk bundle that has grosvenor momordica leaf extract granule, and the second section filter core is grosvenor momordica leaf granule, and the third section filter core is the acetate fiber through the bonding of triacetin.
The inner wrapping layer is three sections of forming paper, and the outer wrapping layer is tipping paper.
The mass percentage of the added momordica grosvenori leaf extract particles in the first section of filter element is 0.01-0.5%.
The length proportion of the first section of filter element, the second section of filter element and the third section of filter element is as follows: (35-63):(126-140):(126-140).
The preparation method of the cigarette composite filter rod prepared from the momordica grosvenori leaves comprises the steps of preparing momordica grosvenori leaf particles and momordica grosvenori leaf extract particles by taking the momordica grosvenori leaves as raw materials, adding the momordica grosvenori leaf extract particles into fiber tows, wrapping the particles by an inner wrapping layer I to prepare a first section of filter core, wrapping the particles by an inner wrapping layer II to prepare a second section of filter core, wrapping cellulose acetate bonded by glycerol triacetate by an inner wrapping layer III to prepare a third section of filter core, and wrapping the third section of filter core by an outer wrapping layer to form the cigarette composite filter rod.
The particle size of the momordica grosvenori leaf in the second section of filter core is 100-120 meshes.
The preparation method of the momordica grosvenori leaf extract particles comprises the following steps:
(1) freeze drying fructus Siraitiae Grosvenorii leaf for 10-48 h, pulverizing, sieving with 40-60 mesh sieve, and reflux extracting to obtain fructus Siraitiae Grosvenorii leaf extractive solution;
(2) concentrating the extractive solution under reduced pressure to obtain folium Momordicae extract, freeze drying, and sieving to obtain folium Momordicae extract granule.
The organic solvent used in the reflux extraction in the step (1) is petroleum ether, dichloromethane, acetone, methanol, ethanol solution or a mixture thereof, and the reflux extraction time is 0.5-5.0 h.
The mass ratio of the organic solvent used in the reflux extraction in the step (1) to the crushed and sieved momordica grosvenori leaves is (5-20): 1.
the invention has the beneficial effects that:
according to the ternary composite filter stick, the momordica grosvenori leaves are added into the filter stick for the cigarette for the first time, the three sections of the filter stick have respective effects, the first section of the filter stick is the flavoring section, the natural faint scent and the green scent of the momordica grosvenori leaves can be brought, the dryness is reduced, the fragrance is lasting, and the compatibility of smoke is improved. The second section of filter stick is an adsorption section, which can adsorb tar in smoke and reduce the harm of cigarette to human body. In addition, the filter stick of the invention takes the momordica grosvenori leaves as raw materials, the price is lower, and the production process is simple.
Drawings
FIG. 1 is a schematic structural diagram of a composite filter stick of the invention, wherein 1-an inner wrapping layer I, 2-an outer wrapping layer, 3-an inner wrapping layer II, 4-an inner wrapping layer III, 5-a first section of filter element, 6-a second section of filter element and 7-a third section of filter element.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without inventive effort based on the embodiments of the present invention, are within the scope of the present invention.
Example 1
The preparation method of the composite filter rod for the cigarette prepared from the momordica grosvenori leaves comprises the following steps:
freeze-drying the momordica grosvenori leaves for 24 hours, crushing and sieving to form momordica grosvenori leaf powder of 40-60 meshes. Weighing 50 g of momordica grosvenori leaf powder into a 1000 mL volumetric flask, adding 500mL of 70% ethanol, heating by an electric heating jacket until the momordica grosvenori leaf powder is slightly boiled, performing reflux extraction for 3 h, performing suction filtration, collecting filtrate to obtain momordica grosvenori leaf extract, heating to 45 ℃ for reduced pressure concentration, increasing the heating temperature to 65 ℃ for continuous concentration under the condition that no solvent drips, and keeping for 15 min under the condition that no solvent drips. Removing solvent to obtain extract, freeze drying for 24 hr, pulverizing, and sieving to obtain 40-60 mesh powder. Adding fructus Siraitiae Grosvenorii powder onto fiber tow, bonding the fiber tow with glycerol triacetate, making into first stage filter core, wrapping the filter core with inner wrapping layer to make into flavoring section, and adding fructus Siraitiae Grosvenorii leaf extract in the first stage filter core at an amount of 0.1% (by mass).
Crushing the freeze-dried momordica grosvenori leaves, sieving to form 100-mesh 120-mesh particles, and wrapping the momordica grosvenori leaf particles by an inner wrapping layer to prepare an adsorption section. The fiber tows are bonded by glycerol triacetate, and then are wrapped by the inner wrapping layer to form the third section of filter element to form the suction section. The three sections of filter elements and the inner wrapping layer are wrapped by the outer wrapping layer to prepare the ternary composite filter stick, the first section of filter element accounts for 1/9 of the whole filter element, and the second section of filter element accounts for 4/9 of the whole filter element.
Example 2
The preparation method of the composite filter rod for the cigarette prepared from the momordica grosvenori leaves comprises the following steps:
freeze-drying the momordica grosvenori leaves for 24 hours, crushing and sieving to form momordica grosvenori leaf powder of 40-60 meshes. Weighing 75 g of momordica grosvenori leaf powder into a 1000 mL volumetric flask, adding 500mL of 80% ethanol, heating by an electric heating jacket until the momordica grosvenori leaf powder is slightly boiled, performing reflux extraction for 4 hours, performing suction filtration, collecting filtrate to obtain momordica grosvenori leaf extract, heating to 45 ℃ for reduced pressure concentration, increasing the heating temperature to 65 ℃ for continuous concentration under the condition that no solvent drips, and keeping for 15 min under the condition that no solvent drips. Removing solvent to obtain extract, freeze drying for 24 hr, pulverizing, and sieving to obtain 40-60 mesh powder. Adding fructus Siraitiae Grosvenorii powder onto fiber tow, bonding the fiber tow with glycerol triacetate, making into first stage filter core, wrapping the filter core with inner wrapping layer to make into flavoring section, and adding fructus Siraitiae Grosvenorii leaf extract in the first stage filter core at an amount of 0.3% (by mass).
Crushing the freeze-dried momordica grosvenori leaves, sieving to form 100-mesh 120-mesh particles, and wrapping the momordica grosvenori leaf particles by an inner wrapping layer to prepare an adsorption section. The fiber tows are bonded by glycerol triacetate, and then are wrapped by the inner wrapping layer to form the third section of filter element to form the suction section. The three sections of filter elements and the inner wrapping layer are wrapped by the outer wrapping layer to prepare the ternary composite filter stick, the first section of filter element accounts for 1/7 of the whole filter element, and the second section of filter element accounts for 3/7 of the whole filter element.
Example 3
The preparation method of the composite filter rod for the cigarette prepared from the momordica grosvenori leaves comprises the following steps:
freeze-drying the momordica grosvenori leaves for 24 hours, crushing and sieving to form momordica grosvenori leaf powder of 40-60 meshes. Weighing 100 g of momordica grosvenori leaf powder into a 1000 mL volumetric flask, adding 500mL of 90% ethanol, heating by an electric heating jacket until the momordica grosvenori leaf powder is slightly boiled, carrying out reflux extraction for 5 h, carrying out suction filtration, collecting filtrate to obtain momordica grosvenori leaf extract, heating to 45 ℃ for reduced pressure concentration, increasing the heating temperature to 65 ℃ for continuous concentration under the condition that no solvent drips, and keeping for 15 min under the condition that no solvent drips. Removing solvent to obtain extract, freeze drying for 24 hr, pulverizing, and sieving to obtain 40-60 mesh powder. Adding fructus Siraitiae Grosvenorii powder onto fiber tow, bonding the fiber tow with glycerol triacetate, making into first stage filter core, wrapping the filter core with inner wrapping layer to make into flavoring stage, and adding fructus Siraitiae Grosvenorii leaf extract in the first stage filter core at an amount of 0.5% (by mass).
Crushing the freeze-dried momordica grosvenori leaves, sieving to form 100-mesh 120-mesh particles, and wrapping the momordica grosvenori leaf particles by an inner wrapping layer to prepare an adsorption section. The fiber tows are bonded by glycerol triacetate, and then are wrapped by the inner wrapping layer to form the third section of filter element to form the suction section. The three sections of filter elements and the inner wrapping layer are wrapped by the outer wrapping layer to prepare the ternary composite filter stick, the first section of filter element accounts for 1/5 of the whole filter element, and the second section of filter element accounts for 2/5 of the whole filter element.
Application examples
The ternary composite filter stick prepared in the above embodiment is put into a plug assembler for production, and a smoker performs sensory evaluation according to the sensory evaluation method for tobacco and tobacco products GB5606.4-2005, and the results of the sensory evaluation are shown in Table 1.
TABLE 1 influence of different addition amounts of fructus Siraitiae Grosvenorii essential oil on cigarette sensory quality
1 #: comparing cigarettes; 2 #: a cigarette with the filter stick prepared according to the example 1 connected with a section of cigarette; 3 #: a cigarette with the filter stick prepared according to the embodiment 2 connected with a section of cigarette; 4# cigarette with filter stick prepared according to example 3 attached to a section of cigarette.
The results of the smoking test show that: compared with the control cigarette, the 2# and 3# cigarettes are better in overall thought, the irritation is reduced, the offensive odor is reduced, the aftertaste is better, the obvious sweet feeling is achieved, the natural faint scent is achieved, the smoke is elegant and fine, and the cool smell is given to the cigarettes. The 4# sample is slightly reduced compared with the control cigarette because the addition amount of the momordica grosvenori leaves is more, the herbal fragrance of the cigarette is covered, and the aftertaste is poor.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (6)
1. A preparation method of a composite filter rod for cigarettes prepared from momordica grosvenori leaves is characterized by comprising the following steps: the preparation method comprises the steps of taking momordica grosvenori leaves as raw materials, preparing momordica grosvenori leaf particles and momordica grosvenori leaf extract particles, adding the momordica grosvenori leaf extract particles into fiber tows, wrapping the fiber tows by an inner wrapping layer I (1) to prepare a first section of filter core (5), wrapping the momordica grosvenori leaf particles by an inner wrapping layer II (3) to prepare a second section of filter core (6), wrapping cellulose acetate bonded by triacetin by an inner wrapping layer III (4) to prepare a third section of filter core (7), and wrapping the third section of filter core by an outer wrapping layer (2) to form a composite filter stick for cigarettes;
the preparation method of the momordica grosvenori leaf extract particles comprises the following steps:
(1) freeze drying fructus Siraitiae Grosvenorii leaf for 10-48 h, pulverizing, sieving with 40-60 mesh sieve, and reflux extracting to obtain fructus Siraitiae Grosvenorii leaf extractive solution;
(2) concentrating the extractive solution under reduced pressure to obtain folium Momordicae extract, freeze drying, and sieving to obtain folium Momordicae extract granule.
2. The method for preparing a composite filter stick for cigarettes prepared from momordica grosvenori leaves according to claim 1, wherein the method comprises the following steps: the filter element comprises a filter element and a wrapping layer outside the filter element, wherein the wrapping layer comprises an inner wrapping layer and an outer wrapping layer (2), the inner wrapping layer comprises an inner wrapping layer I (1), an inner wrapping layer II (3) and an inner wrapping layer III (4), the filter element comprises three sections of filter elements with different structures, each section of filter element is wrapped by the inner wrapping layer, the first section of filter element (5) is a fiber tow added with momordica grosvenori leaf extract particles, the second section of filter element (6) is momordica grosvenori leaf particles, and the third section of filter element (7) is acetate fibers bonded by triacetin;
the mass percentage of the added momordica grosvenori leaf extract particles in the first section of filter element (5) is 0.01-0.5%;
the length proportion of the first section of filter element (5), the second section of filter element (6) and the third section of filter element (7) is as follows: (35-63):(126-140):(126-140).
3. The method for preparing a composite filter stick for cigarettes prepared from momordica grosvenori leaves according to claim 1, wherein the method comprises the following steps: the inner wrapping layer is three sections of formed paper, and the outer wrapping layer (2) is tipping paper.
4. The method for preparing a composite filter stick for cigarettes prepared from momordica grosvenori leaves according to claim 1, wherein the method comprises the following steps: the momordica grosvenori leaf particles in the second section of filter element (6) are prepared by freeze drying and sieving momordica grosvenori leaves; the particle size of the momordica grosvenori leaves is 100-120 meshes.
5. The method for preparing a composite filter stick for cigarettes prepared from momordica grosvenori leaves according to claim 1, wherein the method comprises the following steps: the organic solvent used in the reflux extraction in the step (1) is petroleum ether, dichloromethane, acetone, methanol, ethanol solution or a mixture thereof, and the reflux extraction time is 0.5-5.0 h.
6. The method for preparing a composite filter stick for cigarettes prepared from momordica grosvenori leaves according to claim 1, wherein the method comprises the following steps: the mass ratio of the organic solvent used in the reflux extraction in the step (1) to the crushed and sieved momordica grosvenori leaves is (5-20): 1.
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| CN201810698566.4A CN108523221B (en) | 2018-06-29 | 2018-06-29 | Composite cigarette filter rod prepared from momordica grosvenori leaves and preparation method thereof |
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| CN201810698566.4A CN108523221B (en) | 2018-06-29 | 2018-06-29 | Composite cigarette filter rod prepared from momordica grosvenori leaves and preparation method thereof |
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| CN108523221A CN108523221A (en) | 2018-09-14 |
| CN108523221B true CN108523221B (en) | 2021-03-23 |
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| CN109537365A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper |
| CN109527643A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
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| CN101692931A (en) * | 2009-09-01 | 2010-04-14 | 广东神农烟科技术有限公司 | Low-harm cigarette containing mogroside and preparation method thereof |
| CN102860584A (en) * | 2012-10-12 | 2013-01-09 | 红云红河烟草(集团)有限责任公司 | Ternary composite filter rod for cigarettes and application of ternary composite filter rod in preparation of cigarettes |
| CN103865647A (en) * | 2012-12-11 | 2014-06-18 | 新昌县冠阳技术开发有限公司 | Oenothera biennis Siraitia grosvenorii tobacco essence perfume |
| CN104509921A (en) * | 2013-09-29 | 2015-04-15 | 桂林永福宏兴生物科技有限责任公司 | Fructus momordicae beverage preparation method |
| CN104762132A (en) * | 2015-03-05 | 2015-07-08 | 云南中烟工业有限责任公司 | Preparation method and application of Siraitia grosvenorii extract |
| CN105266195A (en) * | 2015-11-23 | 2016-01-27 | 江苏大亚滤嘴材料有限公司 | Ternary composite filter stick, and manufacturing method and application thereof |
| CN105767381A (en) * | 2016-04-26 | 2016-07-20 | 杨在侠 | Siraitia grosvenorii herbal tea |
| CN107692312A (en) * | 2017-09-15 | 2018-02-16 | 红云红河烟草(集团)有限责任公司 | Multifunctional cigarette filter tip capable of improving fluid production feeling of cigarette products |
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