CN106753790A - Uniform, stable tobacco aromaticss of fragrance and preparation method thereof - Google Patents
Uniform, stable tobacco aromaticss of fragrance and preparation method thereof Download PDFInfo
- Publication number
- CN106753790A CN106753790A CN201611100818.6A CN201611100818A CN106753790A CN 106753790 A CN106753790 A CN 106753790A CN 201611100818 A CN201611100818 A CN 201611100818A CN 106753790 A CN106753790 A CN 106753790A
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- parts
- uniform
- fragrance
- root
- raw material
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Botany (AREA)
- General Chemical & Material Sciences (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention discloses a kind of uniform, the stable tobacco aromaticss of fragrance, it is that natural plant raw material is obtained into enzymolysis liquid through enzyme digestion reaction first, ultrasonically treated, centrifugation after most being extracted through ethanol afterwards after absolute ethyl alcohol is subsequently adding, clear liquid is collected and is prepared from through vacuum distillation concentration；The natural plant raw material is counted by weight, including：1~3 part of 5~10 parts of balloonflower root, 8~15 parts of Radix Angelicae Sinensis, 2~5 parts of jujube, 10~15 parts of honeysuckle, 5~10 parts of Radix Glycyrrhizae, 10~20 parts of ginkgo, 2~5 parts of grape pip, 1~3 part of Poria cocos, 1~3 part of root of couch grass, 6~10 parts of Momordica grosvenori, 1~3 part of American aloe, 10~15 parts of the tuber of dwarf lilyturf and fritillaria thunbergii.Balloonflower root is with the addition of, balloonflower root contains substantial amounts of glycoside material, and the fragrance of spices comes from alcohols material mostly, and the stability that glucosides can be achieved on alcohols material is uniform with release.
Description
Technical field
The present invention relates to tobacco additive agent technical field, a kind of tobacco aromaticss of, stabilization uniform in particular to fragrance and its
Preparation method.
Background technology
Blending technology is the core of essence and flavoring agent technology, and various perfume materials are carried out group by it according to certain ratio and compatibility
Close, so as to reach specific fragrance characteristic and functional effect, cigarette odor-absorbing can be significantly improved, and assign the specific of cigarette grace
Style.And the security of smoking is improved, reduce by one that other harmful components in tar content and flue gas are Chinese-style cigarette research
Important directions.But many fragrance matters in tobacco are but present among tar, along with the reduction of tar content, smoke becomes
Light, fragrance is reduced, and cigarette product keeps not losing original style, just can more be received by consumer.Therefore, cigarette is being reduced
While tar, flavouring and improve flue gas concentration and fragrance, so as to improve the inherent quality of Chinese-style cigarette product, also only by
In the scientific and technological content of flavoring and casing technology.But there is release during cigarette combustion in the essence and flavoring agent of addition mostly at present
Fragrance is uneven, over time, the unstable phenomenon of fragrance.Chinese invention patent (Authorization Notice No. CN102899167
B authorized announcement date 2014.04.16) disclose uniform, stable tobacco aromaticss of a kind of fragrance and preparation method thereof, tobacco aromaticss
It is via the extraction that the relative density obtained by the ethanol extraction mixed material that mass ratio is 60%~95% is 1.02~1.20
Thing, the mixed material includes jujube, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, and wherein jujube, the weight ratio between Radix Angelicae Sinensis, the tuber of dwarf lilyturf is：0.2~30.0:
0.5~20.0:0.5~30.0.The degradable cigarette coke tar of tobacco aromaticss for being provided, this perfume of tobacco and natural herbal plant nature
With reference to, simple and elegant and Tianjin is sweet, alcohol and extremely, fragrance is elegant, and hair property is good thoroughly, enrich the fragrance of cigarette, significant increase cigarette
Quality.Present invention also offers the preparation method of above-mentioned tobacco aromaticss, uniform, stable, fragrant and sweet liquid perfume addition can be obtained
Agent, removes impurity, constitutes the crucial fragrance component relative amount of its odor characteristic more than 80%.By jujube, Radix Angelicae Sinensis, the tuber of dwarf lilyturf
And the mixed material of auxiliary material composition has certain flavouring and medical value, but for the uniform stability of fragrance effect simultaneously
Do not refer to.Method for being extracted the fragrance component in mixed material in the invention using ethanol, is first had to molten by ethanol
Immersion bubble mixed material 15~30 days, soak time is oversize, the cycle of technique is influenceed, secondly, only by the extracting of ethanol solution
The yield of the extract of acquisition is low.
The content of the invention
The purpose of the present invention is aiming at drawbacks described above, there is provided a kind of uniform, the stable tobacco aromaticss of fragrance and its preparation
Method, the cycle is short of its preparation method, the yield of the tobacco aromaticss for obtaining is high.
To achieve the above object, designed by the present invention fragrance is uniform, stabilization tobacco aromaticss, and it is that natural plants are former
Material obtains enzymolysis liquid through enzyme digestion reaction first, is subsequently adding ultrasonically treated, centrifugation after most being extracted through ethanol afterwards after absolute ethyl alcohol, receives
Collection clear liquid is prepared from through vacuum distillation concentration；Natural plant raw material is counted by weight, including：5~10 parts of balloonflower root, Radix Angelicae Sinensis 8
~15 parts, 2~5 parts of jujube, 10~15 parts of honeysuckle, 5~10 parts of Radix Glycyrrhizae, 10~20 parts of ginkgo, 2~5 parts of grape pip, Poria cocos 1
1~3 part of~3 parts, 1~3 part of root of couch grass, 6~10 parts of Momordica grosvenori, 1~3 part of American aloe, 10~15 parts of the tuber of dwarf lilyturf and fritillaria thunbergii.
Preferably, the enzyme digestion reaction is to digest natural plant raw material jointly using pectase, protease and cellulase,
The pectase accounts for the 0.1% of gross weight, and the protease accounts for the 0.05% of gross weight, and the cellulase accounts for gross weight
0.2%, the temperature of the enzyme digestion reaction is 20~40 DEG C, and the time is 2~4h；The volume of the absolute ethyl alcohol of the addition is enzymolysis
4 times of liquid；It is to circulate to extract 1~2h by apparatus,Soxhlet's that the ethanol is extracted；The speed of the centrifugation be 4000~
8000rpm, the time is 5~10min；The temperature of the vacuum distillation is 35~45 DEG C.
Preferably, the residue after the centrifugation is through the CO of boundary over zero2Vacuum distillation treatment after mixing with the clear liquid after extraction,
The CO of boundary over zero2The pressure of extraction is 20~30MPa, CO2Flow is 2~4L/min.
Preferably, the natural plant raw material is counted by weight, including：10 parts of balloonflower root, 10 parts of Radix Angelicae Sinensis, 2 parts of jujube, gold
10 parts of honeysuckle flower, 10 parts of Radix Glycyrrhizae, 15 parts of ginkgo, 3 parts of grape pip, 2 parts of Poria cocos, 2 parts of root of couch grass, 6 parts of Momordica grosvenori, 2 parts of American aloe, wheat
2 parts of 10 parts of winter and fritillaria thunbergii.
Present invention also offers a kind of preparation method of fragrance tobacco aromaticss uniformly, stably, its step is：
1) it is milled into powder after natural plant raw material is dried, adds 10 times of water of volume, adds pectase, protease,
Cellulase carries out enzyme digestion reaction and obtains enzymolysis liquid；The pectase accounts for the 0.1% of gross weight, and the protease accounts for gross weight
0.05%, the cellulase accounts for the 0.2% of gross weight；The temperature of the enzyme digestion reaction is 20~40 DEG C, and the time is 2~4h；
2) to 4 times of absolute ethyl alcohols of volume are added in enzymolysis liquid, it is placed in ultrasonically treated 3~6h in Ultrasound Instrument；
3) enzymolysis liquid after ultrasound is placed in apparatus,Soxhlet's, circulation extract centrifugal treating after 1~2h separate clear liquid with it is residual
Slag；The speed of the centrifugation is 4000~8000rpm, and the time is 5~10min,
4) by the tobacco aromaticss that clear liquid vacuum distillation acquisition relative density is 1.23~1.35, the temperature of the vacuum distillation
It is 35~45 DEG C；
Wherein, natural plant raw material is counted by weight, including：5~10 parts of balloonflower root, 8~15 parts of Radix Angelicae Sinensis, jujube 2~5
Part, 10~15 parts of honeysuckle, 5~10 parts of Radix Glycyrrhizae, 10~20 parts of ginkgo, 2~5 parts of grape pip, 1~3 part of Poria cocos, root of couch grass 1~3
Part, 6~10 parts of Momordica grosvenori, 1~3 part of American aloe, 10~15 parts of the tuber of dwarf lilyturf, 1~3 part of fritillaria thunbergii.
Preferably, the step 3) in residue through the CO of boundary over zero2After mixing with the clear liquid after extraction at vacuum distillation
Reason；The CO of boundary over zero2The pressure of extraction is 20~30MPa, CO2Flow is 2~4L/min.
Preferably, the natural plant raw material is counted by weight, including：10 parts of balloonflower root, 10 parts of Radix Angelicae Sinensis, 2 parts of jujube, gold
10 parts of honeysuckle flower, 10 parts of Radix Glycyrrhizae, 15 parts of ginkgo, 3 parts of grape pip, 2 parts of Poria cocos, 2 parts of root of couch grass, 6 parts of Momordica grosvenori, 2 parts of American aloe, wheat
10 parts of winter, 2 parts of fritillaria thunbergii.
The primary efficacy of each composition is as follows in natural plant raw material of the present invention：
Balloonflower root：Facilitaing lung, relieving sore-throat, eliminating the phlegm, apocenosis.For coughing with a lot of sputum, uncomfortable in chest not smooth, pharyngalgia, sound is mute, lung carbuncle pyemesis, sore
Ulcer purulence is not into bursting, and balloonflower root contains substantial amounts of glycoside material.
Radix Angelicae Sinensis：Contain various organic principles such as substantial amounts of volatile oil, vitamin, organic acid and trace element, experimental study
Show, Radix Angelicae Sinensis can expand peripheral vascular, reduce vascular resistence, increase circulating liquid measure etc..
Jujube：Containing substantial amounts of glucide, predominantly glucose, also containing fructose, sucrose, and by glucose and fruit
Oligosaccharide, araban and galacturonan that sugar is constituted etc.；And contain substantial amounts of vitamin C, riboflavin, thiamine, Hu
The multivitamins such as radish element, niacin, with stronger tonic effect, can improve immune function of human body, strengthen resistance against diseases.
Honeysuckle：Honeysuckle is cold in nature, sweet, enters lung, the heart, stomach, has functions that clearing heat and detoxicating, anti-inflammatory, qi-restoratives treat wind,
Cure mainly disease, warm disease heating under turgor, the disease such as heat toxin large carbuncle and tumour.
Radix Glycyrrhizae：Radix Glycyrrhizae sweet taste belongs to return type, that is, it is not to feel sweet taste immediately but one section could release at leisure to enter intraoral
Come, Radix Glycyrrhizae can coordinate the pungent sense of result of combustion of tobacco.
Ginkgo：Ginkgo can be with restraining and sterilizing bacteria, disease of dispelling cough-relieving, waterlogging-resistant suppression worm, check with turbidity and reduce serum cholesterol.In addition,
Ginkgo can reduce level of lipid, reduce freckle, moisten skin, beautiful appearance.Glycosides displayed and flavones in ginkgo leaf
Alcohol is all the street cleaner of free radical, can protect corium confluent monolayer cells, improves blood circulation, prevents cell to be oxidized and produces wrinkle.Silver
Apricot is one of herbal medicine with resistant activity gene ability, and ginkgo hinders in protection lipid (part of cell membrane) from free radical
Evil aspect is very effective.
Grape pip：Active ingredient：OPC, vine polyphenol proanthocyanidin can be divided into monomer, oligomer and polymer, I
Department's grape seed extract is former by two class proanthocyanidin monomer compositions, i.e. catechin and epicatechin based on oligomer (OPC)
Anthocyanidin is high-efficiency antioxidant agent, is maximally effective free radical scavenger, with very strong activity in vivo.
Poria cocos：With clearing damp and promoting diuresis, invigorating the spleen, effect of calming heart.
Root of couch grass：Sucrose containing volume, glucose, a small amount of fructose, xylose and citric acid, oxalic acid, malic acid etc., with cool
Blood, hemostasis, heat-clearing, diuresis function controls pyreticosis polydipsia, spits blood, and bleeding from five sense organs or subcutaneous tissue, lung heat breathes heavily urgency, stomach energy hiccup, gonorrhoea, difficult urination, water
It is swollen, jaundice.
Momordica grosvenori：Sweet cool in nature, return lung, large intestine channel moisten the lung and relieve the cough, promote the production of body fluid to quench thirst, suitable for lung heat or lung
Cough caused by dryness is coughed, pertussis and hot summer weather fluid deficiency and thirsty etc., in addition with the effect for relaxing bowel.
American aloe：Refreshing, containing various steroid saponins, and with moistening lung, resolving sputum, effect of cough-relieving.
Fritillaria thunbergii：The effect of with clearing heat and eliminating phlegm, antibechic.
The tuber of dwarf lilyturf：Fibrous root is more sturdy, and the top or middle part of root are often expanded as fusiform meat fritter.Surface yellow-white is light
It is yellowish-white, there is thin longitudinal grin.Matter is flexible, section yellow-white, and translucent, center pillar is tiny.Gas micro-perfume, sweet, slight bitter.It is sweet cold clear and rich, it is apt to
Clear away heart-fire lung heat and yin-nourishing relieving restlessness, and can clear and rich stomach and intestine and quench the thirst and moisturize.
The pectase that the present invention is used, protease, cellulase is purchased from Wuhan Biological Products Inst., and mixed material is
What in the market can be commercially available.
The beneficial effects of the invention are as follows：
1) with the addition of balloonflower root in the mixed material for being provided, balloonflower root contains substantial amounts of glycoside material, and the fragrance of spices
Come from alcohols material mostly, glucosides can be achieved on the stability of alcohols material and the uniformity of release.
2) Radix Angelicae Sinensis, honeysuckle, ginkgo, jujube, Radix Glycyrrhizae, grape pip, Poria cocos, cogongrass are provided in the mixed material for being provided
The natural herb material such as root, Momordica grosvenori, American aloe, the tuber of dwarf lilyturf, fritillaria thunbergii, good with tobacco harmony, fragrance is pure and fresh, soft not pierce
Larynx.
3) preparation methods of uniform, the stable tobacco aromaticss of fragrance obtain enzymolysis liquid through enzyme digestion reaction first, are subsequently adding
It is ultrasonically treated after absolute ethyl alcohol, it is centrifuged after most being extracted through ethanol afterwards, collect clear liquid and be prepared from through vacuum distillation concentration.After centrifugation
Residue through the CO of boundary over zero2Vacuum distillation treatment after mixing with the clear liquid after extraction.Enzyme-added treatment can tentatively digest mixing
Cellulose in raw material, protein, pectic substance improves plant cell activity, strengthens the surface of effective ingredients in plant molecule
Active power, it is final to promote to improve extraction recovery.And by the CO of boundary over zero2Extraction residue further increases obtaining for extract
Rate.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.In mixed material provided by the present invention
Addition balloonflower root, Radix Angelicae Sinensis, honeysuckle, ginkgo, jujube, Radix Glycyrrhizae, grape pip, Poria cocos, root of couch grass, Momordica grosvenori, American aloe, the tuber of dwarf lilyturf, Zhejiang
The smoking result of fritillaria is shown in Table 1.
Embodiment 1
Count by weight, take 5 parts of balloonflower root, 8 parts of Radix Angelicae Sinensis, 2 parts of jujube, 10 parts of honeysuckle, 5 parts of Radix Glycyrrhizae, 10 parts of ginkgo, Portugal
2 parts of grape seed, 1 part of Poria cocos, 1 part of root of couch grass, 6 parts of Momordica grosvenori, 1 part of American aloe, 10 parts of the tuber of dwarf lilyturf, 1 part of mixed preparing of fritillaria thunbergii is natural
Plant material.
1) it is milled into powder after natural plant raw material is dried, adds 10 times of water of volume, adds pectase, protease,
Cellulase carries out enzyme digestion reaction and obtains enzymolysis liquid；The pectase accounts for the 0.1% of gross weight, and the protease accounts for gross weight
0.05%, the cellulase accounts for the 0.2% of gross weight；The temperature of the enzyme digestion reaction is 20 DEG C, and the time is 2h；
2) to 4 times of absolute ethyl alcohols of volume are added in enzymolysis liquid, it is placed in ultrasonically treated 3h in Ultrasound Instrument；
3) enzymolysis liquid after ultrasound is placed in apparatus,Soxhlet's, centrifugal treating separates clear liquid and residue after 1h is extracted in circulation；
The speed of the centrifugation is 4000rpm, and the time is 5min,
4) by the tobacco aromaticss that clear liquid vacuum distillation acquisition relative density is 1.23, the temperature of the vacuum distillation is 35
℃。
Embodiment 2
Count by weight, take 10 parts of balloonflower root, 15 parts of Radix Angelicae Sinensis, 5 parts of jujube, 15 parts of honeysuckle, 10 parts of Radix Glycyrrhizae, ginkgo 20
Part, 5 parts of grape pip, 3 parts of Poria cocos, 3 parts of root of couch grass, 10 parts of Momordica grosvenori, 3 parts of American aloe, 15 parts of the tuber of dwarf lilyturf, 3 parts of mixing of fritillaria thunbergii are matched somebody with somebody
Natural plant raw material processed.
1) it is milled into powder after natural plant raw material is dried, adds 10 times of water of volume, adds pectase, protease,
Cellulase carries out enzyme digestion reaction and obtains enzymolysis liquid；The pectase accounts for the 0.1% of gross weight, and the protease accounts for gross weight
0.05%, the cellulase accounts for the 0.2% of gross weight；The temperature of the enzyme digestion reaction is 40 DEG C, and the time is 4h；
2) to 4 times of absolute ethyl alcohols of volume are added in enzymolysis liquid, it is placed in ultrasonically treated 6h in Ultrasound Instrument；
3) enzymolysis liquid after ultrasound is placed in apparatus,Soxhlet's, centrifugal treating separates clear liquid and residue after 2h is extracted in circulation；
The speed of the centrifugation is 8000rpm, and the time is 10min, and residue is through the CO of boundary over zero2Depressurized after mixing with the clear liquid after extraction
Distillation is processed；The CO of boundary over zero2The pressure of extraction is 20MPa, CO2Flow is 2L/min.
4) by the tobacco aromaticss that clear liquid vacuum distillation acquisition relative density is 1.35, the temperature of the vacuum distillation is 45
℃。
Embodiment 3
Count by weight, take 8 parts of balloonflower root, 10 parts of Radix Angelicae Sinensis, 3 parts of jujube, 12 parts of honeysuckle, 8 parts of Radix Glycyrrhizae, 15 parts of ginkgo,
3 parts of grape pip, 2 parts of Poria cocos, 2 parts of root of couch grass, 8 parts of Momordica grosvenori, 2 parts of American aloe, 12 parts of the tuber of dwarf lilyturf, fritillaria thunbergii 2 parts of mixed preparings day
Right plant material.
1) it is milled into powder after natural plant raw material is dried, adds 10 times of water of volume, adds pectase, protease,
Cellulase carries out enzyme digestion reaction and obtains enzymolysis liquid；The pectase accounts for the 0.1% of gross weight, and the protease accounts for gross weight
0.05%, the cellulase accounts for the 0.2% of gross weight；The temperature of the enzyme digestion reaction is 30 DEG C, and the time is 3h；
2) to 4 times of absolute ethyl alcohols of volume are added in enzymolysis liquid, it is placed in ultrasonically treated 3~6h in Ultrasound Instrument；
3) enzymolysis liquid after ultrasound is placed in apparatus,Soxhlet's, circulation extract centrifugal treating after 1.5h separate clear liquid with it is residual
Slag；The speed of the centrifugation is 5000rpm, and the time is 60min, and residue is through the CO of boundary over zero2After mixing with the clear liquid after extraction
Vacuum distillation is processed；The CO of boundary over zero2The pressure of extraction is 25MPa, CO2Flow is 3L/min.
4) by the tobacco aromaticss that clear liquid vacuum distillation acquisition relative density is 1.30, the temperature of the vacuum distillation is 40
℃；
Embodiment 4
Count by weight, 10 parts of balloonflower root, 10 parts of Radix Angelicae Sinensis, 2 parts of jujube, 10 parts of honeysuckle, 10 parts of Radix Glycyrrhizae, 15 parts of ginkgo,
3 parts of grape pip, 2 parts of Poria cocos, 2 parts of root of couch grass, 6 parts of Momordica grosvenori, 2 parts of American aloe, 10 parts of the tuber of dwarf lilyturf, 2 parts of fritillaria thunbergii.Mixed preparing day
Right plant material.
1) it is milled into powder after natural plant raw material is dried, adds 10 times of water of volume, adds pectase, protease,
Cellulase carries out enzyme digestion reaction and obtains enzymolysis liquid；The pectase accounts for the 0.1% of gross weight, and the protease accounts for gross weight
0.05%, the cellulase accounts for the 0.2% of gross weight；The temperature of the enzyme digestion reaction is 20~40 DEG C, and the time is 2~4h；
2) to 4 times of absolute ethyl alcohols of volume are added in enzymolysis liquid, it is placed in ultrasonically treated 3~6h in Ultrasound Instrument；
3) enzymolysis liquid after ultrasound is placed in apparatus,Soxhlet's, circulation extract centrifugal treating after 1.5h separate clear liquid with it is residual
Slag；The speed of the centrifugation is 7000rpm, and the time is 8min, and residue is through the CO of boundary over zero2Subtract after mixing with the clear liquid after extraction
Pressure distillation treatment；The CO of boundary over zero2The pressure of extraction is 30MPa, CO2Flow is 4L/min.
4) by the tobacco aromaticss that clear liquid vacuum distillation acquisition relative density is 1.32, the temperature of the vacuum distillation is 42
℃。
The natural plant raw material smoking result of table 1
The yield of the tobacco aromaticss of the control group of embodiment 1~4 and 4 is shown in Table 2：
The raw material extracted in control group 1 is identical with the raw material of embodiment 1, and the technique of extraction uses traditional handicraft：By quality
Than the alcohol solution dipping mixed material 15 days for 75%；Then squeezed in ethanol solution and mixed material that mixed material will be soaked
The liquid for going out suction filtration in the lump, obtains ethanol extract；Finally by ethanol extract by separated ethanol, cigarette is obtained fragrant
Material.
The raw material extracted in control group 2 is identical with the raw material of embodiment 2, and the technique of extraction is identical with the technique of control group 1.
The raw material extracted in control group 3 is identical with the raw material of embodiment 3, and the technique of extraction is identical with the technique of control group 1.
Table 2
| Control group 1 | Embodiment 1 | Control group 2 | Embodiment 2 | Control group 3 | Embodiment 3 | |
| Yield % | 0.58 | 1.01 | 0.51 | 1.12 | 0.61 | 1.06 |
Claims (7)
1. the tobacco aromaticss that a kind of fragrance is uniform, stablize, it is characterised in that：It is first through enzyme digestion reaction by natural plant raw material
Enzymolysis liquid is obtained, ultrasonically treated, centrifugation after most being extracted through ethanol afterwards after absolute ethyl alcohol is subsequently adding, clear liquid is collected through vacuum distillation
Concentration is prepared from；The natural plant raw material is counted by weight, including：5~10 parts of balloonflower root, 8~15 parts of Radix Angelicae Sinensis, jujube 2
~5 parts, 10~15 parts of honeysuckle, 5~10 parts of Radix Glycyrrhizae, 10~20 parts of ginkgo, 2~5 parts of grape pip, 1~3 part of Poria cocos, root of couch grass 1
1~3 part of~3 parts, 6~10 parts of Momordica grosvenori, 1~3 part of American aloe, 10~15 parts of the tuber of dwarf lilyturf and fritillaria thunbergii.
2. the tobacco aromaticss that fragrance according to claim 1 is uniform, stablize, it is characterised in that：The enzyme digestion reaction is to adopt
Natural plant raw material is digested jointly with pectase, protease and cellulase, and the pectase accounts for the 0.1% of gross weight, described
Protease accounts for the 0.05% of gross weight, and the cellulase accounts for the 0.2% of gross weight, and the temperature of the enzyme digestion reaction is 20~40
DEG C, the time is 2~4h；The volume of the absolute ethyl alcohol of the addition is 4 times of enzymolysis liquid；The ethanol is extracted to be carried by Soxhlet
Take device circulation and extract 1~2h；The speed of the centrifugation is 4000~8000rpm, and the time is 5~10min；The vacuum distillation
Temperature is 35~45 DEG C.
3. the tobacco aromaticss that fragrance according to claim 1 is uniform, stablize, it is characterised in that：Residue after the centrifugation
Through the CO of boundary over zero2Vacuum distillation treatment, the CO of boundary over zero after mixing with the clear liquid after extraction2The pressure of extraction is 20~30MPa,
CO2Flow is 2~4L/min.
4. the tobacco aromaticss that fragrance according to claim 1 is uniform, stablize, it is characterised in that：The natural plant raw material
Count by weight, including：10 parts of balloonflower root, 10 parts of Radix Angelicae Sinensis, 2 parts of jujube, 10 parts of honeysuckle, 10 parts of Radix Glycyrrhizae, 15 parts of ginkgo, grape
2 parts of 3 parts of seed, 2 parts of Poria cocos, 2 parts of root of couch grass, 6 parts of Momordica grosvenori, 2 parts of American aloe, 10 parts of the tuber of dwarf lilyturf and fritillaria thunbergii.
5. a kind of preparation methods of the tobacco aromaticss that fragrance is uniform, stablize, it is comprised the following steps：
1) powder is milled into after natural plant raw material is dried, 10 times of water of volume are added, pectase, protease, fiber is added
Plain enzyme carries out enzyme digestion reaction and obtains enzymolysis liquid；The pectase accounts for the 0.1% of gross weight, and the protease accounts for gross weight
0.05%, the cellulase accounts for the 0.2% of gross weight；The temperature of the enzyme digestion reaction is 20~40 DEG C, and the time is 2~4h；
2) to 4 times of absolute ethyl alcohols of volume are added in enzymolysis liquid, it is placed in ultrasonically treated 3~6h in Ultrasound Instrument；
3) enzymolysis liquid after ultrasound is placed in apparatus,Soxhlet's, centrifugal treating separates clear liquid and residue after 1~2h is extracted in circulation；Institute
The speed of centrifugation is stated for 4000~8000rpm, the time is 5~10min,
4) by the tobacco aromaticss that clear liquid vacuum distillation acquisition relative density is 1.23~1.35, the temperature of the vacuum distillation is 35
~45 DEG C；
Wherein, natural plant raw material is counted by weight, including：5~10 parts of balloonflower root, 8~15 parts of Radix Angelicae Sinensis, 2~5 parts of jujube, gold
10~15 parts of honeysuckle flower, 5~10 parts of Radix Glycyrrhizae, 10~20 parts of ginkgo, 2~5 parts of grape pip, 1~3 part of Poria cocos, 1~3 part of root of couch grass, sieve
6~10 parts of Chinese fruit, 1~3 part of American aloe, 10~15 parts of the tuber of dwarf lilyturf, 1~3 part of fritillaria thunbergii.
6. the preparation methods of the tobacco aromaticss that fragrance according to claim 5 is uniform, stablize, it is characterised in that：The step
It is rapid 3) in residue through the CO of boundary over zero2Vacuum distillation treatment after mixing with the clear liquid after extraction；The CO of boundary over zero2Extraction
Pressure is 20~30MPa, CO2Flow is 2~4L/min.
7. the preparation methods of the tobacco aromaticss that fragrance according to claim 5 is uniform, stablize, it is characterised in that：The day
Right plant material is counted by weight, including：10 parts of balloonflower root, 10 parts of Radix Angelicae Sinensis, 2 parts of jujube, 10 parts of honeysuckle, 10 parts of Radix Glycyrrhizae, silver
15 parts of apricot, 3 parts of grape pip, 2 parts of Poria cocos, 2 parts of root of couch grass, 6 parts of Momordica grosvenori, 2 parts of American aloe, 10 parts of the tuber of dwarf lilyturf, 2 parts of fritillaria thunbergii.
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| CN113892673A (en) * | 2021-10-29 | 2022-01-07 | 广西中烟工业有限责任公司 | Emblic leafflower fruit and liquorice compound-flavor bagged mouth-holding cigarette capable of clearing away heat and toxic materials |
| CN113892675A (en) * | 2021-10-29 | 2022-01-07 | 广西中烟工业有限责任公司 | Lung moistening and cough relieving fructus momordicae and Chinese date compound flavor bagged mouth containing cigarette |
| CN115058291A (en) * | 2022-06-08 | 2022-09-16 | 吉林烟草工业有限责任公司 | Composite plant volatile oil, preparation method thereof and tobacco product |
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| CN113892673A (en) * | 2021-10-29 | 2022-01-07 | 广西中烟工业有限责任公司 | Emblic leafflower fruit and liquorice compound-flavor bagged mouth-holding cigarette capable of clearing away heat and toxic materials |
| CN113892675A (en) * | 2021-10-29 | 2022-01-07 | 广西中烟工业有限责任公司 | Lung moistening and cough relieving fructus momordicae and Chinese date compound flavor bagged mouth containing cigarette |
| CN115058291A (en) * | 2022-06-08 | 2022-09-16 | 吉林烟草工业有限责任公司 | Composite plant volatile oil, preparation method thereof and tobacco product |
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Application publication date: 20170531 |