CN105212263A - Electronic cigarette tobacco tar and preparation method thereof and electronic cigarette - Google Patents
Electronic cigarette tobacco tar and preparation method thereof and electronic cigarette Download PDFInfo
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Abstract
Electronic cigarette tobacco tar and preparation method thereof and electronic cigarette.The present invention relates to a kind of electronic cigarette tobacco tar, comprise each component of following mass parts: Chinese herbal medicine extract 1 part ~ 100 parts; Electronic cigarette oil base oil 87 parts ~ 105 parts; Wherein, described Chinese herbal medicine extract is extracted by the medicinal mixture with effect of sobering up and obtains.Above-mentioned electronic cigarette tobacco tar, on the basis of electronic cigarette oil base oil, adds the Chinese herbal medicine extract with effect of sobering up, for the effect making above-mentioned electronic cigarette tobacco tar have health care sobering.Above-mentioned electronic cigarette tobacco tar can reach the double effects suppressing alcohol absorption and acceleration of alcohol excretion, eliminates the precipitation of residual alcohol in liver stomach, reaches the effect of Soboring-up liver-protecting stomach invigorating and health.
Description
Technical field
The present invention relates to electronic cigarette tobacco tar technical field, particularly relate to a kind of electronic cigarette tobacco tar and preparation method thereof and electronic cigarette.
Background technology
Electronic cigarette is as a kind of form in novel tobacco goods, and present huge market prospects, its main cause is: on the one hand, and electronic cigarette can provide the consumption habit similar with conventional cigarette and satisfaction, on the other hand, the hazard index of electronic cigarette reduces greatly than conventional cigarette.Relative to conventional cigarette, the less harmful of electronic cigarette is that what to make to suck human body by incombustible mode is atomized liquid and non-burning pyrolysis product.Electronic cigarette neither burns also can not to produce the harmful substances such as tar, carbon monoxide, carbon dioxide, methacrylaldehyde, produce second-hand-cigarette harm hardly, be regarded as non-harmful smoking cessation product or substitute of tobacco, receive showing great attention to and extensively studying of domestic and international each large tobacco enterprise.
The enforcement made with countries in the world smoking cessation and national governments are to the more and more opening of the policy of electronic cigarette, and the market prospects of future electronic cigarette will be more and more wide.China has put into effect the public place management rule that no smoking in increasing city, believes that electronic cigarette also can occupy a tiny space in Chinese market soon.Electronic cigarette product taste is in the market partial to blended type cigarette, compares the taste custom meeting foreign consumers, and Chinese Consumer's preference flue-cured tobacco, taste is comparatively strong, and the mouthfeel of electronic cigarette is difficult to reach requirement.It is the important means opening Chinese market that improvement electronic cigarette oil formula makes it to meet Chinese Consumer's custom.
In order to the fragrance of traditional cigarette, fragrance and mouthfeel can be simulated to the full extent, the modal additive of current electronic cigarette tobacco tar is tobacco extract, is mixed according to a certain ratio by the tobacco extract and propane diols, glycerine and flavouring essence for tobacco etc. extracting acquisition.
But, although market also exists the electronic cigarette tobacco tar of several functions type, still there is not the electronic cigarette tobacco tar with health care sobering effect.
Summary of the invention
Based on this, be necessary that providing a kind of has electronic cigarette tobacco tar of health care sobering effect and preparation method thereof and electronic cigarette.
A kind of electronic cigarette tobacco tar, comprises each component of following mass parts:
Chinese herbal medicine extract 1 part ~ 100 parts;
Electronic cigarette oil base oil 87 parts ~ 105 parts;
Wherein, described Chinese herbal medicine extract is extracted by the medicinal mixture with effect of sobering up and obtains.
Wherein in an embodiment, described medicinal mixture comprise in elegant jessamine, the root of kudzu vine, green tea, mulberry leaf, honeysuckle, hoveniae semoveniae semen, old orange peel, caulis bambusae in taenian, chrysanthemum and kuh-seng one or more; Wherein:
The mass parts of described medicinal mixture is the elegant jessamine of 1 part ~ 30 parts, the root of kudzu vine of 1 part ~ 30 parts, the green tea of 1 part ~ 10 parts, the mulberry leaf of 1 part ~ 20 parts, the honeysuckle of 1 part ~ 20 parts, the hoveniae semoveniae semen of 1 part ~ 8 parts, the old orange peel of 1 part ~ 10 parts, the chrysanthemum of 1 part ~ 15 parts, the caulis bambusae in taenian of 1 part ~ 10 parts and 1 part ~ 5 parts.
Wherein in an embodiment, described Chinese herbal medicine extract also comprise in white orange peel, ginseng, tsaoko, galangal, Semen Lablab Album and nutmeg one or more; Wherein:
The mass parts of described Chinese herbal medicine extract is the nutmeg removing white orange peel, the ginseng of 1 part ~ 10 parts, the tsaoko of 1 part ~ 10 parts, the galangal of 1 part ~ 15 parts, the Semen Lablab Album of 1 part ~ 12 parts and 1 part ~ 15 parts of 1 part ~ 20 parts.
Wherein in an embodiment, described electronic cigarette oil base oil comprises each component of following mass parts:
Tobacco extract 1 part ~ 5 parts;
Solvent 85 parts ~ 95 parts;
Flavouring essence for tobacco 1 part ~ 5 parts.
Wherein in an embodiment, described electronic cigarette oil base oil also comprises the deionized water that mass parts is 0.5 part ~ 4 parts.
A preparation method for described electronic cigarette tobacco tar, comprises the steps:
Obtain medicinal mixture after being pulverized and mixed by each Chinese herbal medicine, after adopting extractant first time to soak described medicinal mixture, refluxing extraction obtains the first extract, and adopt extractant second time to soak described medicinal mixture, refluxing extraction obtains the second extract;
By described first extract and described second extract mixing, and obtain supernatant after centrifugal filtration, described supernatant liquid filtering is also concentrated, obtain Chinese herbal medicine extract;
To be the Chinese herbal medicine extract of 1 part ~ 100 parts and mass parts by mass parts be, and the electronic cigarette oil base oil of 87 parts ~ 105 parts mixes, and obtains described electronic cigarette tobacco tar.
Wherein in an embodiment, described extractant comprises the one in following mixed solvent:
Volume ratio be the alcohols of the C2 ~ C5 of 1:1 ~ 10 and water form mixed solvent,
Volume ratio be the C3 ~ C7 of 1:2 ~ 5:2 ~ 10 lipid, second alcohol and water composition mixed solvent,
Or volume ratio is the ketone of the C3 ~ C7 of 1:2 ~ 5:2 ~ 10, the mixed solvent of second alcohol and water composition.
Wherein in an embodiment, described extractant first time and second time are soaked in described medicinal mixture, and the mass volume ratio of described medicinal mixture and extractant is 1:5 ~ 15; Described soak time is 1 ~ 3h.
Wherein in an embodiment, twice reflux temperature of described medicinal mixture after first time and second time soak is 70 ~ 90 DEG C.
A kind of electronic cigarette, its inside is filled with described electronic cigarette tobacco tar.
Above-mentioned electronic cigarette tobacco tar, on the basis of electronic cigarette oil base oil, adds the Chinese herbal medicine extract with effect of sobering up, for the effect making above-mentioned electronic cigarette tobacco tar have health care sobering.Above-mentioned electronic cigarette tobacco tar can reach the double effects suppressing alcohol absorption and acceleration of alcohol excretion, eliminates the precipitation of residual alcohol in liver stomach, reaches the effect of Soboring-up liver-protecting stomach invigorating and health.
Accompanying drawing explanation
Fig. 1 is the flow chart of the preparation method of the electronic cigarette tobacco tar of an embodiment of the present invention.
Detailed description of the invention
For enabling above-mentioned purpose of the present invention, feature and advantage become apparent more, are described in detail the specific embodiment of the present invention below in conjunction with accompanying drawing.Set forth a lot of detail in the following description so that fully understand the present invention.But the present invention can be much different from alternate manner described here to implement, those skilled in the art can when without prejudice to doing similar improvement when intension of the present invention, therefore the present invention is by the restriction of following public specific embodiment.
In the mass parts of each material of the present invention, every 1 part represents 1 gram.
The electronic cigarette tobacco tar of one embodiment, it comprises each component of following mass parts:
Chinese herbal medicine extract 1 part ~ 100 parts;
Electronic cigarette oil base oil 87 parts ~ 105 parts;
Wherein, described Chinese herbal medicine extract obtains by having medicinal mixture extraction.
Above-mentioned electronic cigarette tobacco tar, on the basis of electronic cigarette oil base oil, adds the Chinese herbal medicine extract with effect of sobering up, for the effect making above-mentioned electronic cigarette tobacco tar have health care sobering.For the user of things that one must ahre redily with another as a social amenity, in cheerful and light-hearted party and above-mentioned electronic cigarette tobacco tar while drinking happily good wine, can be used, as, the electronic cigarette of suction containing above-mentioned electronic cigarette tobacco tar, the double effects suppressing alcohol absorption and acceleration of alcohol excretion can be reached, eliminate the precipitation of residual alcohol in liver stomach, reach the effect of Soboring-up liver-protecting stomach invigorating and health.
Further, the electronic cigarette tobacco tar of an embodiment, it comprises each component of following mass parts:
Chinese herbal medicine extract 1 part ~ 10 parts;
Electronic cigarette oil base oil 87 parts ~ 105 parts;
Wherein, described Chinese herbal medicine extract obtains by having medicinal mixture extraction.
Further, the electronic cigarette tobacco tar of an embodiment, it comprises each component of following mass parts:
Chinese herbal medicine extract 2 parts ~ 6 parts;
Electronic cigarette oil base oil 87 parts ~ 105 parts;
Wherein, described Chinese herbal medicine extract obtains by having medicinal mixture extraction.
In one embodiment, described medicinal mixture comprises at least one in elegant jessamine, the root of kudzu vine, green tea, mulberry leaf, honeysuckle, hoveniae semoveniae semen, old orange peel, caulis bambusae in taenian, chrysanthemum and kuh-seng.
Wherein, each Chinese herbal medicine in described medicinal mixture has following effect respectively:
Elegant jessamine: nature and flavor are sweet flat, kind relieving alcoholism, is amusing and stomach quenches one's thirst, and cures mainly insobriety, headache and dizziness, and polydipsia is vomitted, and chest diaphragm is glutted waits disease.The root of kudzu vine: Gan Xin, flat vomit inverse, whetting the appetite, main relieving alcoholism, only polydipsia.Green tea: benefit of refreshing oneself is thought, cleared away heart-fire, diuresis, and removing toxic substances, controls headache, blurred vision, kind sleeping of sleeping, restlessness and thirst more.Mulberry leaf: bitter sweet, cold, expelling wind and clearing away heat, cooling blood for improving eyesight.Control wind-warm syndrome heating, headache, hot eyes, thirsty.Honeysuckle: cold in nature, bitter.Clearing heat and detoxicating, wind-heat dissipating.Hoveniae semoveniae semen: the sweet acid of nature and flavor is put down, and can control drunk, dysphoria with smothery sensation, thirsty, vomiting, difficulty in urination and defecation etc.Caulis bambusae in taenian: sweet, be slightly cold, the merit have clearing heat and eliminating phlegm, relieving restlessness and preventing vomiting, effective to the vomiting caused by stomach energy or phlegm heat.Old orange peel: warm in nature, regulating qi-flowing for strengthening spleen is eliminating dampness and eliminating phlegm.Chrysanthemum: belong to and disperse wind-heat class diaphoretic medicine, pungent sweetness and bitterness, to be slightly cold, can dispelling wind and heat from the body, and flat liver improving eyesight is clearing heat and detoxicating.Kuh-seng: nature and flavor bitter cold, the merit of tool heat-clearing and damp-drying drug, desinsection diuresis, " Bencao Jingshu " also carry kuh-seng " disappear wine, except thirsty, improving eyesight, only bloody dysentery, infantile malnutrition due to digestive disturbances or intestinalparasites dysentery pole effect.
Collaborative composite by above-mentioned each Chinese herbal medicine, can prepare the Chinese herbal medicine extract with effect of sobering up, and then prepare the electronic cigarette tobacco tar with effect of sobering up, when it is used on electronic cigarette, for playing the effect of sobering up to user.
In one embodiment, described medicinal mixture comprise in the kuh-seng of the elegant jessamine of 1 part ~ 30 parts, the root of kudzu vine of 1 part ~ 30 parts, the green tea of 1 part ~ 10 parts, the mulberry leaf of 1 part ~ 20 parts, the honeysuckle of 1 part ~ 20 parts, the hoveniae semoveniae semen of 1 part ~ 8 parts, the old orange peel of 1 part ~ 10 parts, the chrysanthemum of 1 part ~ 15 parts, the caulis bambusae in taenian of 1 part ~ 10 parts and 1 part ~ 5 parts one or more.
In one embodiment, described Chinese herbal medicine extract also comprise in white orange peel, ginseng, tsaoko, galangal, Semen Lablab Album and nutmeg one or more.
Wherein, each Chinese herbal medicine in described medicinal mixture has following effect respectively: orange peel (going white): warm in nature, promoting the circulation of qi invigorating the spleen; Lowering the adverse-rising QI and eliminating phlegm.Ginseng: reinforce the spleen to benefit the lung, promotes the production of body fluid, and calms the nerves.Tsaoko: Xin Wen, enters taste warp, and tool eliminating dampness is loose cold, the merit of eliminating phlegm preventing malaria, because of gas fragrance, wards off turbid property in addition.Galangal: hot, enters taste warp, has eliminating cold to stop pain, the merit of warming middle energizer to arrest vomiting.Semen Lablab Album: belong to invigoration spleen qi medicine.Sweet in flavor and warm in property, can invigorating the spleen, dampness elimination, relieve summer heat." Bencao Tujing " carries it, and " main woman is with down.Doublely kill wine poison, also separate fugutoxin ".Nutmeg: Xin Wen, belongs to temperature and stops puckery medicine, have warming middle energizer to promote qi, intestine-stabling and anti-diarrheal, the merit helped digestion.
Collaborative composite by above-mentioned each Chinese herbal medicine, can strengthen effect of sobering up of above-mentioned electronic cigarette tobacco tar, further for strengthening the effect of sobering up to user.
In one embodiment, described Chinese herbal medicine extract also comprise 1 part ~ 20 parts go in the nutmeg of white orange peel, the ginseng of 1 part ~ 10 parts, the tsaoko of 1 part ~ 10 parts, the galangal of 1 part ~ 15 parts, the Semen Lablab Album of 1 part ~ 12 parts and 1 part ~ 15 parts one or more.
The electronic cigarette tobacco tar of one embodiment, it comprises each component of following mass parts:
Chinese herbal medicine extract 1 part ~ 100 parts;
Electronic cigarette oil base oil 87 parts ~ 105 parts;
Wherein, described Chinese herbal medicine extract obtains by having medicinal mixture extraction;
Described medicinal mixture comprises the elegant jessamine of 1 part ~ 30 parts, the root of kudzu vine of 1 part ~ 30 parts, the green tea of 1 part ~ 10 parts, the mulberry leaf of 1 part ~ 20 parts, the honeysuckle of 1 part ~ 20 parts, the hoveniae semoveniae semen of 1 part ~ 8 parts, the old orange peel of 1 part ~ 10 parts, the chrysanthemum of 1 part ~ 15 parts, the caulis bambusae in taenian of 1 part ~ 10 parts, the kuh-seng of 1 part ~ 5 parts, 1 part ~ 20 parts remove white orange peel, the ginseng of 1 part ~ 10 parts, the tsaoko of 1 part ~ 10 parts, the galangal of 1 part ~ 15 parts, the nutmeg of the Semen Lablab Album of 1 part ~ 12 parts and 1 part ~ 15 parts.
It should be noted that there is after said herbal medicine is composite the fragrance component of certain feature, having for making above-mentioned electronic cigarette tobacco tar that fragrance enriches, comfortable taste and the good advantage of satisfaction.In addition, said herbal medicine also has different pharmacological actions, when said herbal medicine work in coordination with composite after, for the pharmacological effect making above-mentioned electronic cigarette tobacco tar have Soboring-up liver-protecting and stomach invigorating health.The above-mentioned Chinese herbal medicine with different pharmacological action carries out rationally screening according to the formula of traditional Chinese medical science prescription and obtains, and more agrees with the health of modern.
In one embodiment, described electronic cigarette oil base oil comprises each component of following mass parts:
Tobacco extract 1 part ~ 5 parts;
Solvent 85 parts ~ 95 parts;
Flavouring essence for tobacco 1 part ~ 5 parts.
In one embodiment, described electronic cigarette oil base oil also comprises the deionized water that mass parts is 0.5 part ~ 4 parts.
Described solvent is including, but not limited at least one in propane diols and glycerine.Such as, described propane diols, glycerine are food grade or pharmaceutical grade product.
Flavouring essence for tobacco is including, but not limited to one or more in Ethyl vanillin, ethyl maltol, citronellol, geraniol, linalool, rhodinol, dorinone, Megastigmatrienone, dihydroactinidiolide and alpha, beta-lonone, by adopting the smell of above-mentioned flavouring essence for tobacco to electronic cigarette tobacco tar to modify, can obtain that fragrance is abundant, rich in taste and the good electronic cigarette tobacco tar of satisfaction.It should be noted that, above-mentioned flavouring essence for tobacco and Chinese herbal medicine extract can play well collaborative composite effect, namely both jointly give that electronic cigarette tobacco tar have that fragrance is abundant, rich in taste and the good advantage of satisfaction.
In one embodiment, described electronic cigarette oil base oil comprises each component of following mass parts:
Above-mentioned electronic cigarette tobacco tar, on the basis of electronic cigarette oil base oil, adds the Chinese herbal medicine extract with effect of sobering up, for the effect making above-mentioned electronic cigarette tobacco tar have health care sobering.Above-mentioned electronic cigarette tobacco tar can reach the double effects suppressing alcohol absorption and acceleration of alcohol excretion, eliminates the precipitation of residual alcohol in liver stomach, reaches the effect of Soboring-up liver-protecting stomach invigorating and health.
Refer to Fig. 1, the preparation method of the electronic cigarette tobacco tar of an embodiment, comprises the steps:
S110: obtain medicinal mixture after being pulverized and mixed by each Chinese herbal medicine, after adopting extractant first time to soak described medicinal mixture, refluxing extraction obtains the first extract, and adopt extractant second time to soak described medicinal mixture, refluxing extraction obtains the second extract.
In one embodiment, described extractant first time and second time are soaked in described medicinal mixture, and the mass volume ratio of described medicinal mixture and extractant is 1:5 ~ 15; Described soak time is 1 ~ 3h.
In one embodiment, twice reflux temperature of described medicinal mixture after first time and second time soak is 70 ~ 90 DEG C.
In one embodiment, when each Chinese herbal medicine is pulverized, each Chinese herbal medicine is crossed 30 order ~ 90 object screen clothes, be beneficial to follow-up when soak medicine mixture, separate out each medium-height grass the effective elements of the medicine.
Further, when each Chinese herbal medicine is pulverized, each Chinese herbal medicine is crossed 50 order ~ 75 object screen clothes, be beneficial to follow-up when soak medicine mixture, separate out each medium-height grass the effective elements of the medicine more fully.
In one embodiment, described extractant comprises the one in following mixed solvent:
Volume ratio be the alcohols of the C2 ~ C5 of 1:1 ~ 10 and water form mixed solvent,
Volume ratio be the C3 ~ C7 of 1:2 ~ 5:2 ~ 10 lipid, second alcohol and water composition mixed solvent,
Or volume ratio is the ketone of the C3 ~ C7 of 1:2 ~ 5:2 ~ 10, the mixed solvent of second alcohol and water composition.
S120: by described first extract and described second extract mixing, and obtain supernatant after centrifugal filtration, described supernatant liquid filtering is also concentrated, obtain Chinese herbal medicine extract.
S130: to be the Chinese herbal medicine extract of 1 part ~ 100 parts and mass parts by mass parts be, and the electronic cigarette oil base oil of 87 parts ~ 105 parts mixes, and obtains described electronic cigarette tobacco tar.
Such as, above-mentioned electronic cigarette tobacco tar adopts the preparation method of the above-mentioned electronic cigarette tobacco tar of above-mentioned any embodiment to prepare.
An example is, a kind of electronic cigarette, its inside is filled with the electronic cigarette tobacco tar described in above-mentioned any embodiment.Such as, described electronic cigarette comprises body and electronic cigarette tobacco tar, electronic cigarette tobacco tar is filled with in described body, when user is when aspirating above-mentioned electronic cigarette, the double effects suppressing alcohol absorption and acceleration of alcohol excretion can be reached, eliminate the precipitation of residual alcohol in liver stomach, reach the effect of Soboring-up liver-protecting stomach invigorating and health.
Be specific embodiment part below.
Embodiment 1:
The preparation of Chinese herbal medicine extract: take elegant jessamine 20g, root of kudzu vine 25g respectively, green tea 2g, mulberry leaf 10g, honeysuckle 8g, hoveniae semoveniae semen 5g, caulis bambusae in taenian 3g, chrysanthemum 5g, kuh-seng 1g, orange peel remove white 8g, tsaoko 8g, galangal 5g.After pulverizer grinds, cross 60 mesh sieves, insert after mixing in round-bottomed flask, add mixed solvent (comprising 100ml ethanol, the 1000ml water) solvent of 1100mL by feed liquid mass volume ratio 1:10, after soaking 3h, add hot reflux 4.5h again, filter, obtain first time extract.Filter residue adds 600mL mixed solvent (comprising 100ml ethanol, 500ml water) by feed liquid mass volume ratio 1:6 and soaks 1.5h, refluxing extraction 2.5h, filters, and obtains second time extract.Merge extracted twice liquid, being that 4000r/min is centrifugal by eccentricity obtains supernatant, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is evaporated to 16mL in 80 DEG C, obtains the Chinese herbal medicine extract of brown liquid shape.
The preparation of electronic cigarette tobacco tar: in the reactor of cleaning, add propane diols 70g and glycerine 20g respectively, under stirring, add Ethyl vanillin 0.24g, ethyl maltol 0.3g, citronellol 0.15g, geraniol 0.15g, linalool 0.45g, rhodinol 0.3g, dorinone 0.21g, Megastigmatrienone 0.45g, dihydroactinidiolide 0.3g, alpha, beta-lonone 0.45g successively.Stirred at ambient temperature 30 minutes, after dissolving, adds tobacco extract 3.5g, deionized water 1g and Chinese herbal medicine extract 2.5g mixes and obtain the electronic cigarette tobacco tar with effect of sobering up.
Embodiment 2:
The preparation of Chinese herbal medicine extract: take elegant jessamine 25g, root of kudzu vine 25g respectively, mulberry leaf 8g, honeysuckle 8g, hoveniae semoveniae semen 5g, caulis bambusae in taenian 6g, chrysanthemum 3g, orange peel remove white 5g, ginseng 2g, tsaoko 5g, galangal 3g, nutmeg 5g.After pulverizer grinds, cross 60 mesh sieves, insert after mixing in round-bottomed flask, add the mixed solvent (comprising 500ml propyl alcohol, 1000ml water) of 1500mL by feed liquid mass volume ratio 1:10, after soaking 2h, add hot reflux 3h again, filter, obtain first time extract.Filter residue adds 600mL mixed solvent (comprising 100ml propyl alcohol, 500ml water) by feed liquid mass volume ratio 1:6 and soaks 1h, refluxing extraction 2h, filters, and obtains second time extract.Merge extracted twice liquid, being that 4000r/min is centrifugal by eccentricity obtains supernatant, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is evaporated to 16mL in 70 DEG C, obtains the Chinese herbal medicine extract of brown liquid shape.
The preparation of electronic cigarette tobacco tar: in the reactor of cleaning, add propane diols 80g and glycerine 10g respectively, under stirring, add Ethyl vanillin 0.28g, ethyl maltol 0.35g, citronellol 0.175g, geraniol 0.175g, linalool 0.525g, rhodinol 0.35g, dorinone 0.245g, Megastigmatrienone 0.525g, dihydroactinidiolide 0.35g, alpha, beta-lonone 0.525g successively.Stirred at ambient temperature 30 minutes, after dissolving, adds tobacco extract 2.5g, deionized water 1g and Chinese herbal medicine extract 3g and mixes and obtain and have effect electronic cigarette tobacco tar of sobering up.
Embodiment 3:
The preparation of Chinese herbal medicine extract: take elegant jessamine 20g, root of kudzu vine 20g, mulberry leaf 13g, honeysuckle 10g, hoveniae semoveniae semen 7g, caulis bambusae in taenian 4g, old orange peel 6g, chrysanthemum 5g, ginseng 1g, tsaoko 6g, Semen Lablab Album 3g, nutmeg 5g respectively.After pulverizer grinds, cross 60 mesh sieves, insert after mixing in round-bottomed flask, add 2000mL mixed solvent (comprising 1000ml amylalcohol, 1000ml water) by feed liquid mass volume ratio 1:10, after soaking 3h, add hot reflux 6h again, filter, obtain first time extract.Filter residue adds mixed solvent (comprising 400ml amylalcohol, 800ml water) 2h, the refluxing extraction 4h of 1200mL by feed liquid mass volume ratio 1:6, filters, and obtains second time extract.Merge extracted twice liquid, being that 4000r/min is centrifugal by eccentricity obtains supernatant, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is evaporated to 32mL in 90 DEG C, obtains the Chinese herbal medicine extract of brown liquid shape.
The preparation of electronic cigarette tobacco tar: in the reactor of cleaning, add propane diols 64g and glycerine 25g respectively, under stirring, add Ethyl vanillin 0.32g, ethyl maltol 0.4g, citronellol 0.2g, geraniol 0.2g, linalool 0.6g, rhodinol 0.4g, dorinone 0.28g, Megastigmatrienone 0.6g, dihydroactinidiolide 0.4g, alpha, beta-lonone 0.6g successively.Stirred at ambient temperature 30 minutes, after dissolving, adds tobacco extract 2.5g, deionized water 1.5g and Chinese herbal medicine extract 3.5g and mixes and obtain and have effect electronic cigarette tobacco tar of sobering up.
Embodiment 4:
The preparation of Chinese herbal medicine extract:
Take elegant jessamine 20g, root of kudzu vine 30g, mulberry leaf 6g, honeysuckle 9g, hoveniae semoveniae semen 5g, caulis bambusae in taenian 5g, old orange peel 5g, kuh-seng 1g, tsaoko 5g, galangal 4g, Semen Lablab Album 5g, nutmeg 5g respectively.After pulverizer grinds, cross 60 mesh sieves, insert after mixing in round-bottomed flask, add 1000mL mixed solvent by feed liquid mass volume ratio 1:10 and (comprise 200ml propyl ester, 400ml ethanol, 400ml water, after soaking 2h, add hot reflux 3h again, filter, obtain first time extract.The mixed solvent (comprising 100ml heptanone, 200ml ethanol, 300ml water) that filter residue adds 600mL by feed liquid mass volume ratio 1:6 soaks 1.5h, refluxing extraction 2.5h, filters, and obtains second time extract.Merge extracted twice liquid, being that 4000r/min is centrifugal by eccentricity obtains supernatant, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is evaporated to 16mL in 75 DEG C, obtains the Chinese herbal medicine extract of brown liquid shape.
The preparation of electronic cigarette tobacco tar: in the reactor of cleaning, add propane diols 55g and glycerine 34g respectively, under stirring, add Ethyl vanillin 0.2g, ethyl maltol 0.25g, citronellol 0.125g, geraniol 0.125g, linalool 0.375g, rhodinol 0.25g, dorinone 0.175g, Megastigmatrienone 0.375g, dihydroactinidiolide 0.25g, alpha, beta-lonone 0.375g successively.Stirred at ambient temperature 30 minutes, after dissolving, adds tobacco extract 4g, deionized water 0.5g and Chinese herbal medicine extract 4g and mixes and obtain and have effect electronic cigarette tobacco tar of sobering up.
Embodiment 5:
The preparation of Chinese herbal medicine extract:
Take elegant jessamine 22g, root of kudzu vine 25g, mulberry leaf 7g, honeysuckle 10g, hoveniae semoveniae semen 5g, caulis bambusae in taenian 7g, chrysanthemum 4g, old orange peel 6g, tsaoko 5g, galangal 5g, Semen Lablab Album 4g respectively.60 mesh sieves are crossed after pulverizer grinds, insert after mixing in round-bottomed flask, 1000mL mixed solvent (comprising 62.5ml nonanone, 312.5ml ethanol, 625ml water) is added by feed liquid mass volume ratio 1:10, after soaking 3h, add hot reflux 4.5h again, filter, obtain first time extract.Filter residue adds mixed solvent (comprising 100ml heptyl ester, 200ml ethanol, 200ml water) 1h, the refluxing extraction 2h of 500mL by feed liquid mass volume ratio 1:6, filters, and obtains second time extract.Merge extracted twice liquid, being that 4000r/min is centrifugal by eccentricity obtains supernatant, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is evaporated to 16mL in 80 DEG C, obtains the Chinese herbal medicine extract of brown liquid shape.
The preparation of electronic cigarette tobacco tar: in the reactor of cleaning, add propane diols 60g and glycerine 27g respectively, under stirring, add Ethyl vanillin 0.32g, ethyl maltol 0.4g, citronellol 0.2g, geraniol 0.2g, linalool 0.6g, rhodinol 0.4g, dorinone 0.28g, Megastigmatrienone 0.6g, dihydroactinidiolide 0.4g, alpha, beta-lonone 0.6g successively.Stirred at ambient temperature 30 minutes, after dissolving, adds tobacco extract 4g, deionized water 1.0g and Chinese herbal medicine extract 4g and mixes and obtain and have effect electronic cigarette tobacco tar of sobering up.
Embodiment 6:
The preparation of Chinese herbal medicine extract: take elegant jessamine 22g, root of kudzu vine 20g, mulberry leaf 10g, honeysuckle 12g, hoveniae semoveniae semen 6g, caulis bambusae in taenian 6g, chrysanthemum 5g respectively, remove white orange peel 6g, ginseng 2g, tsaoko 6g nutmeg 5g.After pulverizer grinds, cross 60 mesh sieves, insert after mixing in round-bottomed flask, add 1000mL mixed solvent (comprising 100ml ester in the ninth of the ten Heavenly Stems, 400ml ethanol, 500ml water) by feed liquid mass volume ratio 1:10, after soaking 3h, add hot reflux 6h again, filter, obtain first time extract.The mixed solvent (comprising 100ml acetone, 200ml ethanol, 300ml water) that filter residue adds 600mL by feed liquid mass volume ratio 1:6 soaks 3h, refluxing extraction 6h, filters, and obtains second time extract.Merge extracted twice liquid, being that 4000r/min is centrifugal by eccentricity obtains supernatant, and supernatant membrane aperture is 0.45 μm of membrane filtration, and filtrate is evaporated to 16mL in 80 DEG C, obtains the Chinese herbal medicine extract of brown liquid shape.
The preparation of electronic cigarette tobacco tar: in the reactor of cleaning, add propane diols 74g and glycerine 15g respectively, under stirring, add Ethyl vanillin 0.32g, ethyl maltol 0.4g, citronellol 0.2g, geraniol 0.2g, linalool 0.6g, rhodinol 0.4g, dorinone 0.28g, Megastigmatrienone 0.6g, dihydroactinidiolide 0.4g, alpha, beta-lonone 0.6g successively.Stirred at ambient temperature 30 minutes, after dissolving, adds tobacco extract 3.5g, deionized water 0.5g and Chinese herbal medicine extract 3.5g and mixes and obtain and have effect electronic cigarette tobacco tar of sobering up.
Each technical characteristic of the above embodiment can combine arbitrarily, for making description succinct, the each piece of all possible combination of technical characteristic in above-described embodiment is not all described, but, as long as the combination of these technical characteristics does not exist contradiction, be all considered to be the scope that this description is recorded.
The above embodiment only have expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. an electronic cigarette tobacco tar, is characterized in that, comprises each component of following mass parts:
Chinese herbal medicine extract 1 part ~ 100 parts;
Electronic cigarette oil base oil 87 parts ~ 105 parts;
Wherein, described Chinese herbal medicine extract is extracted by the medicinal mixture with effect of sobering up and obtains.
2. electronic cigarette tobacco tar according to claim 1, is characterized in that, described medicinal mixture comprise in elegant jessamine, the root of kudzu vine, green tea, mulberry leaf, honeysuckle, hoveniae semoveniae semen, old orange peel, caulis bambusae in taenian, chrysanthemum and kuh-seng one or more; Wherein:
The mass parts of described medicinal mixture is the elegant jessamine of 1 part ~ 30 parts, the root of kudzu vine of 1 part ~ 30 parts, the green tea of 1 part ~ 10 parts, the mulberry leaf of 1 part ~ 20 parts, the honeysuckle of 1 part ~ 20 parts, the hoveniae semoveniae semen of 1 part ~ 8 parts, the old orange peel of 1 part ~ 10 parts, the chrysanthemum of 1 part ~ 15 parts, the caulis bambusae in taenian of 1 part ~ 10 parts and 1 part ~ 5 parts.
3. electronic cigarette tobacco tar according to claim 1 and 2, is characterized in that, described Chinese herbal medicine extract also comprise in white orange peel, ginseng, tsaoko, galangal, Semen Lablab Album and nutmeg one or more; Wherein:
The mass parts of described Chinese herbal medicine extract is the nutmeg removing white orange peel, the ginseng of 1 part ~ 10 parts, the tsaoko of 1 part ~ 10 parts, the galangal of 1 part ~ 15 parts, the Semen Lablab Album of 1 part ~ 12 parts and 1 part ~ 15 parts of 1 part ~ 20 parts.
4. electronic cigarette tobacco tar according to claim 1, is characterized in that, described electronic cigarette oil base oil comprises each component of following mass parts:
Tobacco extract 1 part ~ 5 parts;
Solvent 85 parts ~ 95 parts;
Flavouring essence for tobacco 1 part ~ 5 parts.
5. electronic cigarette tobacco tar according to claim 1, is characterized in that, described electronic cigarette oil base oil also comprises the deionized water that mass parts is 0.5 part ~ 4 parts.
6. a preparation method for electronic cigarette tobacco tar as claimed in claim 1, is characterized in that, comprises the steps:
Obtain medicinal mixture after being pulverized and mixed by each Chinese herbal medicine, after adopting extractant first time to soak described medicinal mixture, refluxing extraction obtains the first extract, and adopt extractant second time to soak described medicinal mixture, refluxing extraction obtains the second extract;
By described first extract and described second extract mixing, and obtain supernatant after centrifugal filtration, described supernatant liquid filtering is also concentrated, obtain Chinese herbal medicine extract;
To be the Chinese herbal medicine extract of 1 part ~ 100 parts and mass parts by mass parts be, and the electronic cigarette oil base oil of 87 parts ~ 105 parts mixes, and obtains described electronic cigarette tobacco tar.
7. the preparation method of electronic cigarette tobacco tar according to claim 6, is characterized in that, described extractant comprises the one in following mixed solvent:
Volume ratio be the alcohols of the C2 ~ C5 of 1:1 ~ 10 and water form mixed solvent,
Volume ratio be the C3 ~ C7 of 1:2 ~ 5:2 ~ 10 lipid, second alcohol and water composition mixed solvent,
Or volume ratio is the ketone of the C3 ~ C7 of 1:2 ~ 5:2 ~ 10, the mixed solvent of second alcohol and water composition.
8. the preparation method of electronic cigarette tobacco tar according to claim 6, is characterized in that, described extractant first time and second time are soaked in described medicinal mixture, and the mass volume ratio of described medicinal mixture and extractant is 1:5 ~ 15; Described soak time is 1 ~ 3h.
9. the preparation method of electronic cigarette tobacco tar according to claim 6, is characterized in that, twice reflux temperature of described medicinal mixture after first time and second time soak is 70 ~ 90 DEG C, and each return time is 2 ~ 6h.
10. an electronic cigarette, is characterized in that, its inside is filled with the electronic cigarette tobacco tar of having the right described in requirement 1 ~ 5.
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| CN106723319A (en) * | 2016-12-27 | 2017-05-31 | 广东中烟工业有限责任公司 | Sober up cigarette and preparation method thereof |
| CN106723301A (en) * | 2016-12-19 | 2017-05-31 | 深圳瀚星翔科技有限公司 | Tobacco juice for electronic smoke |
| CN106912982A (en) * | 2017-01-20 | 2017-07-04 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
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| CN110893008A (en) * | 2018-09-05 | 2020-03-20 | 深圳波顿香料有限公司 | Electronic cigarette tobacco tar and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106723301A (en) * | 2016-12-19 | 2017-05-31 | 深圳瀚星翔科技有限公司 | Tobacco juice for electronic smoke |
| CN106723319A (en) * | 2016-12-27 | 2017-05-31 | 广东中烟工业有限责任公司 | Sober up cigarette and preparation method thereof |
| CN106912982A (en) * | 2017-01-20 | 2017-07-04 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
| CN108125277A (en) * | 2018-03-21 | 2018-06-08 | 福建中烟工业有限责任公司 | A kind of electronic cigarette and preparation method thereof |
| CN110893008A (en) * | 2018-09-05 | 2020-03-20 | 深圳波顿香料有限公司 | Electronic cigarette tobacco tar and preparation method thereof |
| CN113261635A (en) * | 2021-01-22 | 2021-08-17 | 云南品斛堂酒业有限公司 | A beverage with effects of relieving hangover, invigorating stomach, and promoting fluid production, and its preparation method |
| CN115517397A (en) * | 2021-06-25 | 2022-12-27 | 比亚迪精密制造有限公司 | Electronic cigarette liquid, preparation method of taste modifier of electronic cigarette liquid and preparation method of electronic cigarette liquid |
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Application publication date: 20160106 |