CN105969528A - Extracting method for rose essential oil - Google Patents
Extracting method for rose essential oil Download PDFInfo
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- CN105969528A CN105969528A CN201610415114.1A CN201610415114A CN105969528A CN 105969528 A CN105969528 A CN 105969528A CN 201610415114 A CN201610415114 A CN 201610415114A CN 105969528 A CN105969528 A CN 105969528A
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- oil
- flos rosae
- rosae rugosae
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses an extracting method for rose essential oil. High-quality rose flowers are selected, and then the rose flowers are subjected to soaking, homogenizing, distillation, condensation and oil-liquid separation to extract the rose essential oil. According to the extracting method, the technology is simple, operation is convenient, the safety is high, little rose essential oil is lost in the extracting process, the oil obtaining rate is high, the quality of the rose essential oil is high, and the production cost is low.
Description
Technical field
The present invention relates to extraction of essential oil technical field, the concrete extracting method for a kind of Flos Rosae Rugosae quintessence oil.
Background technology
Flos Rosae Rugosae, Rosaceae Rosa fallen leaves bush, its flower, color, perfume (or spice), shape are the most beautiful, have high economic worth.It is described as " JINHUA ".Flos Rosae Rugosae quintessence oil is the hat of flower oil, has gracefulness, the Rose Essentielle overflowed such as honey, fragrance soft, fine and smooth, fragrant and sweet.Flos Rosae Rugosae quintessence oil is expensive, has the good reputation of " liquid golden ", is the famous and precious senior concentration essence in the world, is the fine work in essential oil, is the most important but also expensive raw material manufacturing senior famous and precious perfume.Not only it is used for manufacturing the cosmetics such as beauty treatment, skin protection, hair care, is also widely used in medicine and food.Flos Rosae Rugosae quintessence oil naturally fragrance enters after brain via olfactory nerves, anterior lobe of cerebrum can be stimulated to secret out of interior coffee and eliminate and two kinds of hormone eliminated by brain coffee, make spirit present the state of the most comfortable, be the optimal good recipe guarding soul；Flos Rosae Rugosae quintessence oil can also anti-inflammation and sterilization, anti-communicable disease, anti-inflammation, anti-spasm, promote cell metabolism and cell regeneration function；There is the effects such as blood circulation promoting, nourishes rough skin, slow down aging, promotion hormone secretion, can be used for skin clean, facial massage, body massage, fragrance SPA etc..The extracting method of existing Flos Rosae Rugosae quintessence oil mainly has:
1, fat absorption method, utilizes the quintessence oil in oils and fats absorption Flos Rosae Rugosae, although technique is simple, but later separation quintessence oil is the most difficult with oils and fats.
2, extraction, uses the low boiling point solvent such as organic solvent such as petroleum ether, hexane to soak Flos Rosae Rugosae, the mixture of quintessence oil and organic solvent is obtained by extraction, organic solvent is then distilled off, obtains Flos Rosae Rugosae quintessence oil；This kind of method extraction of essential oil rate height, low cost, but easily cause organic solvent residual, make Flos Rosae Rugosae quintessence oil fragrance the purest.
3, supercritical extraction, uses supercritical carbon dioxide fluid to soak, Flos Rosae Rugosae quintessence oil is obtained by extraction；This kind of method has yield height and high quality；But owing to supercritical carbon dioxide fluid dissolubility is too strong, the non-derived essential oil in Flos Rosae Rugosae also is extracted out, and the moisture content in Flos Rosae Rugosae is not readily separated so that Flos Rosae Rugosae quintessence oil is easy mildew during storage, limits the range of application of products obtained therefrom.
Therefore, developing a kind of technique relatively simple, and quintessence oil pick-up rate is high, can reduce quintessence oil water content simultaneously, the method being suitable to preservation is those skilled in the art institute urgent need to solve the problem.
Summary of the invention
The extracting method of a kind of Flos Rosae Rugosae quintessence oil that the present invention proposes, improves the extraction pick-up rate of Flos Rosae Rugosae quintessence oil, simplifies technique.
The technical scheme is that and be achieved in that: the extracting method of a kind of Flos Rosae Rugosae quintessence oil, comprise the following steps:
(1) full, the new fresh-rose of free from insect pests is selected；
(2) soaking, by the edible salt water of 10%～15%, the Flos Rosae Rugosae chosen, killed by the pathogenic bacteria on Flos Rosae Rugosae, soak time is 1～5 day；
(3) Flos Rosae Rugosae soaked and distilled water being added in refiner, carry out homogenate and pulverize, Homogenization time is 5～10 minutes, and the weight ratio of Flos Rosae Rugosae and distilled water is 1:1.5；
(4) by carrying out distillation 3-4 hour in the Flos Rosae Rugosae serosity after homogenate pulverizing and distilled water addition distillating still, obtaining oil mixing with water steam, vapo(u)rizing temperature is 90～95 DEG C, and distillation time is 4～5 hours；The weight ratio of Flos Rosae Rugosae serosity and distilled water is 1:2.5；
(5) the oil mixing with water steam obtained by distillating still condenses through condenser, obtains oil-water mixture；
(6) being delivered in oil water separator by oil-water mixture, the temperature of oil-water separation is 20～25 DEG C；The upper strata collecting oil water separator isolated is oil reservoir, is Flos Rosae Rugosae quintessence oil.
Further, in still-process, being heated to distillation time is 15～20 minutes, and rear continuation is distilled 3-4 hour.
Further, after having carried out distillation and condensation, the oil mixing with water liquid obtained is carried out second distillation and time condensation.
Further, again carry out distilling and condensing by the liquid of the middle lower floor in oil water separator, again extract Flos Rosae Rugosae quintessence oil.
The invention have the benefit that the extracting method of a kind of Flos Rosae Rugosae quintessence oil of the present invention, technique is simple, easy to operate, and safety is high, and Flos Rosae Rugosae quintessence oil loses few during mentioning, and obtains oil rate high, and the quality of product is high, and production cost is low.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, broadly fall into the scope of protection of the invention.
The extracting method of a kind of Flos Rosae Rugosae quintessence oil, comprises the following steps:
(1) full, the new fresh-rose of free from insect pests is selected；
(2) soaking, by the edible salt water of 10%～15%, the Flos Rosae Rugosae chosen, killed by the pathogenic bacteria on Flos Rosae Rugosae, soak time is 1～5 day；
(3) Flos Rosae Rugosae soaked and distilled water being added in refiner, carry out homogenate and pulverize, Homogenization time is 5～10 minutes, and the weight ratio of Flos Rosae Rugosae and distilled water is 1:1.5；
(4) by carrying out distillation 3-4 hour in the Flos Rosae Rugosae serosity after homogenate pulverizing and distilled water addition distillating still, obtaining oil mixing with water steam, vapo(u)rizing temperature is 90～95 DEG C, and distillation time is 4～5 hours；The weight ratio of Flos Rosae Rugosae serosity and distilled water is 1:2.5；
(5) the oil mixing with water steam obtained by distillating still condenses through condenser, obtains oil-water mixture；
(6) being delivered in oil water separator by oil-water mixture, the temperature of oil-water separation is 20～25 DEG C；The upper strata collecting oil water separator isolated is oil reservoir, is Flos Rosae Rugosae quintessence oil.
In still-process, being heated to distillation time is 15～20 minutes, and rear continuation is distilled 3-4 hour.
After having carried out distillation and condensation, the oil mixing with water liquid obtained is carried out second distillation and time condensation.
Again carry out distilling and condensing by the liquid of the middle lower floor in oil water separator, again extract Flos Rosae Rugosae quintessence oil.
The effective ingredient such as the edible salt water first using 10%～15% before homogenate soaks Flos Rosae Rugosae, can promote the cell wall breaking of Flos Rosae Rugosae, its quintessence oil are easier to release, improve the oil rate that obtains of quintessence oil, it is also possible to fresh-keeping, antioxygen anticorrosion, extend Flos Rosae Rugosae and store the time.
Distill for the first time, the oil reservoir purity height extracted through oil water separator after condensation, Flos Rosae Rugosae quintessence oil for high-quality, the oil reservoir purity extracted after the middle lower floor of oil water separator is again distilled and condensed is relatively low, for common Flos Rosae Rugosae quintessence oil, in secondary distillation, the Flos Rosae Rugosae quintessence oil composition in Flos Rosae Rugosae can be fully extracted in condensation.
After having carried out first time distillation, condensation, proceed second time distill, condense, then extract Flos Rosae Rugosae quintessence oil by oil water separator, it is possible to increase the purity of Flos Rosae Rugosae quintessence oil.
Present invention process is simple, easy to operate, and safety is high, and Flos Rosae Rugosae quintessence oil loses few during mentioning, and the quality of product is high, and production cost is low.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (4)
1. the extracting method of a Flos Rosae Rugosae quintessence oil, it is characterised in that: comprise the following steps:
(1) full, the new fresh-rose of free from insect pests is selected；
(2) soak, by the edible salt water of 10%～15%, the Flos Rosae Rugosae chosen, the pathogenic bacteria on Flos Rosae Rugosae killed,
Soak time is 1～5 day；
(3) Flos Rosae Rugosae soaked and distilled water are added in refiner, carry out homogenate and pulverize, Homogenization time
Being 5～10 minutes, the weight ratio of Flos Rosae Rugosae and distilled water is 1:1.5；
(4) the Flos Rosae Rugosae serosity after homogenate pulverizing and distilled water addition distillating still will carry out distillation 3-4 hour,
Obtaining oil mixing with water steam, vapo(u)rizing temperature is 90～95 DEG C, and distillation time is 4～5 hours；Flos Rosae Rugosae serosity
It is 1:2.5 with the weight ratio of distilled water；
(5) the oil mixing with water steam obtained by distillating still condenses through condenser, obtains oil-water mixture；
(6) being delivered in oil water separator by oil-water mixture, the temperature of oil-water separation is 20～25 DEG C；Receive
Integrate the upper strata of oil water separator isolated as oil reservoir, be Flos Rosae Rugosae quintessence oil.
The extracting method of a kind of Flos Rosae Rugosae quintessence oil the most according to claim 1, it is characterised in that: in distillation
During, being heated to distillation time is 15～20 minutes, and rear continuation is distilled 3-4 hour.
The extracting method of a kind of Flos Rosae Rugosae quintessence oil the most according to claim 1, it is characterised in that: will carry out
After complete distillation and condensation, the oil mixing with water liquid obtained is carried out second distillation and time condensation.
The extracting method of a kind of Flos Rosae Rugosae quintessence oil the most according to claim 1, it is characterised in that: by profit
The liquid of the middle lower floor in separator carries out distilling and condensing again, again extracts Flos Rosae Rugosae quintessence oil.
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| CN201610415114.1A CN105969528A (en) | 2016-06-14 | 2016-06-14 | Extracting method for rose essential oil |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106561793A (en) * | 2016-10-24 | 2017-04-19 | 丽江花花色玫瑰庄园有限公司 | Sterilization, enzyme (worm eggs) deactivation and color protection method for rose petals |
| CN106726685A (en) * | 2016-12-28 | 2017-05-31 | 安徽檀鑫科技有限公司 | A kind of Essence containing Rosa Damascana |
| CN109554226A (en) * | 2017-09-25 | 2019-04-02 | 宜兴市瑞优娜玫瑰产业有限公司 | A kind of preparation method of Rosa Damascana |
| CN109593610A (en) * | 2019-02-18 | 2019-04-09 | 昆山恒元生物科技有限公司 | A kind of method that Damask Rose flower refines essential oil |
| CN109957452A (en) * | 2017-12-22 | 2019-07-02 | 宜兴市瑞优娜玫瑰产业有限公司 | A kind of Rosa Damascana distillation extraction element |
| CN109957455A (en) * | 2017-12-22 | 2019-07-02 | 宜兴市瑞优娜玫瑰产业有限公司 | A kind of preparation method of high-purity Rosa Damascana |
| CN109957450A (en) * | 2017-12-22 | 2019-07-02 | 宜兴市瑞优娜玫瑰产业有限公司 | A kind of high-purity Rosa Damascana extraction element |
| CN110093211A (en) * | 2019-05-23 | 2019-08-06 | 佛山市欧若拉生物科技有限公司 | A kind of rose extraction process |
| CN110540895A (en) * | 2019-08-27 | 2019-12-06 | 吉林嘉美食品有限公司 | Extraction method of perilla oil |
| CN110839821A (en) * | 2018-08-21 | 2020-02-28 | 庐江县海神面业有限公司 | Preparation method of plant essential oil health-preserving noodles |
| CN111187671A (en) * | 2019-09-29 | 2020-05-22 | 郝兴群 | Extraction method of perilla leaf essential oil containing perilla flavone |
| CN111635828A (en) * | 2020-06-13 | 2020-09-08 | 王瑞雪 | Rose essential oil extraction method |
| CN111635827A (en) * | 2020-06-13 | 2020-09-08 | 王瑞雪 | Rose essence extraction system and extraction method |
| CN114806714A (en) * | 2022-02-11 | 2022-07-29 | 安徽盛世百川农林科技发展有限公司 | Rose essential oil extraction method |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106561793A (en) * | 2016-10-24 | 2017-04-19 | 丽江花花色玫瑰庄园有限公司 | Sterilization, enzyme (worm eggs) deactivation and color protection method for rose petals |
| CN106726685A (en) * | 2016-12-28 | 2017-05-31 | 安徽檀鑫科技有限公司 | A kind of Essence containing Rosa Damascana |
| CN109554226A (en) * | 2017-09-25 | 2019-04-02 | 宜兴市瑞优娜玫瑰产业有限公司 | A kind of preparation method of Rosa Damascana |
| CN109957450A (en) * | 2017-12-22 | 2019-07-02 | 宜兴市瑞优娜玫瑰产业有限公司 | A kind of high-purity Rosa Damascana extraction element |
| CN109957452A (en) * | 2017-12-22 | 2019-07-02 | 宜兴市瑞优娜玫瑰产业有限公司 | A kind of Rosa Damascana distillation extraction element |
| CN109957455A (en) * | 2017-12-22 | 2019-07-02 | 宜兴市瑞优娜玫瑰产业有限公司 | A kind of preparation method of high-purity Rosa Damascana |
| CN110839821A (en) * | 2018-08-21 | 2020-02-28 | 庐江县海神面业有限公司 | Preparation method of plant essential oil health-preserving noodles |
| CN109593610A (en) * | 2019-02-18 | 2019-04-09 | 昆山恒元生物科技有限公司 | A kind of method that Damask Rose flower refines essential oil |
| CN110093211A (en) * | 2019-05-23 | 2019-08-06 | 佛山市欧若拉生物科技有限公司 | A kind of rose extraction process |
| CN110540895A (en) * | 2019-08-27 | 2019-12-06 | 吉林嘉美食品有限公司 | Extraction method of perilla oil |
| CN111187671A (en) * | 2019-09-29 | 2020-05-22 | 郝兴群 | Extraction method of perilla leaf essential oil containing perilla flavone |
| CN111635828A (en) * | 2020-06-13 | 2020-09-08 | 王瑞雪 | Rose essential oil extraction method |
| CN111635827A (en) * | 2020-06-13 | 2020-09-08 | 王瑞雪 | Rose essence extraction system and extraction method |
| CN114806714A (en) * | 2022-02-11 | 2022-07-29 | 安徽盛世百川农林科技发展有限公司 | Rose essential oil extraction method |
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Application publication date: 20160928 |