CN115517397A - Electronic cigarette liquid, preparation method of taste modifier of electronic cigarette liquid and preparation method of electronic cigarette liquid - Google Patents

Electronic cigarette liquid, preparation method of taste modifier of electronic cigarette liquid and preparation method of electronic cigarette liquid Download PDF

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Publication number
CN115517397A
CN115517397A CN202110714172.5A CN202110714172A CN115517397A CN 115517397 A CN115517397 A CN 115517397A CN 202110714172 A CN202110714172 A CN 202110714172A CN 115517397 A CN115517397 A CN 115517397A
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China
Prior art keywords
extract
electronic cigarette
cigarette liquid
taste modifier
parts
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CN202110714172.5A
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Chinese (zh)
Inventor
蒋琼艳
周虎
张家鑫
樊秀兰
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BYD Precision Manufacturing Co Ltd
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BYD Precision Manufacturing Co Ltd
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Priority to CN202110714172.5A priority Critical patent/CN115517397A/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes

Abstract

The embodiment of the application provides electronic cigarette liquid, a preparation method of a taste modifier of the electronic cigarette liquid and a preparation method of the electronic cigarette liquid. According to the mass parts, the electronic cigarette liquid comprises: 0.1-5 parts of taste modifier, 0-10 parts of herbal extract, 2-25 parts of tobacco essence, 0-6 parts of nicotine and 50-90 parts of solvent; wherein the taste modifier comprises an extract of the seeds of an acronychia. The taste modifier comprising the emblic leafflower fruit extract is added into the tobacco juice formula of the electronic cigarette provided by the embodiment of the application, so that the sweet greasy feeling of the electronic cigarette tobacco juice during smoking can be reduced, the sensory quality of the electronic cigarette is closer to that of a traditional cigarette, and the mouthfeel of the electronic cigarette tobacco juice is greatly improved.

Description

Electronic cigarette liquid, preparation method of taste modifier of electronic cigarette liquid and preparation method of electronic cigarette liquid
Technical Field
The application belongs to the technical field of electronic cigarettes, and particularly relates to electronic cigarette liquid, a preparation method of a taste modifier of the electronic cigarette liquid and a preparation method of the electronic cigarette liquid.
Background
The electronic cigarette generally comprises a lithium battery, an atomizer and tobacco juice. The battery supplies power to the atomizer to atomize the tobacco liquid, and the tobacco liquid is converted into mist to be sucked by a user. When a user inhales the electronic cigarette, the user has a feeling similar to 'swallowing and spitting' when smoking.
The cigarette liquid of the electronic cigarette is an electronic atomization liquid used in cooperation with the electronic cigarette as an important component of the electronic cigarette. After being heated by the electronic cigarette atomizer, the smoke liquid of the electronic cigarette can generate mist like a cigarette. The cigarette liquid taste and quality of the electronic cigarette directly determine the acceptance and experience of the user on the mouthfeel of the electronic cigarette.
At present, after the commercially available 'tobacco flavor' electronic cigarette is smoked, the sweet and greasy feeling of tobacco liquid solvents (mainly glycerin and propylene glycol) remained on the tongue surface is too heavy, so that the full hair of the tobacco fragrance is seriously influenced, and the use experience of a user is reduced.
Disclosure of Invention
An object of the embodiment of the application is to provide an electronic cigarette liquid, a preparation method of a taste modifier for the electronic cigarette liquid, and a new technical scheme of the preparation method of the electronic cigarette liquid.
According to a first aspect of the embodiment of the application, an electronic cigarette liquid is provided, which comprises the following components in parts by mass:
0.1-5 parts of taste modifier, 0-10 parts of herbal extract, 2-25 parts of tobacco essence, 0-6 parts of nicotine and 50-90 parts of solvent;
wherein the taste modifier comprises an extract of the seeds of an acronychia.
Optionally, the electronic cigarette liquid comprises, by mass:
1-3 parts of taste modifier, 3-8 parts of herbal extract, 12-20 parts of tobacco essence, 2-5 parts of nicotine and 64-85 parts of solvent.
Optionally, the taste modifier further comprises an adjuvant comprising at least one of bruguiera alba extract, citrus peel extract, grapefruit peel extract, lotus plumule extract, and celery leaf extract.
Optionally, in the taste modifier, the mass ratio of the emblic leafflower fruit extract to the adjuvant is 1: (0.5-10).
Optionally, the weight ratio of the emblic leafflower fruit extract, the bruguiera alba extract, the shaddock peel extract and the celery leaf extract is 1: (0.1-5): (0.1-2): (0.1-1).
Optionally, the mass ratio of the oil orange extract, the white olive extract, the dried orange peel extract, the shaddock peel extract, the lotus plumule extract and the celery leaf extract is 1: (0.1-5): (0.1-2): (0.1-1): (0.1-1): (0.1-2).
Optionally, the solvent comprises a lower alcohol and/or water.
According to a second aspect of embodiments of the present application, there is provided a method for preparing a taste modifier for an electronic cigarette liquid of the first aspect, where the raw material of the taste modifier includes a solid component and a liquid component, and the method for preparing the taste modifier includes:
weighing the solid component, crushing the solid component and then sieving the crushed solid component;
adding the liquid component into the sieved solid component, soaking for 2-6h, and separating out the taste modifier;
wherein the sieving mesh range is 20-100 mesh, the soaking time range is 2-6h, the separation temperature range is 0-100 deg.C, and the separation time range is 0.5-6h.
Optionally, the separation operation is distillation, sonication or extraction.
According to a third aspect of embodiments of the present application, there is provided a method for preparing the electronic cigarette liquid of the first aspect, including:
weighing the taste modifier, the herbal extract, the tobacco flavor and the nicotine, and mixing to obtain a mixture;
and uniformly mixing the mixture with the measured solvent to obtain the electronic cigarette liquid.
One technical effect of the embodiment of the application is as follows:
the embodiment of the application provides an electronic cigarette liquid, wherein a taste modifier is added into a cigarette liquid formula, and the taste modifier comprises an oil orange extract. The taste modifier can make the electronic cigarette liquid slightly bitter during smoking, reduce the sweet and greasy feeling of the electronic cigarette liquid during smoking, is closer to the sensory quality of the traditional cigarette, and greatly improves the taste of the electronic cigarette liquid. And this application electron cigarette tobacco juice is not bitter in the mouth after the suction, has the aftertaste taste of remaining sweet on the contrary, has promoted the experience that the user used the electron cigarette.
Further features of the present application and advantages thereof will become apparent from the following detailed description of exemplary embodiments thereof, which is to be read in connection with the accompanying drawings.
Drawings
The accompanying drawings, which are incorporated in and constitute a part of the specification, illustrate embodiments of the application and together with the description, serve to explain the principles of the application.
Fig. 1 is a flowchart of a method for preparing a taste modifier for an e-cigarette liquid according to an embodiment of the present application.
Detailed Description
Various exemplary embodiments of the present application will now be described in detail with reference to the accompanying drawings. It should be noted that: the relative arrangement of the components and steps, the numerical expressions, and numerical values set forth in these embodiments do not limit the scope of the present application unless specifically stated otherwise.
The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the application, its application, or uses.
Techniques, methods, and apparatus known to those of ordinary skill in the relevant art may not be discussed in detail but are intended to be part of the specification where appropriate.
In all examples shown and discussed herein, any particular value should be construed as exemplary only and not as limiting. Thus, other examples of the exemplary embodiments may have different values.
It should be noted that: like reference numbers and letters refer to like items in the following figures, and thus, once an item is defined in one figure, further discussion thereof is not required in subsequent figures.
Electronic cigarettes, an important class of products in new tobacco products, can atomize a small amount of nicotine-containing or nicotine-free solution into particles, which are then inhaled directly by the consumer. The electronic cigarette generates smoke in an atomizing mode, does not produce tar and carbon monoxide, hardly produces secondary-hand smoke harm, and is regarded as a pollution-free smoking cessation product or a tobacco substitute. The solvent formula of the electronic cigarette liquid has very important influence on the sensory quality of the electronic cigarette, the existing solvent of the electronic cigarette liquid mainly comprises propylene glycol and glycerol, and the taste of the electronic cigarette is seriously influenced due to the excessively greasy sweet taste of the glycerol. Therefore, the electronic cigarette liquid which can provide proper smoking experience for users in the aspects of aftertaste and sweet and greasy feeling on the basis of keeping the fragrance, the dryness and the amount of the cigarette liquid is needed.
The embodiment of the application provides an electron cigarette tobacco juice, by mass fraction, includes:
0.1-5 parts of taste modifier, 0-10 parts of herbal extract, 2-25 parts of tobacco essence, 0-6 parts of nicotine and 50-90 parts of solvent;
wherein the taste modifier comprises an extract of the seeds of an acronychia.
The electronic cigarette liquid provided by the embodiment of the application is added with a taste modifier in a cigarette liquid formula, wherein the taste modifier comprises an oil orange extract with natural bitter taste. The taste modifier can make the electronic cigarette liquid slightly bitter during smoking, reduce the sweet and greasy feeling of the electronic cigarette liquid during smoking, is closer to the sensory quality of the traditional cigarette, and greatly improves the taste of the electronic cigarette liquid. And this application electron cigarette tobacco juice is not bitter in the mouth after the suction, has the aftertaste taste of remaining sweet on the contrary, has promoted the user and has used the experience of electron cigarette.
Specifically, the raw material of the taste modifier may include a solid component and a liquid component, and the taste modifier is prepared by first soaking the solid component in the liquid component, and then separating to obtain the liquid taste modifier, and the liquid component may include at least one of water, ethanol and propylene glycol. For example, the extract of the plant emblica officinalis is prepared by first immersing the plant emblica officinalis in a liquid component and then separating to obtain a liquid extract of the plant emblica officinalis. In addition, the range of the part by mass of the taste modifier in the cigarette liquid of the electronic cigarette is preferably 1-3 parts.
The taste modifier represented by the extract of the citrus reticulata blanco is a food with natural bitter taste, the citrus reticulata blanco has the functions of clearing heat and cooling blood, promoting digestion and strengthening stomach, and promoting the production of body fluid and relieving cough, and if the solvent in the cigarette liquid of the electronic cigarette contains glycerol, the sweet and greasy feeling brought by the solvents such as the glycerol can be well neutralized. The taste of the electronic cigarette liquid during smoking is closer to the taste of the traditional cigarette, and the smoking taste of the electronic cigarette is improved.
Specifically, the range of the parts by weight of the herbal extract in the electronic cigarette liquid is preferably 3-8 parts, and the herbal extract is a plant extract, for example, the herbal extract may be a water extract of flowers such as safflower, lily or peony, or a water extract of grass such as purslane, black nightshade or green cabbage, or a water extract of tobacco such as tobacco leaf, so as to improve the freshness of the electronic cigarette liquid, but the herbal extract is not limited to the plant extract. The cigarette essence in the electronic cigarette liquid preferably accounts for 12-20 parts by weight, is prepared from multiple spices, has a certain fragrance, and can be directly used for a mixture for perfuming tobacco to improve the fragrance in the electronic cigarette liquid. The preferred mass part range of the nicotine in the electronic cigarette liquid is 2-5 parts, and the nicotine is alkaloid existing in solanaceae plants (solanum), is an important component of the electronic cigarette liquid, can ensure the nerve stimulation effect in the electronic cigarette liquid, and brings the smoking pleasure to users.
Optionally, the taste modifier further comprises an adjuvant comprising at least one of bruguiera alba extract, citrus peel extract, citrus grandis peel extract, lotus plumule extract, and celery leaf extract.
Specifically, the white olive has the effects of clearing away heat and toxic materials, eliminating phlegm and removing food retention, the dried orange peel and the shaddock peel have the effects of regulating qi, invigorating stomach, eliminating dampness and eliminating phlegm, the lotus plumule has the effects of clearing away heat, soothing the nerves and strengthening the heart, and the celery leaf has the effects of invigorating stomach, promoting urination, purifying blood, regulating menstruation, reducing blood pressure, calming, supplementing iron, supplementing calcium and the like. After at least one of the white olive, the dried orange peel, the shaddock peel, the lotus plumule and the celery leaves is combined with the oil orange, the extracts of various solid components can have certain fresh mouthfeel and medicinal effect on the basis of keeping certain bitter taste, not only can improve the mouthfeel of the electronic cigarette liquid, but also can play a certain role in medical care and health care.
Optionally, in the taste modifier, the mass ratio of the acronym extract to the adjuvant is 1: (0.5-10).
In particular, when the taste modifier comprises an extract of the citrus reticulata blanco, the extract of the citrus reticulata blanco can enable the electronic cigarette liquid of the application to keep low sweet and greasy feeling when being smoked and has the effect of returning sweet. And the addition of the auxiliary agent can combine the emblic leafflower fruit extract and the auxiliary agent, so that the electronic cigarette liquid has certain fresh mouthfeel and medicinal effect.
Optionally, the weight ratio of the emblic leafflower fruit extract, the bruguiera alba extract, the shaddock peel extract and the celery leaf extract is 1: (0.1-5): (0.1-2): (0.1-1).
In a specific embodiment, the auxiliary agent comprises the white olive extract, the shaddock peel extract and the celery leaf extract, and the weight ratio of the oil orange extract to the white olive extract to the shaddock peel extract to the celery leaf extract is 1.5:2:3:1. in the embodiment, on the basis of ensuring the components of the oil oranges and the white olive, the component content of the shaddock peel is increased, and the effects of regulating qi, invigorating stomach, eliminating dampness and eliminating phlegm of the cigarette liquid of the electronic cigarette are improved. Optionally, the mass ratio of the oil orange extract, the white olive extract, the dried orange peel extract, the shaddock peel extract, the lotus plumule extract and the celery leaf extract is 1: (0.1-5): (0.1-2): (0.1-1): (0.1-1): (0.1-2).
In a specific embodiment, the adjuvant comprises an olive extract, a dried orange peel extract, a shaddock peel extract, a lotus plumule extract and a celery leaf extract, wherein the mass ratio of the oil orange extract, the olive extract, the dried orange peel extract, the shaddock peel extract, the lotus plumule extract and the celery leaf extract is 2:2:1:1:0.5:1. in the embodiment, the flavor modifier takes the olea europaea and the white olive as main components, and combines the effects of heat clearing, blood cooling, digestion promoting, stomach invigorating, body fluid engendering, cough relieving, heat clearing, detoxifying, phlegm eliminating and food retention removing of the olea europaea, so that the flavor modifier can keep high freshness and reduce the sweet and greasy feeling of the electronic cigarette liquid.
In another specific embodiment, the adjuvant comprises the bruguiera gymnorrhiza extract, the dried orange peel extract, the shaddock peel extract, the lotus plumule extract and the celery leaf extract, and the weight ratio of the olea alba extract, the bruguiera gymnorrhiza extract, the dried orange peel extract, the shaddock peel extract, the lotus plumule extract and the celery leaf extract is 1.5:2:0.5:1:0.5:1. in this embodiment, the taste modifier also takes the olea europaea and the bruguiera gymnorrhiza as main components, so that the sweet and greasy feeling of the electronic cigarette liquid can be further reduced.
Optionally, the solvent includes lower alcohol and/or water, and the lower alcohol may include aqueous solvents such as propylene glycol, glycerol, ethanol, and the like.
Specifically, the mass part range of the solvent in the electronic cigarette liquid is preferably 64-85 parts, the propylene glycol in the solvent can be replaced by a propylene glycol instead of the solvent, the glycerol in the solvent can be replaced by a glycerol instead of the solution, and the glycerol can increase the smoke amount when the electronic cigarette liquid is atomized and improve the smoking effect of the electronic cigarette liquid. The solvent in the electronic cigarette tobacco juice can uniformly mix the taste modifier, the herbal extract, the tobacco essence and the nicotine, so that the stability of the electronic cigarette tobacco juice during smoking is ensured. In addition, the solvent may also be an oily solvent, which is not limited in the examples of the present application.
With reference to fig. 1, the embodiment of the application further provides a preparation method of the taste modifier for the cigarette liquid of the electronic cigarette, the raw materials of the taste modifier comprise a solid component and a liquid component, and the preparation method of the taste modifier comprises the following steps:
s101, weighing the solid component, crushing the solid component and sieving the crushed solid component;
s102, adding the liquid component into the sieved solid component, soaking for 2-6h, and separating out the taste modifier;
wherein the sieving mesh range is 20-100 mesh, soaking time range is 2-6h, separation temperature range is 0-100 deg.C, preferably 30-80 deg.C, and separation time range is 0.5-6h, preferably 2-4h.
Specifically, the taste modifier for the electronic cigarette liquid obtained by the preparation method provided by the embodiment of the application can make the electronic cigarette liquid slightly bitter in taste during smoking, reduce the sweet greasy feeling during smoking of the electronic cigarette liquid, is closer to the sensory quality of the traditional cigarette, and greatly improves the taste of the electronic cigarette liquid. And this application electron cigarette tobacco juice is not bitter in the mouth after the suction, has the aftertaste taste of remaining sweet on the contrary, has promoted the experience that the user used the electron cigarette.
Optionally, the raw material of the taste modifier comprises a solid component and a liquid component, and the mass ratio of the solid component to the liquid component is in the range of 1 (8-15).
Specifically, in the preparation process of the taste modifier, a solid component and a liquid component need to be mixed firstly, and then the mixture is separated to obtain the taste modifier, so that the solid component and the liquid component are fully fused. The mass ratio of the solid component to the liquid component is controlled within the range, so that the solid component can be better fused into the liquid component in the distillation process of the taste modifier, the required taste modifier is extracted, the sweet and greasy feeling effect during smoking of the electronic cigarette liquid is effectively reduced, and the cigarette taste of the electronic cigarette liquid is improved. The solid component comprises at least one of oil orange, white olive, dried orange peel, shaddock peel, lotus plumule and celery leaf, and the liquid component comprises at least one of water, ethanol and propylene glycol. The solid component is soaked in the liquid component and separated to obtain one or more of an oil orange extract, a white olive extract, a dried orange peel extract, a shaddock peel extract, a lotus plumule extract and a celery leaf extract, namely the taste modifier.
Optionally, the separation operation is distillation, sonication or extraction.
Specifically, after the taste modifier is formed, in order to improve the fusion degree of the solid component and the liquid component and fully exert the function of the solid component, the solid component and the liquid component can be subjected to separation operations such as distillation, ultrasound and extraction under a certain high-temperature condition, so that the sweet and greasy feeling of the electronic cigarette liquid can be effectively inhibited by the taste modifier, and the smoking experience of the electronic cigarette can be improved. The embodiment of the application also provides a preparation method of the electronic cigarette liquid, which comprises the following steps:
s201, weighing the taste modifier, the herbal extract, the tobacco essence and the nicotine, and mixing to obtain a mixture;
s202, uniformly mixing the mixture with the measured solvent to obtain the electronic cigarette liquid.
Specifically, the electronic cigarette liquid obtained by the preparation method provided by the embodiment of the application has a slightly bitter taste during smoking, the sweet and greasy feeling during smoking of the electronic cigarette liquid is reduced, the sensory quality of the electronic cigarette liquid is closer to that of a traditional cigarette, and the taste of the electronic cigarette liquid is greatly improved. And this application electron cigarette tobacco juice is not bitter in the mouth after the suction, has the aftertaste taste of remaining sweet on the contrary, has promoted the experience that the user used the electron cigarette.
The invention is further illustrated by the following specific examples and comparative examples (except the taste modifier, other raw materials are all common goods in the electronic cigarette industry and meet the edible standard).
Example 1
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
3% of herbal extract, 15% of tobacco essence, 2% of nicotine, 1% of taste modifier and 79% of solvent (specifically comprising 29% of propylene glycol and 50% of glycerol);
wherein the taste modifier is obtained by steam distilling fructus Phyllanthi.
The preparation method of the electronic cigarette liquid comprises the following steps:
(1) Preparing a taste modifier: weighing 50g of emblic leafflower fruit, removing cores of the emblic leafflower fruit and crushing, adding the obtained product into 500g of water according to a solid-to-liquid ratio of 1;
(2) Uniformly mixing the herbal extract, tobacco essence, nicotine, propylene glycol, glycerol and the taste modifier obtained in the step (1) according to a mass ratio to obtain the electronic cigarette liquid.
Example 2
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
4% of herbal extract, 12% of tobacco essence, 3% of nicotine, 3% of taste modifier and 78% of solvent (specifically comprising 28% of propylene glycol and 50% of glycerol);
wherein the taste modifier is prepared from oil orange, white olive, dried orange peel, shaddock peel, lotus plumule and celery leaf according to the mass ratio of 2:2:1:1:0.5:1, mixing, and extracting by steam distillation.
The preparation method of the electronic cigarette liquid comprises the following steps:
(1) Preparing a taste modifier: weighing 20g of emblic leafflower fruit, 20g of white olive, 10g of dried orange peel, 10g of shaddock peel, 5g of lotus plumule and 10g of celery leaf, crushing the raw materials, sieving the crushed raw materials by a 50-mesh sieve, adding the crushed raw materials into 1125g of water according to a solid-liquid ratio of 1;
(2) Uniformly mixing the herbal extract, tobacco essence, nicotine, propylene glycol, glycerol and the taste modifier obtained in the step (1) according to a mass ratio to obtain the electronic cigarette liquid.
Example 3
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
2% of herbal extract, 20% of tobacco essence, 3% of nicotine, 2% of taste modifier and 73% of solvent (specifically comprising 10% of propylene glycol, 15% of diglycerol, 20% of triethylene glycol and 28% of glycerol);
wherein the taste modifier is prepared from oil orange, white olive, dried orange peel, shaddock peel, lotus plumule and celery leaf according to the mass ratio of 1.5:2:0.5:1:0.5:1, mixing, performing ultrasonic treatment, and extracting to obtain the product.
The preparation method of the electronic cigarette liquid comprises the following steps:
(1) Preparing a taste modifier: weighing 15g of emblic leafflower fruit, 20g of white olive, 5g of dried orange peel, 10g of shaddock peel, 5g of lotus plumule and 10g of celery leaf, crushing the raw materials, sieving the crushed raw materials by a 30-mesh sieve, adding the crushed raw materials into 520g of 60% ethanol according to the solid-to-liquid ratio of 1:8, soaking the raw materials for 2 hours, performing ultrasonic treatment for 30min at 250W, and extracting the mixture at 30 ℃ to obtain a taste modifier;
(2) Uniformly mixing the herbal extract, tobacco essence, nicotine, propylene glycol, glycerol and the taste modifier obtained in the step (1) according to a mass ratio to obtain the electronic cigarette liquid.
Example 4
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
8% of herbal extract, 15% of tobacco essence, 5% of nicotine, 1.5% of taste modifier and 70.5% of solvent (specifically comprising 25.5% of propylene glycol and 45% of glycerol);
wherein the taste modifier is prepared from oil orange, white olive, shaddock peel and celery leaves according to the mass ratio of 1.5:2:3:1, mixing, performing ultrasonic treatment, and extracting to obtain the product.
The preparation method of the electronic cigarette liquid comprises the following steps:
(1) Preparing a taste modifier: weighing 15g of emblic leafflower fruit, 20g of white olive, 30g of shaddock peel and 10g of celery leaf, crushing the raw materials, sieving the crushed raw materials by a 30-mesh sieve, adding the crushed raw materials into 650g of water according to a solid-to-liquid ratio of 1;
(2) Uniformly mixing the herbal extract, tobacco essence, nicotine, propylene glycol, glycerol and the taste modifier obtained in the step (1) according to a mass ratio to obtain the electronic cigarette liquid.
Example 5
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
5% of herbal extract, 15% of tobacco essence, 3% of nicotine, 1% of taste modifier and 76% of solvent (specifically comprising 26% of propylene glycol and 50% of glycerol);
wherein the taste modifier is obtained by steam distilling fructus Phyllanthi.
The preparation method of the electronic cigarette liquid is the same as that of the embodiment 1.
Example 6
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
10% of herbal extract, 15% of tobacco essence, 3% of nicotine, 1% of taste modifier and 71% of solvent (specifically comprising 21% of propylene glycol and 50% of glycerol);
wherein the taste modifier is obtained by steam distilling fructus Phyllanthi.
The preparation method of the electronic cigarette liquid is the same as that of the embodiment 1.
Example 7
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
5% of herbal extract, 2% of tobacco essence, 3% of nicotine, 1% of taste modifier and 89% of solvent (specifically comprising 39% of propylene glycol and 50% of glycerol);
wherein the taste modifier is obtained by steam distilling fructus Phyllanthi.
The preparation method of the electronic cigarette liquid is the same as that of the embodiment 1.
Example 8
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
5% of herbal extract, 25% of tobacco essence, 3% of nicotine, 1% of taste modifier and 66% of solvent (specifically comprising 16% of propylene glycol and 50% of glycerol);
wherein the taste modifier is obtained by steam distilling fructus Phyllanthi.
The preparation method of the electronic cigarette liquid is the same as that of the embodiment 1.
Example 9
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
5% of herbal extract, 15% of tobacco essence, 6% of nicotine, 1% of taste modifier and 73% of solvent (specifically comprising 23% of propylene glycol and 50% of glycerol);
wherein the taste modifier is obtained by steam distilling fructus Phyllanthi.
The preparation method of the electronic cigarette liquid is the same as that of the embodiment 1.
Example 10
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
5% of herbal extract, 15% of tobacco essence, 3% of nicotine, 0.1% of taste modifier and 76.9% of solvent (specifically comprising 26.9% of propylene glycol and 50% of glycerol);
wherein the taste modifier is obtained by steam distilling fructus Phyllanthi.
The preparation method of the electronic cigarette liquid is the same as that of the embodiment 1.
Example 11
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
5% of herbal extract, 15% of tobacco essence, 3% of nicotine, 5% of taste modifier and 72% of solvent (specifically comprising 22% of propylene glycol and 50% of glycerol);
wherein the taste modifier is obtained by steam distilling fructus Phyllanthi.
The preparation method of the electronic cigarette liquid is the same as that of the embodiment 1.
Comparative example 1
The electronic cigarette liquid is prepared from the following raw materials in percentage by mass:
5% of herbal extract, 15% of tobacco essence, 3% of nicotine and 77% of solvent (specifically comprising 27% of propylene glycol and 50% of glycerol);
the difference from example 5 is that no taste modifier is included.
The preparation method of the electronic cigarette liquid comprises the following steps:
uniformly mixing the herbal extract, tobacco essence, nicotine, propylene glycol and glycerol according to the mass ratio to obtain the electronic cigarette liquid.
The industry standard for the electronic cigarette liquid quality judgment is given in table 1.
TABLE 1
Figure BDA0003134172230000121
The electronic cigarette liquids prepared in the above examples and comparative examples were added to smoking sets at the same addition amount, and smoking evaluation was performed according to the industry scoring standards of table 1, and the evaluation results are shown in table 2.
TABLE 2
Figure BDA0003134172230000122
As can be seen from table 2, the electronic cigarette liquid with the taste modifier provided in the embodiment of the present application is significantly superior to the electronic cigarette liquid of the comparative example in aftertaste and sweet and greasy feeling on the basis of maintaining the fragrance, dryness and smoke amount, so that the sweet and greasy feeling of the electronic cigarette liquid during smoking is reduced, and the sensory quality of the electronic cigarette liquid is closer to that of a conventional cigarette. Make the electron cigarette tobacco juice that this application embodiment provided can bring better electron cigarette suction for the consumer and experience, improve the travelling comfort that the consumer used the electron cigarette.
Although some specific embodiments of the present application have been described in detail by way of example, it should be understood by those skilled in the art that the above examples are for illustrative purposes only and are not intended to limit the scope of the present application. It will be appreciated by those skilled in the art that modifications may be made to the above embodiments without departing from the scope and spirit of the present application. The scope of the application is defined by the appended claims.

Claims (10)

1. The electronic cigarette liquid is characterized by comprising the following components in parts by mass:
0.1-5 parts of taste modifier, 0-10 parts of herbal extract, 2-25 parts of tobacco essence, 0-6 parts of nicotine and 50-90 parts of solvent;
wherein the taste modifier comprises an extract of the seeds of an acronychia.
2. The e-cigarette liquid of claim 1, wherein the e-cigarette liquid comprises, in parts by mass:
1-3 parts of taste modifier, 3-8 parts of herbal extract, 12-20 parts of tobacco essence, 2-5 parts of nicotine and 64-85 parts of solvent.
3. The e-cigarette liquid of claim 1, wherein the taste modifier further comprises an adjuvant comprising at least one of bruguiera alba extract, citrus peel extract, grapefruit peel extract, lotus plumule extract, and celery leaf extract.
4. The e-cigarette liquid of claim 3, wherein the flavor modifier comprises the following components in a mass ratio of the emblic leafflower fruit extract to the auxiliary agent of 1: (0.5-10).
5. The electronic cigarette liquid as claimed in claim 3, wherein the mass ratio of the oil orange extract, the white olive extract, the shaddock peel extract and the celery leaf extract is (1 (0.1-5): 0.1-2): 0.1-1.
6. The electronic cigarette liquid of claim 3, wherein the weight ratio of the Citrus reticulata extract, the Canarium album extract, the dried orange peel extract, the shaddock peel extract, the lotus plumule extract and the celery leaf extract is 1: (0.1-5): (0.1-2): (0.1-1): (0.1-1): (0.1-2).
7. The e-liquid of claim 1, wherein the solvent comprises a lower alcohol and/or water.
8. A method for preparing a taste modifier for an electronic cigarette liquid as claimed in any one of claims 1 to 7, wherein the raw material of the taste modifier comprises a solid component and a liquid component, and the method for preparing the taste modifier comprises the following steps:
weighing the solid component, crushing the solid component and then sieving the crushed solid component;
adding the liquid component into the sieved solid component, soaking for 2-6h, and separating out the taste modifier;
wherein the sieving mesh range is 20-100 mesh, the soaking time range is 2-6h, the separation temperature range is 0-100 deg.C, and the separation time range is 0.5-6h.
9. The process for preparing a taste modifier according to claim 8 wherein said separation operation is distillation, sonication or extraction.
10. The method for preparing the electronic cigarette liquid according to any one of claims 1 to 7, comprising:
weighing the taste modifier, the herbal extract, the tobacco flavor and the nicotine, and mixing to obtain a mixture;
and uniformly mixing the mixture with the measured solvent to obtain the electronic cigarette liquid.
CN202110714172.5A 2021-06-25 2021-06-25 Electronic cigarette liquid, preparation method of taste modifier of electronic cigarette liquid and preparation method of electronic cigarette liquid Pending CN115517397A (en)

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