CN106912982A - A kind of electronic cigarette tobacco tar and preparation method thereof - Google Patents
A kind of electronic cigarette tobacco tar and preparation method thereof Download PDFInfo
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- CN106912982A CN106912982A CN201710042408.9A CN201710042408A CN106912982A CN 106912982 A CN106912982 A CN 106912982A CN 201710042408 A CN201710042408 A CN 201710042408A CN 106912982 A CN106912982 A CN 106912982A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/287—Chrysanthemum, e.g. daisy
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/534—Mentha (mint)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/60—Moraceae (Mulberry family), e.g. breadfruit or fig
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/63—Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
- A61K36/734—Crataegus (hawthorn)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/752—Citrus, e.g. lime, orange or lemon
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/758—Zanthoxylum, e.g. pricklyash
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/82—Theaceae (Tea family), e.g. camellia
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/888—Araceae (Arum family), e.g. caladium, calla lily or skunk cabbage
- A61K36/8884—Arisaema, e.g. Jack in the pulpit
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Abstract
The invention provides a kind of electronic cigarette tobacco tar, including following mass percent component：90% 99% atomized liquid, 1% 10% Chinese medical extract；Chinese medical extract includes the extract of Chinese medicine material, and Chinese medicine material includes at least one in peppermint, rhizoma arisaematis, Radix zanthoxyli, honeysuckle, chrysanthemum and fig.Contain a certain amount of Chinese medical extract in the electronic cigarette tobacco tar that the present invention is provided, can prepare that fragrance is abundant, comfortable taste, satisfaction are good and with the electronic cigarette tobacco tar of certain functions of relieving cough and reducing phlegm.Present invention also offers a kind of preparation method of electronic cigarette tobacco tar, comprise the following steps：Mass percent is respectively 90% 99% atomized liquid and 1% 10% Chinese medical extract mixes, be stirred at room temperature uniform, the electronic cigarette tobacco tar is obtained；Chinese medical extract includes the extract of Chinese medicine material, and Chinese medicine material includes at least one in peppermint, rhizoma arisaematis, Radix zanthoxyli, honeysuckle, chrysanthemum and fig.Preparation method of the invention is simple to operation, is adapted to industrialization production.
Description
Technical field
The present invention relates to electronic cigarette field, and in particular to a kind of electronic cigarette tobacco tar and preparation method thereof.
Background technology
Electronic cigarette is presented huge market prospects as a kind of form in novel tobacco product, and reason essentially consists in one
It provides the consumption habit and satisfaction similar with traditional cigarette to aspect, and the hazard index of another aspect electronic cigarette compares traditional cigarette
Substantially reduce.The public place management rule that no smoking is put into effect in Chinese increasing city, it is believed that electronic cigarette exists soon
Chinese market can occupy a tiny space.
Electronics smoke product taste in the market is partial to blended type cigarette, and the taste for being more conform with foreign consumers is practised
Used, and Chinese Consumer's preference flue-cured tobacco, taste is more strong, and the mouthfeel of electronic cigarette is extremely difficult to require.Therefore, electronic cigarette is improved
It is to open the important means of Chinese market that tobacco tar formula is allowed to meet Chinese Consumer's custom.
In order to be able to simulate fragrance, fragrance and the mouthfeel of traditional cigarette to the full extent, current electronic cigarette tobacco tar is most common
Be addition tobacco extract, by extracting the tobacco extract and propane diols, glycerine, the flavouring essence for tobacco that obtain according to a certain ratio
Mix, although in the market has various functional electronic cigarette tobacco tar, also not for the preventing phlegm from forming and stopping coughing work(of modern
Can type electronic cigarette tobacco tar.
The content of the invention
In consideration of it, the invention provides a kind of electronic cigarette tobacco tar, Chinese medical extract, Chinese medicine are contained in the electronic cigarette tobacco tar
Extract is extracted by the Chinese medicine material with functions of relieving cough and reducing phlegm and formed, the electronic cigarette tobacco tar good in taste and with resolving sputum
The health-care efficacy of cough-relieving.Present invention also offers the preparation method of the electronic cigarette tobacco tar.
First aspect present invention provide a kind of electronic cigarette tobacco tar, including following mass percent component：
The atomized liquid of 90%-99%, the Chinese medical extract of 1%-10%；
The Chinese medical extract includes the extract of Chinese medicine material, and the Chinese medicine material includes peppermint, rhizoma arisaematis, two sides
At least one in pin, honeysuckle, chrysanthemum and fig.
Wherein, in the electronic cigarette tobacco tar, the mass percent of the Chinese medical extract is 2%-6%.
Wherein, at least one in dried orange peel, sweet osmanthus, hawthorn, green tea, Radix Glycyrrhizae and loquat is also included in the Chinese medicine material.
Wherein, the Chinese medicine material includes the component of following parts by weight：
Peppermint 5-30 parts, rhizoma arisaematis 1-30 parts, Radix zanthoxyli 1-20 parts, honeysuckle 2-20 parts, chrysanthemum 2-20 parts, fig 1-
8 parts, dried orange peel 1-20 parts, sweet osmanthus 1-10 parts, hawthorn 1-10 parts, green tea 2-15 parts, Radix Glycyrrhizae 1-12 parts, criticize 1-15 parts.
Wherein, the Chinese medical extract extracts obtain in accordance with the following steps：After the Chinese medicine material is crushed, add and extract
Solvent is soaked, refluxing extraction, obtains extract solution；To be concentrated after extract solution centrifugation, filtering, obtain final product the traditional Chinese medicine extraction
Thing.
Wherein, the Chinese medicine material and the mass ratio of the Extraction solvent are 1:5-1:15, the soak time is 1-3h,
The soaking temperature is 40 DEG C -60 DEG C, and the reflux extracting time is 2-6h.
Wherein, after the Chinese medicine material is crushed, add Extraction solvent to carry out first time immersion, carried out after immersion for the first time
Refluxing extraction, obtains the first extract solution and filter residue after filtering；The mass ratio of the Chinese medicine material and the Extraction solvent is 1:8-
1:10, first time soak time is 2-3h, and first time reflux extracting time is 3.5-5h；
Second immersion is carried out to the filter residue addition Extraction solvent, second refluxing extraction, mistake are carried out after immersion
The second extract solution is obtained after filter；The mass ratio of the filter residue and the Extraction solvent is 1:5-1:8, second soak time is 1-
2h, second reflux extracting time is 2-3.5h；
Merge first extract solution and second extract solution, supernatant is obtained after centrifugation, by the supernatant liquid filtering
After obtain filtrate, obtain the Chinese medical extract after the filtrate decompression concentration.
Wherein, the Extraction solvent includes that carbon number is C2-C5Alcohols solvent, C3-C7Lipid solvent or C3-C7's
The mixed solvent of at least one and water in ketone solvent.
Wherein, the atomized liquid includes tobacco extract, flavouring essence for tobacco, deionized water and organic solvent, described organic molten
Agent includes at least one in propane diols and glycerine.
Contain a certain amount of Chinese medical extract, the electronic cigarette salted cake fried in sesame oil in the electronic cigarette tobacco tar that first aspect present invention is provided
Gas is abundant, comfortable taste, satisfaction are good and with certain functions of relieving cough and reducing phlegm.
Second aspect present invention provides a kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
The Chinese medical extract of mass percent is respectively into 90%-99% atomized liquid and 1%-10% mixes, in room temperature
Under stir, be obtained the electronic cigarette tobacco tar；The Chinese medical extract includes the extract of Chinese medicine material, the Chinese medicine material
Including at least one in peppermint, rhizoma arisaematis, Radix zanthoxyli, honeysuckle, chrysanthemum and fig.
The preparation method of the electronic cigarette tobacco tar that second aspect present invention is provided, by the way that atomized liquid and Chinese medical extract etc. is several
Kind of component is simply mixed, and mouthfeel has been obtained gentle, comfortable and with fragrance is abundant, comfortable taste, satisfaction are good and with one
Determine the electronic cigarette tobacco tar of functions of relieving cough and reducing phlegm.Preparation method of the invention is simple to operation simultaneously, is adapted to industrialization production.
To sum up, beneficial effect of the present invention includes the following aspects：
1st, not only there is the electronic cigarette tobacco tar that the present invention is provided fragrance to enrich, gently comfortable, satisfaction is good for mouthfeel
Advantage, also with health-care efficacies such as preventing phlegm from forming and stopping coughing.
2nd, the preparation method of the electronic cigarette tobacco tar that the present invention is provided is simple to operation, is adapted to industrialization production.
Specific embodiment
As described below is the preferred embodiment of the present invention, it is noted that for those skilled in the art
For, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications are also considered as
Protection scope of the present invention.
Embodiment of the present invention first aspect provide a kind of electronic cigarette tobacco tar, including following mass percent component：
The atomized liquid of 90%-99%, the Chinese medical extract of 1%-10%；
The Chinese medical extract includes the extract of Chinese medicine material, and the Chinese medicine material includes peppermint, rhizoma arisaematis, two sides
At least one in pin, honeysuckle, chrysanthemum and fig.
In an embodiment of the present invention, atomized liquid includes tobacco extract, flavouring essence for tobacco, deionized water and organic solvent,
The organic solvent includes at least one in propane diols and glycerine.
In an embodiment of the present invention, the tobacco extract is conventional tobacco extract；Such as, including non-nitrogen containing chemical combination
Thing, nitrogen-containing compound, mineral matter and tobacco flavor material etc.；Wherein, non-nitrogen containing compound includes monosaccharide and disaccharide, starch, organic
Acid, phenols, lipid, sterols, terpenoid, cellulose and pectic substance etc.；Tobacco flavor material includes organic acid, phenol
Class, lipid, sterols and terpenoid.Alternatively, in electronic cigarette tobacco tar, the mass percent of tobacco extract is 1%-
15%.Still optionally further, the mass percent of tobacco extract is 1.5%-4%.Specifically, tobacco extract selects Yunnan
Pure tobacco oil.
In an embodiment of the present invention, flavouring essence for tobacco includes Ethyl vanillin, ethylmaltol, citronellol, geraniol, virtue
At least one of camphor tree alcohol, rhodinol, dorinone, Megastigmatrienone, dihydroactinidiolide and alpha, beta-lonone.Flavouring essence for tobacco
It is to specialize in each tobacco articles perfuming flavoring to use, makes tobacco product that a system of growing tobacco of good flue gas effect is produced when burning and sucking
The additive of product, therefore proportioning to flavouring essence for tobacco in electronics tobacco tar is particularly significant.Alternatively, in electronic cigarette tobacco tar, cigarette is used
The mass percent of essence is 1%-15%.Still optionally further, in electronic cigarette tobacco tar, the mass percent of flavouring essence for tobacco is
2.5%-3.5%.
In an embodiment of the present invention, in electronic cigarette tobacco tar, the mass percent of deionized water is 0.5%-4%, optional
Ground, the mass percent of deionized water is 0.5%-1.5%.
In an embodiment of the present invention, propane diols, glycerine are food grade or pharmaceutical grade product.Alternatively, electronic cigarette
In tobacco tar, the mass percent of propane diols is 50%-85%, and the mass percent of glycerine is 5%-35%.It is further optional
Ground, the mass percent of propane diols is 55%-80%, and the mass percent of glycerine is 10%-34%.
In an embodiment of the present invention, electronic cigarette tobacco tar includes the component of following mass percent：Propane diols 50%-
85%, glycerine 5%-35%, tobacco extract 1%-5%, flavouring essence for tobacco 1%-5%, Chinese medical extract 1%-10%.
In an embodiment of the present invention, in the electronic cigarette tobacco tar, the mass percent of the Chinese medical extract is 2%-
6%.
In an embodiment of the present invention, the Chinese medicine material includes peppermint, rhizoma arisaematis, Radix zanthoxyli, honeysuckle, chrysanthemum and nothing
At least one in flowers and fruits.Alternatively, the Chinese medicine material includes peppermint 5-30 parts, rhizoma arisaematis 1-30 parts, Radix zanthoxyli 1-20 parts,
Honeysuckle 2-20 parts, chrysanthemum 2-20 parts, fig 1-20 parts.Still optionally further, Chinese medicine material also includes dried orange peel, sweet osmanthus, mountain
At least one in short, bristly hair or beard, green tea, Radix Glycyrrhizae, loquat.At least one in dried orange peel, sweet osmanthus, hawthorn, green tea, Radix Glycyrrhizae, loquat is used as auxiliary
The main ingredients such as medicine and at least one in peppermint, rhizoma arisaematis, Radix zanthoxyli, honeysuckle, chrysanthemum and fig mix, alternatively, described
Chinese medicine material includes the component of following parts by weight：
Peppermint 5-30 parts, rhizoma arisaematis 1-30 parts, Radix zanthoxyli 1-20 parts, honeysuckle 2-20 parts, chrysanthemum 2-20 parts, fig 1-
8 parts, dried orange peel 1-20 parts, sweet osmanthus 1-10 parts, hawthorn 1-10 parts, green tea 2-15 parts, Radix Glycyrrhizae 1-12 parts, criticize 1-15 parts.
Alternatively, the Chinese medicine material can also include the component of following parts by weight：Peppermint 5-25 parts, rhizoma arisaematis 5-20
Part, Radix zanthoxyli 1-15 parts, honeysuckle 2-20 parts, chrysanthemum 2-20 parts, fig 1-8 parts, dried orange peel 5-15 parts, sweet osmanthus 1-10 parts, mountain
Short, bristly hair or beard 1-8 parts, green tea 2-15 parts, Radix Glycyrrhizae 1-10 parts, criticize 1-15 parts.
The Chinese medicine property of the Chinese medicine material each component is：
Peppermint：The pungent energy of nature and flavor dissipates, cool in nature and clear, and the meeting of the sun of tonneau six is first, dispels the ailment said due to cold or exposure of all heat.Take its property sharp and light
Clearly, benefaction head, with aphonia is controlled, treat ability to speak, clearing throat.
Rhizoma arisaematis：Bitter, it is pungent, it is warm in nature.There are expelling wind and relieving convulsion, effect of reducing phlegm and resolving masses.
Radix zanthoxyli：Promoting qi circulation and relieving pain, promoting blood circulation and removing blood stasis, dispelling wind and removing obstruction in the meridians.Cure mainly the traumatic injury that qi depression to blood stasis causes, rheumatism numbness
Bitterly, have a stomachache, toothache, venomous snake bite；Control the burning hot wound of soup outward.
Honeysuckle：It is clearing heat and detoxicating, wind-heat dissipating.For carbuncle swells furunculosis, larynx numbness, erysipelas, toxic-heat and blood stasis, anemopyretic cold, temperature
Disease heating.
Chrysanthemum：Dispelling wind, heat-clearing, improving eyesight, removing toxic substances.Control headache, dizziness, hot eyes, ambition dysphoria with smothery sensation, furunculosis, pyogenic infections.
Fig：Clearing heat and promoting fluid；Spleen benefiting and stimulating the appetite；Removing toxicity for detumescence.Main abscess of throat；Cough caused by dryness trachyphonia；Milk is rare；Intestines heat is just
It is secret；Poor appetite；Indigestion, dysentery；Carbuncle swells；Tinea.
Dried orange peel：Bitter, pungent, regulating qi-flowing for strengthening spleen warm in nature, eliminating dampness and eliminating phlegm for abdominal fullness and distention, deficiency of food is vomited and diarrhoea, coughing with a lot of sputum.
Sweet osmanthus：The broken knot of cold dispelling, preventing phlegm from forming and stopping coughing.For having a toothache, cough and phlegm, Amenorrhea stomachache
Hawthorn：Food digesting stomach fortifying, scattered stasis change turbid lipid-loweringing, for meat stagnation, gastral cavilty turgor, diarrhea dysentery abdominal pain, hemostasis warp
Close, postpartum stasis, confidant sting, chest impediment and cardialgia, hernia pain, hyperlipidemia.
Green tea：Refresh oneself, relieving thirst and restlessness, resolving sputum helps digestion, and diuresis is clearing heat and detoxicating.For having a headache, blurred vision is slept more, and thinking is not
Clearly, restlessness and thirst, dyspepsia phlegm is stagnant, dysentery, difficult urination.And have a reducing blood lipid, anti-aging, anti-cancer, firm tooth, beautiful appearance it
Effect.
Radix Glycyrrhizae：Invigorate the spleen and benefit qi, clearing heat and detoxicating, expelling phlegm and arresting coughing, relieving spasm to stop pain, coordinating the drug actions of a prescription.For weakness of the spleen and the stomach, burnout is weary
Power, palpitation, coughing with a lot of sputum, gastral cavity abdomen, four limbs contraction, carbuncle sore tumefacting virus alleviate drug toxicity, strong.
Loquat：Clearing lung-heat promotes the production of body fluid to quench thirst, expelling phlegm and arresting coughing, harmonizing stomach and lowering adverse Qi；For treating lung heat and coughing, chronic cough is not healed, dry throat
The illnesss such as thirsty and stomach unsaturated vapor.
The Chinese medicine that embodiment of the present invention is provided not only has certain characteristic flavor compounds, while also having different pharmacology
Effect.The above-mentioned plant with different pharmacological actions is rationally preferred by traditional Chinese medical science prescription formula.
It is main body Chinese medicine with peppermint, rhizoma arisaematis, Radix zanthoxyli, honeysuckle, chrysanthemum and fig in embodiment of the present invention,
The first-selected phlegm that stops of main body Chinese medicine coughs the substantially prominent raw material of effect, and arrange in pairs or groups dried orange peel, sweet osmanthus, hawthorn, green tea, Radix Glycyrrhizae, loquat etc. are auxiliary
Medicine, they influence each other, synergy, and each raw material synergy is good so as to play can play maximum effect
Functions of relieving cough and reducing phlegm, and its raw material is simple, with low cost.
, it is necessary to explanation, can individually extract various Chinese medicine materials, by each extract in an embodiment of the present invention
It is mixed to get Chinese medical extract, it is also possible to again extract obtaining Chinese medical extract after various Chinese medicine materials are mixed.Alternatively,
The Chinese medical extract extracts obtain in accordance with the following steps：After the Chinese medicine material is crushed, add Extraction solvent to be soaked,
Refluxing extraction obtains extract solution；To be concentrated after extract solution centrifugation, filtering, obtain final product the Chinese medical extract.Alternatively, it is described
Chinese medicine material is 1 with the mass ratio of Extraction solvent:5-1:15, the soak time is 1-3h, and soaking temperature is 40 DEG C -60 DEG C,
The reflux extracting time is 2-6h.Specifically, the Chinese medical extract extracts obtain in accordance with the following steps：
After the Chinese medicine material is crushed, add Extraction solvent to carry out first time immersion, first time backflow is carried out after immersion
Extract, the first extract solution and filter residue are obtained after filtering；The mass ratio of the Chinese medicine material and the Extraction solvent is 1:8-1:10,
First time soak time is 2-3h, and first time reflux extracting time is 3.5-5h；
Second immersion is carried out to the filter residue addition Extraction solvent, second refluxing extraction, mistake are carried out after immersion
The second extract solution is obtained after filter；The mass ratio of the filter residue and the Extraction solvent is 1:5-1:8, second soak time is 1-
2h, second reflux extracting time is 2-3.5h；
Merge first extract solution and second extract solution, supernatant is obtained after centrifugation, by the supernatant liquid filtering
After obtain filtrate, obtain the Chinese medical extract after the filtrate decompression concentration.
In an embodiment of the present invention, the Extraction solvent includes that carbon number is C2-C5Alcohols solvent, C3-C7Fat
Class solvent or C3-C7Ketone solvent at least one mixed solvent with water.Still optionally further, Extraction solvent includes ethanol
The mixed solvent formed with water, in Extraction solvent, the volume fraction of ethanol is 60%-95%, still optionally further, Extraction solvent
In, the volume fraction of ethanol is 75%-90%.
In an embodiment of the present invention, the temperature that is concentrated under reduced pressure is 50 DEG C -90 DEG C.Still optionally further, be concentrated under reduced pressure temperature
It is 60 DEG C -80 DEG C.Alternatively, filtrate obtains the Chinese medical extract of 30mL-40mL after being concentrated under reduced pressure.
In an embodiment of the present invention, the speed of centrifugation is 3000-4000r/min.
In an embodiment of the present invention, it is 0.45 μm to filter used filter sizes.
In embodiment of the present invention, electronic cigarette tobacco tar includes atomized liquid and Chinese medical extract, and Chinese medical extract includes having
The extract of the Chinese medicine material of functions of relieving cough and reducing phlegm, when in use, Chinese medical extract leads to the electronic cigarette tobacco tar with atomized liquid
Gasify after the atomizer heating for crossing electronic cigarette, drawn by human body, so as to quickly be absorbed, reach effect of preventing phlegm from forming and stopping coughing.This hair
It is bright to be mixed it with tobacco extract by preparing the extract with functions of relieving cough and reducing phlegm, it is aided with fragrant using suitable cigarette
Smart spices is modified, and can prepare that fragrance is abundant, comfortable taste, satisfaction are good and with certain functions of relieving cough and reducing phlegm
Electronic cigarette tobacco tar.
The electronic cigarette tobacco tar that embodiment of the present invention first aspect is provided, is combined by by Chinese medical extract with atomized liquid,
The not enough shortcoming of electronic cigarette tobacco tar taste composition is compensate for a certain extent, while being different from external electronic cigarette tobacco tar, can be built
The electronic cigarette tobacco tar of Chinese style characteristic, meets consumer's custom, while providing the health-care effect of functions of relieving cough and reducing phlegm, allows consumer to take out
Possess pure and fresh straightforward mouthfeel after complete, remove cavity interior point phlegm and foreign odor material, improve oral environment.Can press down simultaneously
Donsole chamber bacteria breed, keeps oral cavity fresh and cool happy.
Second aspect present invention provides a kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
The Chinese medical extract of mass percent is respectively into 90%-99% atomized liquid and 1%-10% mixes, in room temperature
Under stir, be obtained the electronic cigarette tobacco tar；The Chinese medical extract includes the extract of Chinese medicine material, the Chinese medicine material
Including at least one in peppermint, rhizoma arisaematis, Radix zanthoxyli, honeysuckle, chrysanthemum and fig.
In an embodiment of the present invention, the flavouring essence for tobacco is added in the organic solvent, at room temperature stirring and dissolving
20-30min, obtains mixed solution, is subsequently adding the tobacco extract, deionized water and Chinese medical extract and is stirred until homogeneous,
The electronic cigarette tobacco tar is obtained.
The preparation method of the electronic cigarette tobacco tar that second aspect present invention is provided, by by the letter of atomized liquid and Chinese medical extract
Single mixing, has been obtained that mouthfeel is gentle, the comfortable and electronic cigarette tobacco tar with functions of relieving cough and reducing phlegm, while preparation method of the invention
It is simple to operation, it is adapted to industrialization production.
Embodiment 1：
A kind of electronic cigarette tobacco tar, including following mass percent component：
Propane diols 70%, glycerine 20%, tobacco extract 3.5%, flavouring essence for tobacco 3%, deionized water 1%, Chinese medicine is carried
Take thing 2.5%.The flavouring essence for tobacco be Ethyl vanillin, ethylmaltol, citronellol, geraniol, linalool, rhodinol, β-
Damascenone, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone.
The preparation method of above-mentioned electronic cigarette tobacco tar, comprises the following steps：
(1) preparation of Chinese medical extract：
Peppermint (40g), rhizoma arisaematis (50g), Radix zanthoxyli (4g), honeysuckle (20g), chrysanthemum (16g), fig are weighed respectively
(10g), dried orange peel (6g), sweet osmanthus (10g), hawthorn (2g), green tea (16g), Radix Glycyrrhizae (16g), loquat (10g).Size-reduced machine grinds
60 mesh sieves are crossed afterwards, is inserted in round-bottomed flask after being well mixed, be 1 by feed liquid mass ratio:10 add 2000mL Extraction solvents, extract
Solvent is that second alcohol and water is 80% according to volume ratio:20% is mixed to get.After 40 DEG C of immersion 3h, backflow 4.5h is reheated, filtered,
Obtain the first extract solution and filter residue.Filter residue is 1 by feed liquid mass ratio:6 add 1200mL Extraction solvents to soak 1.5h, and Extraction solvent is
Second alcohol and water is 80% according to volume ratio:20% is mixed to get.Refluxing extraction 2.5h, filtering, obtains the second extract solution.Merge twice
Extract solution, is that 4000r/min is centrifuged to obtain supernatant with eccentricity, and supernatant membrane aperture is 0.45 μm of membrane filtration, filtrate in
80 DEG C are concentrated under reduced pressure into 32mL, and gained brown liquid is Chinese medical extract.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (70g) and glycerine are separately added into
Ethyl vanillin (0.24g), ethylmaltol (0.3g), citronellol (0.15g), geraniol are sequentially added under (20g), stirring
(0.15g), linalool (0.45g), rhodinol (0.3g), dorinone (0.21g), Megastigmatrienone (0.45g), dihydro macaque
Peach lactone (0.3g), alpha, beta-lonone (0.45g).Stir 30 minutes at room temperature, after dissolving, addition tobacco extract (3.5g),
Deionized water (1g) and Chinese medical extract (2.5g) are well mixed and obtain final product the electronic cigarette tobacco tar with functions of relieving cough and reducing phlegm.
Embodiment 2：
A kind of electronic cigarette tobacco tar, including following mass percent component：
Propane diols 80%, glycerine 10%, tobacco extract 2.5%, flavouring essence for tobacco 3.5%, deionized water 1%, Chinese medicine
Extract 3%.The flavouring essence for tobacco be Ethyl vanillin, ethylmaltol, citronellol, geraniol, linalool, rhodinol, β-
Damascenone, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone.
The preparation method of above-mentioned electronic cigarette tobacco tar, comprises the following steps：
(1) preparation of Chinese medical extract：
Weigh respectively peppermint (50g), rhizoma arisaematis (50g), Radix zanthoxyli (16g), honeysuckle (16g), chrysanthemum (10g), without flower
Really (12g), dried orange peel (6g), sweet osmanthus (10g), hawthorn (4g), green tea (10g), Radix Glycyrrhizae (6g), loquat (10g).Size-reduced machine grinds
60 mesh sieves are crossed afterwards, are inserted in round-bottomed flask after being well mixed, by feed liquid mass ratio 1:10 add 2000mL Extraction solvents, extract molten
Agent is that second alcohol and water is 80% according to volume ratio:20% is mixed to get.After 40 DEG C of immersion 3h, backflow 4.5h is reheated, filtering is obtained
First extract solution.Filter residue presses feed liquid mass ratio 1:6 add 1200mL Extraction solvents immersion 1.5h, Extraction solvent to be pressed for second alcohol and water
It is 80% according to volume ratio:20% is mixed to get.Refluxing extraction 2.5h, filtering, obtains the second extract solution.Merge extract solution twice, use
Eccentricity is centrifuged to obtain supernatant for 4000r/min, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is dense in 80 DEG C of decompressions
32mL is reduced to, gained brown liquid is Chinese medical extract.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (80g) and glycerine are separately added into
Ethyl vanillin (0.28g), ethylmaltol (0.35g), citronellol (0.175g), geraniol are sequentially added under (10g), stirring
(0.175g), linalool (0.525g), rhodinol (0.35g), dorinone (0.245g), Megastigmatrienone (0.525g), two
Hydrogen actinidia lactone (0.35g), alpha, beta-lonone (0.525g).Stir 30 minutes at room temperature, after dissolving, add tobacco extract
(2.5g), deionized water (1g) and Chinese medical extract (3g) are well mixed and obtain final product the electronic cigarette with functions of relieving cough and reducing phlegm
Oil.
Embodiment 3：
A kind of electronic cigarette tobacco tar, including following mass percent component：
Propane diols 64%, glycerine 25%, tobacco extract 2.5%, flavouring essence for tobacco 4%, deionized water 1.5%, Chinese medicine
Extract 3%.The flavouring essence for tobacco be Ethyl vanillin, ethylmaltol, citronellol, geraniol, linalool, rhodinol, β-
Damascenone, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone.
The preparation method of above-mentioned electronic cigarette tobacco tar, comprises the following steps：
(1) preparation of Chinese medical extract：
Weigh respectively peppermint (40g), rhizoma arisaematis (40g), Radix zanthoxyli (20g), honeysuckle (20g), chrysanthemum (20g), without flower
Really (8g), dried orange peel (12g), sweet osmanthus (10g), hawthorn (2g), green tea (12g), Radix Glycyrrhizae (6g), loquat (10g).Size-reduced machine grinds
60 mesh sieves are crossed afterwards, are inserted in round-bottomed flask after being well mixed, by feed liquid mass ratio 1:10 add 2000mL Extraction solvents, extract molten
Agent is that second alcohol and water is 80% according to volume ratio:20% is mixed to get.After 60 DEG C of immersion 3h, backflow 4.5h is reheated, filtering is obtained
First extract solution.Filter residue presses feed liquid mass ratio 1:6 add 1200mL Extraction solvents immersion 1.5h, Extraction solvent to be pressed for second alcohol and water
It is 80% according to volume ratio:20% is mixed to get.Refluxing extraction 2.5h, filtering, obtains the second extract solution.Merge extract solution twice, use
Eccentricity is centrifuged to obtain supernatant for 4000r/min, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is dense in 80 DEG C of decompressions
32mL is reduced to, gained brown liquid is Chinese medical extract.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (64g) and glycerine are separately added into
Ethyl vanillin (0.32g), ethylmaltol (0.4g), citronellol (0.2g), geraniol are sequentially added under (25g), stirring
(0.2g), linalool (0.6g), rhodinol (0.4g), dorinone (0.28g), Megastigmatrienone (0.6g), dihydro-actinidia
Lactone (0.4g), alpha, beta-lonone (0.6g).At room temperature stir 30 minutes, after dissolving, add tobacco extract (2.5g), go from
Sub- water (1.5g) and Chinese medical extract (3g) are well mixed and obtain final product the electronic cigarette tobacco tar with functions of relieving cough and reducing phlegm.
Embodiment 4：
A kind of electronic cigarette tobacco tar, including following mass percent component：
Propane diols 55%, glycerine 34%, tobacco extract 4%, flavouring essence for tobacco 2.5%, deionized water 0.5%, Chinese medicine
Extract 4%.The flavouring essence for tobacco be Ethyl vanillin, ethylmaltol, citronellol, geraniol, linalool, rhodinol, β-
Damascenone, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone.
The preparation method of above-mentioned electronic cigarette tobacco tar, comprises the following steps：
(1) preparation of Chinese medical extract：
Peppermint (40g), rhizoma arisaematis (60g), Radix zanthoxyli (2g), honeysuckle (12g), chrysanthemum (18g), fig are weighed respectively
(10g), dried orange peel (10g), sweet osmanthus (10g), hawthorn (2g), green tea (10g), Radix Glycyrrhizae (8g), loquat (10g).Size-reduced machine grinds
60 mesh sieves are crossed afterwards, are inserted in round-bottomed flask after being well mixed, by feed liquid mass ratio 1：10 add 2000mL Extraction solvents, extract molten
Agent is that second alcohol and water is 80% according to volume ratio:20% is mixed to get.After 50 DEG C of immersion 3h, backflow 4.5h is reheated, filtering is obtained
First extract solution.Filter residue presses feed liquid mass ratio 1:6 add 1200mL Extraction solvents immersion 1.5h, Extraction solvent to be pressed for second alcohol and water
It is 80% according to volume ratio:20% is mixed to get.Refluxing extraction 2.5h, filtering, obtains the second extract solution.Merge extract solution twice, use
Eccentricity is centrifuged to obtain supernatant for 4000r/min, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is dense in 80 DEG C of decompressions
32mL is reduced to, gained brown liquid is Chinese medical extract.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (55g) and glycerine are separately added into
Ethyl vanillin (0.2g), ethylmaltol (0.25g), citronellol (0.125g), geraniol are sequentially added under (34g), stirring
(0.125g), linalool (0.375g), rhodinol (0.25g), dorinone (0.175g), Megastigmatrienone (0.375g), two
Hydrogen actinidia lactone (0.25g), alpha, beta-lonone (0.375g).Stir 30 minutes at room temperature, after dissolving, add tobacco extract
(4g), deionized water (0.5g) and Chinese medical extract (4g) are well mixed and obtain final product the electronic cigarette with functions of relieving cough and reducing phlegm
Oil.
Embodiment 5：
Electronic cigarette tobacco tar in above-described embodiment is added in electronic cigarette device carries out sensory effects evaluation respectively.
Sensory effects evaluation method is comprised the following steps：
There is provided 6 evaluation indexes, including excitant, satisfaction, feature style, tobacco perfume, fragrance and smoke amount, and root
According to every evaluation index different score values are assigned to the Different Effects degree of electronic cigarette tobacco tar aesthetic quality.
The excitant refers to：Suction electronic cigarette tobacco tar includes oral cavity, throat through the flue gas that atomization is produced to sense organ
The discomfort produced with nasal cavity is received；
The satisfaction refers to：Flue gas strength, concentration and the note that electronic cigarette tobacco tar is produced through atomization are on sense organ
The comprehensive impression of generation；
The feature style refers to：A kind of electronic cigarette tobacco tar is different from the sense of other homogeneous e cigarette tobacco tar in pleasant feeling
Official's Main Differences are showed；
The tobacco perfume (or spice) refers to：Sensory feel this fragrant breath to tobacco during smokeing panel test；
The fragrance refers to：The good and bad degree of pleasant breath is felt during smokeing panel test by smell and the sense of taste；
The smoke amount refers to：Electronic cigarette tobacco tar through atomization produce exhaust gas volumn number.
The member of smoking of 9 people is set, everyone a electronic cigarette tobacco tar sensory quality assessment table, using the marking mode secretly commented,
Smoked panel test method using overall circulation, electronic cigarette tobacco tar is aspirated, according to 6 sensory quality assessment index score values in table 1
Implication, comprehensive grading is carried out to the aesthetic quality of electronic cigarette tobacco tar using hundred-mark system point system, every evaluation index by 15 or
20 system scorings.
The electronic cigarette tobacco tar sensory quality assessment index of table 1 and score value implication table
Evaluation method：Evaluation index and score value in table 1, member of smoking should carry out aesthetic quality to each evaluation index
Evaluate, and record its evaluation result, the minimum score unit of score value is 0.5.
Result is counted：Remove one minimum point and a best result in the sensory quality assessment result of all members of smoking, count
The arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring is calculated, as a result retains two-decimal, the sense of last electronic cigarette tobacco tar
Official's quality evaluation comprehensive grading is the arithmetic mean of instantaneous value sum for calculating each single index scoring, obtains total score, as a result retains one
Decimal, above-described embodiment comparative evaluation the results are shown in Table 2.
The electronic cigarette tobacco tar sensory effects evaluation result of table 2
| Evaluation index | Excitant | Satisfaction | Feature style | Tobacco is fragrant | Fragrance | Smoke amount | Total score |
| Embodiment 1 | 15.2 | 16.2 | 11.73 | 12.22 | 11.85 | 11.5 | 78.7 |
| Embodiment 2 | 15.05 | 16.4 | 11.82 | 12.0 | 11.9 | 11.42 | 78.6 |
| Embodiment 3 | 15.1 | 16.1 | 11.65 | 11.98 | 11.73 | 11.45 | 78.0 |
| Embodiment 4 | 14.89 | 16.15 | 11.59 | 12.05 | 11.65 | 11.5 | 77.8 |
The result of table 2 shows that smoke amount is sufficient when electronic cigarette tobacco tar is embodied in suction in above-described embodiment, and fragrance enriches
Strong, tobacco and faint medicine perfume are coordinated, and strength is moderate, and comfortable taste shortens the aesthetic quality's difference with traditional cigarette.But institute
9 indexs of the Chinese medicine species, extract adding proportion, flavouring essence for tobacco adding proportion for using to being used produce Different Effects；
Chinese medical extract used can provide the action and efficacies such as preventing phlegm from forming and stopping coughing simultaneously.
Embodiment described above only expresses several embodiments of the invention, and its description is more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to guarantor of the invention
Shield scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (10)
1. a kind of electronic cigarette tobacco tar, it is characterised in that the component including following mass percent：
The atomized liquid of 90%-99%, the Chinese medical extract of 1%-10%；
The Chinese medical extract includes the extract of Chinese medicine material, and the Chinese medicine material includes peppermint, rhizoma arisaematis, Radix zanthoxyli, gold
At least one in honeysuckle flower, chrysanthemum and fig.
2. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that in the electronic cigarette tobacco tar, the Chinese medical extract
Mass percent be 2%-6%.
3. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that the Chinese medicine material also includes dried orange peel, sweet osmanthus, mountain
At least one in short, bristly hair or beard, green tea, Radix Glycyrrhizae and loquat.
4. electronic cigarette tobacco tar as claimed in claim 3, it is characterised in that the Chinese medicine material includes the group of following parts by weight
Point：
Peppermint 5-30 parts, rhizoma arisaematis 1-30 parts, Radix zanthoxyli 1-20 parts, honeysuckle 2-20 parts, chrysanthemum 2-20 parts, fig 1-8 parts,
Dried orange peel 1-20 parts, sweet osmanthus 1-10 parts, hawthorn 1-10 parts, green tea 2-15 parts, Radix Glycyrrhizae 1-12 parts, criticize 1-15 parts.
5. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that the Chinese medical extract is extracted in accordance with the following steps
Arrive：After the Chinese medicine material is crushed, addition Extraction solvent is soaked, refluxing extraction, obtains extract solution；By the extract solution
Concentrated after centrifugation, filtering, obtain final product the Chinese medical extract.
6. electronic cigarette tobacco tar as claimed in claim 5, it is characterised in that the quality of the Chinese medicine material and the Extraction solvent
Than being 1:5-1:15, the soak time is 1-3h, and the soaking temperature is 40 DEG C -60 DEG C, and the reflux extracting time is 2-
6h。
7. electronic cigarette tobacco tar as claimed in claim 5, it is characterised in that the Chinese medical extract is extracted in accordance with the following steps
Arrive：
After the Chinese medicine material is crushed, add Extraction solvent to carry out first time immersion, first time refluxing extraction carried out after immersion,
The first extract solution and filter residue are obtained after filtering；The mass ratio of the Chinese medicine material and the Extraction solvent is 1:8-1:10, first
Secondary soak time is 2-3h, and first time reflux extracting time is 3.5-5h；
Second immersion is carried out to the filter residue addition Extraction solvent, second refluxing extraction is carried out after immersion, after filtering
Obtain the second extract solution；The mass ratio of the filter residue and the Extraction solvent is 1:5-1:8, second soak time is 1-2h,
Second reflux extracting time is 2-3.5h；
Merge first extract solution and second extract solution, supernatant is obtained after centrifugation, will be obtained after the supernatant liquid filtering
To filtrate, the Chinese medical extract is obtained after the filtrate decompression concentration.
8. electronic cigarette tobacco tar as claimed in claim 5, it is characterised in that the Extraction solvent includes that carbon number is C2-C5's
Alcohols solvent, C3-C7Lipid solvent or C3-C7Ketone solvent at least one mixed solvent with water.
9. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that the atomized liquid includes tobacco extract, cigarette perfume
Essence, deionized water and organic solvent, the organic solvent include at least one in propane diols and glycerine.
10. a kind of preparation method of electronic cigarette tobacco tar, it is characterised in that comprise the following steps：
The Chinese medical extract of mass percent is respectively into 90%-99% atomized liquid and 1%-10% mixes, and stirs at room temperature
Mix uniform, the electronic cigarette tobacco tar is obtained；The Chinese medical extract includes the extract of Chinese medicine material, and the Chinese medicine material includes
At least one in peppermint, rhizoma arisaematis, Radix zanthoxyli, honeysuckle, chrysanthemum and fig.
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