CN109593610A - A kind of method that Damask Rose flower refines essential oil - Google Patents
A kind of method that Damask Rose flower refines essential oil Download PDFInfo
- Publication number
- CN109593610A CN109593610A CN201910120863.5A CN201910120863A CN109593610A CN 109593610 A CN109593610 A CN 109593610A CN 201910120863 A CN201910120863 A CN 201910120863A CN 109593610 A CN109593610 A CN 109593610A
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- China
- Prior art keywords
- water
- essential oil
- rose flower
- damask rose
- refines
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
A kind of method that Damask Rose flower refines essential oil, the present invention relates to essential oil preparation technical fields；Inner petals are chosen, is soaked in clear water immediately, is slowly stirred cleaning；Damask Rose flower petal feeding after cleaning is mixed up after carrying out being rapidly frozen 4-6 hours in the freezer of temperature in advance, after taking-up, is immediately placed in pre-heated water-bath distillation device；The water-bath distillation device for being put into freezing Damask Rose flower petal is continued to continue to be heated to 100 degrees Celsius under normal pressure；Essential oil is separated from water by the mixing liquid that discharge is condensed out by water cooler into oil water separator, and essential oil is injected in essential oil storage tank.It refines speed and is improved, advantageously account for Damask Rose spend the period it is short, it is perishable brought by defect, essential oil quality is high, and oil yield is significantly improved, and practicability is stronger.
Description
Technical field
The present invention relates to essential oil preparation technical fields, and in particular to a kind of method that Damask Rose flower refines essential oil.
Background technique
Rose is to be grown in a kind of semi-tropical cogongrass fragrance, and rose itself gives out a kind of lemon of natural strong
Fragrance has the special efficacy of stomach function regulating ventilation, restoring consciouness.Have antibacterial ability, cholera, acute gastroenteritis and chronic diarrhea can be treated, grows
Moisten skin, facilitates women skin maintenance and cosmetic benefits.It contains a large amount of vitamin C, is also the good merchantable brand of cosmetology.Adjust grease point
It secretes, is beneficial to oily skin and hair quality, cleaning skin can be added to the water, promoted blood circulation.
The blade of Damask Rose is celadon, has bristle on scape；Hose-in-hose is opened, petal edge color is slightly shallow, has
Texture as silks and satins；Purely, the careful fragrance of a flower makes its hat pressure beautiful and fragrant flowers, becomes the top grade in rose for oil, thus is widely cultivated
To extract Rosa Damascana.Since the period of Damask Rose flower is short, perishable, therefore, needing one kind being capable of rapidly extracting
The method of its essence, for obtaining high quality, the rose essence of high oil recovery.
Summary of the invention
In view of the defects and deficiencies of the prior art, the present invention intends to provide a kind of structure is simple, design rationally, make
The method for refining essential oil with convenient Damask Rose flower is refined speed and is improved, advantageously accounts for Damascus rose
It is rare spend the period it is short, it is perishable brought by defect, essential oil quality is high, and oil yield is significantly improved, and practicability is stronger.
To achieve the above object, the technical solution adopted by the present invention is that: its operating procedure is as follows:
1, raw material preparation:
Intact Damask Rose flower is selected, after outermost petal is rejected, chooses inner petals, immediately will
It is soaked in clear water, is slowly stirred cleaning；
2, broken wall is freezed:
Damask Rose flower petal after cleaning is sent into mix up in advance and carries out fast freezing 4-6 in the freezer of temperature
It after hour, after taking-up, is immediately placed in pre-heated water-bath distillation device, Damask Rose flower cell wall rupture；
3, it distills:
To be put into freezing Damask Rose flower petal water-bath distillation device continue to continue to be heated to 100 under normal pressure it is Celsius
Degree；
4, it condenses:
Water cooler is adjusted to 28 degrees Celsius, and is steamed the water generated under 100 degrees Celsius using water cooler at this temperature
Air cooling；
5, water-oil separating:
The mixing liquid that discharge is condensed out by water cooler, into oil water separator, by the separation of oil water separator,
Essential oil is separated from water, and essential oil is injected in essential oil storage tank.
Further, rose when cleaning in the step 1 to Damask Rose flower petal is in rhizome
On, it is picked after being cleaned using clear water, then by clean Damask Rose flower petal.
Further, the Damask Rose flower petal after cleaning is sent into the step 2 and mixes up temperature in advance
Before freezer, Damask Rose flower petal is shredded using scissors in advance.
Further, the cryogenic temperature of the freezer in the step 2 is 0 to -40 degree Celsius.
Further, the preheating temperature of the pre-heated water-bath distillation device in the step 2 is 40-80 degrees Celsius.
Further, the water in the water-bath distillation device in the step 2 is that the water after cleaning in step 1 passes through filtered pure
Water after change.
Further, the volume ratio of the water in the step water-bath distillation device and petal is 1:2.
After adopting the above method, the invention has the following beneficial effects: a kind of Damask Rose flower of the present invention refines essence
The method of oil is refined speed and is improved, and advantageously accounts for Damask Rose and spends the period short, perishable brought scarce
It falls into, essential oil quality is high, and oil yield is significantly improved, and practicability is stronger, and the present invention has structure simple, and setting is reasonable, system
Make the advantages such as cost is low.
Specific embodiment
Present embodiment (embodiment one) the technical solution adopted is that: its operating procedure is as follows:
Intact Damask Rose flower is selected, after outermost petal is rejected, chooses inner petals, immediately will
It is soaked in clear water, slowly shakes the stem branch being connected on rose, stirring and washing, after cleaning, using scissors by rose
After petal is shredded from stem branch, feeding mixes up in the freezer of temperature (cryogenic temperature is -35 degrees Celsius) in advance, carries out fast quickly cooling
Freeze, at the same time, after the water conservancy after above-mentioned cleaning is carried out water filtration purification with purification of water device, is sent into water-bath distillation device
In, and it is preheated to 60 degrees Celsius；Then, the Damask Rose flower design of scattered small flowers and plants valve after freezing 5 hours takes out, and is immediately placed in advance
In the water-bath distillation device of heating (volume ratio of water and petal is 1:2), Damask Rose flower cell wall rupture；By water-bath distillation
Device continues to continue to be heated to 100 degrees Celsius under normal pressure, generates vapor, and vapor, which is delivered to, is preheated to 28 degrees Celsius of water cooler
In, the vapor generated under 100 degrees Celsius is cooling；The mixing liquid that discharge is condensed out by water cooler, into water-oil separating
In device, by the separation of oil water separator, essential oil is separated from water, and essential oil is injected in essential oil storage tank.
After adopting the above method, present embodiment has the beneficial effect that a kind of big horse described in present embodiment
Scholar removes from office the method that rose refines essential oil, refines speed and is improved, advantageously accounts for Damask Rose and spend the period short, easy
Defect brought by rotten, essential oil quality is high, and oil yield is significantly improved, and practicability is stronger, and the present invention has structure letter
The advantages that list, setting is reasonable, low manufacture cost.
Embodiment two:
The operating procedure of the present embodiment is as follows: selecting intact Damask Rose flower, outermost petal is picked
After removing, chooses inner petals and pick, be soaked in clear water immediately, be slowly stirred cleaning using glass stirring rod, it will
Petal feeding after cleaning mixes up in the freezer of temperature (cryogenic temperature is -40 degrees Celsius) in advance, is rapidly frozen, with this
Meanwhile after the water conservancy after above-mentioned cleaning carried out water filtration purification with purification of water device, it is sent into water-bath distillation device, and pre-
Heat is to 70 degrees Celsius；Then, the Damask Rose flower design of scattered small flowers and plants valve after freezing 6 hours takes out, and is immediately placed in pre-heated
In water-bath distillation device (volume ratio of water and petal is 1:2), Damask Rose flower cell wall rupture；Water-bath distillation device is continued
Continue to be heated to 100 degrees Celsius under normal pressure, generate vapor, vapor is delivered in the water cooler for being preheated to 28 degrees Celsius, will
The vapor generated under 100 degrees Celsius is cooling；The mixing liquid that discharge is condensed out by water cooler, into oil water separator,
By the separation of oil water separator, essential oil is separated from water, and essential oil is injected in essential oil storage tank.
Embodiment three:
The operating procedure of the present embodiment is as follows: selecting intact Damask Rose flower, outermost petal is picked
After removing, chooses inner petals and pick, be soaked in clear water immediately, be slowly stirred cleaning using glass stirring rod, it will
Petal feeding after cleaning mixes up in the freezer of temperature (cryogenic temperature is -40 degrees Celsius) in advance, is rapidly frozen, with this
Meanwhile pure water will be added into water-bath distillation device, and be preheated to 75 degrees Celsius；Then, by the damascene after freezing 4.5 hours
It removes from office rose design of scattered small flowers and plants valve to take out, is immediately placed in pre-heated water-bath distillation device (volume ratio of water and petal is 1:2), big horse
Scholar removes from office the rupture of rose cell wall；Water-bath distillation device is continued to continue to be heated to 100 degrees Celsius under normal pressure, generates vapor, water
Steam is delivered in the water cooler for being preheated to 28 degrees Celsius, and the vapor generated under 100 degrees Celsius is cooling；It is condensed by water cooler
The mixing liquid of discharge of getting off, by the separation of oil water separator, essential oil is separated from water into oil water separator, and will
Essential oil injects in essential oil storage tank.
Example IV:
The operating procedure of the present embodiment is as follows: selecting intact Damask Rose flower, outermost petal is picked
After removing, inner petals are chosen, are soaked in clear water immediately, slowly shake the stem branch being connected on rose, stirring and washing,
After cleaning, after being shredded rose petal from stem branch using scissors, it is sent into and mixes up in the freezer of temperature (cryogenic temperature in advance
It is -20 degrees Celsius), it is rapidly frozen, at the same time, pure water will be added into water-bath distillation device, and it is Celsius to be preheated to 60
Degree；Then, the Damask Rose flower design of scattered small flowers and plants valve after freezing 4.5 hours takes out, and is immediately placed in pre-heated water-bath distillation
In device (volume ratio of water and petal is 1:2), Damask Rose flower cell wall rupture；By water-bath distillation device continue normal pressure under after
It is continuous to be heated to 100 degrees Celsius, vapor is generated, vapor is delivered in the water cooler for being preheated to 28 degrees Celsius, by 100 degrees Celsius
The vapor of lower generation is cooling；The mixing liquid that discharge is condensed out by water cooler, into oil water separator, by grease point
Separation from device, essential oil is separated from water, and essential oil is injected in essential oil storage tank.
The above is only used to illustrate the technical scheme of the present invention and not to limit it, and those of ordinary skill in the art are to this hair
The other modifications or equivalent replacement that bright technical solution is made, as long as it does not depart from the spirit and scope of the technical scheme of the present invention,
It is intended to be within the scope of the claims of the invention.
Claims (7)
1. a kind of method that Damask Rose flower refines essential oil, it is characterised in that: its operating procedure is as follows:
(1), raw material preparation:
Intact Damask Rose flower is selected, after outermost petal is rejected, inner petals is chosen, is soaked immediately
It steeps in clear water, is slowly stirred cleaning；
(2), broken wall is freezed:
Damask Rose flower petal after cleaning is sent into mix up in advance and carries out being rapidly frozen 4-6 hours in the freezer of temperature
Afterwards, it after taking-up, is immediately placed in pre-heated water-bath distillation device, Damask Rose flower cell wall rupture；
(3), it distills:
The water-bath distillation device for being put into freezing Damask Rose flower petal is continued to continue to be heated to 100 degrees Celsius under normal pressure；
(4), it condenses:
Water cooler is adjusted to 28 degrees Celsius, and using water cooler at this temperature that the vapor generated under 100 degrees Celsius is cold
But；
(5), water-oil separating:
The mixing liquid that discharge is condensed out by water cooler, will be smart by the separation of oil water separator into oil water separator
Oil is separated from water, and essential oil is injected in essential oil storage tank.
2. a kind of method that Damask Rose flower refines essential oil according to claim 1, it is characterised in that: the step
Rose when cleaning in (1) to Damask Rose flower petal suddenly is on rhizome, after being cleaned using clear water, then will
Clean Damask Rose flower petal picks.
3. a kind of method that Damask Rose flower refines essential oil according to claim 1, it is characterised in that: the step
Suddenly before the Damask Rose flower petal after cleaning being sent into the freezer for mixing up temperature in advance in (2), in advance by damascene
Leather rose petal is shredded using scissors.
4. a kind of method that Damask Rose flower refines essential oil according to claim 1, it is characterised in that: the step
Suddenly the cryogenic temperature of the freezer in (2) is 0 to -40 degree Celsius.
5. a kind of method that Damask Rose flower refines essential oil according to claim 1, it is characterised in that: the step
Suddenly the preheating temperature of the pre-heated water-bath distillation device in (2) is 40-80 degrees Celsius.
6. a kind of method that Damask Rose flower refines essential oil according to claim 1, it is characterised in that: the step
Suddenly the water in the water-bath distillation device in (2) is the water after cleaning in step (1) by the water after Purification by filtration.
7. a kind of method that Damask Rose flower refines essential oil according to claim 1, it is characterised in that: the step
The volume ratio of water and petal in rapid water-bath distillation device is 1:2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910120863.5A CN109593610A (en) | 2019-02-18 | 2019-02-18 | A kind of method that Damask Rose flower refines essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910120863.5A CN109593610A (en) | 2019-02-18 | 2019-02-18 | A kind of method that Damask Rose flower refines essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109593610A true CN109593610A (en) | 2019-04-09 |
Family
ID=65967350
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910120863.5A Pending CN109593610A (en) | 2019-02-18 | 2019-02-18 | A kind of method that Damask Rose flower refines essential oil |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111363630A (en) * | 2020-04-16 | 2020-07-03 | 倪氏国际玫瑰产业股份有限公司 | Preparation method of refined rose extract |
| CN111909791A (en) * | 2020-07-10 | 2020-11-10 | 玉溪擎禹农业科技有限公司 | Preparation method of rose essential oil and rose essential oil |
| CN113862083A (en) * | 2021-10-08 | 2021-12-31 | 银谷芳香科技有限公司 | Method for improving oil yield and quality of rosa damascena essential oil |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150073161A1 (en) * | 2012-04-19 | 2015-03-12 | South China University Of Technology | Pomelo peel essential oil extraction method by peel icing and breaking |
| CN105969528A (en) * | 2016-06-14 | 2016-09-28 | 云南金大康农业科技有限公司 | Extracting method for rose essential oil |
| CN107582497A (en) * | 2017-08-29 | 2018-01-16 | 陈树平 | A kind of rose fragrant body shower cream and its production method |
-
2019
- 2019-02-18 CN CN201910120863.5A patent/CN109593610A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150073161A1 (en) * | 2012-04-19 | 2015-03-12 | South China University Of Technology | Pomelo peel essential oil extraction method by peel icing and breaking |
| CN105969528A (en) * | 2016-06-14 | 2016-09-28 | 云南金大康农业科技有限公司 | Extracting method for rose essential oil |
| CN107582497A (en) * | 2017-08-29 | 2018-01-16 | 陈树平 | A kind of rose fragrant body shower cream and its production method |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111363630A (en) * | 2020-04-16 | 2020-07-03 | 倪氏国际玫瑰产业股份有限公司 | Preparation method of refined rose extract |
| CN111909791A (en) * | 2020-07-10 | 2020-11-10 | 玉溪擎禹农业科技有限公司 | Preparation method of rose essential oil and rose essential oil |
| CN113862083A (en) * | 2021-10-08 | 2021-12-31 | 银谷芳香科技有限公司 | Method for improving oil yield and quality of rosa damascena essential oil |
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Application publication date: 20190409 |