CN110511813A - A kind of preparation method of giving off a strong fragrance sunflower oil - Google Patents
A kind of preparation method of giving off a strong fragrance sunflower oil Download PDFInfo
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- CN110511813A CN110511813A CN201910643910.4A CN201910643910A CN110511813A CN 110511813 A CN110511813 A CN 110511813A CN 201910643910 A CN201910643910 A CN 201910643910A CN 110511813 A CN110511813 A CN 110511813A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of preparation methods of giving off a strong fragrance sunflower oil, comprising: selected sunflower seeds carries out cleaning removal impurity；Moisture regulation is carried out to the sunflower seeds after removal impurity；It peels off to the sunflower seeds after softening；Kernel-hull separation is carried out to the mixture after peeling off；The polly seed nucleole obtained through Kernel-hull separation is crushed；Polly seed nucleole after crushing is divided into polly seed nucleole main road and polly seed nucleole path；Polly seed nucleole main road is crushed；Supercritical carbon dioxide process extraction processing is carried out to smashed polly seed nucleole main road, obtains polly seed nucleole main road crude oil；Polly seed nucleole path is carried out to fry seed processing；Squeezing is carried out to the polly seed nucleole path after stir-fry seed and takes oil, obtains polly seed nucleole path crude oil；Polly seed nucleole main road crude oil and polly seed nucleole path crude oil are mixed, then the grease after sedimentation filtration carries out aquation degumming dewaxing treatment, obtains giving off a strong fragrance sunflower oil.The preparation method of the giving off a strong fragrance sunflower oil, process safety, it is convenient to prepare.
Description
Technical field
The present invention relates to sunflower oil technical fields, and in particular to a kind of preparation method of giving off a strong fragrance sunflower oil.
Background technique
China is not only a populous nation, while being also the big producer and consumption big country of a grain and oil.Edible oil is people
The required consumer goods of living, human body thermal energy and essential fatty acid are provided, the absorption of liposoluble vitamin is promoted.As China passes through
The rapid development of Ji, living standards of the people increase substantially, and people constantly promote the quality requirement of edible oil.Edible oil market
Also passed by the expansion of quantity, the expansion of kind and the big stage of the promotion of quality three, come health, personalization,
The developing stage of high-technicalization.The appearance of high-end giving off a strong fragrance oil just embodies these features, because of its pleasant strong perfume (or spice)
Taste and liked by the majority of consumers.
Sunflower seeds is rich in unsaturated fatty acid, multivitamin and microelement, be a kind of important edible oil materials it
One.In recent years, the continuous development of Chinese sunflower seeds industry is grown, and foreign trade scale steps up.Sunflower oil is rich in a variety of
The nutriment beneficial to human body, such as linoleic acid, vitamin E, carrotene, and human consumption's absorptivity of sunflower oil
Up to 96% or more.Research points out that often edible sunflower oil can protect skin health, enhances human immune system's function, changes
Mercy cranial vascular disease, the generation of the diseases such as prevention.Before the consumption figure of sunflower oil in the international market occupies the world
Column, wherein Japan, the consumption proportion of South Korea it is high by 70%.The annual consumption of China's sunflower oil had reached 800,000~90 in recent years
Ten thousand t.The raising of appearance and popularization and target level of product quality however as full refining technology, sells currently on the market
Full refining sunflower oil has lost its giving off a strong fragrance flavor, and whether what consumer cannot be bought by sense organ intuitive judgment is pure
Sunflower oil, the decline and market for directly resulting in consumption figure is lost, and not only causes resource and the energy in the overrefinement of grease
Waste aggravates environmental pollution, increases grease loss, and have lost the natural beneficial micronutrient in grease, and can not keep away
Generate new nuisance with exempting from.Frying seed is the critical process for producing giving off a strong fragrance sunflower oil, the generation of sunflower oil fragrance and stir-fry seed
Temperature has direct relation.Temperature is too low, and fragrance is thin；Temperature is too high, and oil plant is easily burnt burnt and can generate harmful substance, therefore wants
Strict control fries well the temperature and time of seed.Supercritical CO2Fluid extraction technology, has simple process, and organic solvent-free is residual
It stays, the incomparable advantage of traditional handicrafts such as operating condition is mild.In the production of grease, it overcomes solvent extraction method point
From needing distillation to heat in the process, the shortcomings that grease is oxidizable rancid, and there are dissolvent residuals；Squeezing method low yield is also overcomed, essence
Technique processed is cumbersome, the undesirable disadvantage of product color, and obtained oil and fat product quality is high.
Summary of the invention
Shortcoming present in view of the above technology the present invention provides a kind of process safety, prepares convenient and fast giving off a strong fragrance
The preparation method of sunflower oil.
The technical solution adopted by the present invention to solve the technical problems is: a kind of preparation method of giving off a strong fragrance sunflower oil, packet
Include following steps: A, clear up impurity elimination: selected sunflower seeds carries out cleaning removal impurity, all kinds of miscellaneous in the sunflower seeds after clearing up impurity elimination
Matter is less than 1%；B, soften: moisture regulation is carried out to the sunflower seeds after removal impurity；C, it peels off: the sunflower seeds after softening is shelled
Shell machine is peeled off；D, Kernel-hull separation: Kernel-hull separation is carried out to the mixture after peeling off, so that rate of kernel in hull≤0.9%；E,
It is broken: the polly seed nucleole obtained through Kernel-hull separation is crushed；F, branch: by a certain percentage by polly seed nucleole after crushing
It is divided into polly seed nucleole main road and polly seed nucleole path；G, it crushes: polly seed nucleole main road being crushed, the powder of polly seed nucleole main road
Broken degree is 40~60 mesh；H, supercritical extract: smashed polly seed nucleole main road is carried out at supercritical carbon dioxide process extraction
Reason, obtains polly seed nucleole main road crude oil；I, it fries seed: polly seed nucleole path being carried out to fry seed processing；J, it squeezes: to the certain herbaceous plants with big flowers after stir-fry seed
Flower seed benevolence path carries out squeezing and takes oil, obtains polly seed nucleole path crude oil；K, sedimentation filtration: by polly seed nucleole main road crude oil and certain herbaceous plants with big flowers
Flower seed benevolence path crude oil mix, then through oil-filtering box at 10~20 DEG C natural subsidence 48~72 hours；L, degumming: to through settling
Grease after filter carries out aquation degumming process；M, it dewaxes: dewaxing treatment being carried out to the grease after degumming, obtains giving off a strong fragrance sunflower seeds
Oil.
Preferably, in the step B, the water content of the sunflower seeds after softening is 6%~10%.
Preferably, in the step C, the whole seed content in the polly seed nucleole after peeling off is 18%~22%.
Preferably, in the step E, polly seed nucleole particle size after cracking is 5~8 valves, and fines content is no more than 6%.
Preferably, in the step F, polly seed nucleole main road ratio be 60%~90%, polly seed nucleole path ratio be 10%~
40%。
Preferably, in the step H, supercritical carbon dioxide process extraction processing condition are as follows: 25~40kg/h of CO2 flow,
Extract 30~40MPa of pressure, 38~50 DEG C of extraction temperature, 120~150min of extraction time.
Preferably, in the step I, seed condition is fried are as follows: fry 140~160 DEG C of seed temperature, fry 20~30 min of seed time.
Preferably, in the step J, squeezing takes deep-fried twisted dough sticks part are as follows: enters to squeeze 110~130 DEG C of temperature, enters to squeeze moisture 3~5%.
Preferably, in the step L, aquation de-alkali additives are as follows: 50~80 DEG C of hydration temperature, 15~40min of hydration time.
Preferably, in the step M, dewaxing treatment condition are as follows: filter aid is diatomite, and crystallization temperature is 10~30 DEG C,
Growing the grain temperature is 5~10 DEG C.
Compared with prior art, the present invention the beneficial effect is that: the preparation method of giving off a strong fragrance sunflower oil provided by the invention,
Raw material is divided into size two-way, path carries out stir-fry seed and obtains strong fragrance, and stir-fry seed temperature and stir-fry seed time are reasonable, reduce energy
The consumption of amount；Main road uses supercritical carbon dioxide extraction method, environmental-friendly, can compared with traditional grease preparation technique
Protect physiological activator；Last only to carry out sedimentation filtration, degumming and dewaxing technique, appropriateness refines, and remains more vitamin E
Etc. nutritional ingredients, safe and reliable, power consumption of polymer processing and pollution it is lower.
Specific embodiment
The present invention is described in further detail below, to enable those skilled in the art's refer to the instruction text being capable of evidence
To implement.
The present invention provides a kind of preparation methods of giving off a strong fragrance sunflower oil, include the following steps:
A, clear up impurity elimination: selected sunflower seeds carries out cleaning removal impurity, and all kinds of impurity in sunflower seeds after clearing up impurity elimination are less than
1%；
B, soften: moisture regulation being carried out to the sunflower seeds after removal impurity, the water content of the sunflower seeds after softening is 6%~10%；
C, it peels off: being peeled off to the sunflower seeds after softening with decorticator, the whole seed content in the polly seed nucleole after peeling off is 18%
~22%；
D, Kernel-hull separation: Kernel-hull separation is carried out to the mixture after peeling off, so that rate of kernel in hull≤0.9%；
E, it is crushed: the polly seed nucleole obtained through Kernel-hull separation is crushed, polly seed nucleole particle size after cracking is 5~8 valves, powder
Degree is no more than 6%；
F, polly seed nucleole after crushing branch: is divided into polly seed nucleole main road and polly seed nucleole path, sunflower by a certain percentage
Seed benevolence main road ratio is 60%~90%, and polly seed nucleole path ratio is 10%~40%；
G, it crushes: polly seed nucleole main road is crushed, the degree of grinding of polly seed nucleole main road is 40~60 mesh；
H, supercritical carbon dioxide process extraction processing, CO2 flow supercritical extract: are carried out to smashed polly seed nucleole main road
25~40kg/h, extraction 30~40MPa of pressure, 38~50 DEG C of extraction temperature, 120~150min of extraction time, obtain sunflower seeds
Benevolence main road crude oil；
I, it fries seed: polly seed nucleole path being carried out to fry seed processing, 140~160 DEG C of seed temperature is fried, fries 20~30 min of seed time；
J, squeeze: to fry seed after polly seed nucleole path carry out squeezing take oil, enter to squeeze 110~130 DEG C of temperature, enter to squeeze moisture 3~
5%, obtain polly seed nucleole path crude oil；
K, sedimentation filtration: polly seed nucleole main road crude oil and polly seed nucleole path crude oil are mixed, then through oil-filtering box at 10~20 DEG C
Lower natural subsidence 48~72 hours；
L, degumming: to after sedimentation filtration grease carry out aquation degumming process, 50~80 DEG C of hydration temperature, hydration time 15~
40min；
M, it dewaxes: dewaxing treatment being carried out to the grease after degumming, filter aid is diatomite, and crystallization temperature is 10~30 DEG C, growing the grain
Temperature is 5~10 DEG C, obtains giving off a strong fragrance sunflower oil.
Embodiment 1
Selected sunflower seeds carries out cleaning removal impurity, carries out moisture regulation to the sunflower seeds after removal impurity, the sunflower after softening
The water content of seed is 6%；It is peeled off to the sunflower seeds after softening with decorticator, the whole seed content in the polly seed nucleole after peeling off
It is 21%；Kernel-hull separation is carried out to the mixture after peeling off；The polly seed nucleole obtained through Kernel-hull separation is crushed, sunflower seeds
Benevolence particle size after cracking is 5 valves；Polly seed nucleole after crushing is divided into polly seed nucleole main road and polly seed nucleole path by a certain percentage,
Polly seed nucleole main road ratio is 90%, and polly seed nucleole path ratio is 10%；Polly seed nucleole main road is crushed, polly seed nucleole is big
The degree of grinding on road is 50 mesh；Supercritical carbon dioxide process extraction processing, CO2 flow are carried out to smashed polly seed nucleole main road
30kg/h, extraction pressure 30MPa, 40 DEG C of extraction temperature, extraction time 120min, obtain polly seed nucleole main road crude oil；To sunflower
Seed benevolence path carries out frying seed processing, fries 150 DEG C of seed temperature, fries 20 min of seed time；Polly seed nucleole path after stir-fry seed is carried out
Squeezing takes oil, enters to squeeze 115 DEG C of temperature, enters to squeeze moisture 4%, obtains polly seed nucleole path crude oil；By polly seed nucleole main road crude oil and certain herbaceous plants with big flowers
Flower seed benevolence path crude oil mix, then through oil-filtering box at 11 DEG C natural subsidence 48 hours to remove big suspended particulate；To through settling
Filtered grease carries out aquation degumming process to remove peptized impurities, and 66 DEG C of hydration temperature, hydration time 20min；To de-
Grease after glue carries out dewaxing treatment, and filter aid is diatomite, and crystallization temperature is 27 DEG C, and growing the grain temperature is 8 DEG C, obtains giving off a strong fragrance certain herbaceous plants with big flowers
Flower seed oil.
Embodiment 2
Selected sunflower seeds carries out cleaning removal impurity, carries out moisture regulation to the sunflower seeds after removal impurity, the sunflower after softening
The water content of seed is 7%；It is peeled off to the sunflower seeds after softening with decorticator, the whole seed content in the polly seed nucleole after peeling off
It is 19%；Kernel-hull separation is carried out to the mixture after peeling off；The polly seed nucleole obtained through Kernel-hull separation is crushed, sunflower seeds
Benevolence particle size after cracking is 8 valves；Polly seed nucleole after crushing is divided into polly seed nucleole main road by a certain percentage and polly seed nucleole is small
Road, polly seed nucleole main road ratio are 80%, and polly seed nucleole path ratio is 20%；Polly seed nucleole main road is crushed, sunflower seeds
The degree of grinding of benevolence main road is 60 mesh；Supercritical carbon dioxide process extraction processing, CO2 stream are carried out to smashed polly seed nucleole main road
30kg/h, extraction pressure 40MPa, 38 DEG C of extraction temperature, extraction time 125min are measured, polly seed nucleole main road crude oil is obtained；To certain herbaceous plants with big flowers
Flower seed benevolence path carries out frying seed processing, fries 155 DEG C of seed temperature, fries 30 min of seed time；To fry seed after polly seed nucleole path into
Row squeezing takes oil, enters to squeeze 125 DEG C of temperature, enters to squeeze moisture 4.5%, obtains polly seed nucleole path crude oil；By polly seed nucleole main road crude oil
With polly seed nucleole path crude oil mix, then through oil-filtering box at 18 DEG C natural subsidence 65 hours to remove big suspended particulate；To warp
Grease after sedimentation filtration carries out aquation degumming process to remove peptized impurities, and 77 DEG C of hydration temperature, hydration time 25min；
Dewaxing treatment is carried out to the grease after degumming, filter aid is diatomite, and crystallization temperature is 18 DEG C, and growing the grain temperature is 6 DEG C, is obtained dense
Fragrant sunflower oil.
Embodiment 3
Selected sunflower seeds carries out cleaning removal impurity, carries out moisture regulation to the sunflower seeds after removal impurity, the sunflower after softening
The water content of seed is 10%；It is peeled off to the sunflower seeds after softening with decorticator, the whole seed content in the polly seed nucleole after peeling off
It is 20%；Kernel-hull separation is carried out to the mixture after peeling off；
The polly seed nucleole obtained through Kernel-hull separation is crushed, polly seed nucleole particle size after cracking is 6 valves；By certain herbaceous plants with big flowers after crushing
Flower seed benevolence is divided into polly seed nucleole main road and polly seed nucleole path by a certain percentage, and polly seed nucleole main road ratio is 60%, polly seed nucleole
Path ratio is 40%；Polly seed nucleole main road is crushed, the degree of grinding of polly seed nucleole main road is 40 mesh；To smashed certain herbaceous plants with big flowers
Flower seed benevolence main road carries out supercritical carbon dioxide process extraction processing, CO2 flow 33kg/h, extraction pressure 38MPa, extraction temperature 44
DEG C, extraction time 138min, obtain polly seed nucleole main road crude oil；Polly seed nucleole path is carried out to fry seed processing, fries seed temperature 146
DEG C, fry seed time 20min；Squeezing is carried out to the polly seed nucleole path after stir-fry seed and takes oil, enters to squeeze 120 DEG C of temperature, enters to squeeze moisture 4%,
Obtain polly seed nucleole path crude oil；Polly seed nucleole main road crude oil and polly seed nucleole path crude oil are mixed, then through oil-filtering box 20
At DEG C natural subsidence 72 hours to remove big suspended particulate；Aquation degumming process is carried out to remove to the grease after sedimentation filtration
Peptized impurities, 55 DEG C of hydration temperature, hydration time 35min；Dewaxing treatment is carried out to the grease after degumming, filter aid is diatom
Soil, crystallization temperature are 17 DEG C, and growing the grain temperature is 10 DEG C, obtain giving off a strong fragrance sunflower oil.
Although the embodiments of the present invention have been disclosed as above, but it is not limited in listed fortune in specification and embodiments
With it can be fully applied to various fields suitable for the present invention, for those skilled in the art, easily realize in addition
Modification, therefore without departing from the general concept defined in the claims and the equivalent scope, the present invention is not limited to specific
Details.
Claims (10)
1. a kind of preparation method of giving off a strong fragrance sunflower oil, which comprises the steps of:
A, clear up impurity elimination: selected sunflower seeds carries out cleaning removal impurity, and all kinds of impurity in sunflower seeds after clearing up impurity elimination are less than
1%；
B, soften: moisture regulation is carried out to the sunflower seeds after removal impurity；
C, it peels off: being peeled off to the sunflower seeds after softening with decorticator；
D, Kernel-hull separation: Kernel-hull separation is carried out to the mixture after peeling off, so that rate of kernel in hull≤0.9%；
E, it is crushed: the polly seed nucleole obtained through Kernel-hull separation is crushed；
F, polly seed nucleole after crushing branch: is divided into polly seed nucleole main road and polly seed nucleole path by a certain percentage；
G, it crushes: polly seed nucleole main road is crushed, the degree of grinding of polly seed nucleole main road is 40~60 mesh；
H, supercritical extract: supercritical carbon dioxide process extraction processing is carried out to smashed polly seed nucleole main road, obtains sunflower
Seed benevolence main road crude oil；
I, it fries seed: polly seed nucleole path being carried out to fry seed processing；
J, it squeezes: squeezing being carried out to the polly seed nucleole path after stir-fry seed and takes oil, obtains polly seed nucleole path crude oil；
K, sedimentation filtration: polly seed nucleole main road crude oil and polly seed nucleole path crude oil are mixed, then through oil-filtering box at 10~20 DEG C
Lower natural subsidence 48~72 hours；
L, aquation degumming process degumming: is carried out to the grease after sedimentation filtration；
M, it dewaxes: dewaxing treatment being carried out to the grease after degumming, obtains giving off a strong fragrance sunflower oil.
2. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step B, after softening
The water content of sunflower seeds is 6%~10%.
3. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step C, after peeling off
Whole seed content in polly seed nucleole is 18%~22%.
4. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step E, polly seed nucleole
Particle size after cracking is 5~8 valves, and fines content is no more than 6%.
5. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step F, polly seed nucleole
Main road ratio is 60%~90%, and polly seed nucleole path ratio is 10%~40%.
6. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step H, overcritical two
Carbonoxide method extraction processing condition are as follows: 25~40kg/h of CO2 flow, extraction 30~40MPa of pressure, 38~50 DEG C of extraction temperature,
120~150min of extraction time.
7. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step I, fry seed condition
Are as follows: 140~160 DEG C of seed temperature are fried, 20~30 min of seed time is fried.
8. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step J, squeezing takes oil
Condition are as follows: enter to squeeze 110~130 DEG C of temperature, enter to squeeze moisture 3~5%.
9. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step L, aquation degumming
Condition are as follows: 50~80 DEG C of hydration temperature, 15~40min of hydration time.
10. the preparation method of giving off a strong fragrance sunflower oil as described in claim 1, which is characterized in that in the step M, at dewaxing
Manage bar part are as follows: filter aid is diatomite, and crystallization temperature is 10~30 DEG C, and growing the grain temperature is 5~10 DEG C.
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| CN112574811A (en) * | 2020-12-15 | 2021-03-30 | 佳格食品(厦门)有限公司 | Moderate processing method of sunflower seed oil |
| CN113100296A (en) * | 2021-04-13 | 2021-07-13 | 武汉轻工大学 | Preparation method of flavored sunflower seed oil |
| CN116042310A (en) * | 2022-12-28 | 2023-05-02 | 中粮营养健康研究院有限公司 | Processing method of sunflower seed oil and grease obtained by processing method |
| CN116042310B (en) * | 2022-12-28 | 2023-11-03 | 中粮营养健康研究院有限公司 | Processing method of sunflower seed oil and grease obtained by processing method |
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